CDU II Operating Manual PDF

OPERATING MANUAL
PLANT NO: 10, 11 & 12

Chapter No: 1
PLANT NAME: CDU II
Page No Page 1 of 562
Chapter Rev No: 0
ADMINISTRATIVE REQUIREMENTS
SECTION A: PREFACE
The principal objective of an operating manual is to describe relevant operating procedures,
instructions and process safety information in an orderly manner for use by operating personnel for
safe and efficient operation of a plant facility. These operating procedures and instructions shall be
up-to-date reflecting changes in plant hardware and operating practices carried out from time to time.
The Crude and Vacuum Distillation Unit-II was commissioned under the Visakh Refinery Expansion
Project-I (VREP-I) to enhance the crude refining capacity of VR by 3.0 MMTPA. CDU-II is
equipped with the latest technology. Its design provides for energy conservation; operational
flexibility and maximization of product recoveries.
The original edition of operating manual of Crude Distillation Unit-II (CDU-II) was prepared prior to
the commissioning of the unit in the year 1985 by M/s EIL. It was later updated in July 2008, based
on the standard operating manual and process package provided by EIL. Plant Standing Instructions
(PSI) issued from time to time based on operating experience and learning are available separately in
field room.
Primary purpose of this revised operating manual is to integrate all the scattered operating
procedures and instructions into a single operating manual while simultaneously fulfilling the
requirements under Process Safety Management System (PSM) of Visakh Refinery. PSM-PR-04,
which is based on OSHA-1910.119 standard, specifies the methodology and the format to be
followed and the contents to be included in the preparation of an operating manual. Some of the new
subjects that are incorporated in the manual due to PSM format are:
• Operating Limits and Consequence Deviations
• Upset Conditions and Stabilization
• Avoiding Deviations and Plant Upsets
• Temporary Operations
• Process Safety Information
• Special or Unique Hazards
Efforts have been made to include the relevant information in a concise, step-by-step, easy-to-read
format so that they are within the comprehension of the readers. The users of this manual are
encouraged to suggest ideas for further refinement and highlight typographical errors if any, to
improve the overall quality of the manual.
Operating procedures & conditions given in this manual are indicative. These should be treated as
general guide only for routine start-up and operation of the unit. The actual operating parameters and
procedures may require minor modifications/changes from those contained in this manual as more
experience is gained in operation of the Plant. For detailed specifications and operating procedures
of specific equipment, corresponding Vendor's operating manuals/instructions need to be referred to.
Signature
Approved by
Name G S JOSHI
Designation DGM- Operations
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION B: TABLE OF CONTENTS
FROM REV DATE

CHAPTER LATEST
TITLE PAGE
No: REV NO.
NO
1 Administrative Requirements of the 31-03-2012
Manual 0
Section A : Foreword 1
Section B : Table of Contents
Section C : Annual Certificate of Validity
and accuracy
Section D : Document control
Section E : Procedure for revision of the
Manual
Section F : List of Abbreviations
Section G : List of Copy Holders
Section H : Record of Revisions to the
Manual
Section I : List of Standing Instructions
2 Introduction 17 0 31-03-2012
3 Basis of Design 20 0 31-03-2012
4 Feed and Product Characteristics 38 0 31-03-2012
5 Brief Process Description & Process 46 0 31-03-2012
Chemistry
6 Detailed Description of Configuration 60 0 31-03-2012
and Process
7 Description of critical control schemes 127 0 31-03-2012
8 Description of Distributed control System 136 0 31-03-2012
(DCS)
9 Description of Advanced Process control 138 0 31-03-2012
10 Pre-commissioning Activities 161 0 31-03-2012
11 Preparatory Operations & Activities for 168 0 31-03-2012
Commissioning
12 Initial Start up Procedure 171 0 31-03-2012
13 Start up Procedure after T&I 195 0 31-03-2012
14 Operating Limits & Consequences of 199 0 31-03-2012
Deviations
15 Normal Operation of the Plant 203 0 31-03-2012
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
FROM REV DATE

CHAPTER LATEST
TITLE PAGE
No: REV NO.
NO
16 Major equipment description and 224 0 31-03-2012
operating Procedure
17 Upset Conditions & Stabilization. 270 0 31-03-2012
18 Avoiding Deviations and Plant Upsets 283 0 31-03-2012
19 Emergency Procedures and Shutdowns. 287 0 31-03-2012
20 Re-Startup after Emergency Shutdowns 301 0 31-03-2012
21 Normal Shutdown Procedure 304 0 31-03-2012
22 Temporary Operations 324 0 31-03-2012
23 Process Safety Information 325 0 31-03-2012
a. ‘Information on Deviation From the
Design Limits of Major Equipment and
Minimum Consequence’-(PSM/FR/2.6)
b. ‘Information of plant Relief System’-
(PSM/FR/2.7)
c. ‘List of Process System Interlocks and
Trips’ -(PSM/FR/2.10)
d. ‘List of Enclosed Facilities’-
(PSM/FR2.8)
e. ‘Information on Plant Holdups’-
(PSM/FR/2.5)
f. ‘Design Codes and Standards
Employed’-(PSM/FR/2.9)
24 Sampling requirement and Sampling 326 0 31-03-2012
Procedures
25 List of Plant Equipment 338 0 31-03-2012
26 Plant Chemicals 347 0 31-03-2012
a. Withdrawal management
b. Max Storage allowable in the Plant
c. Storage precautions
d. Loading procedures
e. Empty container disposal
f. Handling Precautions
g. Description of Chemical dosing system.
27 Occupational Safety & Health 361 0 31-03-2012
a. Chemical Hazards (MSDS)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
FROM REV DATE

CHAPTER LATEST
TITLE PAGE
No: REV NO.
NO
b. First aid Procedures
c. PPE requirements, type and Usage
d. Fire Fighting System 0& equipment
e. Spill Handling
28 Plant Drainage System Description 379 0 31-03-2012
29 Environmental Management 382 0
a. Effluent Generation and Control 31-03-2012
b. Plant Emissions
c. Solid Waste
30 Special or Unique Hazards 390 0 31-03-2012
31 Safe Work Practices 404 0 31-03-2012
a. Work Permit Procedures.
b. Confined Space Entry procedure
c. Procedure for Opening Process
equipment and
Piping
d. Lockout/ Tag out Procedures
e. Electrical isolation procedure
f. Procedure for entry, presence, access
and exit
control in the Plant
32 Standard Operating Procedures of Process 444 0 31-03-2012
Equipment.
33 Chemical/HC spillage Handling 478 0 31-03-2012

Procedure
34 List of Annexures : 492 0 31-03-2012
a) Unit master blind list
b) Individual equipment blind list
c) List of Vendor manuals
d) Start – up & Shutdown check lists
e) LEL detectors status
f) Instrument air fail to open control
valves
g) DCP cylinders, First aid fire hose
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
FROM REV DATE

CHAPTER LATEST
TITLE PAGE
No: REV NO.
NO
reels and safety showers
h) Auto ignition temperatures
i) Corrosion probes, coupons and
FSM technology.
35 Description of Utility systems 540 0 31-03-2012
36 Instrumentation Tags Description 549 0 31-03-2012
Signature
Name P N VARA PRASAD

Approved by
Designation DIVISION HEAD- PRODUCTION

BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
CERTIFICATE OF AUTHENTIFICATION
This is to certify that this Operating Manual is current and accurate.
DATE
CERTIFIED BY SIGN NAME
CERTIFICATION
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION D: DOCUMENT CONTROL
1. The administrative sections (Chapter 1 of PSM/GL/4.1) are approved by Division

Head- Operations.
2. The original operating manual in file and tab format is maintained with the Division
Head.
3. Three hard bound copies of the manual are issued as “Controlled Copy” to the
respective plants- one for plant Manager, one for DCS and one for Field room.
Controlled copy stamping is done on the following pages: “Title Page”, “Table of
Contents” and First Page of every chapter.
4. Uncontrolled hard bound copies are made available to the plant personnel, Section
Head, “Disaster Control Room” (formerly “Central Control Centre”), Refinery
Engineering Documentation, Technical Department , HOD-Operations & YSF as
training copies. The training copies are marked as “Training Copy”
5. In case of any doubt regarding the latest revision, the Original Copy is the reference
document for confirmation.
6. All obsolete sections/chapters are removed by the Respective Division Heads.
Revisions & additions are managed by way of “Plant Standing Instructions” which are
annually integrated with the manual.
Approved By Sign

Designation DIVISION HEAD-
PRODUCTION BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION E : REVISION OF THE OPERATING MANUAL
1. This Operating Manual is revised for the following :
• Change in Operating practice in any part of the Plant short and long duration.
• Implementation of changes in Hardware and/or software systems of the Plant which
have impact on procedure.
• Change in Chemicals.
• Changes in Safety systems.
2. The revision of the Operating Manual is done in two stages :

• Managing changes in the Operating Manual within one year cycle.
• Updating Operating Manual annually.
3. The revisions are issued as ‘Standing Instructions’. The list of Standing Instructions is
maintained in Section I of Chapter 1-Administrative Requirements of the Manual’.
4. The Standing Instructions are backward integrated into the Operating Manual once in a
year.
5. The chapters which get revised at the time of revising operating manual, the Revision
number of the Chapter which is revised is increased by “1”. The Chapters which are not
revised retain the same Revision Number.
Approved By Sign

Designation DIVISION HEAD-PRODUCTION BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
II. SECTION F : LIST OF ABBREVIATIONS
ABBREVIATION EXPANSION
ATF Aviation Turbine Fuel
ATP Additional Tank age Project
BARC Bhabha Atomic Research Centre
BA Breathing Apparatus
BCW Bearing Cooling Water
BFW Boiler Feed Water
CCR Continuous Catalytic Reformer
CAS Chemical Abstracts Service
CBD Closed Blow Down
CISF Central Industrial Security Force
CPP Captive Power Plant
CPWD Central Public Works Department
DAF Dissolved Air Floatation
DCP Dry Chemical Powder
DOB Daily Order Book
DMP De-Mineralization Plant
DRN Disposal Requirement Notice
DCN Design Change Note
EPM Environmental Procedures Manual
ESA External Safety Audit
EHS Environment Health Safety
ETP Effluent Treatment Plant
ELCB Earth Leakage Circuit Breaker
EMS Environmental Management System
EDMS Engineering Document Management System
E&P Economics & Planning
FCCU Fluid Catalytic Cracking Unit
HLPH High Lift Pump House
HSD High Speed Diesel
IA Instrument air
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
ISA Internal Safety Audit
IWL Inspection Work List
IFO Internal Fuel Oil
JBO Jute Batching Oil
KOD Knock Out Drum
LLPH Low Lift Pump House
LSHS Low Sulfur Heavy Stock
MOC Management of Change
MSIHC Rules Manufacture, Storage , Import of Hazardous Chemical
Rules
MSDS Material Safety Data Sheet
MEROX Mercaptan Oxidation
MES Mechanical Engineering Services
MS Motor Spirit
NDT Non-Destructive Test
NHT Naphtha Hydro-Treater
NRV Non return Valve
OISD Oil Industry Safety Directorate
OCP Operational Control Procedure
OSTT Off Shore Tanker Terminal
PDI Plant Daily Instructions
P&ID Piping & Instrumentation Diagram
PFD Process Flow Diagram
PLC Programmable Logic Control
PPM Parts Per Million
PSI Process Safety Information
PS&E Process Safety & Environment
PSV Pressure Safety Valve
PHA Process Hazard Analysis
PAD Process Analysis & Design
PPE Personnel Protective Equipment
PMS Project Management System
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
PSMS Process safety management system
PA Paging Announcement
PSSR Pre- Start Up Safety Review
PESO Petroleum & Explosives Safety Organization
PIR Project Initiation Request
QAP Quality Assurance Plan
QRA Quantitative Risk Analysis
RCA Root Cause Analysis
RCW Recirculating Cooling Water
RCR Ramsbottom Carbon Residue
ROV Remote Operated Valve
RED Refinery Engineering Documentation
STEL Short Term Exposure Limit
SSA Surprise Safety Audit
SRU Sulfur Recovery Unit
SWP Safe Work Practice
SMPV Static & Mobile Pressure Vessels
SKO Superior Kerosene Oil
SAC Strong Acidic Cations
SBA Strong Basic Anions
SRN Straight Run Naphtha
SR Short Residue
T&I Turnaround & Inspection
TLV Threshold Lower Value
TSV Thermal Safety Valve
TC Turnaround Cycle
TOB Turnover Book
TBP True Boiling Point
UEL Upper Explosive Limit
VRCFP Visakh Refinery Clean Fuels Project
VGO Vacuum Gas Oil
VBU Visbreaker Unit
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
VREP Visakh Refinery Expansion Project
VD Vacuum Diesel
YSF Yard Shift Foreman
Sign
Approved By
Designation DIVISION HEAD-

PRODUCTION BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION G: LIST OF COPY HOLDERS
List of the Controlled Copy holders are as given below:
S.NO COPY TYPE DESIGNATION OF THE COPY HOLDER
1 Original Division Head-Production Block
2 Controlled Unit Manager, CDU II Unit DCS, Field room

Copy
HOD-Operations
3 Training Copy HOD-F&S
(Hard Copy) Technical Services
Refinery Engineering Documentation.
All Plant Personnel
YSF
Note:
1. “Controlled Copy” means that the Plant Division Head will monitor it for its status,
incorporate changes as & when required, ensure its applicability and accessibility.
2. Training copy will be available in soft as well as hard copies.
Sign
Approved By Name P N VARA PRASAD

Designation DIVISION HEAD-PRODUCTION BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION H: RECORD OF REVISIONS TO THE MANUAL
1. The revisions to the Operating Manual are made through issue of Standing Instruction.
2. The Standing Instructions are issued either to revise the existing operating procedure in
the Operating Manual in part or as an addendum.
3. The Standing Instructions are issued by the Respective Division Head-Operations.
4. The Standing Instructions for respective plants are filed in a separate File with tab
separators and kept as records.
5. List of Standing Instructions issued are recorded and maintained in Chapter 1, Section I
of the respective operating manual.
6. The Standing Instructions which describes recurring operational activity are identified
among the standing instructions issued and incorporated in the corresponding chapter of
the Operating Manual.
7. The revision of the Operating Manual is carried out annually to ensure the operating
procedures are current and accurate.
8. The record of the Standing Instructions issued is retained long term in Operations
Department.
Approved
Sign
By

Designation DIVISION HEAD-PRODUCTION
BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
SECTION I: PART-I: STANDING INSTRUCTIONS - IN USE

SL. STANDING STANDING INSTRUCTION DATE OF
NO INSTRUCTION NO. TITLE ISSUE
1. ADM/OPRN/PRODN/ Equipment draining Aug 2000 Standing Instructions
SI/003 Incorporated in Operations
Manual Chapter-28
2. ADM/OPRN/PRODN/ CDU-II startup Check-List March Standing Instructions
SI/008 2000 Incorporated in Operations
Manual Chapter-34
3. ADM/OPRN/ PROD CDU-II Desalter Online De- Feb’ 2002 Standing Instructions
/SI/07 sludging Incorporated in Operations
Manual Chapter-16
4. OPRN/PROD/SI/011 Process Units Effluent Nov’ 2001 Standing Instructions
Monitoring incorporated in Operations
Manual Chapter-28
5. ADM/OPRN/ PROD VREP I/ VREP- II –OWS Aug’ 2001 Procedure incorporated in
/SI/012 System Operations manual Chapter-
28
6. ADM/OPRN/ PROD Refinery Fuel Gas System Feb’ 2005 Standing Instructions
/SI/016 Management and Control incorporated in Operations
Manual Chapter-15
7. ADM/OPNRN/OM&S/ 11-E-40A/B commissioning May’2005 Standing Instructions
SI/017 procedure incorporated in Operations
Manual Chapter-.16
8. OPRN/ADMN/SI/20 Standing Instructions on feed Dec’ 2005 Incorporated in Operations
tank change over Manual Chapter-15
9. ADM/OPRN/PRODN/ Empty oil & chemical drums March’ Standing Instructions

SI/23 collection for washing in CDU 2006 incorporated in Operations
block Manual Chapter-26.
10. ADM/OPRN/PROD/SI Standing Instruction for May’ 2010 Standing Instructions
/30 Improving Aesthetics of MOI incorporated in Operations
Control Room Manual Chapter-8
11. ADM/OPRN/PRODN/ procedure for monitoring online Dec’2010 Standing Instructions
SI/32 ER probes, PIN matrixes and incorporated in Operations
corrosion coupons for high acid Manual Chapter-.34
crudes in CDU-II
12. ADM/OPRN/PRODN/ Procedure for commissioning of April’ 2011 Standing Instructions
SI/34 PFD in CDU-II incorporated in Operations
Manual Chapter-.16
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 1
PLANT NAME: CDU II
Chapter Rev No: 0
13. ADM/OPRN/PRODN/ Avoid congealing of Heavy oil May 2011 Standing Instructions
SI/035 R/D lines from CDU-2 incorporated in Operations
Manual Chapter-.15
14. ADM/OPRN/PRODN/ APH water washing procedure July 2011 Standing Instructions
SI/036 incorporated in Operations
Manual Chapter-.06
15. ADM/OPRN/PRODN/ To apprise Merox DCS shift-In- Aug 2011 Standing Instructions
SI/037 charge in case of fluctuation in incorporated in Operations
sour water flow. Manual Chapter-15
16. ADM/OPRN/PRODN/ Procedure for fuel oil gun Sept’2011 Standing Instructions
SI/038 cleaning incorporated in Operations
Manual Chapter-15
17. ADM/OPRN/PRODN/ Car seals Management Dec 2011 Standing Instructions
SI/042 incorporated in Operations
Manual Chapter-15
PART-II: RECORD OF STANDING INSTRUCTIONS CANCELLED

