Operating Manual: English
Operating Manual: English
Operating Manual: English
Operating manual
19510306.doc 24.01.11
Operating manual
Congratulations!
You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the operation
and possible applications of our circulators. For optimal utilization of all functions, we
recommend that you thoroughly study this manual prior to beginning operation.
2
MB
TABLE OF CONTENTS
3
Operating manual
8.1. Excess temperature protection ........................................................................27
8.1.1. Early warning system, low level protection .............................................. 28
8.2. Switch-over from warning to shutdown function ..............................................29
8.3. Over and Sub temperature warning function ...................................................30
9. Menu functions.........................................................................................31
9.1. MENU Configuration ........................................................................................32
9.1.1. Configuration of the mode of the key ........................................... 33
9.1.2. Remote control: activate – deactivate...................................................... 33
9.1.3. Automatic / non-automatic start mode ..................................................... 33
9.1.4. Reset - Factory setting ............................................................................. 34
9.2. MENU Control parameters – Xp, Tv, Tn ..........................................................34
9.3. MENU SERIAL - BAUDRATE, PARITY, HANDSHAKE ..................................36
9.4. MENU ATC - Absolut Temperature Calibration ...............................................37
9.4.1. ATC STATUS - YES / NO........................................................................ 39
9.4.2. ATC - TYPE: 1 -/ 2 -/ 3 POINT................................................................. 39
9.4.3. Example: 3-point calibration for internal control...................................... 40
9.5. MENU LIMITS ..................................................................................................42
10. Troubleshooting guide / error messages .............................................................43
11. Electrical connections ..........................................................................................45
12. Remote control.....................................................................................................46
12.1. Setup for remote control ..............................................................................46
12.2. Communication with a PC or a superordinated data system.......................46
12.3. List of commands.........................................................................................47
12.4. Status messages .........................................................................................48
12.5. Error messages............................................................................................48
13. JULABO Service – Online remote diagnosis .......................................................50
14. Cleaning / repairing the unit .................................................................................51
4
MB
Operating manual
1. Intended use
JULABO circulators have been designed to control the temperature of specific fluids in a bath
tank.
The units feature pump connections for temperature control of external systems (loop circuit).
JULABO circulators are not suitable for direct temperature control of foods, semi-
luxury foods and tobacco, or pharmaceutical and medical products. Direct
temperature control means unprotected contact of the object with the bath
medium (bath fluid).
1.1. Description
The circulators are operated via the splash-proof keypad. The implemented
microprocessor technology allows to set and to store different values that
can be indicated on the MULTI-DISPLAY (LED). Three menu keys facilitate
adjusting setpoints, warning and safety functions and menu functions.
The PID temperature control adapts the heat supplied to the thermal
requirements of the bath.
Absolute Temperature Calibration (ATC3) provides a high temperature
PID2 stability in the bath. With the 3-point calibration an offset is adjusted at three
temperatures to ensure an accurate temperature pattern at the selected spot
in the bath over the full temperature range.
ATC3 Electrical connections:
The serial interface RS232 to allows modern process technology without
RS232 additional interface.
Alarm output for external alarm message or control of JULABO refrigerating
baths or solenoid valve (cooling water).
The excess temperature protection conforming to IEC 61010-2-010 is a
safety installation independent from the control circuit. This protection can be
indicated and set on the MULTI-DISPLAY (LED).
The early warning system for low level signals that bath fluid needs to be
refilled before the low level protection conforming to IEC 61010-2-010
causes a complete shut-down of the main functional elements.
5
Operator responsibility – Safety recommendations
Make sure all persons tasked with operating, installing, and maintaining the unit have read
and understand the safety information and operating instructions.
When using hazardous materials or materials that could become hazardous, the circulator
may be operated only by persons who are absolutely familiar with these materials and the
circulator. These persons must be fully aware of possible risks.
If you have any questions concerning the operation of your unit or the information in this
manual, please contact us!
