BRITISH STANDARD BS EN

1423:1998
Incorporating
Amendment No. 1

Road marking
materials — Drop on
materials — Glass
beads, antiskid
aggregates and
mixtures of the two

The European Standard EN 1423:1997, with the incorporation of

amendment A1:2003, has the status of a British Standard

ICS 93.080.20

12&23<,1*:,7+287%6,3(50,66,21(;&(37$63(50,77('%<&23<5,*+7/$:
BS EN 1423:1998

National foreword
This British Standard is the official English language version of EN 1423:1997,
including amendment A1:2003, published by the European Committee for
Standardization.
The start and finish of text introduced or altered by amendment is indicated in
the text by tags !" . Tags indicating changes to CEN text carry the number
of the CEN amendment. For example, text altered by CEN amendment A1 is
indicated by !".
The UK participation in its preparation was entrusted by Technical Committee
B/509, Road equipment, to Subcommittee B/509/2, Horizontal road markings
and road studs, which has the responsibility to:

— aid enquirers to understand the text;

— present to the responsible international/European committee any

enquiries on the interpretation, or proposals for change, and keep the
UK interests informed;
— monitor related international and European developments and
promulgate them in the UK.

A list of organizations represented on this subcommittee can be obtained on

request to its secretary.
This standard partially supersedes BS 6088:1981 which will be declared
obsolescent on the publication of this standard. The declaration of obsolescence
does not affect the current kitemark certification scheme for road marking
products.
Cross-references
The British Standards which implement international or European
publications referred to in this document may be found in the BSI Catalogue
under the section entitled “International Standards Correspondence Index”, or
by using the “Search” facility of the BSI Electronic Catalogue or of British
Standards Online.
This publication does not purport to include all the necessary provisions of a
contract. Users are responsible for its correct application.

Summary of pages
This British Standard, having This document comprises a front cover, an inside front cover, the EN title page,
been prepared under the pages 2 to 33 and a back cover
direction of the Sector Board for
Building and Civil The BSI copyright notice displayed in this document indicates when the
Engineering, was published document was last issued.
under the authority of the
Standards Board and comes
into effect on
15 January 1998

© 17 September 2004 Amendments issued since publication

Amd. No. Date Text affected

15312 17 September 2004 See national foreword

ISBN 0 580 29075 1

EUROPEAN STANDARD EN 1423
August 1997
NORME EUROPÉENNE
+ A1
EUROPÄISCHE NORM July 2003

ICS 93.080.20

Descriptors: Roads, signalling, marking, balls, glass, aggregates, definitions, grain size, specifications, quality, defects tolerances,
sampling

English version

Road marking materials — Drop on materials — Glass

beads, antiskid aggregates and mixtures of the two
(includes Amendment A1:2003)

Produits de marquage routier — Produits de Stra"enmarkierungsmaterialien —

saupoudrage — Microbilles de verre, granulats Nachstreumittel — Markierungs-Glasperlen,
antidérapants et mélange de ces deux composants Griffigkeitsmittel und Nachstreugemische
(inclut l’amendement A1:2003) (enthält Änderung A1:2003)

This European Standard was approved by CEN on 1997-06-20, Amendment A1

was approved by CEN on 2003-05-02. CEN members are bound to comply with
the CEN/CENELEC Internal Regulations which stipulate the conditions for
giving this European Standard the status of a national standard without any
alteration.
Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Central Secretariat or to any
CEN member.
This European Standard exists in three official versions (English, French,
German). A version in any other language made by translation under the
responsibility of a CEN member into its own language and notified to the
Central Secretariat has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Czech
Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia,
Spain, Sweden, Switzerland and United Kingdom.

CEN
European Committee for Standardization
Comité Européen de Normalisation
Europäisches Komitee für Normung

Central Secretariat: rue de Stassart 36, B-1050 Brussels

© 1997 CEN — All rights of exploitation in any form and by any means reserved worldwide for CEN
national Members.
Ref. No. EN 1423:1997 + A1:2003 E
EN 1423:1997

Foreword Contents
This European Standard has been prepared by Technical Page
Committee CEN/TC 226, Road equipment, the
Foreword 2
Secretariat of which is held by AFNOR.
This document has been prepared under a mandate given 1 Scope 3
to CEN by the European Commission and the Free Trade 2 Normative references 3
Association and support essential requirements of EU 3 Definitions 3
Directive(s).
4 Requirements for glass beads 4
For relationship with the Construction Products Directive
(89/106/EEC) see informative Annex ZA. which is an 5 Requirements for antiskid aggregates 6
integral part of this document. 6 Mixture of glass beads and antiskid
This European Standard shall be given the status of a aggregate 7
national standard, either by publication of an identical
7 Sampling 7
text or by endorsement, at the latest by February 1998,
and conflicting national standards shall be withdrawn at Annex A (normative) Test method to determine
the latest by February 1998. the refractive index of the glass beads 8
According to the CEN/CENELEC Internal Regulations, Annex B (normative) Test methods to determine
the national standards organizations of the following the resistance of the glass beads to the effects of
countries are bound to implement this European water, hydrochloric acid, calcium chloride and
Standard: Austria, Belgium, Czech Republic, Denmark, sodium sulfide 10
Finland, France, Germany, Greece, Iceland, Ireland,
Italy, Luxembourg, Netherlands, Norway, Portugal, Annex C (normative) Glass bead imperfections 11
Spain, Sweden, Switzerland and the United Kingdom. Annex D (normative) Test method to determine
Twelve (12) months after the date of publication of the the quality of the glass beads 14
harmonised part of this European standard (Annex ZA) in Annex E (normative) Test method to determine
the Official Journal of the European Communities (which
the presence of the moisture-proof coating 16
follows its availability and notification to the European
Commission by CEN/CENELEC), compliance with all the Annex F (normative) Test method to determine
provisions of the Construction Products Directive the presence of floatation coating 17
(CE-marking) becomes compulsory for all products falling Annex G (normative) Test method to determine
within the scope of this European standard that are
the friability index of the antiskid aggregates 18
placed on the EEA market.
Annex H (informative) Alternative test methods
to determine the quality of glass beads 20
Foreword to amendment A1
Annex ZA (Informative) Clauses of this European
This document (EN 1423:1997/A1:2003) has been Standard addressing the provisions of the EU
prepared by Technical Committee CEN/TC 226, Road Construction Products Directive 26
equipment, the Secretariat of which is held by AFNOR.
Bibliography 33
This European Standard shall be given the status of a
national standard, either by publication of an identical
text or by endorsement, at the latest by January 2004, and
conflicting national standards shall be withdrawn at the
latest by April 2005.
This document has been prepared under a mandate given
to CEN by the European Commission and the European
Free Trade Association, and supports essential
requirements of EU Directive(s).
For relationship with EU Directive(s), see informative
Annex ZA, which is an integral part of this document.
This amendment is included in a package with
EN 1463-1:1997/prA1 and EN 13212:2001, with a
common DOW fixed on 2003-09-30.
According to the CEN/CENELEC Internal Regulations,
the national standards organizations of the following
countries are bound to implement this European
Standard: Austria, Belgium, Czech Republic, Denmark,
Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Luxembourg, Malta, Netherlands, Norway,
Portugal, Slovakia, Spain, Sweden, Switzerland and the
United Kingdom.

2 © BSI 17 September 2004

 EN 1423:1997

1 Scope
This European Standard specifies the requirements for laboratory tests (production control) and
qualification procedures for the following drop on materials used in road markings.
These materials are dropped on to paints, thermoplastics, cold plastics and any other marking product
applied in a liquid state, immediately after application to the road surface.
The requirements taken into consideration in this standard are:
— glass beads: granulometry, refractive index of the glass, chemical resistance, quality, surface
treatments;
— antiskid aggregates: granulometry, chemical characteristics, friability, colour;
— mixtures of glass beads and antiskid aggregates; and the requirements for both components.