SL. STANDING STANDING INSTRUCTION DATE RE EXPIRED/
NO INSTRUCTION NO. TITLE V. INCORPORATED
1. ADM/OPRN/PROD Effluent Monitoring Aug 2000 0 EXPIRED
N/SI/002
2. ADM/OPRN/PROD Work Permit System in the Sep 2000 0 Invalid. New work permit
N/SI/013 Units system Procedure
incorporated in Operations
Manual Chapter-31
3. ADM/OPRN/PROD Safety Job Card (Red Job Card Oct 2000 0 Invalid. New work request
N/SI/014 System) Procedure incorporated in
Operations Manual Chapter-
31
Sign
Approved By Name P N VARA PRASAD

Designation DIVISION HEAD- PRODUCTION
BLOCK
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 2
PLANT NAME: CDU II
Chapter Rev No: 0
INTRODUCTION
INTRODUCTION
The Crude and Vacuum Distillation Unit-II was commissioned under the VISAKH Refinery
Expansion Project-I (VREP-I) to enhance the crude refining capacity by 3.0 MMTPA.
The facilities put up under VREP-I are listed below:
i) Grass-root Crude and Vacuum Unit of 3.0 MMTPA capacity designed to process Basrah
crude.
ii) Grass-root Fluidized Catalytic Cracking Unit of 0.6 MMTPA
iii) Bitumen Blowing Unit which was later revamped to 225 TMTPA unit in VREP–II with a
new Biturox reactor
iv) VREP-I BCW system.
v) Capacity augmentation of the existing utilities and offsite facilities to meet the additional
requirements.
CDU / VDU-II have a design capacity to process 3.0 MMTPA of crude oil. The crude
processing capacity was enhanced to 3.2 MMTPA by installing Pre-Flash Drum in 1996.The
design feed stocks for the unit are Basrah and Bombay High (BH). In addition, two check
cases have been considered for the unit design, namely Kuwait and Heavy Arabian Mix
crudes. The unit was designed based on 330 on-stream days per annum. The CDU is designed
to produce Liquefied Petroleum Gas (LPG), Straight Run Naphtha,(SRN), Heavy Naphtha
(HN), Superior Kerosene Oil (SKO), High Speed Diesel (HSD),and Reduced Crude Oil
(RCO). The unit is also designed for special product Aviation Turbine Fuel (ATF)
The CDU also comprises the Naphtha Stabilizer section and the SRN Caustic and
Water Wash sections.
The VDU is designed to process RCO from CDU and to produce Light Vacuum Gas
Oil (LVGO), Heavy Vacuum Gas Oil (HVGO), Slop cut and Short Residue (SR). CDU /
VDU are designed to operate in conjunction and independent operation of either of these
units is not considered.
The crude oil is pumped from the off-site storage tanks to the Crude Distillation Unit.
The various stages of operation it undergoes are as follows:
Crude Pre-heating in process heat exchangers and desalting of crude in Desalter.

Again preheating the desalted crude in process heat exchangers.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 2
PLANT NAME: CDU II
Chapter Rev No: 0
INTRODUCTION
Heating of pre-heated crude oil in Atmospheric Fired Heaters.

Fractionation in Atmospheric Distillation Column.
Stabilization of Straight run naphtha in Stabilizer unit & Caustic - Water wash Treatment.
Products steam stripping (Heavy Naphtha, Kero and Diesel) and routing to designated
Product tanks or treatment facilities (in case of special products like ATF, Bitumen etc.).
Heating of Atmospheric Column bottoms (Reduced Crude Oil) in Vacuum Heater.
Fractionation of RCO in Vacuum Distillation Column.
Routing of products (VGO, Slop Cut, and Vacuum Residue) to designated tanks/units.
The products from CDU can be routed as follows:-
1) Stabilizer off Gas to FCCU-II
2) LPG to the Amine Treating Unit (ATU)
3) Stabilized Naphtha to
a. Stabilized Naphtha storage tanks
b. MS tanks
c. 6” T/o downstream of 11-E-19for giving hook-up to VRCFP.
4) Heavy Naphtha to
a. ATP diesel line
b. Heavy naphtha intermediate tank
c. Stabilized naphtha rundown line
d. Storage
e. Slop
f. 4”line hook-up given to route HN to VRCFP (NHT-CCR).
5) Kerosene to
a. Storage
b. Diesel Header
c. ATP Diesel Header
d. FO Blend
e. MEROX when on ATF regulation
f. Slop.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 2
PLANT NAME: CDU II
Chapter Rev No: 0
INTRODUCTION
6) DSL to
a) Sour diesel storage tanks
b) ATP diesel header
c) FO blend to HFO header
d) FO blend to RFO header
e) LDO blend header
f) To FCCU-2
g) To DHDS upstream of 11-E-23
h) To CDU-3 for flushing oil.
i) Slop
The VDU products are routed as follows:-

1. Hot well oil to TK 17.
2. VGO to
(a) FCCU-I/FCCU-II as hot feed
(b) VGO storage tanks
(c) Slop
(d) LDO header.
3. Slop Cut to
(a) Vacuum furnace along with RCO (As recycle stream)
(b) As product rundown, second part gets mixed with SR product up stream to 12-E-
01 A/B/C. (provision also there to mix with SR down-stream of 12-E-01A/B/C).
(c) To CDU-I cooler box.
(d) To FCCU-II via recycle control valve.
4. SR to
a) VBU storage
b) Direct VBU feed.
c) To HFO line
d) To RFO line
e) To BBU feed
f) Slop header
g) 10” startup line/circulation line back to crude inlet line to Preheat train – I.
h) LDO header.
The unit is designed for a turndown capacity of 50%.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
DESIGN BASIS
The Crude Distillation Column has been designed to process 3 MMTPA. Design of all the
equipments other than crude column was based on Basrah crude. Crude column design was
based on Kirkuk crude for both Kerosene (SKO) and Aviation Turbine Fuel (ATF)
operations.
The unit was designed to process the crudes of API 31.3 ° to 36 ° API with marginal
shortfalls in throughput. All the exchangers are specified to process Basrah crude only.
Modifications, under the “BH Conversion Project”, have been done in the plant to process 3
MMTPA of Bombay High crude also.
3.1.1 ELECTRICAL DESALTER:

a) Design feed:
Crude Basrah Bombay high

Kg/ hr 367647 367647
Sp. Gravity @ 15 °C 0.848 0.8284
API @16 °C 33.6 39.2
Total Sulfur, wt % 1.9 0.15
Wax content wt% 6.0 14.7
RVP @ 100 °F, psi 7-9 5.5
H2S content Nil Nil
Viscosity @ 20 °C 9.0 cst -
Viscosity @ 37.8 °C 5.9 cst -
Pour point °C -15 +30
Conradson carbon residue, wt% 4.3 -
Characterization factor 11.9 -
Water &sediments, vol % 0.15 0.05
Salt content, (ptb) 3.0 5.0
Vanadium, ppm 18.0 4.24
Nickel, ppm 5.4 6.2
Iron, ppm 1.0 7.14
TBP distillation, wt% wt%
IBP-150 °C 19 24.5
150- 250 °C 16.7 19.6
250-370 °C 19.8 23.2
370 °C plus 45.5 32.7
b) Design product:
Salt content: 5 mg/l or 5% of the salt content of the raw crude whichever is greater.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.1.2 DISTILLATION UNIT:
a) Design feed:
The design feed for the unit is BASRAH crude oil with the characteristics indicated in the
table 1.
b) Design products:
i. Product battery limit conditions:
Atmos section:
Product TBP cut range °C Temperature °C Pressure,

Kg/cm2A
LPG C3-C4 40 8.0
Stabilized naphtha C5-130 43 5.0
Heavy Naphtha 130-160 43 5.0
Kerosene/ATF 160-270/160-230 43 5.0
Diesel 270-380/230-380 43 5.0
RCO 380+ 343 14.4
Vac section:
Product TBP cut range °C Temperature °C Pressure,

Kg/cm2A
Light vacuum gas oil 380-400 70/213 5.0
Heavy vacuum gas oil 400-530 70/240 5.0
Slop distillate 530-550 90 9.0
Vacuum residue 550+ 90 9.0
Vacuum residue(bitumen 550+ 250 9.0
unit feed)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.2 Equipment Design Basis:
3.2.1 ELECTRIC DESALTER :
Design inlet chloride as NaCl 85.601 mg/l

Design outlet chloride as NaCl 5 mg/l
Required process water 5 vol, %
Insoluble water in desalted crude 0.2 vol.%
Oil content of effluent brine 100 ppm Max.
Required pH 7.0-8.5
Operating temperature 120-130 °C.
3.2.2 ATMOSPHERIC DISTILLATION COLUMN:
The crude distillation column has been designed to handle KIRKUK crude at capacity of 3
million tons/yr. the crude distillation column has been processed various other crudes like
Kirkuk, Kuwait and 50:50 light heavy Arabian crudes with the same heat removal at the
circulation reflux exchangers as for designed for Basrah crude.
3.2.2.1 Pressure:
The atmospheric column reflux drum operating pressure was set to 2.6 Kg/cm2 abs. in order
to obtain total condensation of the over head product at 45 °C. Accordingly the flash zone
pressure has been fixed at 3.2 Kg/cm2.
3.2.2.2 Over flash and bottom stripping steam:

Over flash (6 vol % on crude) and bottom stripping steam rate (28 kg/m3 of reduced crude)
have been fixed to produce reduced crude containing not more than 10 volume per cent of gas
oil boiling below 380 °C.
3.2.2.3 Heat removal:

The location and amounts of heat removal by the various circulating refluxes are selected to
balance the tower loading and also to make it possible to recover heat in reboiler. The heat
removal from the column is as below:
Diesel CR 5.0 MM K.cal/hr

Kerosene CR 11.0 MM K.cal/hr
Top pump around 7.4 MM K.cal/hr
50 °C temperature drop is taken for circulating reflux.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.2.2.4 Top Reflux:

The design reflux is selected to give an overhead temperature which prevents condensation of
water at the top of the tower.
3.2.3 NAPHTHA STABILISER:
The stabilizer has been designed to make a naphtha bottom product of RVP 10 max. and top
overhead product of LPG contains not more than 1 mol. %. Mol. % C5.
3.2.4 NAPHTHA CAUSTIC/ WATER WASH SYSTEM:
The caustic wash system is designed to remove all hydrogen sulphide in naphtha and reduce
the mercaptan content to 10 ppm. A circulation rate of 25 % of naphtha is taken for caustic
and water circulation. The caustic hold has been fixed to give a batch time of 6 days.
3.2.5 VACUUM DISTILLATION COLUMN:
3.2.5.1 Number of stages:

A single stage dry vacuum distillation system is provided for FCC feed preparation.
3.2.5.2 Flash zone temperature:

The flash zone temperature is set at 395 °C to achieve the desired vaporization at the pressure
in the flash zone.
3.2.5.3 Tower pressure:

The operating pressure is selected such that there is no requirement of steam to achieve the
desired vaporization and the tower diameter is minimized. A pressure of 24 mm Hg at flash
zone ensures that the ejector system suction pressure will be 5 mm Hg. Abs.
3.2.5.4 Column internals:

Packed column has been provided for achieving low pressure drop. Glitsch grid has been
provided in the wash zone. Chimney trays are provided for the draw off of the side stream
products. Demister pads are provided above the wash zone to prevent carryover of
asphaltenes and at the top of the tower (to minimize carryover of hydrocarbons into the
ejectors system).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.2.5.5 Recycle:
The vacuum column is designed with a recycle rate equal to 6 v% of the tower feed in order
to ensure satisfactory product quality.
3.2.5.6 Pump Around:

Pump around locations and duties are chosen to balance the column internal loading while
maximizing the crude preheat.
3.2.5.7 Bottom Quench:

The tower bottom temperature is kept at 350 °C to reduce possible cracking during hold up in
the tower. The quenching is achieved by returning a quench streams to the tower at a
temperature of 250 °C after heat exchange between vacuum residue and crude.
3.3 Material Balance (design case):
3.3.1.1 Atmospheric Distillation column: (Basrah Crude)

i.) SKO operation:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
ii.) ATF operation:
3.3.1.2 Naphtha Stabilizer Material Balance for Basrah crude:
3.3.1.3 Vacuum Distillation Column Material Balance for Basrah crude:

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.3.2.1 Crude Distillation Column Material Balance for Bombay High crude:
*ATF cannot be produced from BH crude due to high Aromatics in it
3.3.2.2 Naphtha Stabilizer Material Balance for Bombay High crude:
** LPG quantity corresponds to 94% recovery based on 2.2% by wt. LPG on crude
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.3.2.3 Vacuum Distillation Column Material Balance for Bombay High crude:
The performance of the above design has further been checked even for the following cases.
The material balance has been tabulated given as under.
a) Crude Distillation Column Material Balance for Basrah crude SKO operation
without Heavy Naphtha production
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
b) Crude Distillation Column Material Balance for Basrah crude ATF operation
without Heavy Naphtha production
3.3.3.1 Crude Distillation Column Material Balance for Kuwait crude SKO operation:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.3.3.2 Vacuum Distillation Column Material Balance for Kuwait crude:
3.3.4.1 Crude Distillation Column Material Balance for Kirkuk crude SKO operation:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.3.4.2 Vacuum Distillation Column Material Balance for Kirkuk crude:
3.3.5.1 Crude Distillation Column Material Balance for 50:50 Light: Heavy Arabian crude
SKO operation:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.3.5.2 Vacuum Distillation Column Material Balance for 50:50 Light: Heavy Arabian crude:
3.4 FEED/ PRODUCT BATTERY LIMIT CONDITION
FEED STOCK: CRUDE (@ 1.0 kg/cm2 & 30 oC)
PRODUCT Pressure (kg/cm2) Temp (OC)
LPG 8.0 40
Stabilized Naphtha 5.0 43
Heavy Naphtha 5.0 43
Kerosene/ATF 5.0 43
Diesel 5.0 45
RCO 14.4 343
LVGO 5.0 *213/70
HVGO 5.0 *240/70
(Slop/RFO/HFO) 9.0 90
Short Residue(BBU feed) 9.0 250
Short Residue 9.0 90
Hot well Oil 5.0 40
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.5 UTILITIES CONDITIONS AT UNIT BATTERY LIMIT:

Utilities And Their Specifications:
3.5.1 LP Steam:
Minimum Normal Maximum Mech. Design

2
Pressure (Kg/cm ) 3.5 4.0 5.0 6.5
Temperature (°C) Saturated 150 170 190
3.5.2 MP steam:

2
Pressure (Kg/cm ) 10.0 11.0 12.0 13.5
Temperature (°C) Saturated 250 280 300
3.5.3 HP steam:

2
Pressure (Kg/cm ) 34 36
Temperature (°C) Saturated 370 390
3.5.4 Instrument Air:

2
Pressure (Kg/cm ) 5.0 6.0 7.0 9.5
Dew Point (°C) at 1.0 Kg/cm2 -40°C -40°C -40°C -40°C
Oil Content (ppm) 0.0 0.0 0.0 0.0
Temperature (°C) 30 40 45 65
3.5.5 Plant air:

2
Pressure (Kg/cm ) 4.0 5.0 6.0 9.5
Dew Point (°C) No Free - No Free -
Moisture Moisture
Oil Content (ppm) 0.0 0.0 0.0 0.0
Temperature (°C) 30 40 45 65
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.5.6 Raw Water:

Turbidity (ppm) 15
M. Alkalinity as CaCO3 (ppm) 50-192
Ca Hardness as CaCO3 (ppm) 30-150
Total Hardness as CaCO3 (ppm) 22-300
Silica as SiO2 (ppm) 50 (max)
Chlorides as Cl ((ppm) 30-200
Sulfates as SO4 (ppm) 80-
Iron as Fe (ppm) 0.25
TDS as CaCO3 (ppm) 700
Total Suspended Solids (ppm) 23
pH 7.0-9.0
Conductivity at 250C micro mho/cm approx 5.0
Pressure Kg/cm2 Operating =3.5, Mech. Design = 7.0
Temperature 0C Operating =32, Mech. Design = 65
3.5.7 Cooling water:
Unboosted Boosted Mech. Design