Contact: JULABO Labortechnik GmbH Tel. +49 (0) 7823 / 51-0 [email protected]
Eisenbahnstraße 45
Fax +49 (0) 7823 / 24 91 www.julabo.de
77960 Seelbach / Germany
Appropriate operation
Only qualified personnel is authorized to perform configuration, installation, maintenance and
repairs of the circulator.
Routine operation can also be carried out by untrained personnel who should however be
instructed by trained personnel.
Use:
The bath may not be filled with flammable materials. Fire hazard!
Only use recommended materials (bath fluids). Only use non-acid and non corroding
materials.
6
MB
When using hazardous materials or materials that could become hazardous, the operator
must affix the enclosed safety labels (1 + 2) to the front of the unit so they are highly visible:
1 Warning label W00: Colors: yellow, black
Danger area. Attention! Observe instructions.
(operating manual, safety data sheet)
2 Mandatory label M018: Colors: blue, white
Carefully read the user information prior to beginning operation.
Scope: EU
or
2 Semi S1-0701 Table A1-2 #9
Carefully read the user information prior to beginning operation.
Scope: USA, NAFTA
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be
touched.
Warning label W26: Colors: yellow, black
Hot surface warning.
(The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to
the circulator, particularly the respective safety recommendations. Also observe the pin
assignment of plugs and technical specifications of the products.
2.1. Disposal
The circulator contains a back-up battery that supplies voltage to the memory chips when the
unit is switched off. Do not dispose of the battery with household waste!
Depending on battery regulations in your country, you may be obligated to return used or
defective batteries to collection sites.
Valid in EU countries
Directive 2002/96/EC of the European Parliament and of the Council of 27
January 2003 on waste electrical and electronic equipment (WEEE).
This directive requires electrical and electronic equipment marked with a
crossed-out trash can to be disposed of separately in an environmentally
friendly manner.
Contact an authorized waste management company in your country.
Disposal with household waste (unsorted waste) or similar collections of
municipal waste is not permitted!
7
Operator responsibility – Safety recommendations
2.2. EC Conformity
With the ‘1PLUS warranty’ the user receives a free of charge extension to the warranty of up
to 24 months, limited to a maximum of 10 000 working hours.
To apply for this extended warranty the user must register the unit on the JULABO web site
www.julabo.de, indicating the serial no. The extended warranty will apply from the date of
JULABO Labortechnik GmbH’s original invoice.
JULABO Labortechnik GmbH reserves the right to decide the validity of any warranty claim. In
case of faults arising either due to faulty materials or workmanship, parts will be repaired or
replaced free of charge, or a new replacement unit will be supplied.
8
MB
9
Operator responsibility – Safety recommendations
MB
Temperature selection digital
via keypad indication on MULTI-DISPLAY(LED)
remote control via personal computer indication on monitor
Temperature indication MULTI-DISPLAY (LED)
Resolution °C 0.01
Absolute Temperature Calibration °C ±3
Temperature control PID 2
Heater wattage (at 230 V) kW 2,0
Heater wattage (at 115V) kW 1,0
Circulating pump:
discharge, max.at 0 bar l/min 10
pressure, max. at 0 l bar 0.12
Electrical connections:
External alarm device Vdc/mA 24-0 / max. 25
Computer interface RS232
Ambient temperature °C 5 ... 40
10
MB
Caution:
The unit is not for use in explosive environment
11
Operating instructions
Operating instructions
Caution:
Describes a possibly dangerous situation. If this is not avoided, slight or minor
injuries could result. A warning of possible property damage may also be
contained in the text.
Notice:
Describes a possibly harmful situation. If this is not avoided, the product or
anything in its surroundings can be damaged.
Important!
Indicates usage tips and other useful information.
12
MB
• Some parts of the bath cover and the pump connections may become
extremely warm during continuous operation. Therefore, exercise particular
caution when touching these parts.
13
Safety notes for the user
Caution:
The temperature controlling i.e. of fluids in a reactor constitutes normal
circulator practice.
We do not know which substances are contained within these vessels.
Many substances are:
• inflammable, easily ignited or explosive
• hazardous to health
• environmentally unsafe
i.e.: dangerous
The user alone is responsible for the handling of these substances!