2 Normative references
This European Standard incorporates by dated or undated reference, provisions from other publications.
These normative references are cited at the appropriate places in the text and the publications are listed
hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply
to this European Standard only when incorporated in it by amendment or revision. For undated references
the latest edition of the publication referred to applies.
ISO 565, Test sieves — Metal wire cloth, perforated metal plate and electroformed sheet — Nominal sizes of
openings
ISO 7879, General methods of test for pigments and extenders — Part 9: Determination of pH value of an
aqueous suspension
ISO 25911, Test sieving — Part 1: Methods using test sieves of woven wire cloth and perforated metal plate
ISO 77242, Paints and varnishes — Colorimetry — Part 2: Colour measurement
ISO/CIE 10526, CIE Standard colorimetric illuminants

3 Definitions
For the purpose of this standard, the following definitions apply:
3.1
glass bead
transparent spherical glass particle, used to provide night visibility for the road markings by
retroreflecting the incident headlight beams of a vehicle towards the driver
3.2
antiskid aggregate
hard grain of natural or artificial origin, used to provide antiskid qualities for the road markings
3.3
intermediate bulk container (IBC)
container with a capacity of up to 1000 kg, used as an intermediate solution in between bags and tins
(25 kg to 50 kg) and bulk transport

© BSI 17 September 2004 3

EN 1423:1997

4 Requirements for glass beads

4.1 Granulometry
The granulometry of the glass beads shall be described giving the minimum and the maximum percentages
by mass of the cumulative retained glass beads on metal wire cloth test sieves: ISO 565 - Sizes R 40/3 using
the test sieving procedure defined in ISO 2591-1.
!Granulometries shall be described by selecting sieves in accordance with the following rules
(see Table 1):"
— the upper safety sieve shall retain less than 0 % to 2 % of the total mass of the glass beads;
— the upper nominal sieve shall retain 0 % to 10 % of the beads;
— if necessary, intermediate sieves shall be added to limit the ratio between the nominal sizes of
openings of two successive sieves to a maximum of 1,7 : 1;
— for each of the intermediate sieves, the range by mass between the minimum N1 % and the maximum
N2 % of the cumulative retained percentages shall be not more than 40 % (N2 – N1 k 40);
— the lower nominal sieve shall retain 95 % to 100 % of the beads.
Table 1 — Selecting sieves for glass beads
Sieves ISO 565 R 40/3 Cumulative retained mass
%
Upper safety 0 to 2
Upper nominal 0 to 10
Intermediate N1 to N2
Lower nominal 95 to 100
Examples of the interpretation of the rules to specify the granulometry of glass beads are given in
Table 2 and Table 3.
Table 2 — Fine grading
Sieves ISO 565 R 40/3 Cumulative retained mass
µm %
500 0 to 2
425 0 to 10
250 20 to 60
150 60 to 95
90 95 to 100
Table 3 — Medium grading
Sieves ISO 565 R 40/3 Cumulative retained mass
µm %
710 0 to 2
600 0 to 10
355 30 to 70
212 70 to 100
125 95 to 100
The granulometry of the glass beads shall be determined in accordance with ISO 2591-1.

4 © BSI 17 September 2004

 EN 1423:1997

4.2 Refractive index

The refractive index n of the glass beads, when determined in accordance with Annex A, shall conform to
the following classes:
Class A: n U 1,5;
Class B: n U 1,7;
Class C: n U 1,9.
4.3 Resistance to water, hydrochloric acid, calcium chloride and sodium sulfide
When tested in accordance with Annex B, glass beads shall not develop any surface haze or dulling when
in contact with any of the following: water, hydrochloric acid, calcium chloride and sodium sulfide.
4.4 Quality requirements
!When tested in accordance with Annex D (reference method), glass beads with imperfections as
described in Annex C, shall be considered defective."
!Using the reference method, and taking" into consideration only one defect per bead, the maximum
weighted percentage of defective beads shall be 20 % for beads with a diameter lower than 1 mm and 30 %
for beads with a diameter equal to or greater than 1 mm, in both cases including a maximum of 3 % of
grains and foreign particles (see Table 4). If a granulometry includes beads with diameters lower
than 1 mm and diameters equal to or greater than 1 mm they shall be separated by means of a sieve with
nominal sizes of openings of 1 mm and checked separately.
Table 4 — Maximum weighted percentage of defective glass beads
Diameter of glass beads Maximum weighted percentage of Maximum weighted percentage of
defective glass beads1) grains and foreign particles
mm % %
<1 20 3
U1 30 3
!
1) When alternative test methods are used as in Annex H (informative) of this European Standard, the correlated values shall be

applied. Method described in Annex D (normative) of EN 1423:1997 shall be always considered as the reference test method.
"

4.5 Surface treatments of the glass beads

Special coatings may be applied to the surface of the glass beads to enhance their properties.
4.5.1 Moisture proof coatings
When the manufacturer states the presence of a moisture proof coating the glass beads shall be tested in
accordance with Annex E. When procedure A of Annex E is used, 80 % of the glass beads shall pass the test
showing the presence of the moisture proof coating. When procedure B of Annex E is used the glass beads
shall pass the test without any flow stoppage. When procedure A fails, procedure B shall be used.
4.5.2 Floatation coatings
When the manufacturer states the presence of a floatation coating the glass beads shall be tested in
accordance with Annex F. When it is agreed between the supplier of the glass beads and the specifying
authority that Annex F is not applicable, then an alternative test method shall be agreed between them.
4.5.3 Adhesion coating
When the manufacturer states the presence of an adhesion coating it shall be proved by testing the glass
beads in accordance with a test method agreed between the supplier of the glass beads and the specifying
authority.
4.5.4 Other coatings
When the manufacturer states the presence of a coating other than those in 4.5.1, 4.5.2 and 4.5.3, it shall
be proved by testing the glass beads in accordance with a test method agreed between the supplier of the
glass beads and the specifying authority.

© BSI 17 September 2004 5

EN 1423:1997

5 Requirements for antiskid aggregates

5.1 Chemical characteristics
!When tested in accordance with ISO 787-9, the pH value of the antiskid aggregates shall be not less
than 5 and not greater than 9.5."
5.2 Friability index
The friability index of the antiskid aggregates shall be determined in accordance with Annex G. The value
of the friability index shall be indicated in the data sheet of the product.
NOTE Example: for cristobalite the maximum friability index is 20 %.

5.3 Colour co-ordinates and luminance factor

If the antiskid aggregate is not transparent, the chromaticity co-ordinates and the luminance factor shall
be determined in accordance with ISO 7724-2. The chromaticity co-ordinates shall lie inside the region
defined by the corner points given in Table 5 and the luminance factor ¶ shall be greater than 0,70.
Table 5 — Corner points of the chromaticity regions for non-transparent antiskid aggregates
Corner point No. 1 2 3 4
x 0,355 0,305 0,285 0,335
y 0,355 0,305 0,325 0,375
NOTE Sample preparation; since the grains of the antiskid aggregates are not fine enough to form a tablet when pressed without a
binder, as done for the barium sulfate reflectance standard in accordance with ISO 7724-2, the antiskid aggregates are pressed as for
the BaSO4 standard in ISO 7724-2; but after removing the glass the material is kept in the container with the uncovered surface
upward in a horizontal position for illumination and observation.