2
Pressure Kg/cm 2.0 3.5
Temperature 0C 33 44 65
3.5.8 Boiler feed Water (MP):
Supply Mech. Design

2
Pressure Kg/cm 5.2
Temperature 0C 120 150
3.5.9 DM feed water:
Turbidity (ppm) Nil

Hardness as CaCO3 (ppm) Nil
Silica as SiO2 (ppm) 0.05
Chlorides as NaCl ((ppm) 0.05
Iron as Fe (ppm) Nil
Conductivity at 200C micro mho/cm 1.0 (max)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
pH 6.5-8.0
Pressure (Kg/cm2 )at grade 3.0
Temperature 0C Ambient
Mech. Design Pressure (Kg/cm2 ) 7.0
Mech. Design Temperature (0C) 65
3.5.10 LP condensate:
Maximum Mech. Design

2
Pressure (Kg/cm ) 4.5 6.5
Temperature 0C 147 170
Oil Content 15 15
Conductivity micro mho/cm 1.0 1.0
3.5.11 Fuel oil at unit Battery Limit:

2
Pressure (Kg/cm ) 8.0 10.0 11.0 18.0
Temperature 0C 110 130 200 200
Fuel Oil LSHS

0
Specific Gravity @ 15 C 0.959 0.9756
Viscosity, cst at 82 0C 100 39.4
Viscosity, cst at 100 0C 45 23.6
Sulfur content (wt.%) 4.5 0.7
Ash Content (ppm) - 0.1 (max)
Sediment (ppm) - 0.25(max)
Flash Point 0C >93 >93
Pour Point 0C +30 +51
Heating Value (Kcal/kg gross) 10,200 10,200
Net H/C ratio 9480 9480
Normally LSHS only will be used. However FO will be used for short duration when LSHS is
not available.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.5.12 Fuel gas at unit Battery limit:

2
Pressure (Kg/cm ) 3.5 4.0 4.5 7.0
Temperature 0C 30 40-50 60 70
3.5.13 Electricity supply to unit:
Volts Phases Cycles

Lighting 230 1 5C CPS
Emergency power for 110 1 50
instruments
For interlocks 110 DC
3.6 UTILITY CONSUMPTION:

Utility consumption rate:-
Utility Consumption
L.P Steam (Kg/hr) 1800
M.P Steam (Kg/hr) 17260-10000
H.P Steam (Kg/hr) *21100
Cooling Sea Water (m3/hr) 3257 (*3606)
D.M Water (m3/hr) 27*
Service Water (m3/hr) 17.4*
Fuel Oil (T/hr) 6.54
Fuel Gas (T/hr) 5.45
1. (*) When FCC is down

2. * intermittent Generation
3.7 CHEMICAL CONSUMPTION
Chemical Chemical name Average consumption(w.r.t crude feed rate)
Neutralizer Ammonia 2 PPM *
Filmer EC1021A 1.4 PPM
Demulsifier EC2040A 5 PPM
caustic ---- 5 PPM max.
* 1 PPM for ATMOS neutralizer and 1 ppm for VAC neutralizer.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.8 EQUIPMENTS DESIGN CONSIDERATION:

3.8.1 Roto-dynamics Machinery:
All roto-dynamic machines are over designed to 120% of limiting design flow. All the pumps
are motor driven and following pumps however will have a turbine driven spare: crude
charger, crude booster (presently for PFD), atmos col. Reflux and KERO CR.
3.8.2 Heat Exchangers:
All the coolers, condensers and other heat exchangers are over designed to 110% of limiting
design on flow and duty. Condensers must have 20% spare philosophy, i.e., 20% overdesign
on flow and duty (ex. Trim condenser (2+1) each of 60% duty. There are no spares available
for other exchangers. For air fin coolers, extent of cooling can be maximized up to 42°C.
Preheat exchangers are for obtaining maximum possible preheat and each exchanger has
block and bypass valves. Stacked exchangers are not more than two or three.
3.8.3 Heaters:
The combination burner firing as well as individual burner firing facility is there. Either FO
or FG can take the full load if required. Turn down ratio of heater is 50%. Turndown ratio of
burners for oil firing is 1:3 and for gas firing is 1:5. Atomizing steam is MP steam at pressure
of 11.5 Kg\cm2. Stack height has to be maximum of 60 meters and the diameter has to be
such that flue gas exit velocity shall be more than 20meters/sec at turndown condition. Soot
blowers operating with electric motors for 11-F-01 and for 12-F-01 inst. Air operated with
pneumatic and retractable soot blowers. Both heaters are provided with air pre-heater.
3.8.4 Instruments:
All the instruments are under Centralized (Distributed Digital Control) Automatic
Computerized control and pneumatically controlled. There are no local controls on
instruments. All instruments have power supply of 110V, 50Hz. Safety valves have 100%
spares and they are all provided with block valves and bypass valves. All control valves must
have isolation and bypass valves. All field junction box have to be explosion proof. All the
pressure gauges and dial thermometers should have 6” diameter.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 3
PLANT NAME: CDU II
Chapter Rev No: 0
DESIGN BASIS
3.8.5 Atmospheric Column:
The material of construction is Carbon steel with SS410 cladding up to light diesel and
Monel clad is present up to tray#4 from top. Trays are SS410 except top four trays which are
made up of Monel. The trays are valve trays except the chimney trays at draw-off. Overhead
condenser shell is Monel clad 3mm over CS. Tubes are of titanium (and before 2010 T&I
tubes are made of copper and nickel (70:30)). Channel section is of Monel clad 3mm thick.
Overhead drum has to be 100% cement lined.
3.8.6 Vacuum Column:
The column has structured packing and the material of construction is CS with SS410 clad up
to 250°C limit during T&I material is upgraded to SS316 2.5 Mo (min) metallurgy. The top
section and the overhead vapor line are of only CS. Surface condenser is floating head type
and its shell is made up of CS + Monel clad 3mm. Tubes are made up of Cu & Ni and
upgraded to titanium tubes. Channel section also has 3 mm Monel clad and the drum needs
100% cement lining. The associated lines to drum are of CS. Surface condensers are floating
head type and only 12-E-07A having back flushing facility.
3.8.7 Stabilizer:
The stabilizer also has valve trays and internals are of SS410. Overhead vapor line is made of
CS. Condensers shell is of CS with Monel lining and tubes are of Cu & Ni in ratio (70:30).
Channel section is having Monel clad of 3 mm. Drum has 100% cement lining and re-boiling
is provided by KERO CR stream
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
FEED AND PRODUCT CHARACTERISTICS
4.1 FEED SPECIFICATIONS AND INLET BATTERY LIMIT CONDITIONS
4.1.1 Feed Characteristics:
• The Crude Distillation Column has been designed to process 3 MMTPA of Basrah crude for
both Kerosene (SKO) and Aviation Turbine Fuel (ATF) operations. Modifications, under the
“BH Conversion Project”, have been done in the plant to process 3 MMTPA of Bombay High
crude also.
•
Property Basrah Bombay high
SP.GR 0.848 0.8284
API @ 16 °C 35.4 39.2
RVP@38 0C psi 5.8 5.5
Pour point , 0C -15 +30
Wax Content % Wt 6.0 14.7
Total Sulfur % Wt 1.9 0.15
Salt content (ptb) 3.0 5.0
Viscosity 9.0 cst @ 20°C 2.876 KV @ 40 °C
5.9 cst @ 37.8°C 2.404 KV @ 50 °C
Asphaltenes (wt %) 1.0 0.05
Total light ends (wt%) 5.02 2.62
4.1.2 Feed at battery limit Conditions:
Feed Stocks Pressure Temperature Source

Crude oil 1.0 Kg/cm2 Ambient (300C) Storage tank
4.1.3 TBP Distillation:
Temperature, °C Basrah (wt%) BH (wt%)

IBP-150 19.0 24.5
150-250 16.7 19.6
250-370 19.8 23.2
370 Plus 45.5 32.7
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
4.1.4 Metal content weight ppm:
Metal Basrah Bombay high

Vanadium 18.0 4.24
Iron 1.0 7.14
Nickel 5.4 6.2
Sodium - -
4.2 PRODUCT SPECIFICATIONS AND OUTLET BATTERY LIMIT CONDITIONS:
4.2.1 Products TBP at ranges for crude and vacuum unit are as follows:
Product PG Case (0C) BH Case (0C)

Overheads IBP-130 IBP-110
Heavy Naphtha 130-160 110-140
ATF/KERO 160-230/160-270 140-240 /140-270
Diesel 230-380/270-380 240-380/270-380
LVGO 380-400 IBP-410
HVGO 400-530 400-510
Slop 530-550 510-550
Short Residue (VR) 550+ 550+
4.2.2 Liquefied Petroleum Gas (LPG) (As per IS-4576 standards)
Property Basrah Bombay High

Yield tones/annum 68075 62100
Sp. Gravity at 15/4 °C 0.554 0.549
Vapor Pressure at 65 0C 16.87 Kg\Cm2 16.88
Sulphur wt% <0.003 -
H2S Wt% 0.45* -
Dryness no free entrained water no free entrained water
Volatility: evaporation 2 2
Weathering 95% Vaporization by volume 95% Vaporization by volume
at 760 mm HG pressure at 760 mm HG pressure
* LPG for further treatment.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
4.2.3 Stabilized Naphtha (SRN):

Rate tones/annum 401423 356950
Pour point °C 0.69 -
Sulfur mercaptans, PPM 10 27
Sp.Gravity@400C NA 0.726
RVP (max) Psi 10 7.0
E.O.N clear 53.4
Paraffins vol % 77.8 60.9
Naphthenes, vol % 16.9 29.2
Aromatics, vol % 5.3 9.9
ASTM-distillation Temperature
IBP - 49
10% 51.5 70
30% 65.5 83
50% 84 94
70 % 96 105
90% 111.5 120
FBP 118 138
4.2.4 Heavy Naphtha (HN) Product:

Sp.Gravity@150C 0.7723 0.747
ASTM D-86(Vol. %) Temperature 0C
IBP 118 126
10% 136 138
30% 141 143
50% 144 149
70% 148 153
90% 156 161
FBP 177 177
Viscosity 20°C CST NA NA
Sulfur wt% 0.016 48 ppm
Paraffins vol % 65.8 52.7
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
Naphthenes, vol % 19.5 30.0

Aromatics, vol % 14.7 17.2
Flash point °C 20 20
4.2.5 Kerosene Product:

Flash point 0C 45 48
Smoke point mm. 25
Sp.Gravity@150C 0.8104 0.803
Sulfur Wt % 0.158 0.25
Viscosity Cst @ 20° C 2.2 1.32
Viscosity Cst @37.8 °C 1.5 1.30
Diesel index 68.7 33
ASTM D-86(VOL %) Temperature 0C
IBP 148 143
10% 175 177
30% 192.2 195
50% 206 208
70% 221 222
90% 251 241
FBP 291.9 260
4.2.6 ATF product:

Flash point 0C 43
Smoke point mm. 25
Sp.Gravity@150C 0.7886 0.791
Sulfur Wt % 0.098 0.013
Viscosity Cst @ 20° C 1.6 0.93
Viscosity Cst @37.8 °C 1.2 0.95
Freezing point, °C -50 -47
Diesel index 71
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
IBP 150 110

10% 170 149
30% 182 161
50% 190 171
70% 199 183
90% 218 202
FBP 249.6 240
4.2.7 Diesel (DSL):

Flash point 0C 115
Smoke point mm. NA
Sp.Gravity@150C 0.8527 0.855
Sulfur Wt % 1.6 0.129
Viscosity Cst 8.7
Viscosity Cst @37.8 0C 5.2
N2 NA 52 mg/l
IBP 236.9 241
10% 272 269
30% 293 284
50% 307 300
70% 323 322
90% <366 366
4.2.8 Diesel (DSL): (during ATF regulation)

Flash point 0C 94
Smoke point mm. NA
Sp.Gravity@150C 0.8525 0.852
Sulfur Wt % 1.32 0.129
Viscosity Cst @ 20 °C NA 3.74
Viscosity Cst @37.8 0C 4.0 3.2
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0

IBP 213.5 175
10% 246 224
30% 270.5 246
50% 289.5 264
70% 311.5 289
90% <366 348
4.2.9 Light Vacuum Gas Oil (LVGO):

Flash point 0C 79
Rate tones/yr 93309 125830
Sp.Gravity@150C 0.891 0.861
Sulfur Wt % 2.45 0.174
Viscosity Cst @ 20 °C 34 17.3
Viscosity Cst @ 37.8 °C 16 12.5
Metal Content NA
96% distillate 400 467
4.2.10 FCCU FEED : (LVGO + HVGO)

Pour point 0C +48 +30
Sulfur Wt % 3.5 0.19
Rate Kg/hr 50980
Sp.Gravity@150C 0.933 0.90
Viscosity Cp 1.12@2460C NA
[email protected] NA
Metal Content NA
ASTM D-86 (VOL %) Temperature 0C
5% 410.1 379
10% 422.0 395
30% 444.7 425
50% 462.0 442
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
70% 480.0 467

90% 511.4 512
95% 529.2 538
4.2.12 Slop Distillate:

Flash point 0C NA
Pour point 0C +55 +34
Rate Kg/hr 4831 9950
Sp.Gravity@150C 0.961 0.93
Sulfur Wt % 6.0 0.35
Viscosity Cp [email protected] NA
Metal Content NA
5% 469.1 425
10% 486.7 448
30% 511.3 505
50% 525.3 549
70% 546.4 -
90% 573.8 -
95% 599.0 -
4.2.13 Vacuum Residue (VR/SR):

Pour point 0C +60 NA
Rate Kg/hr 91931
Sp.Gravity@150C 10.56 0.99
Sulfur Wt % 5.50 0.68
Viscosity Cp 3.0@3820C NA
37.2@2200C NA
Metal Content NA
5% 513.1 464
10% 526.5 520
30% 574.8 601
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 4
PLANT NAME: CDU II
Chapter Rev No: 0
50% 616.2 641

70% 661.2 702
90% 711.5 794
95% 713.7 819
4.3 PRODUCT’S BATTERY LIMIT CONDITIONS:
Products Pressure Kg/cm2 Temperature 0C Destination

Stabilizer off 8.1 35 FCCU-2/FG header
Gas
LPG 16.0 40 MEROX
Light Naphtha 5.5 40 storage tank
Heavy Naphtha 5.5 40 into Diesel
Kerosene/ATF 5.5 44 storage tank
Diesel(DSL) 5.5 44 storage tank
VGO 7.0 70/140 Storage tank/FCCU
Vacuum Residue 9.0 90/250/160 Storage
tank/BBU/VBU/FO
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
BRIEF PROCESS CHEMISTRY & PROCESS DESCRIPTION
CRUDE CHEMISTRY
Crude oil is one of the two major fossil fuels on earth, the other being coal. It is the major and
a cost effective energy source today; though efforts are on to discover other means. Crude
oils vary widely in appearance and consistency from country to country and from field to
field. However, all crude oils consist essentially of hydrocarbons.
Hydrocarbons:
Organic compounds of carbon and hydrogen are known collectively by the name
hydrocarbons. As carbon has a valency of four and hydrogen is monovalent, it can normally
be expected that carbon should form only one tetra-hydride by combining with four atoms of
hydrogen. Such a compound known as methane or CH4 does exist, but as carbon can also
combine with itself and can also leave some of its valencies unsatisfied by getting involved in
unsaturated bonds or linkages, the number of hydrocarbons is truly myriad.
Saturated and Unsaturated Hydrocarbon Compounds:
In any compound made up of carbon and hydrogen the carbon atoms behave as though they
had four arms and the hydrogen atoms behave as though each had only one arm. Each arm of
the carbon atom must always be occupied, that is, it must be holding something, either a
hydrogen atom or another carbon atom. When all the carbon arms or bonds are used to hold
other atoms, the compound is said to be “saturated”. Similarly, a compound which does not
have all the carbon arms or bonds taken up by other atoms is said to be “unsaturated”. There
are millions of different ways in which carbon and hydrogen atoms can be connected together
to form hydrocarbon molecules. To help describe these in a systematic way, Science has
classified hydrocarbons into various families depending on their molecular structure. In
petroleum chemistry, hydrocarbons are classified primarily into four groups
Type of Hydrocarbon Group:
Type of Hydrocarbon Group

