International Journal of Scientific & Engineering Research, Volume 5, Issue 7, July-2014 1532

ISSN 2229-5518

Effect of heat input on microstructure and mechanical properties of the TIG

welded joints of AISI 304 stainless steel

T.A.Tabish*,1 T.Abbas*, M.Farhan*, S.Atiq*, T.Z.Butt**

Abstract:

AISI 304 stainless steel plates were butt-welded through manual tungsten inert gas
welding (TIG) process. The process was applied to different specimens by varying heat inputs
(low, medium and high). The microstructural features and mechanical properties of the welded
joints were examined. The results showed that the tensile strength of welded specimens was
greater than that of the base metal. Maximum tensile strength was possessed by the specimen
welded using low heat input and vice versa. Microhardness measurements implied that hardness

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near the upper surface of the weld is high and that near the center of the weld is low because of
the faster cooling of the exterior than the interior of the weld. Microhardness increased from 205
VHN to 230 VHN for low heat input, 194 VHN to 211 VHN for medium heat input, and 182
VHN to 195 VHN for high heat input welded specimens. The microstructural study indicated
that the high heat input produced larger dendrites than those produced with medium, and low
heat input.

Keywords:

Tungsten inert gas are welding, Microstructure, Micro hardness, Tensile Test

Introduction: important structural material for nuclear

plants. Consequently, reactor coolant piping,
Excellent mechanical properties of
valve bodies and vessel internals have been
austenitic stainless steels made them an
manufactured from these steels. However,
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International Journal of Scientific & Engineering Research, Volume 5, Issue 7, July-2014 1533
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welding frequently leads to poor mechanical coarser structure and carbides, which are
properties of the weldment due to the rich in chromium, deteriorate the mechanical
metallurgical changes associated with fusion properties of the weldment [2,3]. Therefore,
welding processes such as segregation, type 300 series is often joined through gas
precipitation of secondary phases, presence tungsten arc welding (GTAW), also known
of porosities, solidification cracking and as tungsten inert gas (TIG) welding,
grain growth in the heat affected zone essentially consisting of production of an arc
(HAZ) etc. [1]. Type 300 series of austenitic between a non-consumable tungsten
stainless steels contain considerable amounts electrode and the work piece. An inert gas,
of chromium and nickel; the former provides usually argon, protects the arc, electrode and
corrosion resistance and the latter stability of molten pool from atmospheric
austenite phase at room temperature. The contamination. While joining the thinner
basic composition of traditional austenitic surfaces, edge joints and flanges, filler

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stainless steel includes 18% chromium and metals are generally not required. However,
8% nickel, but can also include small for thicker cross-sections, a filler metal is
proportions of molybdenum, titanium, needed to feed the joint. TIG welding is
niobium, copper and nitrogen. Other useful equally capable of joining thin as well as
properties of engineering significance such thick materials to achieve quality welds for
as excellent corrosion resistance, superior materials ranging from stainless steels to
creep rupture strength and impact resistance non-ferrous alloys. TIG welding has some
at low temperatures make austenitic limitations as compared to gas metal arc
stainless steels a competitive choice for welding (GMAW), major being inferior
industrial plants encompassing applications joint penetration and poor tolerance to many
in chemical processing, food production, material compositions [4,5]. However,
marine hardware, furnaces, heat exchangers, penetrating ability of activated TIG arc can
gas turbines, and cryogenic vessels. markedly be improved by applying fluxes,
generally composed of oxides of Mn, Mo,
To fabricate stainless steel structures,
Ti, Si and Al, on surfaces prior to welding [6
welding is generally the most convenient
– 8]. However, the primary drawback of
process. But the common arc welding results
TIG welding process is its inability to join
in coarse grains and carbides formation
thicker surfaces in a single pass. For butt-
along the grain boundaries in HAZ. Both the
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International Journal of Scientific & Engineering Research, Volume 5, Issue 7, July-2014 1534
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joint penetration, multi-pass technique must microstructural observations and mechanical

be used when thickness of stainless steel properties.
plates to be joined exceeds 3mm [2,8]. The
Materials and Experimental Procedures:
laser-TIG hybrid welding overcomes these
limitations allowing improved welding AISI 304 stainless steel plates of
stability and greater melting efficiency [1]. sizes 200mm x 100mm x 6mm cut from a
rolled sheet and the filler 308 stainless steel
In preceding studies, joints made
solid electrode EW-Th-2 (thoriated
from the TIG welding process have not been
tungsten) of 3.15 mm diameter were utilized
examined in detail with reference to
for this study. The measured compositions
microhardness varying across the joint. The
of base and filler materials are given in
present work expatiates the TIG joints of
Table 1.
AISI 304 stainless steel plates through

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Table 1. Composition of Base & Filler Material