5.4 Granulometry
In order to be effective, the fraction of the particles smaller than 90 4m shall be less than 1 % by mass. The
granulometry of the antiskid aggregates shall be described giving the minimum and the maximum
percentages, by mass, of the cumulative retained particles on metal wire cloth test sieves ISO 565 –
sizes R 40/3 – using the test sieving procedure defined in ISO 2591-1.
!For a period of 5 years after the date of publication of this European standard existing national
standard granulometries can be used, even if they use sieves other than those defined in ISO 565 –
sizes R 40. Thereafter, granulometries shall be described by selecting sieves in accordance with the
following rules (also see Table 1):"
— the upper safety sieve shall retain less than 2 % of the total mass of the antiskid aggregates;
— the upper nominal sieve shall retain 0 % to 10 % of the aggregates;
— if necessary, intermediate sieves shall be added to limit the ratio between the nominal sizes of
openings of two successive sieves to a maximum of 1,7 to 1;
— for each of the intermediate sieves, the range by mass between the minimum N1 % and the maximum
N2 % of the cumulative retained percentages shall be not more than 40 % (N2 p N1 k 40);
— the lower nominal sieve shall retain 95 % to 100 % of the aggregates;
— the lower safety sieve shall retain 99 % to 100 % of the aggregates.
Table 6 — Selecting sieves for aggregates
Sieves ISO 565 R 40/3 Cumulative retained mass
%
Upper safety 0 to 2
Upper nominal 0 to 10
Intermediate N1 to N2
Lower nominal 95 to 100
Lower safety 99 to 100
Examples of the interpretation of the rules to specify the granulometry of the antiskid aggregates are given
in Table 7 and Table 8.

6 © BSI 17 September 2004

 EN 1423:1997

Table 7 — Fine grading

Sieves ISO 565 R 40/3 Cumulative retained mass
µm %
1 000 0 to 2
710 0 to 10
425 0 to 25
250 40 to 80
150 95 to 100
90 99 to 100
Table 8 — Medium grading
Sieves ISO 565 R 40/3 Cumulative retained mass
µm %
1 180 0 to 2
1 000 0 to 10
600 10 to 50
355 50 to 80
212 85 to 100
150 95 to 100
90 99 to 100

6 Mixture of glass beads and antiskid aggregate

In a mixture of glass beads and antiskid aggregates the glass beads shall conform to Clause 4 and the
antiskid aggregates shall conform to Clause 5. The tests on the glass beads and the antiskid aggregates to
be incorporated in mixtures shall be conducted separately before mixing.

7 Sampling
In order to test glass beads, antiskid aggregates and mixtures of them, a representative sample of the
material to be tested shall be taken as follows.
The drop on material sample shall be taken from at least three bags or one Intermediate Bulk Container
(IBC).
When M, in kilograms, is the mass of the drop on material to be tested, at least 1,5 kg of the material shall
be taken by inserting an appropriate probe in the full height of a certain number ‘S’ of bags, or inserting
the probe S times in the whole height of an IBC. The probe shall be driven to the bottom of the bags, in an
upright position, or into the IBC containing the material to be tested.
S is calculated by the formula:
S= M ⁄ 150 ;
and it shall be rounded up to the next higher unit.
A representative sample shall be obtained by mixing the material taken with the S insertions of the probe
in the bags. The representative sample shall be split by means of a 1/1 splitter in the number of samples
necessary for the tests.
NOTE A test probe can be constructed from a tube of 28 mm to 34 mm diameter and 1 000 mm to 1 200 mm in length. The end of
the probe which reaches the bottom of the bag should be fitted with a plugging system. After penetration of the probe to the full depth
of the bag, the plug is inserted and the probe removed. The contents of the probe represent a single sample of the material to be tested.
!Text deleted"

© BSI 17 September 2004 7

EN 1423:1997

Annex A (normative)
Test method to determine the refractive index of the glass beads
The method used to determine the refractive index of glass beads is immersion with oblique illumination.
This technique, known as the Shröber van der Kolk method, only applies to isotropic or to monorefracting
bodies, as is the case where glass beads are concerned.
A.1 Principle
Viewed under the microscope, transparent solids which are immersed in a liquid give an image bounded by
dark or luminous bands. The appearance will vary, depending upon the difference between the refractive
indices of the two bodies, according to their dispersing capacity and illumination.
Under axial lighting conditions index differences are perceptible; but they become considerably more
pronounced under oblique lighting, due to the fact that under such conditions the bands become sharper
on one side than on the other. Their position is determined by the direction of the incident beam and by the
difference between the index of the solid under examination and that of the liquid in which it is immersed.
Figure A.1 provides an illustration of the technique used for determination of the refractive index by
immersion with oblique illumination.

+ refractive index for the body higher

than that for the liquid. Shadow on
screen side.

= refractive index for the body equal to

that for the liquid. No shadow coloured
edging.

– refractive index for the body lower

than that for the liquid. Shadow on the
opposite side to the screen.

Figure A.1 — Schematic diagram showing the technique for determining the refractive index

A.2.1 Microscope
The microscope used in this procedure should be of a conventional type, of a design which affords the user
access to the area between the light source and the condenser.
The microscope shall be fitted with a 10× or 15× magnification lens and with a 6× or 8× magnification eye
piece.
The phenomena do not appear clearly unless the condenser is turned to the maximum setting with the iris
at full aperture and using an average magnification (20× diameter).

8 © BSI 17 September 2004

 EN 1423:1997

A.2.2 Liquids with known refractive index

In order to obtain liquid scales graduate indices, either pure bodies with known constants may be used or,
alternatively, mixtures.

– Vaseline oil 1,470

– 1-iodopropane 1,505
– cedar oil 1,510
– methyl salicylate 1,530
– bromobenzene 1,560
– diphenylethylene 1,610
– monobromonaphthalene 1,658
– diiodomethane 1,755
– methylene iodide 1,800
– arsenic tribromide 2,000

Refractive indices may be checked by the use of an Abbe refractometer, with the temperature corrected
to 23 ºC.
A.3 Procedure
Take the glass beads and place them on the concave slide, then immerse them in a liquid with a known
refractive index:
— place the concave slide in the specimen holder of the microscope;
— turn the condenser to the maximum setting;
— open the iris to the full aperture;
— light the specimen from below;
— slip the board with the straight edges in below the condenser, so as to obscure half of the field visible
through the eye piece, which will give angled illumination of the remaining visible part of the field;
— observe the glass beads in the illuminated area of the field in view through the eye piece;
— compare observations with the diagram in Figure A.1;
— depending upon the conclusions reached, repeat the above procedure and continue to repeat this
procedure, using liquids with different refractive indices, until a liquid is found with a refractive index
identical to that of the glass beads; or until two liquids are found with close refractive indices, as listed
in A.2.2, which sandwich the index for the glass beads.
A.4 Expression of the results
Show the index found, or the indices for the two liquids on either side of the index for the test subjects,
specifying the temperature at which the test was carried out and quoting references for the glass beads
which have been examined.

© BSI 17 September 2004 9

EN 1423:1997

Annex B (normative)
Test methods to determine the resistance of the glass beads to the effects of
water, hydrochloric acid, calcium chloride and sodium sulfide
Samples taken for testing shall be weighed on scales with an accuracy of 0,1 g.
B.1 Resistance to the effects of water
In a distillation flask fitted with a glass tube at the top, this tube to serve as a reflux condenser,
boil 10 g ± 0,1 g of glass beads for 60 min ± 10 s in 100 g ± 1 g of CO2 free water. After the test objects have
been boiled for the required period, filter the glass beads, cool the liquid to room temperature and then add
two drops of phenolphthalein solution as an indicator.
Using a 0,01 mol/l solution of hydrochloric acid, titrate the liquid until the phenolphthalein changes colour.
A blank test shall be carried out in parallel.
Note any changes which appear in the surface using the microscope at an enlargement of between 20× and 50×; note also the
quantity of 0,01 mol/l HCI also the quantity of 0,01 mol/l HCl used.