The following questions shall help to recognize possible dangers and to reduce
the risks to a minimum.
• Are all tubes and electrical cables connected and installed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
• Do dangerous steams or gases arise when heating?
Is an exhaust needed when working?
• What to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and
determine the method of decontamination.
14
MB
4.1. Circulator
Front view Rear view
Navigation keys
2 1. Key: >OK< Start / Stop (pump / heater )
2. >OK< in the menu Menu item / select submenu for setting
Save set value
Save selected parameter
A beep signals the end of setting
After the actions Start, Stop and change from VFD Display to
standard display the key is locked for a short time.
The above graph “front side” shows an example for standard display.
15
Operating controls and functional elements
Navigation aids
Flashing segments show the position
within the structure of the menu.
Item „P“ flashes simultaneously in the
submenu.
Menu keys
5 Key: start the menu > warning and safety values<
6 Key: start the menu >temperature setpoints<
7 Key: display of MENU structure
16
MB
5. Preparations
5.1. Installation
Notice:
Plexiglas and Makrolon baths are not resistent to solvents.
Avoid contamination of the bath fluid with solvents.
MB-5
• The circulator (A) mounted on a stainless steel bridge is
A placed on the back of bath tank.
Close the bath tank with the bath cover (B).
Top view • The circulator (A) fitted with a stainless steel bridge is
placed on the right side of the bath tank leaving the bath
open on the left side.
MB-13A / MB-19A
17
Preparations
Caution:
No liability for use of other bath fluids!
Do not use flammable bath fluids!
Caution:
Fire or other dangers when using bath fluids that are not recommended:
Please contact JULABO before using other than recommended bath fluids.
Use only nonacidic and noncorrosive bath fluids.
JULABO assumes no liability for damage caused by the selection of an
unsuitable bath liquid.
Unsuitable bath fluids are fluids which, e.g.,
• are highly viscous
(much higher than recommended at the respective working temperature)
• have a low viscosity and have creep characteristics
• have corrosive characteristics or
• tend to crack.
• No liability for use of other bath fluids!
18
MB
15
(24a) and return flow (24b).
A
M
P
24a 24b
15
A
M
P
15
A
M
P
⇐ MB-5
24a 24b
5.1.1. Tubing
Recommended tubing:
Order No. Length Temperature range
8 930 008 1 m CR® tubing 8 mm inner dia. -20 °C to 120 °C
®
8 930 010 1 m CR tubing 10 mm inner dia. -20 °C to 120 °C
8 930 108 1 m Viton tubing 8 mm inner dia. -50 °C to 200 °C
8 930 110 1 m Viton tubing 10 mm inner dia. -50 °C to 200 °C
8 930 410 1 m Insulation for tubing 8 mm or -50 °C to 100 °C
10 mm inner dia.
19
Preparations
Warning: Tubing:
At high working temperatures the tubing used for temperature application and
cooling water supply represents a danger source.
A damaged tubing line may cause hot bath fluid to be pumped out within a
short time.
This may result in:
• Burning of skin
• Difficulties in breathing due to hot atmosphere
Safety recommendations
• Employ suitable connecting tubing.
• Make sure that the tubing is securely attached.
• Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
• Regularly check the tubing for material defects (e.g. for cracks).
• Preventive maintenance: Replace the tubing from time to time.
Examples:
Internal applications in the bath
A
A 100 % internal bath circulation
B internal100 % (for large bath tanks)
B Reduced internal bath circulation
(for smooth surface of bath fluid)
C
External/internal applications
C 40 % external discharge,
internal 20 % 60 % internal circulation
external 80 % (for large bath tanks)
D D 80 % external discharge,
20 % internal circulation
(for small bath tanks)
20
MB
Filling
• Take care that no liquid enters the interior of the circulator.
• Recommended maximum filling level with water as bath liquid:
20 mm below the tank rim
L After filling, immerse the samples in the bath or place the lid on
the bath, in case the opening is not to be used.