Alloy C Si Mn P S Cr Ni Fe

304
0.07 0.41 1.89 0.03 0.015 18.6 8.48 Balance
SS

308
0.08 1.0 1.59 0.045 0.03 18.10 10.09 Balance
SS

Table 2 (a – c) for samples welded at low,

medium and high heat respectively.
Argon gas was used as shielding
medium during the TIG Welding and the
pressure was maintained at 15 L/min.
Cleaning of the surfaces to be joined was
accomplished by a combination of vapor and
liquid cleaners. Samples were supported by
conventional fixtures to facilitate smooth
Table 2 (a) Process Parameters used for fabrication butt
welding. The conditions used during the welded joints (Low Heat)

TIG welding process are mentioned in

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Average
Heat
Average
input per Total heat input per
Side of Current Voltage Welding
Pass unit unit length of the
Plate (A) (V) Speed
length per weld (kJ/mm)
(mm/min)
pass
(kJ/mm)
Root Pass 125 30 2.2 1.02
Side A Hot Pass 125 30 2.3 0.98
Capping Pass 125 30 2.6 0.87 4.96
Filling Pass 125 30 2.2 1.02
Side B
Capping Pass 125 30 2.1 1.07
Table 2 (b) Process Parameters used for fabrication
butt welded joints (Medium Heat)

Average
Heat
Average
input per Total heat input per

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Side of Current Voltage Welding
Pass unit unit length of the
Plate (A) (V) Speed
length per weld (kJ/mm)
(mm/min)
pass
(kJ/mm)
Root Pass 155 35 3.01 1.08
Side A Hot Pass 155 35 3.005 1.08
Capping Pass 155 35 3.03 1.07 5.41
Filling Pass 155 35 2.999 1.09
Side B
Capping Pass 155 35 3.01 1.08

Table 2 (c) Process Parameters used for fabrication butt welded joints (High Heat)

Average Heat
Average
Side of Current Voltage input per unit
Pass Welding Total heat input per unit length of the weld (kJ/mm
Plate (A) (V) length per pass
Speed (mm/min)
(kJ/mm)

Root Pass 185 40 3.88 1.14

Side A Hot Pass 185 40 3.784 1.17
Capping Pass 185 40 3.7 1.20 5.82
Filling Pass 185 40 3.901 1.14
Side B
Capping Pass 185 40 3.81 1.17

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The specimens used for tensile (ɛ=10-4 to 10-2 s-1). Hardness distribution at
testing, microstructure study, and micro- transverse and longitudinal axis on the joints
hardness testing were sectioned, cleaned, was measured using a Vickers hardness
grounded, polished and electrolytically tester (FM-800) with testing load and
etched. An electrolytic oxalic acid (10g) holding time of 1 kg and 15 s respectively.
with distilled water (100mL) supplied with a
cell voltage of 6 V with etching time of 1
min was provided for electrolytic etching of Results & Discussions:
the sample. The microstructure was finally
examined by optical microscope (METKON The ultimate tensile strength (UTM)

IMM901). The specimens were tested on a values, % elongation and weld efficiencies

computerized tensile testing machine of are mentioned in Table 3.

100KN capacity with very slow strain rates

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Table 3 Tensile Test Result
Tensile Properties

Sample No. Location of Fracture Joint Efficiency (%)

Ultimate Tensile Strength (MPa) Percentage Elongation (%)

Base Metal 609.68 40 - -

1 655 25 Base Metal 107.4
2 643.02 23 Base Metal 105.5
3 620.4 22 Base Metal 101.8
Sample 1: Welded at Low Heat Input, Sample 2: Welded at Medium Heat Input, Sample 3: Welded at High Heat Input.
current of 80 A (much lower than that
applied in this work), found tensile strength
Results showed that, in each case,
of the weldment about 1800 MPa. Hence it
the tensile strength of welded specimen is
can be inferred that tensile strength inversely
greater than that of the base metal.
relates to electrode current provided that
Maximum tensile strength is possessed by
welding speed remains comparable. Weld
the specimen which was welded using low
efficiency of the specimen employed low
heat input and the converse was observed in
heat input was greater than other ones.
case of high heat input. All the three welded
Microhardness measurement results,
samples fractured at the base metal which is
graphically represented in Figure 1 (a and
the indication of the higher tensile strength
b), illustrated that the hardness varied as the
of the weld. A similar study [9], employing

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probe traversed from the surface of the weld

to its center.