B.2 Resistance to the effects of hydrochloric acid

Immerse 10 g ± 0,1 g of glass beads in 100 ml ± 0,1 ml of dilute hydrochloric acid solution, buffered to give
a pH of 5,0 to 5,3, for 90 h at a temperature of 20 °C ± 3 °C.
With the help of a microscope with 20× to 50× magnification, note any changes which may have appeared
on the surface after the glass beads have been rinsed in distilled water and dried.
B.3 Resistance to the effects of calcium chloride
Immerse 10 g ± 0,1 g of glass beads in 100 ml ± 0,1 ml of a normal solution of calcium chloride for 3 h at a
temperature of 20 °C ± 3 °C.
With the help of a microscope with 20× to 50× magnification note any changes which may have appeared
on the surface after the glass beads have been rinsed in distilled water and dried.
B.4 Resistance to the effects of sodium sulfide
B.4.1 Apparatus and reagents
— microscope, with minimum magnification of 10;
— 50 ml bottle with a glass stopper;
— distilled water;
— !a saturated solution of sodium sulphide in distilled water at 20 ºC with the addition of 2,0 % anionic
wetting agent"
B.4.2 Procedure
Take 10 g ± 0,1 g of glass beads from a representative sample.
Place the glass beads in a stoppered bottle and cover with the solution containing the sodium sulfide and
allow to stand for 1 h. Pour off the solution containing the sodium sulfide and rinse three times with
distilled water.
Dry the glass beads in an oven at 100 ºC ± 5 ºC and, using the microscope, compare these with an untreated
sample.
B.4.3 Results
When compared with an untreated sample the glass beads shall not be darker.

10 © BSI 17 September 2004

 EN 1423:1997

Annex C (normative)
Glass bead imperfections
C.1 Oval glass beads (see Figure C.1)
When the ratio of the major diameter D to the minor diameter d is greater than 1,3 (D/d > 1,3), the oval
glass bead is considered defective.

Figure C.1 — Oval glass bead

C.2 Satellites (see Figure C.2)

When a glass bead supports more than two smaller glass beads, called satellites, or when, in the case of
two satellites, the ratio of the diameter d of the major of them to the diameter D of the supporting glass
bead is greater than 0,25 (d/D > 0,25), the glass bead is considered defective.

Figure C.2 — Satellite

C.3 Tear shaped glass beads (see Figure C.3)

When the ratio of the major dimension L to the minor dimension l is greater than 1,3 (L/l > 1,3), the glass
bead is considered defective.

© BSI 17 September 2004 11

EN 1423:1997

Figure C.3 — Tear shaped glass bead

C.4 Glass beads fused together (seeFigure C.4)

When the ratio of the major dimension D2 to the minor dimensions D1 is greater than 1,3 (D2/D1 > 1,3), the
particle is considered a defective glass bead.

Figure C.4 — Two glass beads fused together

C.5 Roundish glass beads (see Figure C.5)

When the ratio of their major dimension L to the minor dimension l is greater than 1,3 (L/t > 1,3), the glass
bead is considered defective.

Figure C.5 — Roundish glass bead

12 © BSI 17 September 2004

 EN 1423:1997

C.6 Opaque glass beads (see Figure C.6)

Opaque glass beads are always considered defective.

Figure C.6 — Opaque glass bead

C.7 Milky glass beads (see Figure C.7)

The milky appearance is due to gaseous inclusions in part of in the whole volume of the bead. Milky glass
beads are always considered defective.

Figure C.7 — Milky glass bead

C.8 Gas inclusions (see Figure C.8)

!When the ratio of the sum of the projected area of the bubbles inside a glass bead Csi to the projected
area of the glass bead S is greater than 0.25 (Csi/S > 0,25), the glass bead is considered defective."

Figure C.8 — Gas inclusions

© BSI 17 September 2004 13

EN 1423:1997

C.9 Grains (see Figure C.9)

Glass particles which present one or more sharp angles.

Figure C.9 — Grain

C.10 Foreign particles

Particles which are not composed of glass.

Annex D (normative)
Test method to determine the quality of the glass beads
D.1 Procedure
In a representative sample, the determination of the percentage of defective glass beads shall be made
using the fraction quantities retained on each sieve after the granulometric analysis carried out in
conformity with ISO 565 and ISO 2591-1; the residue of the last sieving shall not be deemed to constitute
a fraction. The study of the defects of the glass beads shall be made using an optical device with a
magnification which results in the glass beads having an apparent diameter of 4 mm to 5 mm in its visual
field.
The glass beads collected from a sieve (e.g. 300 4m) shall be homogenized by passing them at least five
times through a small divider, after which a small sample shall be prepared (approximately 0,5 g) by
repeated division.
This sample is then passed in its entirety through a sieve with a mesh size very slightly larger than that
of the sieve from which the refuse material was collected (e.g. a 500 4m mesh where the refuse material
was left by a sieve with a 300 4m mesh) on to a transparent adhesive strip with a width of 20 mm or less
and with a length equal to the diameter of the sieve. Any glass beads which are not held on the strip shall
be gathered and repositioned until all have been affixed to the adhesive strip. Where there is an excess, a
fresh sample shall be prepared and a fresh adhesive strip shall be made up. It is recommended that the
glass beads be laid without rolling them, thus avoiding separation of the spherical glass beads from the
remainder.
The specimen thus prepared shall be examined in the following manner under the optical device. In order
to make the examination easier, the adhesive strip holding the glass beads may be cut into pieces, all of
which shall be treated under exactly the same conditions:
— the minimum requirement for assessment of the number of defective glass beads shall be the
observation of 600 glass beads per sieve, obtained from at least six different areas spread evenly over the
whole surface of the adhesive strip (or the whole collection of pieces) on which the glass beads have been
placed. In the case of the sieve associated with the highest amount of retained material, the following
two additional conditions shall also be fulfilled:
1) each area shall contain not less than 100 glass beads. Where this is not the case, a number of
adjoining areas shall be assembled in order to satisfy the criterion;
2) the difference between the highest and the lowest number of defective glass beads for the various
areas containing no less than 100 glass beads (a single area or adjoining areas which have been
assembled) shall not exceed 20 in absolute terms. If this criterion cannot be satisfied, another adhesive
strip shall be prepared.

14 © BSI 17 September 2004

 EN 1423:1997

EXAMPLE:
area 1: 17 defective glass beads in 108 glass beads;
area 2: 21 defective glass beads in 119 glass beads;
area 3: 18 defective glass beads in 103 glass beads;
area 4: 23 defective glass beads in 141 glass beads;
area 5: 16 defective glass beads in 123 glass beads;
area 6: 27 defective glass beads in 106 glass beads.
The range between the extreme number of defective glass beads is: 27 – 16 = 11.
— only those glass beads which are entirely located in the visual field are examined;
— first of all, count all the glass beads present in the visual field, and then all the glass beads which
feature at least one of the imperfections referred to in 4.4 and defined in Annex C.
Where examination is made by screen projection, the glass beads shall be immersed totally in a liquid with
a refractive index close to that of glass in order to highlight any gas inclusions, amongst other defects.
NOTE Where direct examination is made using stereoscopic microscopy, it may assist if an eye piece with a grid is used and if the
areas studied are restricted to about 20 glass beads at a time.