Paraffins Saturates
Naphthenes Cyclic saturates
Olefins Unsaturated
Aromatics Unsaturated
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Paraffinic Family:
The first family of hydrocarbons is Paraffins. They are saturated hydrocarbons with the
general formula CnH2n+2.
Normal (Straight Chain) Paraffins & Isomers:
There are two ways in which carbon and hydrogen can be combined in butane
In the normal butane, the chain is straight where as in the iso-butane, the chain is branched,
although both compounds have the same number of carbon and hydrogen atoms. For heavier
hydrocarbons there can be more isomers.
Properties of Paraffins:
1) Good natural stability. However, high reactivity in presence of oxygen or under the
influence of heat.
2) Low effect of temperature on viscosity. Highly paraffinic lubricants have high viscosity
index.
3) At a sufficiently high molecular weight they form waxy solids. Paraffinic crudes are good
sources of waxes.
4) Paraffinic hydrocarbons in the gasoline range burn too readily and lead to the ‘knocking’
phenomenon. They are poor components in gasoline blends.
5) In lubricants they lead to high pour points.
6) As motor oil components they tend to form hard carbon deposits,
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Properties of Iso-Paraffins:
1) For the same carbon number (number of carbon atoms in the hydrocarbon molecule), iso-
paraffins have lower boiling points than paraffins.
2) They make better components in gasoline blends; they have better (higher) octane rating.
Naphthenic Family:
Naphthenic hydrocarbons have fewer hydrogen atoms per molecule than paraffins. This is
because they have a closed or ring structure. Naphthene molecules with one ring have the
general formula CnH2n. They are also known as cyclo-paraffins. While rings can be small (3,
4 carbon atoms) or large (above 6) many naphthenes in petroleum have 5 or 6 membered
rings.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Properties of Naphthenes:
1) Naphthenes in motor oils form soft fluffy carbon deposits
2) Viscosity is affected more by temperature change. Viscosity index is lower for naphthenic
lubricants for paraffinic ones.
3) Naphthenic lubricants have low pour points.
4) Naphthenes in gasoline improve its octane rating e.g. n-heptane has 0 octane and methyl
cyclo-hexane, 78octane number.
Olefin Family:
Olefinic are unsaturated hydrocarbons with the general formula CnH2n. While olefins as
such are not normally found in natural crude oil, they are produced by cracking reactions.
The simplest member of this family is ethylene. Like paraffins, the higher members of the
olefinic family can exist in straight chain (normal) or branch (iso) structure. The location of
the double bond can vary, leading to different isomeric compounds.
Properties of Olefins:
1) Olefins are highly reactive. Thus their presence in gasoline or lubricating oils leads to
interaction with oxygen to form sludge, gum and varnish.
2) In gasoline the presence of some olefins does improve octane rating (anti –knock
properties). However, anti-oxidants will have to be added to suppress oxidation tendencies.
Aromatic Family:
Aromatics are unsaturated ring type hydrocarbons of a special chemical category. In these
structures, alternating double and single bonds having a property known as resonance confer
some stability and other special characteristics.
Aromatic streams from a refinery normally contain benzene or its derivatives, condensed
aromatic hydrocarbons like naphthalene or their derivatives.
Properties of Aromatics:
1) In view of the property of electronic resonance, benzene hydrocarbons are quite stable.
2) High octane values render aromatics excellent blended components.
3) Have high solvency power. They make good commercial solvents.
4) They are poor viscosity index components in lubricating oils.
5) Aromatics in kerosene produce smoky flames (low smoke point).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Crude Oil:
Various systems of classification have been attempted since the early production of crude oil
from the last century. Based on the nature of hydrocarbons present in Crude Oils, they are
broadly classified into
Paraffin Based Crude Oils: These consist mainly of paraffinic hydrocarbons and little / no
Asphaltenes matter. They usually give good yields of paraffinic wax, high grade SKO and
high grade lubricating oils.
Asphaltene Based Crude Oils: They contain little / no paraffin wax but Asphaltene material
is usually present in large proportions. They consist of mostly Naphthenes. Lube
Oils of these crude oils are more sensitive to temperature. These crude oils give high quality
Gasoline.
Mixed Base Crude Oils: These crude oils exhibit considerable overlapping of the both types
described above. A majority of the crude oils are of this type.
Recent classifications are based on their API gravity (calculated from specific gravity) and
sulphur content. Generally the higher the API gravity (or lighter the crude) the more distillate
products it contains and the higher is its value.
Sulphur is a significant factor in the crude cost as it is an impurity. The sulphur content in the
petroleum products is restricted by product specifications. High sulphur crudes also have to
be processed after all, but the investment and operational costs are high. Sulphur in crude
occurs in different forms like free Sulphur, Hydrogen Sulphide, Mercaptans, etc.
Nitrogen is also present in crude oils in very minute quantities in the form of Indoles,
Pyridines, Quinolines, etc. Nitrogen compounds create problems while processing and to the
stability of the products. Catalyst deactivation or poisoning, gum formation are some of the
offshoots of Nitrogen.
Pour point is also important factor to the extent of handling the crude oil. Crude oils with
high pour point require special handling facilities such as heat tracing and tank heating coils.
Sometimes pour depressing additives are also used. Pour point is an indication of-wax
content in crude oil.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Low Sulfur crudes:

Crude Origin API gravity Sulfur (Wt %)
Tapis Malaysia 47.6 0.05
Skua Australia 40.6 0.09
Bombay High India 39.2 0.15
Qua Iboe Nigeria 36.1 0.26
Ratna India 35.2 0.26
Ravva India 35.13 <0.1
Labuan Malaysia 33.2 0.09
Mirri Light Malaysia 29.19 0.23
High Sulphur crudes:

Crude Origin API gravity Sulfur (Wt %)
Kuwait Kuwait 31.2 2.53
Dubai UAE 31.05 2.0
Kirkuk Iran 35.6 1.99
Basrah Iraq 33.6 1.9
Umm Shalf UAE 35.77 1.39
Upper Zakum UAE 33.9 1.05
RANGE OF HYDROCARBONS IN TYPICAL CRUDE

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
RANGE OF PRODUCTS MADE FROM CRUDE OIL

Propylene
Liquefied Petroleum Gas - LPG
Gasoline (Petrol)/SRN
Naphtha
Aviation Turbine Fuel (ATF)
Mineral Turpentine Oil (MTO)
Kerosene
Diesel Oils
Jute Batching Oil
Lube Oils
LSHS / Fuel Oils
Asphalt
Sulphur
The Crude Distillation Unit of Visakh Refinery Expansion Project consists of Atmospheric
and vacuum Distillation Sections. The unit was originally de-signed to process 3.0MMPTA
of Basrah crude. It is also capable of processing other feed stocks like Kuwait (31.3 API),
Kirkuk (36 API) and 50:50 light / heavy Arabian mix crudes. Besides the unit is also capable
of processing Bombay High crude (39.2 API) at 90% design capacity without any change in
unit configuration or equipments and for capacities higher than 90%, the following
constraints are encountered.
Low preheat and consequent overloading of Atmospheric Furnace.
High product rundown temperatures
Stabilizer Re-boiler duty.
The main equipment of the unit include an electrostatic Desalter, an Atmospheric
Distillation Column (ADU), strippers, furnaces, Vacuum Distillation Column
(VDU),ejectors, pumps, exchangers, etc. The plant produces straight run products as well as
Heavy Vacuum Gas Oil (HVGO) the feed stock for FCC units and Vacuum Residue (VR),
the feed stock for Bitumen Blowing Unit (BBU).
From 1991 with the non-availability of Basrah crude, the unit processed mostly BH crude
with reduced throughputs due to the above mentioned constraints. To overcome these
constraints, the unit was modified in two stages in 1991 and 1993 to process BH crude (or
similar crudes) at 100% capacity.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
BRIEF PROCESS DESCRIPTION
The unit process can be classified into two sections as given under.
5.1 ATMOSPHERIC SECTION
Crude oil from the off-site tanks is supplied as feed to the unit. In the Atmospheric Section,
crude is preheated in a series of preheat- exchangers. The sensible heat of various products
and circulating refluxes (CRs) is used for this purpose. After the crude attains a preheat of
125 oC, it is sent into a Desalter for removal of water, salts, metals, sludge and any other
impurity. This is achieved by controlled addition of water to the crude to form an emulsion
and the separation of the emulsified water from the crude under an electric field. The water
thus injected into the crude extracts the salts in the crude. After desalting, the crude is boosted
to a higher pressure and is split into two streams. One stream is preheated by the Atmospheric
Distillation Column products and the other by the Vacuum Distillation Column products and
refluxes .After passing through the preheat exchangers, crude from both the streams is
combined and sent into a Pre-Flash Drum (PFD), which facilitates the removal of lighter
products from the preheated crude. This works on the principle of flashing. The bottoms of
the PFD are then boosted again in a turbine driven pump and sent into an exchanger for
further preheat gain in the form of sensible heat of Circulating Oil from FCCU-II. There is
also a provision to route crude to the PFD downstream of the Circulating Oil exchanger. The
outlet of this exchanger is routed to the Atmospheric Furnace for further heat gain. Once the
crude attains the required coil outlet temperature, which is dependent on the crude being
processed, it is sent into the flash zone of the Atmospheric Distillation Column.
Crude when it enters the Column is partly converted into vapor phase, which travels up in the
Column (enriching section). The balance crude oil which is in the liquid form travels to the
bottom section (stripping section) of the column. Stripping steam is introduced at the bottom
of the column to strip off the lighter fractions in the bottom product. This also helps in the
vaporization of hydrocarbons by lowering of partial pressure† (Dalton’s law of pressures).
The vapors in the enriching section are separated into four fractions namely the overhead
fractions and three side draw-offs. The overhead fraction is condensed totally in the overhead
condensers and is collected in the reflux drum. To control the top temperature of the column,
a part of the above condensed vapors, known as Unstabilized Naphtha, is sent to the column
as top reflux. The balance is used as a feed to Naphtha Stabilizer. The stripping steam used in
the Atmospheric column gets condensed along with the overhead vapors and is accumulated
in the boot of the reflux drum. This condensate, known as Sour water, can either be used for
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
Desalter wash water injection, or can be routed to the Sour Water Stripping Unit (SWSU) for
treatment.
Heavy Naphtha, Kerosene / ATF and Diesel are the three side draw-offs. They are further
steam stripped† (importance of steam stripping) in strippers to meet the product
specifications. Three Circulating Refluxes (CR’s) Top Pump Around, Middle Pump Around
(Kerosene CR) and Bottom Pump Around (Diesel CR) are also drawn separately; their
sensible heat is removed and then they are returned to the column to maintain the temperature
profile inside the column .Unstabilized Naphtha, which is a mixture of Naphtha and LPG,
from the overhead reflux drum, is sent to the Stabilizer. The process in the Stabilizer is a
simple two-component distillation with a reboiler and overhead condensers. Unstabilized
Naphtha is preheated in an exchanger, which extracts the sensible heat from Stabilized
Naphtha, and sent into the Stabilizer. The heat input to maintain the bottom temperature of
the Stabilizer is provided by a reboiler, which uses Middle Pump Around (Kero CR) as the
heating medium. The overhead vapors from the Stabilizer are condensed in the overhead
condensers and collected in the reflux drum. To maintain the top temperature, a part of the
above condensed liquid i.e., LPG is sent as reflux to the Stabilizer. The balance LPG is routed
to MEROX for further treatment. The Stabilized Naphtha or Straight Run Naphtha (SRN)
from the Stabilizer bottom is routed to the Caustic Wash Section for the removal of
mercaptans and H2S present in it by washing it with caustic solution. The outlet of the
Caustic Wash Section is then routed to the Water Wash Section where the caustic treated
SRN is washed with water to remove any caustic carry-over in SRN. The outlet of this
section is routed to storage tank.
The bottom product of the Atmospheric Distillation Column, known as the Reduced Crude
Oil is sent to the Vacuum Distillation Column for further processing.
5.2 VACUUM SECTION
The Reduced Crude Oil from the Atmospheric Distillation Column is mixed with Slop-Cut
Distillate Recycle, heated and partially vaporized in the Vacuum Furnace and is introduced
into the flash zone of the Vacuum Distillation Column. The liquid portion of the feed drops
into the bottom section of the Column and is withdrawn as Short residue. The vaporized
portion rises up in the tower and is fractionated into three side stream products. The Short
Residue is partially routed back to the Vacuum Distillation Column bottom as quench after
transferring some of its sensible heat to the crude oil. The balance can be routed either as feed
to the Bitumen Blowing Unit, or the Vis-Breaker Unit or can be sent to Fuel Oil storage
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
tanks. Slop-Cut Distillate is withdrawn as the first side draw-off from the Wash Zone of the
Vacuum Distillation Column. The vapors rising from the Wash Zone pass through the
demister pad to ensure the removal of entrained Asphaltenes and metals to achieve the quality
of FCCU feed. A slip stream of Slop Distillate, known as Slop-cut Recycle, can be routed to
the Reduced Crude Oil stream which is then routed to the Vacuum Furnace.
The Slop-Cut Distillate is mixed with the Short Residue and sent to the Fuel Oil pool. In case
the Short Residue is being regulated for Bitumen directly from the column, then there is a
provision to route the Slop Distillate to a Cooler Box in CDU-I. The hydrocarbon vapor from
the Wash Zone is condensed in the HVGO and LVGO sections. HVGO is drawn off as the
second side stream along with the Internal Reflux and the Circulating Reflux. Internal Reflux
(Wash Oil) is a hot HVGO stream from the pump discharge routed to the Column below the
HVGO bed to avoid coke formation in the Wash Zone. Circulating Reflux is used to preheat
the crude, generate steam and then returned to the Vacuum Column at the top of the HVGO
section. The product can be routed either as hot feed to FCCU-II or to the storage tank.
LVGO is the third side stream drawn along with the Circulating Reflux and Internal Reflux to
the HVGO packing. Circulating Reflux is used to preheat the crude and is cooled further
before returning to the Vacuum Column at the top of the LVGO section.
Vacuum is maintained by a three-stage ejector system, with three ejectors in each stage, and
surface condensers. The Vacuum Column overhead vapor flows through the 1st stage
ejectors. The discharge from the 1st stage ejectors goes to the primary condenser. The non-
condensable in this condenser are drawn by the 2nd stage ejectors, whose outlet is again
routed to a secondary condenser. The non-condensable of the secondary condenser are drawn
by the 3rd stage ejectors. The discharge of the 3rd stage ejectors goes to an after-condenser
and non-condensable vapors are routed to atmos Heater (hot well off gas burners) or vented
to the Atmosphere through the Hotwell Drum. The condensate from all the condensers is
routed to the Hotwell Drum through dip legs. Water and oil carry over in the condensate are
separated in the Hotwell Drum. Water can be used for Desalter wash water injection or can
be routed to the Sour Water Stripping Unit. Oil which is carried over along with the tower
overheads and enters the Hotwell is pumped to the Hotwell Oil intermediate storage tank or
the slop oil tank.
5.3 CHEMICAL INJECTIONS

i. De-emulsifier
De-emulsifier solution is added to the crude at the feed pump suction to break the water-
crude emulsion. De-emulsifiers are surface activating agents and act on the interfacial surface
tension of crude and water emulsion.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
ii. Caustic
Caustic solution is injected either at the feed pump suction or at the suction of the feed
booster pump. Caustic is injected to remove the hydrolysable salts, which if not removed, can
get converted into HCl and cause corrosion in the system.
iii. Neutralizer
Neutralizer solution is injected to the overhead vapour line and top reflux line of Atmospheric
Column and the Vacuum Column overhead system. This helps in maintaining a stable pH at
the column overhead area, which is very essential for a good Corrosion control.
iv. Corrosion Inhibitor