L The circulator provides an early warning system for low level
that may be triggered when changing samples in the bath.
Draining
• Press the mains switch to turn the circulator off.
• Remove the circulator from the bath tank.
• Empty the bath tank.
21
Preparations
5.4. Countercooling
Notice:
Securely attach all tubing to prevent slipping.
Observe the laws and regulations of the water distribution company valid in the
location where the unit is operated.
15
A
M
P
15
A
M
P
Cooling coil
⇐ MB-5A / MB-7A / MB-5M
25a 25b
15
A
M
P
15
A
Cooling coil
M
⇐ MB-5
P
25a 25b
22
MB
JULABO MVS By installing the MVS controller (26)
and a solenoid valve (27), sudden
RS 232
temperature increases can be rapidly
reversed by tap water flowing through
26 the built-in cooling coil.
For applications requiring constant
27 15
A
15
A
M
P
NOTE: Immersion coolers are used for countercooling instead of tap water in
applications below room temperature.
Order No. Description
9 650 820 FT200
9 650 840 FT400
8 970 400 Clamp for cooler probe for stainless steel or
plexiglass bath tanks
23
Operating procedures
6. Operating procedures
Check to make sure that the line voltage matches the supply voltage
specified on the identification plate.
Switching on:
• Turn on the mains power switch (1).
24
MB
7. Setting of temperatures
The function of the key is configurable.
1. If the key is pressed, normally only one adjustable working
temperature is displayed (factory setting).
2. Using the Menu Configuration which is started by pressing the
key a menu with three pre-set setpoints can be
assigned to the key.
L Press key if a value is to be retained.
26
MB
Recommendation:
Set the excess temperature protection at 5 °C to 10 °C above the
working temperature setpoint.
27
Safety installations, warning functions
Turn off the unit with the mains switch, refill bath fluid and turn
the unit on again!
3. Float
4. Circulating pump
5. Heater
28
MB
29
Safety installations, warning functions
Recommendation:
Set the over temperature warning value > t High < 5 °C to 10 °C
above the working temperature setpoint.
Set the sub temperature warning value > t Low < 5 °C to 10 °C
below the working temperature setpoint.
30
MB
9. Menu functions
The term „Menu functions“ refers to settings such as
Menu level 1
>CFG< - Configuration of the unit page 32
>3SP< - 3-setpoint mode
>rt< - REMOTE – on / off (remote control via RS232)
>Aut < – AUTOSTART on / off
>rST< - RESET – factory settings
Control parameter XP
Control parameter Tn
Control parameter Tv
>br< - Baudrate
>Pty< - Parity
>HS< - Handshake
31
Menu functions
32
MB
AUTOSTART on.
AUTOSTART off.
Notice:
The circulator has been configured and delivered by JULABO in
accordance with the NAMUR recommendations. This means for the
start mode that the unit must enter a safe operating status after a
power failure. This safe operating status is indicated by the message
„OFF“ or „r OFF“ on the MULTI-DISPLAY (LED).
A complete, all-pole shutdown of the main functional elements such
as heater and pump motor is effected.
The values set on the circulator remain saved and the unit is
restarted by pressing the start/stop key in manual control.
In remote control mode the values need to be resent by the PC via
the interface.
If such a safety standard is not required, the NAMUR
recommendations can be bypassed with the AUTOSTART function
thus allowing a direct start of the circulator by pressing the mains
switch or using a timer.
33
Menu functions
Warning:
For supervised or unsupervised operation with the “AUTOSTART“ function
avoid any hazardous situation to persons or property
Take care to fully observe the safety and warning functions of the circulator.
34
MB
35
Menu functions
>PtY< - PARITY
• The parameter flashes, switch by pressing
and
0 no: Datenbits = 8; Stopbits = 1
1 odd: Datenbits = 7; Stopbits = 1
2 even: Datenbits = 7; Stopbits = 1
>HS< - HANDSHAKE
• The parameter flashes, switch by pressing
and
Xon/Xoff-protocol (Software handshake)
Protocol RTS/CTS (Hardware handshake)
36
MB
Principle:
Example: For ATC calibration, in steady state the bath temperature at the
1-point calibration location of the temperature sensor (CT) is determined at the
°C respective adjusted working temperature. This value is then set on
the circulator in the menu >ATCalibration< under menu item >Ctx<.