D.2 Results of counting

Sieving a representative sample of a glass bead granulometry through its n specific sieves, the total
weighted percentage of the defective glass beads shall be calculated using the following equation:
M 1 D1 + M 2 D 2 + Mn D n
W = --------------------------------------------------------------
M1 + M2 + Mn
where

W is the total weighted percentage of defective glass beads;

M1 is the percentage by mass of the glass beads retained on each of the n sieves;
D1 is the arithmetic mean of the percentage by number of the defective glass beads counted on five or
more samples properly taken from the glass beads retained on each of the n sieves.

The total weighted percentage of grains and foreign particles shall be calculated in the same manner.
Results of counting are presented in conformity with Table D.1 as an example for a granulometry ranging
from 125 4m to 600 4m.
Table D.1 — Example for presenting the results of counting with opening of sieves
(600 4m to 125 4m)
Opening Retained Percentage of defective glass beads on the different areas Arithmetic Weighted
of the percentage mean of the percentage
sieves on the sieves percentage of defective
M1 D1 beads1)
µm % n1 n2 n3 n4 n5 n6 % %
600 6,2 31 27 36 28 25 30 29,5 1,87
500 30,3 24 28 17 23 22 19 22,2 6,87
300 24,1 16 21 23 18 19 15 18,7 4,60
250 19,1 14 17 11 13 15 15 14,2 2,76
125 18,2 9 11 8 10 11 9 9,7 1,80
125 2,1
Total weighted percentages of defective glass bead 17,90
1) The values in this column are calculated as shown below for the first row.

6, 2 × 29, 5
1,87 = ----------------------------- with 97,9 = (6,2 + 30,3 + 24,1 + 19,1 + 18,2)
97, 9

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EN 1423:1997

Annex E (normative)
Test method to determine the presence of the moisture-proof coating
E.1 Procedure A
Procedure A shall be used when a quick indication is required.
The percentage of moisture-proofed glass beads is checked in accordance with the following test method.
For this test, 1 ml of glass beads is required, measured using a tube with an inside diameter ranging from
2 mm to 5 mm and which is graduated in 1/20 ml.

Figure E.1 — Funnel

The glass beads are sprinkled from a height of 5 mm onto a roughly 1 dm2 still water surface lying in a
funnel equipped with a graduated tube whose inside diameter ranges from 2 mm to 5 mm and which is
graduated in 1/20 ml from its sealed base.
Ensure that:
— the inner wall of the container above the water is dry;
— the surface of the water is still;
— the glass beads do not fall on top of one another.
Results
With V being the volume in millilitres of glass beads collected in the tube 5 min after sprinkling, the
percentage of moisture-proofed glass beads is equal to: (1-V) × 100.
WARNING ever put glass beads which have not been moisture-proofed into a container previously used to
hold moisture-proofed glass beads or the moisture-proofing agent.
E.2 Procedure B
Procedure B shall be used when precise results are required.
E.2.1 Apparatus
— a funnel 120 mm deep, with a top diameter of 150 mm and a 6,25 mm inside diameter stem;
— a washed cotton bag with 48 × 48 thread count (size approximately 450 mm × 250 mm);
— a bucket with a minimum capacity of 4 l filled with clear water at room temperature;
— a 500 ml beaker.

16 © BSI 17 September 2004

 EN 1423:1997

E.2.2 Procedure
Using the glass beads taken from a representative sample (see Clause 7) check the mass, which should be
approximately 400 g.
Turn the cotton bag (see E.2.1) inside out and pour in the sample.
Immerse the bag containing the test sample in the bucket of water for 30 s or until the bag is completely
immersed, whichever is the longer.
Remove the bag and sample from the water and squeeze the excess water out of the bag by twisting the
neck of the bag. With the neck of the bag still twisted tight, hang the bag up to drain at room temperature
for 2 h.
At the end of the 2 h period, mix the sample thoroughly by releasing the tension on the neck of the bag and
shaking it, thus loosening the beads from the bottom and sides of the bag.
Transfer the sample to a clean dry funnel (see E.2.1 and Figure E.1). The entire sample should flow through
the funnel without stoppage. Failure to flow shall be considered as failure to pass the test.
If the result is as described above as flowing without stoppage, the glass beads shall pass the test.
NOTE In cases when the beads block the funnel when first introduced, it is permissible to tap the funnel stem lightly to initiate the
flow.

Annex F (normative)
Test method to determine the presence of floatation coating
NOTE This test method is only valid if the granulometry of the glass beads is between 180 µm and 300 µm.

F.1 Principle
To determine the presence of floatation coating by estimating the percentage of glass beads floating on the
surface of xylene or n-heptane.
F.2 Apparatus and reagents
— a watch glass or Petri dish 50 mm to 75 mm in diameter;
— a syringe, pipette or eye dropper of 5 ml to 20 ml capacity;
— test sieves conforming with the requirements of ISO 565;
— xylene, of reagent grade;
— n-heptane, of reagent grade.
F.3 Procedure
a) Sieve out from a representative sample (see Clause 7) the fraction passing a 300 4m sieve but retained
on a 180 4m sieve.
b) Spread a monolayer of glass beads onto the clean watch glass and, using the syringe, slowly introduce
the xylene at the edge of the watch glass until the liquid is deep enough to allow the beads to float.
Care should be taken to avoid agitation of the glass beads whilst the xylene is being added.
c) Visually estimate the percentage of glass beads floating on the surface of the xylene.
d) Repeat a) and b) using a new sample of glass beads and using n-heptane in place of xylene.

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EN 1423:1997

F.4 Results
In order to pass the test the minimum percentage of glass beads floating shall be as in Table F.1.
Table F.1 — Percentages of floating glass beads
Liquid Minimum percentage floating
Xylene 90 %
n-heptane 75 %

Annex G (normative)
Test method to determine the friability index of the antiskid aggregates
G.1 Purpose
The purpose of this test method is to specify the procedure for determining the resistance of aggregates to
fragmentation.
G.2 Scope
This test method applies to aggregates of natural or artificial origin used in buildings or public works.
G.3 References
Test sieving: the granulometric analysis shall be conducted in accordance with ISO 2591-1.
Statistical consideration: the reproducibility of the test method has been verified following ISO 5725
Precision of test methods — Determination of repeatability and reproducibility for a standard test method
by inter-laboratory tests.
G.4 General
G.4.1 Principle
The test consists of measuring the granulometric variation of aggregates produced in a rotating cylinder
under strictly defined conditions by a process of fragmentation using a load in the presence of water.
The representative sample granulometry of the aggregates shall be: 0,2 mm to 2 mm or 0,2 mm to 4 mm.
Aggregates finer than 0,2 mm are not taken into consideration.
G.4.2 The friability index shall be defined by the quantity of material of less than 0,1 mm produced during
the test.
If M is the mass of the material subjected to testing and m is the mass of the material of less than 0,1 mm
produced during the test, the friability index will be, by definition:

m
F s = 100 -----
M

G.5 Apparatus
G.5.1 Standard apparatus
Equipment necessary for sampling the material and carrying out the granulometric analysis by sieving,
together with a set of sieves at least 200 mm in diameter with opening sizes of 0,1, 0,2, 1, 2, 4 and 8 mm.
G.5.2 Special apparatus
Rotating cylinder (micro-Deval apparatus).
An abrasive load consisting of balls of X30 Cr13 stainless steel with diameters:

+0,1 +0,1
30 – 0,5 mm, 18 – 0,5 mm and (10 ± 0,5) mm

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 EN 1423:1997

G.6 Material to be tested

G.6.1 Obtaining the sample
The mass of the material sent to the laboratory shall be at least 2 000 g.
The test shall be conducted on a sand of 0,2 mm to 2 mm or 0,2 mm and 4 mm.
G.6.2 Preparing the sample for testing
Prepare the sample for testing as follows:
— sieve the 2 000 g of material, when damp, using the sieves 0,2 mm and 2 mm or of 0,2 mm and 4 mm;
— dry the material in an oven at 105 ºC until its mass is constant, that is until successive weighings of
the sample separated by 1 h do not differ more than 0,1 %;
— homogenize and weigh a (500 ± 2) g test sample.
Prepare the steel balls used for the load as follows:

+10
— take nine balls 30 mm in diameter, the total mass being  975 – 50  g;
 

+10
— add 21 balls 18 mm in diameter, the mass being  490 – 50  g;
 
— complete the load, using balls of 10 mm diameter so that the total mass of the load is (2 500 ± 4) g.