Corrosion Inhibitor solution is injected into the overhead vapour line and the Top Reflux line
of the Atmospheric Distillation Column and in the overhead vapour line of the Vacuum
Distillation Column. This helps in preventing the contact of corrosive water and acids with
the shell of the column. It acts by forming a film on the surface of the shell in the overhead
area. This film is impervious to the acids formed.
5.4 DISTILLATION
The Chemical Engineering operation used in the Crude / Vacuum Distillation Unit to process
crude oil (or range of hydrocarbons) into a range of products is Distillation. Distillation
technique is employed to separate various product cuts from the crude petroleum in this
primary distillation unit.
Distillation is one of the many separation processes employed in chemical industry. It is a
physical process (not necessarily involving chemical reactions) where separation is achieved
using differences in their boiling points or, in other words, difference in volatility. The
application of this technique ranges from the simplest binary distillation to the most complex
distillations like azeotropic or extractive distillations.
5.4.1 PRINCIPLE
If solution of two components with different boiling points is allowed to flash in a vessel, the
liquid and vapour portions separate and after sufficient time attain equilibrium. The vapors
will be richer in lighter components and the liquid residue therefore leaner. Suppose the
vapours are condensed and flashed again, the resulting vapours will be richer in the lighter
components. By repeating the procedure, we will reach a stage when vapours will be full of
the lighter components (ideally). Similarly, by repeatedly heating and flashing the liquid
portion, we will eventually end up with a liquid which is hundred per cent the heavier
component. The same principle is used in a distillation column with an integration of the
above process and each step where the heavier component in the vapours is condensed and
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
the lighter component in the liquid is vaporized known as an equilibrium stage. The total
number of theoretical stages will be decided by the extent of separation relative volatility of
the components involved.
In a typical distillation operation, the feed is introduced into a vertical cascade of stages.
Vapour rising in the section above the feed (called enriching / rectifying section) is washed
with liquid to remove the less volatile components. The wash liquid is provided by
condensing the vapour from the top (rich in more volatile component) called reflux; a portion
of the condensate is removed as distillate. In the section below the feed (called stripping
section), the liquid is stripped of the volatile component by vapours rising from bottom. The
vapours are generated by supplying the necessary energy at the bottom through a reboiler or
furnace. The liquid rich in less volatile component is removed from the bottom.
5.4.2 MULTICOMPONENT SYSTEM
Through a binary system is ideal to design and operate, many of the separations encountered
in the industry are not so; they involve more than two components. The principles of binary
solutions are generally applicable to such distillations but nevertheless some special
consideration and techniques are needed more volatile components are designated as light
and the less volatile, heavy. Suppose a solution has to
be separated by distillation, the majority component among the bottom product components
compared to the other lighter components is called the light key component. Similarly, the
one among the distillate components which is present in considerable amount when compared
to the other heavier components is the heavy key component. With this key component as the
basis, now the problem of multi-component distillation is treated in much the same way as
binary distillation. The difficulty of separation, as measured by the number of trays for a
given reflux ratio, is fixed by the key component concentrations in the products. It is,
therefore, important to establish the key components in a multi-component distillation.
The distillations involved in petroleum industry are further complicated by aspects like
withdrawal of side streams (apart from top and bottom products), circulating refluxes,
stripping steam, etc. Here, the separation is achieved not directly on the basis of components
but by boiling ranges. Each product comprises multiple components and its end use
requirements specify certain properties such as boiling range, flash point, specific gravity,
viscosity, etc., rather than component purity. The design of such systems is very complex and
cannot be accomplished by totally theoretical methods; pilot plant studies coupled with past
experience generally yield satisfactory results. Many software packages are available in the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
present day market to evaluate the performance of the existing columns and also to design
new columns.
5.4.3 DISTILLATION TOWERS
Fractionating towers and related equipment are mechanical devices for repeatedly
establishing equilibrium between ascending vapour and descending liquid and repeated
separation of the two phases. Hence, a means of attaining a large interface for contact and
affecting a complete separation of the two phases must be incorporated in any successful
design. The choice of contacting device in a column depends on
Operating pressure and pressure drop.
Turn-down ratio
Nature of the solution (foaming tendency, presence of solids, etc.)
Number of side streams
The most generally used in the industry are tray towers in which the liquid and vapour are
contacted in steps or trays or plates.
Types of trays:
Trays with down-comers (Bubble -cap, Sieve, Valve)
Trays without down-comers (Duel flow, baffle)
Multi down-comer trays
Collection or chimney trays
In tray towers, the liquid from the stage above flows across each tray and through a down-
comer to the tray below. The gas passes upward through opening in the tray, then bubbles
through the liquid, disengages and passes on to the next tray above. The depth of liquid on
the tray required for gas contacting is maintained by an overflow weir. Each tray of the
column is a stage. The number of equilibrium stages (theoretical trays) determines the
number of actual trays. Tray spacing is usually decided on the basis of adequate insurance
against flooding & entrainment and on expediency in construction, maintenance & cost. It
varies from 300 - 900 mm depending on the diameter and service of the tower. Column
diameter or cross sectional area is determined on the basis of gas/liquid volumes to be
handled. Packed columns are preferred to tray towers under the following circumstances:
for columns of less than 2 ft. diameter
for acids and other corrosive materials
for foaming liquids
for thermally sensitive liquids which require low liquid hold-up
for lower pressure drop or for vacuum operation
for greater mass transfer efficiency
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 5
PLANT NAME: CDU II
Chapter Rev No: 0
The design of packed towers involves the determination of HETP (Height Equivalent to
Theoretical Plate). Packings can be either random or structured. The various types of
packings available are
Generation Type of packing

First Raschig, Lessing, Cross Partion Rings, Berl saddles
Second Pall Rings, Hypak, Intalox Metal Tower packing(IMTP), Cascade Mini Rings
(CMR), Nutter rings
Third Gempak, Mellapak, Intalox ( structured )
Care should be exercised to distribute feed and reflux streams uniformly throughout the
cross-section of the packing to avoid channeling. The withdrawals will be from collector or
chimney trays.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
DETAILED DESCRIPTION OF CONFIGURATION & PROCESS
GENERAL
CDU-II is an integrated unit which has both CDU/VDU and BBU. The CDU/VDU unit
process can be divided into 7 sections as given under.
1) Crude Distillation Unit

2) Naphtha Stabilizer Unit
3) Caustic / Water Wash Section
4) Vacuum Distillation Unit
5) Tempered Water / DM Water System
6) Steam Generation
7) Chemical Injection Facilities
6.1 CRUDE DISTILLATION UNIT
The Crude Distillation Unit is further classified into the following sub sections
• Feed supply
• Pre-Heat Train-I
• Desalter
• Pre-Heat Train-II
• Pre-Flash Drum
• Atmospheric Heater
• Atmospheric Distillation Column/Main Column
• Product Strippers
• Product Coolers and Routing to Storage Tanks
6.1.1 FEED SUPPLY
Crude is supplied to the unit as feed from the crude tanks. Crude enters the unit in a 10”
header line at a pressure of 1-2 kg/cm2 or 6-8 kg/ cm2 in the case of Refinery tanks or ATP
tanks respectively. 11-PG-101 is provided to indicate pressure of the crude from the storage
tanks.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
This crude is fed to a crude charge pump 11-P-01A/B to raise the feed crude pressure to 24
kg/cm2 g. The rated capacity of the pumps is 482 m3/h. However, the pump can be operated
at a design limit of 520 m3/h. Both the pumps are centrifugal type. While one pump (01A)
is motor driven, the other (01B) is turbine driven one. Normally 01A is used and 01B is
kept as a standby. The discharges of 01A and 01B have PG’s 11-PG-103 and 11-PG-102
respectively. The discharge pressure of the pumps is indicated on the DCS panel as 11-PI-
101. There is a low pressure switch 11-PSL-101 on the pump discharge which sounds alarm
on the annunciator panel in the DCS room to indicate low discharge pressure. Turbine auto
cut-in facility was provided in case the discharge pressure of the discharge pressure of the
motor driven pump comes below 18 kg/cm2 g. However this facility has been defunct.
There are provisions for injecting Demulsifier and Caustic at the pump suction with
individual isolation valves. A 4” service water connection and a 4” flushing oil connection
are provided for use during shut-down. There is also a 6” provision to route the feed pump
suction or RCO pump discharge to slop via the unit slop header. The crude charged to the
unit is recorded and integrated in 11-FR/FQ-104. From the pump discharge header, the
crude is sent into the Preheat Train-I. Crude pre-heating is done in two modes – BH mode
and PG mode depending on the type of the crude being processed. Though BH mode
operation is more common, PG mode is also used in special cases. For this reason, both the
cases are discussed in the following sections.
6.1.2 PREHEAT TRAIN-I (PHT-I)
This preheat train is totally upstream of the Desalter. It has 7 exchangers from 11-E-01 to
11-E-07. This preheat train helps in heating the crude to the desalting temperature which
helps in improving the crude oil’s fluidity by decreasing its viscosity and also helps in
thorough mixing of desalting water. Various product streams are used to preheat the crude
in this train.
1.BH Mode: The unit is required to be run in Bombay High (BH) mode whenever low
sulphur crude is processed. Low sulphur crudes have low tar content and lighter ends are
more. Hence, these crudes require lesser preheat.
2.PG Mode: The unit is operated in Persian Gulf mode for processing high sulphur crude.
High sulphur crudes have high tar content and the percentage of lighter components is
lesser. Hence, the pre-heat required for such crudes is more.
The following table given on the next page gives operating temperatures for both BH and
PG cases. All those exchangers (listed on the table) can be bypassed and isolated
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
individually on the shell and tube side. There are TI’s on all the shell and tube-side outlets
of the above exchangers and the condition can be monitored from the DCS panel. The
crude thus preheated to 125-135oC goes to the Desalter.
Facility to Place 11-E-7 before /After Desalter
11-E-07 can be placed before as well as after the Desalter. Normally it is placed in the
upstream of the Desalter. For better efficiency of the Desalter, its pressure has to be
maintained between 10.0 -11.0 kg/cm2 at a temperature ranging from 120 to 130 °C. If the
temperature is high and pressure is low, crude will vaporize, which is undesirable for
Desalter operation. This can occur only when preheat at the upstream of Desalter is high
and hence the above facility was proposed. The switching over of 11-E-07 to the
downstream of desalter will help in reducing vaporization in desalter and thereby would
lead to a gain in total crude preheat.
Heat exchanger BH mode operation PG mode operation

(shell side and Crude inlet Crude outlet Crude inlet Crude outlet
tube side fluids) temperature, temperature, temperature, temperature,
°C °C °C °C
11-E-01 30 37.5 30 35
(crude/ HN)
11-E-02 37.5 52.5 35 44
(Crude/ KERO)
11-E-03 52.5 66 44 60
(crude/diesel)
11-E-04A/B 66 101 60 95
(crude/TPA)
11-E-05 101 117.6 95 111.5
(Crude/ KERO)
11-E-06 117.6 128.3 111.5 118
(crude/diesel)
11-E-07 * 128.3 135.1 118 125
(crude/ LVGO)
* There is a provision to place 11-E-07 either upstream or down-stream of Desalter.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
6.1.3 DESALTER
Crude oil brings along with it salts of Sodium, Magnesium etc., metals like Arsenic,
Vanadium etc., and sludge. Although these are present only in small amounts, their
presence can result in serious problems in down-stream equipment viz., heat exchangers
heaters and columns.
Specific effects resulting from salts in the crude are:

a) At high temperatures, hydrolysable salts in the crude like MgCl2 hydrolyse to
Hydrochloric acid which causes severe corrosion in Crude Distillation Column and piping.
b) Salts of Sodium and Calcium act as a catalyst for coke formation in furnace and heat
exchanger tubes which cause plugging and reduced heat transfer rates in the exchangers.
Excessive coke formation results in escalation of hot spots on heater tubes which can have
serious and disastrous consequences for heater tubes.
c) Salts and solids, concentrated in the residuum of distillation towers, result in high ash
content and degradation of the product
d) The presence of metals like Arsenic and Nickel act as poison to catalysts that may be
used in the down-stream process units.
Thus removal of the impurities in the crude oil is very essential to avoid their deleterious
effects. Desalting of the crude is a very effective method to remove these impurities.
The advantages of crude Desalting are given below:

a) A Desalter is a shock absorber for smoothing out abnormalities due to slugs of water
during feed tank switches.
b) Slop oil injection to the crude can be achieved.
At a modest cost Crude + Desalter wash water mixture enters the Desalter which employs
electrostatic elements to coalesce and separate water from oil. Wash water is used for
reducing the salt content in crude oil so that the salts are within acceptable and specified
limits in the desalted crude. Application of strong electric field hastens the process of
coalescing and therefore settling of all unwanted material. When the crude-water mixture is
subjected to a high-potential electric field, the tiny water droplets get distributed between
the electrodes forming dipoles. This makes it possible for the tiny particles to coalesce and
form bigger particles of sufficient weight to settle down. The force of attraction between
two droplets must be of sufficient magnitude to break through the oil film. Thus in effect,
oil-water mixture separates into two phases in Desalter. While the oil phase floats on top
and overflows, water with its dissolved salts, metals, mud and iron oxides settle down at the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
bottom. At a level below the electrodes an interface is formed between hydrocarbons and
water. This inter phase level is controlled by regulating the effluent water withdrawal rate
from the vessel.
Caustic injection in crude, upstream of Desalter, is done to neutralise acids present in crude
and convert them into salts. These salts are then removed by wash water in the Desalter.
Caustic injection down-stream of Desalter is provided to neutralise any other acid traces
formed at the Desalter operating conditions. Brine is associated with crude both as a fine
suspension of droplets and more permanent emulsion. To break these light emulsions
Demulsifier chemical is added to the crude line at the Battery Limit. This ensures better
functioning of the Desalter.
Exact details of the Desalter can be obtained in the vendor’s manual.
The description of desalting process in CDU-II is dealt in three subsections

a) Desalter (11-V-02) Description
b) Desalter Wash Water System
c) Desalter Operation
Desalter (11-V-02) Description:
This is a single stage Desalter unit with the following specifications:

Parameter Specifications
Electric power requirement 20 Kv
Pressure drop across the mixed valve (kg/cm2) 0.7 - 1.0
Operating temperature °C 120-130 ° C
Operating pressure (kg/cm2) 10.5
Salt content of fresh crude (max. lb/1000bbl) 20
Salt content of desalted crude, max. 10
Water content of the product crude (%wt.) 0.1 BS&W
Effluent water oil content (% vol ppm) 100
Crude and Desalter wash water enter the vessel (11-V-02) at the bottom. Desalted crude
leaves from the top of the vessel. There is a provision to bypass the Desalter if required
through a 12” line. Crude outlet from top of the vessel is connected to the crude booster
pumps (11-P-02 A/B) suction. Drain connections to CBD / OWS are also provided on the
Desalter for maintenance activities.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Since Desalter is a liquid filled vessel, the Desalter pressure control (11-PIC-105) is
achieved by manipulating 11-PV-105 provided on crude line at the inlet of Preheat Train-I.
11-PSV-101 (set pressure 12.5 kg/cm2 g.) is provided to protect the Desalter from over-
pressurization due to blocked outlet. Discharge of the Pressure Safety Valve is connected to
the flash zone of Atmospheric Column. The Pressure Safety Valve is located close to the
Atmospheric Distillation Column to reduce the discharge pipe length where two phase flow
may occur after PSV discharge. The Desalter approach temperature of the crude-wash
water mixture downstream of the mix valve is indicated on the DCS panel by 11-TI-101.
The crude-wash-water mixture is subjected to intense electric field created by two grid type
electrodes located in the Desalter. The power to these electrodes is supplied by 3
transformers mounted on the Desalter. Panel mounted push button are provided to control
the power supply. There is a provision of 3 ammeters and 3 voltmeters in the field to
indicate the condition of the electric field. There is also an indication of the voltage on the
DCS panel as V1901A&B and VC1901. The higher the amperage, the more conducting is
the electric field in the Desalter. There is a trip provision on the power supply to the
Desalter which gets activated at high amperage.
Two types of instruments are provided for measuring and controlling the inter phase level
1) 11-LIC-101 which is a Displacer type instrument
2) Agar ID and OW (Interface Detector and Oil-Water) probe.
The Agar Probe System has three probes on the Desalter which measure the water
concentration in the zone they are present. The details of the Agar Probe System are given
in the table below.
Probe # Location Significance

LC1101A At 45 ° angle Indicates the interphase level
LI1101B Below the lower electrode Indicates the water concentration in the crude layer.
Also known as the emulsion level indicator
LI1101C Bottom Indicates the sludge level
Either of the two LIC’s can be used for controlling the inter-phase level. This is achieved
by changing the software switch LC1101SS on the DCS panel. The LIC controls the inter
phase level by operating the control valve LCV-1101 (on the brine line in the SWSU),
which controls the flow of effluent water in a 4” line from the Desalter.LIC-1101A has
software LAL and LAH alarms. A low level switch 11-LSL-102 is mounted on the top of
the Desalter drum to protect the system. Actuation of 11-LSL-102 switches off the power
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
supply to Desalter locally. There is a provision of 5 try-cocks in the lower half of the
Desalter for physical verification of the interphase level.
The material that collects at Desalter bottom is a thick sludge that is corrosive and often has
a tendency to choke piping. This sludge material needs to be cleaned periodically. There is
a provision to carry out desludging operation with the unit online. Desalter wash-water
pumps (11-P-12 A/B) are used for this purpose. A 3” line (Desludging connection) is
provided from the pump discharge. There are distributors / Spargers inside the Desalter for
effective desludging. Desludging is a batch process. It loosens up the muck collected at the
bottom and facilitates easy exit from outlet. Care should be taken during this operation as
sudden jerk can upset oil-water interphase leading to water and salt carryover downstream
of the Desalter.
The degree of mixing between the crude and the wash-water can be varied by changing the
pressure drop (DP) across the mix-valve 11-DPV-101. Sample points are provided on
Crude oil inlet to Desalter, sludge water, from vessels itself and crude oil outlet from
Desalter. Hot samples are cooled in a sample cooler. Sampling cock lines have been
provided with a 3” LP steam flushing line to clean the line of any crude after taking
samples. Sample cocks, called try cocks, are provided on Desalter at various elevations of
the vessel. These are used to check interphase level physically against that indicated by
LIC-1101A.There is also a bypass provision for the Desalter for operational flexibility.
There is a 2” LP steam provision to serve as a steam out point.
Desalter Wash Water System:

Stripped water from Sour Water Stripping Unit, Atmos Sour water, Hotwell water, MAB
condensate from FCCU-II (if the chloride content is less than 240 .ppm), Service water and
also DM water can be used as wash-water for desalting. This water is first collected in
Desalter Water Vessel (11-V-04) whose level is maintained by the level controller 11-LIC-
103. A low level alarm 11-LAL-103 is provided to indicate the low level in the water drum.
Desalter water pumps 11-P-12 A/B delivers water from 11-V-04 to 11-E-18 where LP
steam is used to preheat the water to 125 °C. The flow of the wash water is controlled by
the FCV 11-FIC-102. There is a 3” water injection provision with a check valve and
isolation upstream of a manually operated mix-valve to supply the preheated water to the
Desalter. There is also a provision to route the stripped water from SWSU directly to the
Desalter in a 4” line at a temperature of 110 to 120 °C.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
The degree of mixing between the crude and the wash water can be varied by changing the
pressure drop (DP) across the mix-valve. Normally a DP of 0.5 kg/cm2 gives efficient
mixing. The crude approach temperature to the Desalter can be controlled manually by
operating the bypass of one of the exchangers between 11-E-01 and 11-E-07.
Desalter Operation
Some of the Parameters that are to be closely monitored to realize good Desalter operation
are:
1) Wash water
Dilution is the primary purpose of wash water injection. Acids like HCl and cyanide lose
their corrosive potency and salts can be washed out in solution with sufficient quantity of
water. Most Desalters are designed to use 4-6 volume percent water based on the crude
charge.
Wash water injection provision provided just upstream of Desalter mix valve is to be used
in crudes which have severe tendency to emulsify. Wash water can also be injected before
the crude charge pump. Injection at this point results in maximum contact and also prevents
the sediments from settling in the exchanger tubes and fouling them. But care should be
taken such that the intense shearing agitation in the preheat train does not create so tight an
emulsion that cannot be resolved in the Desalter. The severe shearing effect due to the
crude pump impellers should also be considered here. The quality of water is a very
important aspect.
It is recommended that ammonia-free and caustic-free wash water having a pH of 6.5 is

used in the desalter for effective removal of chloride salts, scaling salts, sediments and
water in the crude. Lower Desalter wash water pH of 6.5 reduces the amount to hydrogen
sulphide in the effluent water, lowers the filterable solids, i.e., iron sulphides in the desalted
crude, reduces the quantity of oil in the effluent water and keeps the magnesium and
calcium carbonates in the water phase. These salts become insoluble in water with
increasing pH and deposit at the bottom of the Desalter as sludge. Both ammonia and
caustic will accelerate the precipitation of sludge in the Desalter.
The use of un-stripped sour water recycle to the Desalter can lead to operational problems
of the Desalter. The most common problems are listed below
a) It stabilizes the crude emulsions in the Desalter resulting in water carry over from
Desalter which can upset the overhead corrosion control. The following disadvantages
result when water is carried over from Desalter.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
• Water carried over from the Desalter results in increased pressure drop in heat
exchanger train and the heater.
• Steam occupies 7 to 10 times the volume compared to hydrocarbon. This causes
fractionators tray vapour loading.
• Energy consumption increases due to vaporization of the entrained Desalter wash
water.
• Higher quantities of water in the overhead will raise the dew point temperature of the
water in the overhead that may result in the condensation of water inside the tower.
This can result in an aggressive level of corrosion attack on the top tray.
b) Ammonia present in the sour water recycle causes high pH which has several
disadvantages.
1. The filterable solids and metals from the crude oil will not be removed.
2. Higher amounts of filterable solids (less than 20 microns) have been found in the
desalted crude compared to the raw crude. These solids are found to have the same
elemental makeup as the deposits found in the heat exchangers and heaters.
2) Settling time
The settling time of the water droplets is very critical for the removal of water from the oil.
Settling time is directly proportional to the viscosity of the fluid and inversely proportional
to the square of the droplet size and difference in density if the drop and the fluid.
3) Temperature
The water separation is accelerated by the rise in temperature of the oil as the viscosity of
settling medium – oil – decreases with temperature, but water carryover in desalted crude
increases with temperature due to the greater solubility of water in hydrocarbons at higher
temperatures. Hence care should be taken that the design operating temperature is not
exceeded for most of the time
4) Desalting Chemicals
There are two types of emulsions. One is a continuous phase of oil with some emulsified
water and the other has water in the continuous phase with hydrocarbons suspended in it.
Generally, solid particles are coated with heavy oil or wax, which inhibits water contact.
Wetting agents or emulsifiers, strip the oil and aid in water contact. But emulsifiers being
semi-polar in nature induce polarity on water droplets and also change the surface tension,
making it difficult for the droplets to coalesce. Demulsifiers either weaken the water film or
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
reduce / change polarity of the droplet. This helps in resolving the emulsified oil. Caustic is
used to control the pH in the Desalter.
5) Alternating Electric Fields

The thin film of emulsifier surrounding the water globule is ruptured by the sharp force of
the alternating electric field and the water so released coalesces. This mechanism involves
the vibration of all the water droplets within the electric field. The same effect is also
achieved by the collision of water globules with each other.
6) Mixing valve
This is used to produce maximum contact of wash water with the crude oil and is critical
for optimising the Desalter performance. The pressure differential (dP) across the mix valve
controls the degree of emulsification. Increase in the mix valve dP causes a proportional
increase in salt removal. But the emulsions formed under very high dP are so tight that the
water droplets will not coalesce, resulting in water and salt carryover, defeating the very
purpose of Desalter.
7) Pressure
The purpose of pressure is to keep the system from boiling. The agitation resulting from
boiling would result in severe carryover of BS&W and salts. The operating pressure of
Desalter is determined by adding 1.021 to 1.361 kg/cm2 to the vapour pressure of the crude
oil at the operating temperature.
8) Level
A steady interface is to be maintained between the oil emulsion and water phase in the
Desalter. An emulsion usually of oil in water exists below this interface. This interface
supports particulates, solids encapsulated by oil and emulsified with the water. The
operating level of this interface should be maintained below the lower electrode in order to
avoid an amperage overload, which could shut-down the electrical system. Also high
interface level can result in not only emulsion carry over to the distillation tower upsetting
its conditions, but also can accelerate the fouling of exchangers. At the same time, too low
interface level can result in oil carry-under, upsetting the downstream Effluent Treatment
Plants.
9) Agar Probe System

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Agar instruments function by the principle of energy absorption. All the materials absorb at
different rates. AGAR technology uses this fundamental physical property to differentiate
between two materials based on the rate at which the energy is absorbed. One common
example of two such materials is oil and water. Water absorbs energy at a much higher rate
than hydrocarbons. When an AGAR ID and OW (Interface Detector and Oil-Water)
antenna is surrounded by water, the energy from that antenna is absorbed very quickly. This
puts a high load on the attached transmitter, and the transmitter then sends a high signal
back to the PS (Power Supply / Signal). However, when oil is present at the antenna, the
rate at which energy is absorbed from the antenna is much lower, resulting in a lower load
and signal sent to the PS. When calibrated properly for oil and water, an AGAR ID and OW
will use this transmitter load to determine the concentration of oil. The signal from the
transmitter to the PS is then converted to a 4-20 mA current that is proportional to the
amount of water (water concentration by volume) in the area around the antenna from 0%
(all oil) to 100% (all water).
This system is very effective since it achieves control not by measuring the imaginary
interface level but by measuring the actual water content at different elevations in the
system. There are 3 agar probes on the Desalter at the locations as shown in the figure.
AGAR ID and OW, LC-1101A located at 45° inclination indicates the interface level of
crude and water in that location. AGAR ID and OW, LI-1101B located horizontally just
below the central line of the Desalter vessel (just below the power grid), indicates the water
concentration in the crude layer at that location. During normal operation, it reads 0 to 1%,
indicating that the water concentration in that zone is 0 or 1%. If it shows a value greater
than 0, it indicates that the emulsion level is rising in the Desalter.
LI-1101C located at the bottom of the Desalter vessel indicates the concentration of water
at that location. During normal operation without any sediment, it reads 100%, indicating
the water concentration to be 100% at that level. However, an indication below 100
indicates the accumulation of sludge in the Desalter and the necessity for online desludging.
The desalted crude from the Desalter is taken from the top of the vessel to the suction of the
Crude Booster Pump 11-PM-02A. The standby pump 11-PT-02B is used for PFD service.
However, this pump can be used when in Crude Booster mode, when PFD is out of service.
The Booster Pumps give a discharge pressure of 33.6 kg/cm2 g. The discharge pressure of
02A and 02B are indicated in the field by 11-PG-113 and 11-PG-114 respectively. There is
a provision for caustic injection at the suction of the Booster Pump. The crude thus boosted
is sent to the Preheat Train-II for further preheating.
6.1.4 PREHEAT TRAIN-II

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
The crude from the Desalter is split into 2 streams. One stream goes to the Atmos-side
exchangers, whereas the other goes to the Vac-side exchangers. The flow to the Atmos-side
exchangers is indicated and recorded by 11-FI/FR-105. The flow to the vac side exchangers
is controlled, indicated and recorded by split flow control valve 11-FRC-101.
Since, the pre-heat requirement of both the types of crude is different, so, the sequence of
exchangers in preheat train II is slightly different for the two operating modes. This motive
of the alignment is to add more pre-heat to the high sulphur crudes. The sequence of the
exchangers in the path of the crude flow in the BH and PG modes is given as follows.
BH Mode
Atmos-side Exchangers
Heat exchanger( shell side/ tube side fluid) Crude inlet Crude outlet
temperature, °C temperature, °C
11-E-08 (crude/ diesel) 131.1 140.6
11-E-11 (Kero CR / crude) 140.6 169.3
11-E-10 (crude/ Kero) 169.3 172.2
11-E-09 (Kero CR / crude) 172.2 180.9
11-E-12 (Diesel/ Crude) 180.9 204.1
11-E-14 (Diesel CR / crude) 204.1 236.6
11-E-13 (diesel/ crude) 236.6 252.2
11-E-15 A/B ( diesel CR/ crude) 252.2 278.8
11-E-16 (SR/ crude) 278.8 281.1
Note:-Now a days, the sequence of exchangers that is being followed in BH mode of

operation is 11E8→11E11→11E10→11E9→11E12→11E13→11E14→11E15→11E16
Vac-side Exchangers
12-E-01ABC (Kero CR / crude) 131.1 172.1
12-E-02 (crude / HVGO) 172.1 193.9
12-E-03 (SR/ crude) 193.9 204.7
12-E-04 (crude/ HVGO) 204.7 233.4
12-E-05 A/B ( HVGO CR/ crude) 233.4 258.8
12-E-06A/B ( crude/ SR) * 258.8 265.5
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
PG Mode
Atmos-side Exchangers
11-E-08 (crude/ diesel) 120 126
11-E-09 (Kero CR / crude) 126 161.5
11-E-10 (crude/ Kero) 161.5 168
11-E-11 (Kero CR / crude) 168 204.5
11-E-12 (Diesel/ Crude) 204.5 218
11-E-13 (diesel/ crude) 218 235
11-E-14 (Diesel CR / crude) 235 251.5
11-E-15 A/B ( diesel CR/ crude) 251.5 278
11-E-16 (SR/ crude) 278 290
Vac-side Exchangers
12-E-01ABC (Kero CR / crude) 120 164
12-E-02 (crude / HVGO) 164 181
12-E-03 (SR/ crude) 181 213.5
12-E-04 (crude/ HVGO) 213.5 241.5
12-E-05 A/B ( HVGO CR/ crude) 241.5 271.5
12-E-06A/B ( crude/ SR) * 271.5 290
*RCO can be routed to 12-E-06 A/B on its tube side.
The crude thus pre-heated goes to the PFD and 11-E-40 A/B for flashing and further
preheating respectively.
6.1.5 PRE-FLASH DRUM (11-V-10)

Pre-Flash Drum was introduced to enhance the crude throughput of the unit by 0.2
MMTPA. This is achieved by the removal of lighter components in the crude by flashing it
and thereby reducing the load on 11-F-01. A maximum of 20 – 25% by volume of the total
crude entering the PFD can be achieved depending on the type of crude being processed.
The temperature and pressure of the crude after the pre-heat train is 250 oC+ and 20 kg/cm2
g. respectively. When this crude is allowed to flash i.e., its pressure is suddenly decreased,
the lighter fractions in the crude whose vapour pressure at that temperature equals the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
system pressure will vaporize. The operating pressure of the PFD varies with the crude
being processed.
Crude enters the PFD approximately in the middle of the vessel. There is a provision to
record the crude inlet pressure and temperature on DCS panel as P1901R and T1901R
respectively. Crude that flashes in the PFD exits in the form of vapours from the top of the
PFD and enters the 12th tray of the Atmos Column. A demister pad is provided on the
vapour line to knock off any liquid droplets entrained in the vapour. The amount of flashing
depends on the pressure in the PFD, which is controlled by PR1902. The crude level in the
PFD is controlled by LR1902. Level gauge glasses are also provided on the shell of the
PFD for physical verification of the level. There is also a high-level and low level switch
provision. The un-flashed heavier crude goes to the PFD turbine 11-PT-02B from where it
is boosted to 25 kg/cm2 g. and sent to the PFD manifold through 11-E-40 A/B. The crude
outlet flow from the PFD and its temperature are indicated on the DCS panel by F1902R
and T1902R (provided on the outlet of crude from PFD) respectively. The PFD has two
pressure safety valves (120-PSV-1201 A&B) set at 25.5 kg/cm2 g. The discharge of the
PSV is connected to the flash zone of the Atmospheric Distillation Column (down stream
of Desalter RV).
There is a provision to bypass crude flow to PFD in case of emergency, from the DCS
panel. This is done by operating the ROV switch on the auxiliary panel. There is an
interlock on this ROV operation. When ROV is opened, the LCV-1902 gets closed. This
interlock is provided to prevent the crude entry into the PFD when it is bypassed. A switch
is provided on the auxiliary panel to trip the turbine (11-P-02B) from the DCS panel.
Operating this switch on the auxiliary panel will close the steam shut off valve on the steam
inlet to the turbine, thereby cutting off steam to the turbine. There is a provision to reset the
SDV manually in the field, by which the SDV can be reset to open position. The outlet* of
the PFD is routed to 11-E-40 A/B for further heat gain. Sensible heat from Circulating Oil
of FCCU-II is utilized to preheat the crude cover heat further in this exchanger. The outlet
of 11-E-40 A/B, goes to the Atmospheric Furnace for further heat gain.
*There is a provision to place 11-E-40 A/B either upstream or downstream of the PFD.
This provision is made at the PFD manifold.
11-E-40 A/B (Crude/Circ. Oil)
Atmospheric Furnace (11-F-01) was limiting the throughput due to low preheat. In spite of
repeated cleaning of the preheat exchangers, the feed preheat was low and hence high load
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
on 11-F-01. Hence to reduce the load on the furnace, the above scheme has been
implemented.
11-E-40 A/B can be placed before PFD or after PFD. But it usually it is placed on the
downstream of PFD because 11-E-16 & 12-E-06 A/B outlet stream temperature are
sufficient enough for flashing out the light ends of the crude in PFD. This exchanger can be
placed in service even after bypassing PFD. This scheme has experienced preheat pick up
of up to 15 °C when feed was 500 m3/hr. Thus 11-E-40 A/B has helped in recovering the
heat lost In PFD due to flashing, thereby sustaining higher throughput.
6.1.6 ATMOSPHERIC HEATER:

Refer P&ID No.
The major equipments of this section are Atmospheric Heater, Air Pre-heater, ID Fan, FD
Fan and Steam Decoking Pot. The description of the Atmos Heater is divided into the
following sub sections:
1) Process System
2) Fuel System
3) Air Preheating System
4) Trip and Interlock System
5) Steam Air Decoking
6.1.6.1 Process System:
The crude from the PFD enters the Atmospheric Furnace, where it is heated further so that
it reaches the required flashing temperature. This is a vertical cylindrical type heater with
absorbed design heat duty of 40.226 MM Kcal/h for crude oil and 0.9 MM Kcal/h for
superheated steam same was revamped during 2010 T&I and heat duty was raised to 45.68
MM Kcal/h and 0.92 MM Kcal/hr for superheated steam (total 46.6 MM Kcal/h). The crude
coming to the heater gets split into 4 streams and enters the 4 crude passes of the furnace
under the flow recorders and controllers 11-FRC-301/302/303/304. Low flow alarms 11-
FAL-301/302/303/304 are provided on all the passes to protect the heater pass tubes in case
of low flow through each pass. Steam connections are provided downstream of the FCV’s
for purging the respective coils in case of emergency. The isolation valve for the purging
steam line is provided at a safe distance from the heater.
The feed enters the convection zone of the heater first. It is located at the top of the furnace
above the radiation zone. The purpose of this zone is to increase the thermal efficiency of
the furnace by extracting heat from the flue gas leaving the radiation zone. This zone
consists of 12 rows of tubes with 8 tubes per row. These 12 rows are arranged in 3 bundles
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
with 4 rows per bundle. While the top 2 rows of this zone are finned type the bottom two
are bare tubes. All the others are studded type. The effective length of each tube in this zone
is 9058mm. The material of construction of the tubes is 5% Chromium + 0.5%
Molybdenum. Additional convection zone was provided during 2010 T&I to increase the
heater efficiency and heat duty. The additional convection zone consists of 8 rows of tubes
with 8 tubes per row. In these 8 rows, top 4 rows of this zone are 24 SPP studded tubes,
below it 2 rows of 12 SPP studded tubes and the bottom two are bare tubes.
Soot in the flue gas gets deposited on the tubes in the convection zone. This reduces the
heat transfer efficiency of the tubes which can be noticed by increasing flue gas
temperature and decreasing heat pick up in the convection zone. Hence a provision for the
external cleaning of convection tubes is made in the form of soot-blowers. They are
retractable motor-operated soot-blowers. They are arranged in 2 rows with 4 blowers in
each row and additional 1 row was provided in 2010 T&I for new convection zone.
Procurement of soot blowers for this zone is in progress. Soot blowers can be operated from
the grade level at the bottom of the furnace. Pressure gauges are provided on the inlet and
outlet of each pass in the convection zone. The pressure drop across each pass is a measure
of coke formation in the tubes. Temperature indicators (11-TI-302, 307, 312, and 317) are
provided on outlet of the convection zone to measure the temperature gain in this zone.
The convection zone has a single row (8 tubes) of steam coil in which saturated MP steam
(@10.5 kg/cm2 g.) generated in the unit gets superheated (~ to 350 °C). This superheated
steam is used as stripping steam in Atmospheric Distillation Column and Product Side
Strippers. The material of construction of these tubes is carbon steel. Pressure gauges, 11-
PG-323 & 11-PG-324 and temperature gauges 11-TG-301 & 11-TG-324 are provided on
the inlet and outlet of the coil respectively. Temperature indicator 11-TI-324 is provided to
indicate the superheated steam outlet temperature on the DCS panel. The superheated steam
coil is provided with 2 safety valves 11-PSV-301 & 11-PSV-302. One PSV is kept
bypassed in lock-open position, while the other is kept bypassed in lock-close position. The
vent in the steam line is routed to the Atmosphere through a silencer. The temperature of
the superheated steam is controlled by the 11-TRC-303, by injecting BFW through 11-TV-
303. Temperature can also be controlled by allowing more superheated steam into the LP
steam header (by operating the MP steam to LP steam globe valve at the grade level near
the 12-F-01 FD fan).
The coils come out from the bottom of the convection zone, and enter the radiation zone.
Radiation zone is the combustion chamber which is the cylindrical casing of the furnace,
lined with refractory materials and ceramic fibres. In this zone, heat is primarily transferred
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
by radiation from the flame and hot combustion products. The radiation zone Coils have
vertical tubes arranged concentric to the casing. Each pass has 22 tubes each of 19090mm
(weld to weld). These tubes are 6” NB Sch 40 type. Each pass has provision to monitor skin
temperatures at three different levels in the furnace. They are used to monitor the condition
in the furnace and also give an indication of hotspots in the furnace. There is also a
provision of temperature indicators in the firebox near the floor level.
After gaining heat in the radiation zone, the outlets of the four passes combine and enter the
Atmospheric Distillation Column through the 24” transfer line. The outlet temperature of
each pass is measured by 11-TI-306, 311, 316, and 321. The common outlet transfer line
temperature is measured by the 11-TI-322 and is controlled and recorded by the COT (coil
outlet temperature) 11-TRC-301. The control is achieved by varying the quantity of fuel to
the furnace. There is an alarm for high transfer line temperature as 11-TAH-133.
6.1.6.2 Fuel System

11-F-01 is a dual fired furnace i.e., either fuel oil or fuel gas or both can be used. The
atmospheric heater has a total of 12 burners. Of late, 3 burners (No. 2, No. 5 & No. 8) have
been dedicated to utilize off gases from the vacuum distillation column’s hot well drum as
the burning fuel. During 2010 T&I all the burners were replaced with 20 new burners
ZEECO make (16 are combined firing and 4 are hot well off gas burners).
a) Fuel Gas System

Fuel gas is supplied to the unit from the Battery Limit in an 8” header. This is further
branched into a 6” header to the Atmospheric heater. This FG line is steam traced to avoid
condensation of heavier components, as carry over of liquid droplets of Hydrocarbon to the
burner must be avoided.
FG to main burners passes through a mass flow meter (F1315) and shutdown valve 11-
SDV-303. This SDV is connected to interlock logic. 11-FR/FQ-308 indicates FG flow in
DCS room. It is provided with FAL and FAH. A local PG and a TG are provided to
indicate pressure and temperature at field. 11-PI-308 indicates FG pressure in the DCS
room. A low pressure alarm 11-PAL-303 is also provided. Fuel gas pressure low trip is set
at 0.2 kg/cm 2g.
In case the fuel gas pressure goes below the trip value, only 11-SDV-303 will get closed. If
fuel gas tip pressure falls below the set value, chances of flame failure and subsequent
accumulation of un-burnt hydrocarbons in the firebox is possible. This can lead to the
possibility of explosion or back fire in the heater. Hence the provision of “FG pressure
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
low” trip was provided. There is a provision to cascade the fuel gas pressure to the 11-F-01
COT, 11-TRC-301 through a selector switch on the auxiliary panel on the DCS panel. A 2”
FG tapping upstream of 11-SDV-303 has been branched off for pilot burners. The pilot gas
pressure is normally adjusted manually and is maintained at a pressure of 0.7 kg/cm2 g. In
case of low pilot gas pressure, 11-PAL-302 is provided to actuate an alarm. Low pilot gas
pressure will alert the operator when pilot gas pressure falls.
b) Fuel Oil System

Fuel oil is supplied to the unit from the Battery Limit in a 3" header. This is further
branched into a 3” header to the Atmospheric heater. FO line is steam traced to maintain
temperature and avoid congealing. Mass flow recorder and integrator 11-FR/FQ-305 are
provided on main FO supply line and 11-FR/FQ-306 is provided on the main FO return line
from heater. Since this is a closed circuit through which FO circulation is maintained, the
net consumption of fuel oil is measured as the difference between FI-305 and FI-306.
Shutdown valves 11-SDV-301 A/B are provided on the FO supply and return headers
respectively. Local PG’s and TG’s are provided on the supply line to show pressure and
temperature of FO supply. 11-PRC-301 indicates the pressure of fuel oil on the DCS panel.
Pressure is maintained by 11-PRC-301, which regulates 11-PV-301 on the fuel oil supply
line. There is a provision to cascade the fuel oil pressure 11-PRC-301 to the 11-F-01 COT,
11-TRC-301 through selector switch, on the auxiliary panel.
A low-pressure trip alarm has been provided on supply line. Actuation of this alarm shuts
11-SDV-301 A/B and cuts off only the fuel oil firing in the Furnace. Since FO is normally a
thick heavy liquid, it needs to be always maintained in circulating state. If it is left stagnant
and unused in burners and piping, it can get congealed despite the fact that tracing steam of
the FO circuit is on. Circulation in heater area (FO piping forming a closed circuit across all
passes called fuel oil ring) is maintained even when no fuel oil burner is in use. A ratio of
2:1 FO supply to return is normally maintained to obtain a good control on firing and
prevent congealing of FO system. FO is drawn by individual burners through ¾” lines from
header and balance quantity is sent to the return line. When there is no need of FO firing in
the heater, circulation can be maintained. Purge steam connections are provided on each oil
burner. FO burners are to be kept steam purged when idle.
When FO is fired, it is atomised or sprayed as a fine mist for realising complete

combustion. The spraying of FO is done by de-superheated MP steam in FO burners.
Atomising steam is supplied to heater through a 4” header. The differential pressure
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
controller 11-DPIC-301 controls the atomising steam pressure, taking pressure signal from
FO supply and MP steam simultaneously. Atomising steam pressure is maintained about
2.0 kg/cm2 above the FO pressure. Atomising steam flow is recorded by 11-FR-307. Local
PG and TG are also provided on this line.2” flushing oil connection is provided on FO
supply line up stream CBD/OWS drain is provided on FO return line. These provisions are
to flush the line within Battery Limit during heater shut down. When furnace operates on
combination fuel-either Fuel Gas operates on PIC and Fuel Oil on PIC/TIC cascade or Fuel
Oil operates on PIC and Fuel Gas on PIC/TIC cascade mode. Selector switch is used to
select only one fuel for COT control by cascading.
c) Off Gas System

In earlier mode of operations, the off gases from the vacuum column hot well drum used to
be released to atmosphere through a vent. Later, an 8” provision was given for serving 3
burners on atmospheric heater, during 2010 T&I number of burners were increased to 4
ZEECO burners.
6.1.6.3 Air Preheating System

11-F-01 is balanced draft furnace. Both the convection and radiation sections are used for
heating crude. The combustion chamber houses the radiation section of tubes. The
convection section provided at the top of radiation section serves to increase the thermal
efficiency of the furnace by utilizing further heat from the flue gas. Tubes are arranged
vertically in the radiation zone and horizontally in the convection zone.
The following are the major parts in the Air Preheating system of the furnace
a) Forced Draft Fan

This is a centrifugal type fan. It supplies the air required for combustion in the balanced and
forced draft operation of the furnace. The inlet of this fan is provided with variable guide
vanes to regulate the flow of air. The guide vanes are journalled in the fan shaft vicinity
with a spherical pivot in a hub ring with cylindrical drilling and at the outside with
cylindrical pivots. Sealing discs below and above the bearings keep the dirt away.
The guide vanes have a regulator which is actuated by a swivel-stem actuator. The actuator
is steered pneumatically and is designed in such a way that, in case of air failure, the guide
vane regulator will move to open position by means of an installed spring. There is also a
provision to operate the inlet guide vane regulator manually by means of a hand wheel
which is located at the bottom of the actuator. The duct connection on the suction and
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
discharge sides of the fan is effected via a soft material compensator, which prevents the
transfer of external forces, like the forces due to thermal expansion, to the fan. The
discharge side of the fan has a multi-vane damper in between the fan casing and soft
material compensator, which isolates the discharge duct of the fan. The fan shaft with the
impeller and guide vanes is seated in two oil-lubricated sliding bearings. The fixed bearing
is located on the motor-side and the mobile bearing is situated opposite to it.
These bearings are lubricated by means of rotating lubrication rings and have intermediary
chamber. The oil level is seen in the sight glass and the oil operating temperature should not
exceed 80 °C and brief peak temperatures up to 90 °C are sealed off by a labyrinth seal. The
fans are driven by polyphase induction motors via couplings, which are directly coupled to
the fan. The fans are dynamically balanced. This warrants a running performance which is
free of any vibration. In case of ID fans, an uneven caking on the impeller will create
unsteadiness of run.
b) Induced Draft Fan

This is a centrifugal type fan. It controls the flue gas flow from the furnace by the variable
inlet guide vane mechanism same as mentioned above. There is a provision to indicate the
wide open position of the suction vanes in the DCS room on the auxiliary panel.
c) Recuperative type Air Preheater

This is an assembly of rectangular cast tubes that have fins on either side at the hot end and
fins only on the flue side at the cold end. The tube lengths, size and pitch will vary as per
requirements in individual cases. Using the tubes as building block, air preheater of any
size can be made to suit heat duty and pressure drop. The entire tube assembly is built
inside a steel frame made by beams and fully insulated casings. Flue gas and air terminal
connections are made of rectangular flanges formed from rolled steel sections.
These flanges form an integral part of the air preheater frame and are sturdy and are capable
of carrying considerable external loads. The entire air preheater assembly forms part of the
ducting system. Because of the orientation of flat surfaces it is essential that flue gas flow is
always in the vertical direction.
The flue gas will be on single pass, vertically down and air can have a number of passes
depending upon allowable pressure drops. The pressure drop allowable is decided on a
case-to-case basis. Generally it is 50-100 mm WC on the air side and slightly lower side on
the flue-gas side. The tube is made of two half sections, cast independently and then bolted
together. To prevent air leakage in the longitudinal direction, two grooves have been
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
provided on the flanges on the either side. Asbestos ropes are placed in the grooves before
bolting. The flanges provide the necessary gap for the flue gas passage. The flanges also
have peripheral groves on all four sides to accommodate rope to ensure air tightness
between adjacent tubes.
d) Drop-Out Doors
Drop-Out Doors are provided to supply combustion air in case of Natural Draft operation or
in case of emergency. The drop-out doors are double-flap isolator type, actuated
pneumatically by double-acting power cylinders and 4-way solenoid valves. The following
provisions are also made to operate them in case of Instrument air failure as extra safety
devices.
• Weight loading to open the DOD’s by the force of gravity.
• An air accumulator tank of sufficient capacity to operate the DOD’s.
Explosion proof limit switches are provided to indicate fully open and fully close positions
by means of indication lamps provided on the auxiliary panel in the control room. Switches
are provided in the control room to open and close each drop out door. The open or close
position of the DOD’s is indicated by the lamps provided on the auxiliary panel. These are
actuated by the limit switches.
e) Stack Damper:
Stack Damper is provided to prevent the flue gases from escaping directly without heat
exchange in the Air-Preheater. It also helps in the direct escape of flue gases when the
furnace is in Forced Draft or Natural Draft operation. The stack damper operates either full
open or full close. During 2010 T&I the stack damper was replaced with full shut off
damper with controlled damper operation. The new stack Damper is a multi-Louver
isolation and control damper with pneumatic plus manual control. The damper is provided
with counter weight to the FAIL SAFE OPEN position.
The damper is designed as FAIL OPEN position and it shall attain FAIL OPEN position on
failure of:
1. Supply air failure with supply air pressure switch set at 2.5 Kg/Cm2 falling.
2. Electric Supply to the Control Panel by auto operation of solenoid valve.
3. The Signal failure i.e. signals pressure falling below 0.2 Kg/Cm2.
The damper shall open with decrease in signal air pressure and accordingly close with
increase in signal air pressure. It is provided with Pneumatic linear actuators for operation
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
and control of the damper. The damper is also provided with Winch and cable for manual
operation of the stack damper from grade. In auto operation, disconnect the winch by either
removing shackles from winch arm at damper level or by disengaging the worm wheel and
shaft provided on the winch machine by rotating the hand wheel in anti-clockwise direction
at grade level. The worm shaft can be locked by the lever below hand wheel in clockwise
direction.
are provided in the control room to open and close the Stack Damper. The open or close
position of the Stack Damper is indicated by the lamps provided on the auxiliary panel.
These are actuated by the limit switches. There is a provision to open the Stack Damper
manually from the field by winch operation in case of emergencies. Air is required for the
combustion of fuels in a furnace. It is supplied by the FD fan (11-FM-01). The air flow is
regulated by adjusting the variable inlet guide vane mechanism to maintain proper dP
across the furnace and for maintaining the required excess air in the flue gas. About 15 to
20% excess air in case of fuel oil and 10 to 15% in case of fuel gas is found to give
satisfactory performance of the furnace. An oxygen analyzer (AR-1801) is also provided at
the outlet of the flue gas to monitor the excess air regularly.
Air pre-heating system helps in recovering the sensible heat from the flue gas further, after
the furnace convection zone, which is utilized to preheat the combustion air. This increases
the fuel economy and also the heater efficiency approximately by 10 %. There are separate
Air Preheating systems (APH) for Atmos and Vacuum furnaces.
Forced Draft fan (11-FM-01) draws atmospheric air and forces it through the APH. Induced
Draft fan (11-FM-02) draws the flue gas through the APH, and returns it to the stack above
the stack damper after recovering heat from it. Care should be taken to maintain the return
temperature of flue gas above its dew point (typically 175 °C) to avoid condensation which
would otherwise result in acid corrosion. The design of the furnaces in CDU-II gives
immense flexibility in their operation. There are 3 modes of operation as given under.
2.5% O2 on AR-1801 equals to 10-15% of excess air
a) Balanced Draft operation

In this mode of operation, the FD and ID fans both function simultaneously and help in
recovering the heat from the flue gas. Flue gas is drawn by the ID fan through a duct
connection that is taken from the castable below the Stack Damper. This duct is lined with
refractory. Pressure and temperature gauges are provided to give local indication of the
pressure and temperature of flue gas entering the air pre-heater. PI and TI are also provided
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
to give the indication in the control room. A winch operated shut-off blade hand controller
is provided in the duct to isolate the flue gas duct. Hot flue gas enters the APH at the top
and exchanges the heat with combustion air. Flue gas exiting the APH is routed to the ID
fan suction. This fan draws the flue gas and conveys them back to the stack above the stack
damper through a duct. 11-TAL-803 at the ID fan inlet provision is there to give an alarm
when the flue gas temperature falls below the dew point temperature to avoid corrosion. In
case of low temperature, the air flow through the APH can be adjusted so that the
temperature can be increased. In case there is an abnormal rise in temperature of flue gas
leaving the APH, TAH will give an alarm. 11-PAH-808 is also provided to give an alarm in
case of high furnace box pressure in the arch zone.
Combustion air under pressure from the FD fan is ducted through the bottom of the APH.
PG and TG give the local indication of the pressure and temperature of the cold air entering
the APH and a PI gives the cold air pressure indication in the control room. A PAL (11-
PAL-806) is provided on the discharge of the FD fan to indicate malfunction of FD fan
controls or tripping of the fan. After exchange of heat with the flue gas, hot air is sent into
the hot air distribution duct running around the circumference of the heater. This duct is
provided with a TG and PG to give a local indication of the temperature and pressure of the
hot air. There is also a TI and a PI to give an indication in the control room. A TAH (11-
TAH-801) is provided to give a high temperature alarm. This hot air duct branches into the
plenum chamber of the furnace, where the burners are mounted. Hot air for combustion
enters the burners and is used for firing with corresponding saving in fuel.
b) Forced Draft
In this mode of operation, the FD fan of the furnace will be running and the ID fan is
stopped and the stack damper is kept open. Flue gas escapes to the Atmosphere directly
without preheating the combustion air. This is done mainly when isolation of the APH or
ID fan is required to carry out maintenance activities.
c) Natural Draft
There is also a provision to operate the furnaces in natural draft, wherein there is no
requirement of FD and ID fans. There is a provision of 5 Drop Out Doors (DOD’s) on the
combustion air duct of 11-F-01.To operate the furnace in Natural Draft, DOD’s and stack
damper are opened. Atmospheric air goes inside the furnace by the action of the draft in the
furnace and aids in combustion. The flue gas escapes directly through the Stack Damper
without preheating the combustion air.
Standing Instruction on APH water washing (SI: 36):