Figure 1 Microhardness a and b in Transverse Direction and longitudinal directions respectively

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Comparatively faster cooling rate and high heat input respectively. High
hardened the upper surface of the weld. As hardness of the fusion boundary was
the indenter moved away from the center of because of the presence of the partially
the weld towards the fusion zone, melted grains. After reaching the maximum
microhardness increased from 205 VHN to hardness value, the hardness decreased in
230 VHN for low heat input, 194 VHN to the heat affected zone (HAZ). In all the
211 VHN for medium heat input and 182 welds, area adjacent to the fusion boundary
VHN to 195 VHN for high heat input (heat affected zone) was coarse grained
welded specimen. Proportionate hardness which possessed low hardness whereas the
values were reported in another work [9]. heat affected zone adjacent to the base metal
The phenomenon of decrease in hardness of was fine grained which possessed high
the weldment with increasing heat input is hardness. The reason for this trend of
specific for TIG welding [10]. While microhardness is the heat affected zone
moving away from the weld towards the experienced slow cooling rate and hence had
fusion zone, fusion boundary came across coarse grained microstructure, whereas the
which was responsible for the abrupt area adjacent to base metal went through
increase in hardness values of 275 VHN, faster cooling rate and hence fine grained
264 VHN and 251 VHN for low, medium microstructure was obtained. Microhardness
values of specimens using low, medium and
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high heat input are given in Table 4 (a and

b) respectively.

Table 4 a Microhardness Values in Transverse Direction for low, medium, & High Heat input

Distance from Weld Center Micro-Hardness (HV 0.5)

Sample 1(Low Heat Sample 2 (Medium Sample 3 (High
Input) Heat Input) Heat Input)
-3.5 229 208 196
-3 227 206 194
-2.5 226 202 193
-2 224 200 199
-1.5 219 197 191
-1 213 195 188
-0.5 211 194 185
0 206 194 181
0.5 209 196 184

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1 214 198 186
1.5 217 201 188
2 222 204 191
2.5 224 206 193
3 229 207 194
3.5 230 208 195
4

Table 4 b Microhardness values in Longitudinal Direction for low, medium, and high heat input

Distance VICKER HARDNESS (HV0.5)

from Weld Sample 1 Sample 2 Sample 3
Center (low heat input) (medium heat (high heat
input) input)
-7 240 242 226
-6 244 236 216
-5 237 224 252
-4 270 263 196
-3 226 209 194
-2 222 201 191
-1 213 197 186
0 205 194 182
1 209 199 188
2 221 199 191
3 227 207 197

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4 275 211 197

5 237 220 251
6 240 231 213
7 242 240 220
the area of heat affected zone
correspondingly. Optical micrographs, given
Full penetration welds were obtained
in Figure 2 (a – c), revealed the
in all samples made using low, medium, and
microstructures of weld zone, fusion
high heat input. It became evident from the
boundary and heat affected zone (HAZ) for
microstructures that the area of heat affected
different heat input combinations.
zone (HAZ) was proportional to the heat
input. An addition to heat input increased

heat input respectively

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Fig 2 Microstructure a,b and c showing HAZ, Fusion Boundary, & Weld Metal Low Heat Input, medium heat and high

It is clear from the microstructures

that the high heat input produced larger
consequently detailed out in order to
evaluate their microstructure and mechanical
properties for different conditions of low,
medium and high inputs. The major results
dendrites. In case of low heat input, the
exhibited that the weldment was stronger
cooling rate was faster so there was lesser
than the base metal and strength varies
time for the dendrites to grow resulting in
across the joint, maximum being at the
finer microstructure. Similar reason was
surface of the same. The process using low
responsible for smaller dendritic structure
heat input produced fine structured fusion
when laser-TIG process was practiced [1].
and heat affected zones which in turn

Conclusion: performed vigorously under applied stress

thereby offering greater strength and
Butt-joints of AISI 304 stainless hardness.
steel plates were developed by exercising
manual TIG welding process and
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International Journal of Scientific & Engineering Research, Volume 5, Issue 7, July-2014 1540
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T.A.Tabish, Institute of Advanced Materials, mechanical and metallurgical properties of

Bahauddin Zakariya University, 60800,
Multan.Pakistan ferritic stainless steel, The International
T.Abbas, Institute of Advanced Materials, Journal of Advanced Manufacturing
Bahauddin Zakariya University, 60800,
Multan.Pakistan Technology, 31, 11-12 (2007) 1076–1082
M.Farhan, Institute of Advanced Materials,
Bahauddin Zakariya University, 60800,
Multan.Pakistan [4] Hidetoshi Fujii, Toyoyuki Sato,
S.Atiq, Institute of Advanced Materials, Shanping Lua, Kiyoshi Nogi, Development
Bahauddin Zakariya University, 60800,
Multan.Pakistan of an advanced A-TIG (AA-TIG) welding
T.Z.Butt,Faculty of Engineering and
method by control of Marangoni convection,
Technology, University of the Punjab, 54590,
Lahore, Pakistan Materials Science and Engineering A, 495
1
Corresponding author: email (2008) 296–303
address: [email protected] (T.A.Tabish)
[5] Zhiguo Gao, Yixiong Wu, Jian Huang,

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