The load wear shall be checked periodically. The 18 mm and 30 mm balls are checked by weighing as a
whole and replacing those which are most work, by separate weighing until the load is again within the
tolerances. The 10 mm balls are controlled per lot of 10; below a 34 g lot they shall be replaced by
conforming balls.
G.7 Carrying out the test
— Introduce the load into the test cylinder arranged with its opening upward; then insert 500 g of the
material prepared in accordance with the requirements of G.6.1 and G.6.2.
— Add 2,5 l of water and replace the cover.
— Rotate the cylinder at a speed of (100 ± 5) min–1 for 1 500 rotations or 15 min.
— Slowly pour all the contents of the tray over two superimposed sieves of 8 mm (to collect the abrasive
load) and of 0,1 mm respectively.
— Wash the whole, using a jet of water, until the water runs clear, then remove the 8 mm sieve.
— Dry the 0,1 mm sieve in an oven at 105 ºC until the mass is constant.
— Dry sieve the oversize material using the 0,1 mm sieve.
— Weigh all the oversize material on the 0,1 mm sieve. Let this mass be m½.
G.8 Expression of results
The mass m of the material less than 0,1 mm produced during the test, from the initial 500 g is equal to
500 – m½ (m = 500 m½).
The friability index is therefore:

( 500 – m′ ) m
F s = 100 × ---------------------------- = -----
500 5

rounded off to the nearest integer.

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EN 1423:1997

G.9 Precision
The repeatability (r) and the reproducibility (R) were determined according to the repetition of tests done
for each product in 18 laboratories. The interpretation was done according to ISO 5725. The estabished
values between the levels 16 and 38 are as follows:

— for Fs = 16: repeatability r = 2,0

reproducibility R = 4,2
— for Fs = 38: repeatability r = 6,2
reproducibility R = 8,4

!Annex H (informative)
Alternative test methods to determine the quality of glass beads
H.1 Scope
This annex establishes two alternative methods to determine the quality of glass beads. The test method
defined in Annex D shall be considered as the reference test method.
These alternative methods incorporate the correlated values to be used, in accordance with the maximum
weighted percentage of defective glass beads given in Table 4.
H.2 VISUAL TEST METHOD
H.2.1 Equipment and materials
— A complete series of 1/1 splitters.
— A projector shall be fitted with a 25 × magnification lens placed at a distance which gives an image
diameter of between 750 mm and 800 mm onto a screen provided with a 500 mm square screen divided
into 25 squares, or an optical magnifying device which allows a glass bead projection of between 50
and 150 units.
— A plane base capsule, between 60 mm and 70 mm in internal diameter or a glass plate with a
minimum area of 700 mm2.
— A silicone grease or a transparent adhesive tape.
— A liquid with a similar refractive index to that of the glass beads.
H.2.2 Procedure
A representative sample of an approximate mass of 0,3 g shall be prepared by reductions with splitters 1/1.
The representative sample so obtained is placed in the plane base capsule, previously wetted with a thin
coat of silicone grease, or on a transparent adhesive tape, distributed uniformly in order to cover completely
the square part of the screen with a single thickness of glass beads.
In case of obtaining a projection of over 150 glass beads, the count of the total number of glass beads is made
in three alternate diagonal squares. The obtained number is multiplied by 25 and is divided by 3. In case
of obtaining a projection of below 150 glass beads, the counting operation will include the total glass beads
in the visual field. The total number of glass beads shall include between 150 and 400.
After that, a second count is made of the number of non-round defective glass beads existing in the whole
squared screen, that is to say oval, satellites, tear shaped, fused together, roundish glass beads, grains and
foreign particles.
The sample is then covered by the liquid with refraction index similar to glass beads. In these conditions,
only the shape of those will be seen, and the glass inclusions will appear as black spots.
A third count is made of the number of round defective glass beads existing in the whole squared screen,
that is to say those which present black spots over 25 % of their surface, opaque and milky glass beads.
The defective glass beads will be counted only once although they present several defects."

20 © BSI 17 September 2004

 EN 1423:1997

!H.2.3 Results of counting

The percentage of defective glass beads will be calculated by the formula:
Md = (100 × Nmd)/Nm
where
Md is the percentage of defective glass beads;
Nmd is the total number of defective glass beads resulting from the sum obtained in those last two
counts;
Nm is the total number of glass beads.
The final result of Md is the average of, at least, three determinations.

H.2.4 Correlated values

When this alternative visual test method is used, the maximum weighted percentage of defective glass
beads, as defined in Table 4, shall comply with Table H.1.
Table H.1 — Maximum weighted percentage of defective glass beads
Diameter of glass beads Maximum weighted percentage of Maximum weighted percentage of
defective glass beads grains and foreign particles
mm % %
<1 18 3
U1 28 3

H.3 AUTOMATIC TEST METHOD

H.3.1 Principle
The method is applicable to glass beads with particle diameters of between 0,08 mm and 1 mm used for
road marking purposes.
The method relies upon: the optical properties of glass microbeads and defects to visually separate out
these elements; and image analysis techniques to determine the percentage of defects of the glass
microbeads.
The glass beads spread onto an opaque and shiny adhesive base (tape) are observed using reflected light
through a microscope lens.
The glass beads applied onto the adhesive tape constitute the test specimen.
The distinction between the specimen's various elements is governed by the phenomena of specular
reflection, diffusion and retro-reflection.
Under these observation conditions:
— the supporting base is reflective;
— the glass beads are both reflective and retro-reflective;
— the defects exhibit the same properties as the glass beads, but are less retro-reflective; they may be
diffusive;
The specimen is positioned perpendicularly to the optical axis. This experimental set-up makes it possible
to visually separate the glass beads, the defects and the supporting base. In these conditions:
— the observed spherically-shaped glass beads appear grey in colour;
— defects of beads appear darker than spherically-shaped glass beads;
— the supporting base appears white in colour."

© BSI 17 September 2004 21

EN 1423:1997

!H.3.2 Equipment
The measurement device consist of: an optical component that allows the observation of the test specimen
under reflected light, an image-acquisition system, and a software program to coordinate image acquisition
and processing
Optical system (see Figure H.1).
As regards both lighting and observation, the optical system is composed of microscope parts.
The selected lens provides for a 2.5× enlargement capacity and a 0,075 digital aperture.
The specimen is placed on a three axis mobile table:
— vertical motion allows focus adjustment;
— longitudinal and transversal motions allow the observation of various parts of the specimen.
In order to observe the specimen, the table shall be capable of rotating around its longitudinal axis.
The light intensity can be adjusted by means of a system of filters and diaphragms.
The acquisition and processing system comprises:
— a camera fastened to the optical system and a video screen;
— a computer;
— a specialized interface between the camera and the computer."