This can be a 1-point, 2-point or 3-point calibration.
TT1 M B (INT) T
°C
°C
3-point calibration
°C
TT
TT1
M = Temperature measuring instrument with temperature sensor
B = Bath tank (INTernal or EXTernal)
T = circulator
°C
CT = Temperature on measuring point
TT 1 = Original curve
TT = Temperature on circulator
Menu level 1
37
Menu functions
38
MB
L In the > ATC STATUS < >YES< the ATC calibration always affects
the current working temperature; also the one set via interface.
Pairs of values:
tt X: Circulator temperature 1 or 2 or 3 (actual value TT )
The actual temperature of the bath is simultaneously saved with
the “calibration value“ >CALVAL< and can be indicated for control
purposes (value does not flash).
39
Menu functions
3. Calibration
40
MB
41
Menu functions
Factory settings:: The limitation of the operating temperature range effects the
temperature setting in the menu with the key .
200 °C Only setting of working temperatures which lie within the
(Setpiont High) determined limits is possible
This applies to settings in the MENU ,
-50 °C (refer to page 25)
(Setpoint Low)
and for settings in the MENU
high temperature low temperature
42
MB
8
heater and circulating pump is effected.
43
Troubleshooting guide / error messages
60
By quickly switching off and restarting the unit the alarm is
45 15
4s cancelled.
30 If the error occurs once more after the restart, a remote diagnosis is
required.
„Configuration Error“
The configuration of the circulator does not correspond with its current
application.
Press the key for a non-recurring, automatic change of the
configuration.
In this case please call the JULABO Technical Service or an authorized
dealer.
15
A
M
P
Mains circuit breakers (resettable) 15 A
44
MB
/ Control output
The connector may be used for control of JULABO refrigerated
circulators or as output for alarm messages.
In remote control mode, the start command and all values to be set
must be resent by the PC via the interface in case of a power
interruption.
AUTOSTART is not possible.
46
MB
48
MB
ERROR MESSAGES Description
-05 WORKING SENSOR ALARM Working temperature sensor short-circuited or
interrupted.
-06 SENSOR DIFFERENCE ALARM Sensor difference alarm.
Working temperature and safety sensors
report a temperature difference of more than
35 K.
-07 I2C-BUS ERROR Internal error when reading or writing the I2C
bus.
-08 INVALID COMMAND Invalid command.
-09 COMMAND NOT ALLOWED IN Invalid command in current operating mode.
CURRENT OPERATING MODE
-10 VALUE TOO SMALL Entered value too small.
-11 VALUE TOO LARGE Entered value too large.
-12 TEMPERATURE MEASUREMENT Error in A/D converter.
ALARM
-13 WARNING : VALUE EXCEEDS Value lies outside the adjusted range for the
TEMPERATURE LIMITS high and low temperature warning limits. But
value is stored.
-14 EXCESS TEMPERATURE Excess temperature protection alarm
PROTECTOR ALARM
49
JULABO Service – Online remote diagnosis
see example
50
MB
Caution:
• Always turn off the unit and disconnect the mains cable from the power
source before cleaning the unit.
• Prevent humidity from entering into the circulator.
• Electrical connections and any other work must be performed by qualified
personnel only.
Cleaning:
For cleaning the bath tank and the immersed parts of the
circulator, use low surface tension water (e.g., soap suds).
Clean the outside of the unit using a wet cloth and low surface
tension water.
The circulator is designed for continuous operation under normal
conditions. Periodic maintenance is not required.
The tank should be filled only with a bath fluid recommended by
JULABO. To avoid contamination, it is essential to change the
bath fluid from time to time.
Repairs
Before asking for a service technician or returning a JULABO
instrument for repair, please contact an authorized JULABO
service station.
51