22 © BSI 17 September 2004

 EN 1423:1997

Key
1 Camera 8 Rotation
2 Source filter 9 Vertical
3 Camera filter 10 Transversal
4 Source 11 Longitudinal
5 Diaphragm F 12 Glass beads
6 Diaphragm A 13 Semi-reflective mirror
7 Table
Figure H.1 — Diagram of the optical system

"

© BSI 17 September 2004 23

EN 1423:1997

!H.3.3 Image analysis

These techniques allow for the automatic separation of those elements displaying different grey levels and
then performing the series of calculations necessary to obtain the percentage of defects.
Determination of the percentage of defects in the glass microbeads consists of:
— computing a grey-level histogram of the image (pixels);
— computing the surface area occupied by each category of object (defects/glass beads/ supporting base)
in the picture on the basis of the histogram generated.
NOTE The graphic should show enough contrast to enable each category of object to be identified by a peak on the histogram
(see Figure H.2)


Key 1
1 Supporting base
2 Glass beads
3 Defects
X Grey level
Y % of grey levels
Figure H.2 — Sample histogram of the levels of grey

The normalized histogram of the shades of grey for all of the specimen's pictures exhibits three modes; their
separation is performed automatically.
H.3.4 Operating mode
H.3.4.1 Test specimen
The glass beads coming from a representative sample are applied onto the adhesive part of an opaque and
shiny adhesive tape. Its characteristics shall allow for a distinct separation of the various histogram peaks.
In order to preserve the representativity of the specimen under examination in comparison with the overall
test sample, the tested products shall correspond with entire fractions obtained at the time of the
successive divisions described in Annex D.
This tape shall be perfectly taut and flat.
The particles cannot be superimposed, yet may touch one another."

24 © BSI 17 September 2004

 EN 1423:1997

!H.3.4.2 Conducting measurements

To examine the glass beads, the specimen shall be placed perpendicular to the optical axis under the lens.
Ensure that the image being viewed is clearly in focus.
Verify the proper adjustment of both the light source intensity and the contrast by means of controlling the
picture histogram: the position of the various peaks shall comply with the calibration characteristics.
Refer to the user's instruction manual regarding how to perform the measurements and interpret the
readings.
H.3.4.3 Calibration
The calibration characteristics are specific to each test apparatus and pertain to the position of the peaks
of the various elements in the histogram. They shall be controlled on a regular basis by means of reference
sample.
H.3.4.4 Number of measurement points
The level of enlargement specified in H.3.2 enables zones of the specimen to be observed within the range
of 3 mm to 4 mm.
The supporting base shall allow observing at least 50 zones (minimum number of zones to be analysed),
thus equivalent to roughly 3,000 particles.
Since the breakdown in the various types of glass beads on the adhesive tape is not homogeneous, it
becomes essential for the zones analysed to be spread evenly over the entire surface of the specimen.
H.3.4.5 Result of Counting
Result for a given specimen is expressed as average of the results obtained for all zones.
The result corresponds to the following surface area ratio:

Surface area of defects

Percentage of defects = ------------------------------------------------------------------------------------------------------------------------------------------------
Surface area of defects + Surface area of glass beads
H.3.5 Correlated values
When this alternative automatic test method is used, the maximum percentage of defective glass beads, as
defined in Table 4, shall comply with Table H.3.
Table H.3 — Maximum percentage of defective glass beads
Diameter of glass beads Maximum percentage of defective glass Maximum percentage of grains and
beads foreign particles
mm % %
<1 30 3
"

© BSI 17 September 2004 25

EN 1423:1997

!Annex ZA (Informative)
Clauses of this European Standard addressing the provisions of the EU
Construction Products Directive
ZA.1 Scope and relevant characteristics
This European Standard has been prepared under mandate M/111 “Circulation Fixtures”, as amended by
mandate M/132, given to CEN by the European Commission and the European Free Trade Association.
The clauses of the European standard shown in this annex, and/or another standard where relevant, meet
the requirements of the mandate given under the EU Construction Products Directive (89/106/EEC).
Compliance with these clauses confers a presumption of fitness of drop on materials for the intended uses
indicated herein.
NOTE 1 Other requirements and other EU Directives, not affecting the fitness for intended use may be applicable to the drop on
materials falling within the scope of this annex.
NOTE 2 In addition to any specific clauses relating to dangerous substances contained in this European Standard, there may be
other requirements applicable to drop on materials (e.g. transposed European legislation and national laws, regulations and
administrative provisions). In order to meet the provisions of the EU Construction Products Directive, these requirements need also
to be complied with, when and where they apply. An informative database of European and national provisions on dangerous
substances is available at the Construction web site on EUROPA (CREATE, accessed through http://europa.eu.int).
This annex establishes the conditions for the CE-marking of the drop on materials intended for the use
indicated in Table ZA.1 and shows the relevant clauses applicable. The scope of this annex is defined by
Table ZA.1."

26 © BSI 17 September 2004

 EN 1423:1997

!
Table ZA.1 — Relevant clauses
Product: Drop materials – Glass beads, anti-skid aggregates and mixtures of the two
Intended use(s): For circulation areas
Essential characteristics Requirement clauses in this Mandated level(s) or Notes
[and/or another] standard Class(es)
Visibility characteristics
• Refractive index (of • EN 1423:1997/4.2 Threshold level is
the glass beads) specified. The refractive
index shall comply at least
with the requirement for
Class A.
• Quality (proportion of • EN 1423:1997/4.4 None Pass/fail criteria is
defective glass beads) established, for defective
glass beads, in Table 4
• Granulometry • EN 1423:1997/4.1 The European Standard
and/or 5.4 establishes rules and
limits for the sieves.
• Colour co-ordinates • EN 1423:1997/5.3 Pass/fail criteria is
(x,y), of specified in Table 5.
non-transparent
anti-skid aggregates None
• Luminance factor ("), • EN 1423:1997/5.3 Pass/fail criteria is
of non-transparent specified.
anti-skid aggregates
Durability characteristics
• Against chemicals • EN 1423:1997/4.3 Pass/fail criteria is
(for glass beads) specified.
• Resistance to • EN 1423:1997/5.2 None The value of the “friability
fragmentation (for index” shall be indicated.
anti-skid aggregates)

The requirement on a certain characteristic is not applicable in those Member States where there are no
regulatory requirements on that characteristic for the intended use of the product. In this case,
manufacturers placing their products on the market of these Member States are not obliged to determine
nor declare the performance of their products with regard to this characteristic and the option
"no performance determined" (NPD) in the information accompanying the CE marking (see ZA.3) may be
used.
The “no performance determined” (NPD) option may not be used, however, where the essential
characteristic being relevant for the intended use of the product is subjected to a threshold level or pass/fail
criteria.
ZA.2 Procedure(s) for the attestation of conformity of drop on materials
ZA.2.1 System of attestation of conformity
The system of attestation of conformity for the drop on materials, in accordance with the decision of the
Commission of 18 June 1999 (1999/453/EC) which amends Decision 96/579/EC, as given in Annex III of the
mandate M111 "Circulation Fixtures”, as amended by M/132, is shown in Table ZA.2 for the indicated
intended use."

© BSI 17 September 2004 27

EN 1423:1997

!
Table ZA.2 — System of attestation of conformity

Product(s) Intended use(s) Level(s) or class(es) Attestation of

conformity
system(s)

— Permanent marking
tapes and preformed road
markings

— Traffic paints, hot

applied thermoplastics, cold
applied plastics: (with or
without anti-skid
aggregates) including
premixed glass beads

— Traffic paints, hot

applied thermoplastics, cold
applied plastics: (to be used
for road marking) put on the
For circulation areas None 1
market with indications on
types and proportions of
dropped-on glass beads
and/or anti-skid aggregates

— Retroreflecting road
studs

— Drop on materials: glass

beads, anti-skid aggregates
and mixtures of the two

System 1 : See CPD Annex III.2.(i), without audit-testing of samples

NOTE Despite the fact that this European Standard is limited, in its scope, to drop on materials, in Table ZA.2, the list of mandated
products has been copied exactly as it is in mandate M/111 and M/132.
The attestation of conformity of the drop on materials falling within the scope of this European Standard
shall be carried out according to the evaluation of conformity procedures indicated in Table ZA.3.
"

28 © BSI 17 September 2004

 EN 1423:1997

!
Table ZA.3 — Assignment of evaluation of conformity tasks (for system 1)
Tasks Content of the task Clauses to apply
(1) Factory production All characteristics of EN 13212:2001
Tasks for the control (F.P.C) Table ZA.1
manufacturer (2) Further testing of All relevant characteristics of 6.4 of EN 13212:2001 as
samples taken at factory Table ZA.1 appropriate
(3) Initial type testing All characteristics of 4.2, 4.3, 4.4, 5.2, 5.3 and
Table ZA.1 5.4 of EN 1423:1997, as
appropriate
Tasks for the (4) Initial inspection of All characteristics of EN 13212:2001, as
notified body factory and of F.P.C Table ZA.1 appropriate
(5) Continuous All relevant characteristics of EN 13212:2001, as
surveillance, assessment Table ZA.1 appropriate
and approval of F.P.C.
A manufacturer having a Quality System conforming with EN ISO 9002:1994 or EN ISO 9001:2000 and
which addresses the requirements of this annex, is recognised as satisfying the F.P.C requirements
specified in Table ZA.3.
Where the drop on materials falling within the scope of this European Standard have previously been
tested in accordance with all the relevant requirements herein specified, such tests may be taken into
account for initial type testing purposes in order to avoid unnecessary additional testing burden.
ZA.2.2 Certificate and Declaration of Conformity
When compliance with the system of attestation of conformity is achieved, the notified body shall draw up
a Certificate of Conformity (EC Certificate of Conformity) with the information indicated below.
The EC Certificate of Conformity shall include the following information:
— name, address and identification number of the notified body;
— name and address of the manufacturer, or his authorised representative established in the EEA and
place of production;
— description of the product (type of drop on material: glass beads, anti-skid aggregates or a combination
of the two; in addition: a) for anti-skid aggregates, if they are transparent or non transparent; b) in a
combination of glass beads and anti-skid aggregates, the proportion of the components);
— the presence of a surface treatment and its intended use;
— provisions to which the product conforms (Annex ZA of this European Standard);
— particular conditions applicable to the use of the product, if any;
— the certificate number;
— conditions and period of validity of the certificate, where applicable, and;
— name of, and position held by, the person empowered to sign the certificate.
This EC Certificate of Conformity entitles the manufacturer to affix the CE marking, as described in ZA.3
of this annex.
In addition, for each product covered by an EC Certificate of Conformity, the manufacturer shall draw up
a Declaration of Conformity (EC Declaration of Conformity) including the following information:
— name and address of the manufacturer, or his authorised representative established in the EEA;
— name and address of the notified body;
— description of the product and a copy of the information accompanying the CE marking;
— number of the attached EC Certificate of Conformity and;
— name of, and position held by, the person empowered to sign the declaration on behalf of the
manufacturer or of his authorised representative.
Both documents shall be presented, by supplying with the original documents the corresponding
translations, in the official language or languages of the Member State of the EU in which the product is
to be used."

© BSI 17 September 2004 29

EN 1423:1997

!ZA.3 CE marking and labelling

The CE marking shall be affixed visibly, legibly and indelibly, with the form as described in Council
Directive 93/68/EC and Council Decision 93/465/EC, and shall be easily accessible to the market
surveillance authorities.
The manufacturer or his authorised representative established within the EEA is responsible for the
affixing of the CE marking. The CE marking shall be affixed before the product is placed on the market.
The manufacturer, or his authorised representative established within the EEA, may decide when to affix
the CE marking depending upon the circumstances of the production process of the product. Where the CE
marking is affixed sometime after the manufacture of the product, the validity of the testing carried out
during production shall be confirmed.
The CE conformity marking consists exclusively of the letters “CE”, in the previously specified form,
followed by the identification number of the notified body and then the following additional information:
— name or identifying mark of the manufacturer* and registered address;
— the last two digits of the year in which the product was manufactured;
— the number of the EC certificate of conformity;
— the number and the year of this European Standard (i.e. EN 1423:1997);
— description of the product (type of drop on material: glass beads, anti-skid aggregates or a combination
of the two; in addition: a) for anti-skid aggregates, if they are transparent or non transparent; b) in a
combination of glass beads and anti-skid aggregates, the proportion of the components);
— the batch number;
— the presence of a surface treatment and its intended use;
— indications to identify the mandated characteristics of the product.
*NOTE This is the name of the manufacturer not the authorised representative established in the EEA. The purpose of this
information is to identify the legal entity responsible for the manufacture of the product. The CPD does not require the manufacturer
to be established in the EEA nor does it require that a manufacturer from a non-EEA country has an authorised representative
established in the EEA.
The CE marking and the accompanying information shall be placed on the packaging of the product. When
not possible, such as bulk deliveries, it shall be done on the accompanying commercial documents such as
delivery notes.
The identification of the mandated characteristics shall be made as follows:

EN 1423:1997 – European Standard of reference including the year of publication of

the last applicable version;
Refractive index (of the – Specify the class of performance according to EN 1423:1997/4.2;
glass beads)
Granulometry – According to the rules established in EN 1423:1997/4.1 and/or 5.4, as
appropriate. Specify the upper and lower nominal sieves;
Resistance – Specify the value of the “friability index”.
to fragmentation
(for anti-skid aggregates)
"

30 © BSI 17 September 2004

 EN 1423:1997

!In the following examples, a format for the presentation of the CE marking and accompanying
information is given:
Table ZA.4 — Example of CE-marking information for glass beads

CE CE conformity marking, consisting of the “CE”-

symbol as given in directive 93/68/EEC.

0123-CPD-0001 Identification number of the notified body

AnyCo Ltd, PO Box 21, B-1050 Name or identifying mark and registered
address of the producer

Date of manufacturing: 2001 Last two digits of the year in which the product
was manufactured

Notified Body 0123-CPD-0456 Number of the EC Certificate of Conformity

EN 1423:1997 Number and year of this European standard

Mandated characteristics: According to EN 1423:1997, as appropriate:

• Refractive index: Class A See 4.2

• Granulometry: 600-125µm See 4.1

Batch 13032001 Batch number

20 Kg Net mass

"

© BSI 17 September 2004 31

EN 1423:1997

!
Table ZA.5 — Example of CE-marking information for a combination of glass beads and
anti-skid aggregates

CE CE conformity marking, consisting of the “CE”-symbol

as given in directive 93/68/EEC.

0123-CPD-0001 Identification number of the notified body

AnyCo Ltd, PO Box 21, B-1050 Name or identifying mark and registered
address of the producer

01 Last two digits of the year in which the product

was manufactured

0123-CPD-0457 Number of the EC Certificate of Conformity

EN 1423:1997 Number and year of this European standard

Mandated characteristics: According to EN 1423:1997, as appropriate:

1. for the glass beads :

• Refractive index: Class A See 4.2

• Granulometry: 425-90 µm See 4.1

2. for the anti-skid aggregates :

• Friability index: 9 See 5.2

• Granulometry: 710-150 µm See 5.4

3. for the combination of the two :

• Proportion
of the components: 80-20 See clause 6

17152001 Batch number

20 Kg Net mass

"

32 © BSI 17 September 2004

 BS EN 1423:1998

! Bibliography

EN ISO 9002:1994, Quality systems — Model for quality assurance in production, installation and servicing
(ISO 9002:1994).
EN ISO 9001:2000, Quality management system — Requirements (ISO 9001:9000)."

© BSI 17 September 2004 33

BS EN
1423:1998
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