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
1. STANDING INSTRUCTIONS:
1.1. APH water washing is to be carried out after meeting all the requirements specified under
S.no 2.
1.2. Follow the procedure specified under S.no 3 and also additional precautions mentioned in
the PDI by the unit manager.
2. Requirements for APH water washing :

2.1. Technical Clearance
2.2. PDI instructions from unit manager
2.3. Clearance from ETP
2.4. Clearance from power plant for service water usage
2.5. Sufficient caustic inventory in the unit
2.6. LP steam availability for APH hot water wash
2.7. Utility air hose arrangement up to APH bottom man way for purging.
2.8. Clearance from YSF
2.9. Maintenance help for opening and closing of APH bottom & top man ways
2.10. Universal PH indicator for checking effluent water PH in field
3. Procedure to be followed during APH water washing:

1. APH water washing to be carried out based on flue gas side pressure drop and glass APH
approach/APH outlet temperature of flue gas. Technical will organize for a pressure drop
survey and recommend APH cleaning if required. It may be noted that carrying out APH
water wash without necessity may expose the metal components more frequently to thermal
shocks and exposure to lower PH water, which may cause corrosion.
2. After obtaining Technical recommendation, take clearance from YSF, ETP-I and PP-II for
APH water washing (one day in advance).
3. After ensuring all the items under S.no 6 are met, Heater operation to be changed to forced
draft, for that wide open heater Stack damper at the rate of 5% increment, observe heater
fire box, if required adjust fires.
4. Start reducing ID fan loading slowly to Zero Percent and stop ID fan.
5. Before start of water wash, APH to be completely taken out of service and isolated so that
there is no flue gas or air ingression into the APH. Close ID fan suction damper.
6. Flue gas ingression during APH water washing can make the water more acidic (due to Sox
in flue gas) which will result in excessive corrosion of the APH components.
7. Check the condition of APH drain line & unplug the same (if necessary).
8. Open APH bottom man way to prevent water flow along with solid particles in to ID fan
duct during water washing (flue gas will not come out during opening of bottom man way,
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
as draught is from bottom to top, same thing can be checked by placing small piece cotton
at the APH bottom man way, the cotton piece will be sucked in to the APH due to the
draught present).
9. The APH bottom man way can be used for purging of APH with utility air for displacing
the flue gas contained in the APH. Barricading red tape to be tied to the APH bottom man
way, so that no person should enter in to APH.
10. Arrange utility air hose connection up to APH bottom man way.
11. After ensuring that the heater arch pressures are not close to trip value, start APH air
purging with Utility air at slow rate, from bottom man way to top, for about 4 hrs. During
this process around 80% of the flue gases contained in the APH will be displaced through
stack.
12. After 4hrs of air purging, stop air purging, close APH Flue gas inlet damper, open APH top
man way and start air purging with Utility air at slow rate, from bottom man way to top
man way for about 4 hrs.
13. During air purging, it is to be ensured that no person is exposed to the vented air, which
may be high in Sox content.
14. APH to be cooled up to 80-90 0C before start of water washing. After reaching APH
temperature to 80-90 0C, take clearance from YSF, ETP-I and power plant for APH water
washing.
15. Start APH water washing with hot water at 80-90 0C from the top section (Removal of
deposits is more effective at higher temperature). LP Steam is to be introduced along with
wash water for achieving high temperature. The globe valves available on steam lines shall
be used to control steam flow to wash water.
16. Immediately after start of water wash, start Caustic injection into APH O/L water to
neutralize the OWS effluent water (to maintain a PH of 7.0 – 8.0) for protecting biological
treatment step at ETP.
17. During APH water wash, effluent water sample to be physically checked for color and two
samples(one immediately after APH outlet and other after caustic injection) to be sent to
lab as follows
o Immediately after start of water wash
o At the end of water wash (after noting down field result)
18. In between during the progress of water washing, APH effluent water PH to be checked in
field every 2 hours.
19. After 10-12hrs, the APH hot water washing to be shifted from top to bottom section and
APH effluent water PH to be checked in field every 2 hours.
20. APH water wash is to be continued till 2 consecutive sets of water samples are reported to
have PH in the range of 6.5-7.0. After confirmation in field the last sample of APH effluent
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
water to be sent to lab for testing final PH. (Estimated duration of water washing is
typically 24-48hrs, depending on the size of the APH).
21. After stopping water wash, APH is to be purged with Utility air from APH bottom to top, to
dry out the surface of glass tubes and finned plates before allowing flue gas entry.
22. After completion of air purging, close APH bottom & top man ways.
23. After ensuring the APH is dry, open APH flue gas inlet and ID fan suction dampers and
start ID fan at 2%(minimum) loading.
24. Slowly load ID fan and ensure steady and slow raise GAPH Inlet Temp (It should not cross
design temperature) and simultaneously divert combustion Air to APH.
25. While taking APH into service the APH air bypass damper to be adjusted in such a way
that the tube skin temperature in the cast APH section should be at least 10 0C more than
the dew point of flue gases.( dew point of flue gas is 160 0C).
6.1.6.4 Trip and Interlock System:
Trip Values for 11-F-01
Trip Unit Value

FD fan discharge pressure (low) mm Aq. +15
ID fan suction pressure (High) mm Aq. -45
Furnace pressure (high) mm Aq. +2.95
Fuel oil pressure (low) Kg/cm2g. +2.77
Fuel gas pressure (low) Kg/cm2g. 0.20
Furnace pass flow (low) m3/h 42
The following is the description of the consequences arising from the above conditions
given that all the trips are in auto interlock mode.
FD fan discharge pressure (low): The activation of this trip alarm (Annunciator alarm)
may be due to the tripping of FD fan or due to the faulty indication of the combustion air
discharge pressure. This results in the following
a) DOD’s gets opened
b) Stack Damper gets opened and ID fan trips
ID fan suction pressure (high): The activation of this trip alarm (Annunciator alarm) may
be due to the tripping of ID fan or due to the faulty indication of the flue gas suction
pressure. This results in the following
a) Stack Damper gets opened
Furnace pressure (high): The activation of this trip alarm (Annunciator alarm) results in
the following
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
a) Stack Damper gets opened and ID fan trips

b) DOD’s get opened and FD fan trips
If this alarm does not get reset within 30 seconds of its activation, the fuels to the furnace
get cut off (SDV’s get closed)
Fuel oil pressure (low): The activation of this trip alarm (Annunciator alarm) results in the
following
a) Fuel oil SDV’s (supply & return) close if the pressure low alarm does not get reset within
9 seconds.
Fuel gas pressure (low): The activation of this trip alarm (Annunciator alarm) results in
the following
a) Fuel gas SDV closes immediately.
Furnace pass flow (low): The activation of this trip alarm (Annunciator alarm) results in
the following
a) Fuels getting cut-off to the furnace (SDV’s get closed) immediately
b) Stack Damper opens, ID fan trips, FD fan also trips and DOD’s open
The Operator Interface in the DCS room is provided with a set of switches, push buttons
and indications to enable the smooth and safe operation of the plant. The Annunciator panel
has a provision of alarms which alert the operator when unsafe operating conditions arise.
There is a provision to operate (open / close) the DOD’s and Stack Damper from the
Annunciator panel. There is also a provision of lamp indications to indicate the open /close
conditions of the DOD’s and Stack Damper (their activation results only when the limit
switch corresponding to the open / close position is engaged as the case may be). There is a
software alarm provision to indicate the limit switch (open / close) activation on the DCS
panel. There is also a provision of Emergency Shut-Down push buttons to ensure the safety
of the personnel and also the equipment.
The following trip switches are provided on 11-F-01
DOD – SD Check Trip Switch: This trip, when in auto mode, opens stack damper under
the following conditions:
a) Furnace pressure high (Annunciator alarm)
b) FD fan trips / FD fan discharge pressure low (Annunciator alarm)
c) ID fan trips
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
d) Both fuel oil and fuel gas pressure low (Annunciator alarm)
e) Pass flow low-low
f) Activation of the DOD-SD ESD
FD Fan Trip Switch: This trip, when in auto mode, opens the DOD’s under the following
conditions
c) FD fan motor amps low (Annunciator alarm)
d) Any of the DOD’s is not closed completely (close limit switch deactivation)
f) Activation of the DOD-SD ESD
ID Fan Trip Switch: This trip, when in auto mode, opens the SD under the following
conditions
c) ID fan motor amps low / ID fan suction pressure high (Annunciator alarm)
e) Stack Damper is not closed completely (close limit switch deactivation)
f) Pass flow low-low
g) Activation of the DOD-SD ESD
Fuel Oil Trip Switch: This trip, when in auto mode, closes the fuel oil supply and return
SDV’s under the following conditions
a) Fuel oil pressure low (Annunciator alarm)
b) Signal from any of the three timers (details of the timers are given below)
c) Activation of the Fuel-ESD
d) Pass flow low-low
Fuel Gas Trip Switch: This trip, when in auto mode, closes the fuel gas SDV under the
following conditions
a) Fuel gas pressure low (Annunciator alarm)
c) Activation of the Fuel-ESD
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Timers: Three timers are provided in the furnace trip circuit, which will start counting
when their respective alarms are activated. If the alarm is not brought back to normal value
within 30 seconds (as counted by the timer), the timer relay will activate the fuel oil and
fuel gas trips. If the alarm is brought back to normal value within 30 seconds (as counted by
the timer), the timer will get reset i.e., the timer indication will become zero.
a) Furnace Pressure High Timer: It gets activated when furnace pressure high alarm
comes on the annunciator panel and gets reset when the alarm is normalized. If the alarm
condition is not reset, the fuels to the furnace get cut-off (given the fuel trips are in auto
mode)
b) FD Fan Trip Timer: It gets activated when the FD fan trips. This should result in ID
fan tripping and DOD’s and Stack Damper opening with in 30 seconds or else fuels get cut-
off. Gets reset when FD fan is running and all the DODs close or the FD fan trip is
bypassed.
c) ID Fan Trip Timer: It gets activated when the ID fan trips. This trip should result in
the opening of Stack Damper within 30 seconds or else fuels get cut-off. Gets reset when
ID fan is running and the stack damper is completely closed or the ID fan trip is bypassed
Note: There is a provision to set the timer to any time duration between 0-60 seconds
Interlock system: Interlocks are provided to ensure safe operation of the equipment. They
ensure that corrective action is taken automatically whenever unsafe operating conditions
arise due to process upsets, mal-operation of Instruments or equipment etc. But the
interlocks can be made ineffective / inactive by bypassing the trip switches provided on the
DCS panel.
Interlocks on furnace operation: The following interlocks ensure the safe operation of
furnace. The following description is valid only when the trips described above are in auto-
interlock mode.
Note: All the references to the ‘open’ and ‘close’ positions of DOD’s and Stack Damper
mean that the open or close limit switches are engaged and the close indication is active on
the Annunciator panel
a) Drop out doors opening or closing
b) Stack damper opening or closing
c) FD fan starting or stopping
d) ID fan starting or stopping
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
e) Fuel SDV’s opening or closing

f) Low Pass Flow
Interlock 1: DOD Operation

i) When the furnace is in natural draft mode, all the DOD’s have to be in fully open
position. If any one DOD leaves the fully open position (either by operation or by
instrumentation malfunction), then the fuel to the furnace will cut off.
ii) When the furnace is in forced draft mode, DOD’s are in fully closed position and if
any of the DOD’s is not in fully closed position, FD fan is tripped. In case the FD fan is
tripped, the DOD’s open automatically.
iii) When the furnace is in balanced draft mode, DOD’s are in fully closed position. They
get opened automatically if the
• FD fan trips
• Arch pressure high gets activated
• ID fan trips and Stack Dampers gets opened
Interlock 2: Stack Damper Operation

• When the furnace is in natural draft mode, the SD has to be in fully open position. If the SD
leaves this position, the fuel to the furnace is cut off.
• When the furnace is in forced draft mode, the SD has to be in fully open position. If the SD
• When the furnace is in the balanced draft mode, the SD has to be in fully closed position. If it
leaves this position, the ID fan is tripped. The SD gets opened if
• ID fan gets tripped
• Arch pressure high gets activated
• FD fan trips /any DOD leaves fully closed position
• Fuel oil / fuel gas SDV’s both get closed (command)
• Activation of DOD-SD ESD
Interlock 3: FD Fan Operation

• When the furnace is in natural draft mode, the FD cannot run as long as the DODs are in
open position.
• When the furnace is in forced draft mode, FD fan gets tripped if any DOD leaves fully closed
position or the furnace pressure is too high.
• When the furnace is in the balanced draft mode, the FD gets tripped if any DOD leaves fully
closed position.
• FD fan cannot run if furnace pressure high alarm is active
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Interlock 4: ID Fan Operation

i) When the furnace is in natural draft mode, the ID cannot run if FD fan is not running.
ii) When the furnace is in forced draft mode, only FD fan runs and ID fan is stop condition.
iii) When the furnace is in the balanced draft mode, the ID fan gets tripped if
• SD is not fully closed
• any DOD leaves fully closed position (FD trips, hence SD opens)
• FD fan is tripped
• Furnace pressure is high
Interlock 5: Fuel SDV’s Operation

The fuel SDV’s get closed by operating the ESD on the auxiliary panel. Individual ESD’s
are also provided for fuel oil and fuel gas. The fuel SDV’s get opened only after the
individual “SDV Reset” push button on the auxiliary panel is operated. The following are
the interlocks on the Fuel SDVs
i) When the furnace is in natural draft mode, fuel is cut off if any DOD or stack damper leaves
the fully open position.
ii) When the furnace is in forced draft mode, fuel is cut off if stack damper leaves fully open
position / FD fan trips.
iii) When the furnace is in the balanced draft mode, the fuel is cut off in case any of the three
timers gets activated.
Interlock 6: Low Flow in the Furnace Passes

This interlock shuts down the fuel SDV’s to the furnace whenever the furnace pass flow in
any coil is low. The trip value set for the low pass flow is 42 m3/hr.
6.1.6.5 COKE FORMATION ON HEATER TUBES

Coke formation on heater tube surfaces can be attributed to various factors. Here are the
most prominent ones:
Heater Charge Properties
Sodium Content – causes rapid fouling
Asphaltene Content – increases fouling
Calcium Content
Flow Improvers- potential increase in fouling
Crude Properties –API & viscosity
Operating Parameters
High Heater Outlet Temperatures
Process Velocity
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Low Mass Velocity, Increases Film Temperature

Loss of Velocity Steam
Low Cold Oil Velocity (target 6 ft/sec minimum)
Uneven Heat Distribution - “hot spots or cold spots in firebox”
Residence Time Above Cracking Threshold
Low Flow (Turndown) or Poor Flow Distribution
Feed Interruptions
Other Issues
Changes Made During Heater Revamp:
Change to Low NOx Burners
Fuel Heating Value Changes
Heavier API Crude Feed
Addition of Air Preheat
Change Size, Number, and/or Metallurgy
Fuel Contaminants- Tip Plugging
METHODS OF CLEANING HEATER TUBES OR DECOKING
Steam-Air Decoking (Steam & Air Burn)

Performed when heater is off-line
Heater box temperature is reduced/cooled
Mechanical (Pigging)
Performed when heater is off-line
Heater box temperature is cooled
On-Line Spalling
Performed while heater is in service
1 pass is taken out of service while other passes remain on-line
TYPES OF HEAVY OIL HEATERS

DECOKING
CRUDE VACUUM VISBREAKER DELAYED
OPTION
HEATER HEATER HEATER COKER
STEAM-AIR
YES YES YES YES
DECOKING
MECHANICAL
YES YES YES YES
PIGGING
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
SPALLING NA NA YES YES
Two of the most important decoking techniques are steam-air decoking and mechanical
pigging. They have been discussed in the following section:
1. Steam Air Decoking

When petroleum fractions are heated to high temperatures, a fraction of it gets decomposed
unavoidably over a period and accumulates itself as coke deposits inside the tube walls.
This coke layer results in increased pressure drop and increased tube metal skin
temperature, which may result in hot spots.
Steam Air Decoking (SAD†) of atmospheric heater tubes is done to remove coke deposit
from inside heater tubes with the help of steam and air. Removal of coke results in clean
heater tube internals and improves heater performance by better heat transfer to process,
fluid. SAD also achieves low pressure drop through heater tubes and reduces chances of hot
spot on heater tubes. Need for steam air decoking of heater tubes is indicated by increased
pressure drop and harder firing.
This dedicated SAD arrangement comprises decoking drum (11-V-05), piping and
instrumentation for plant air, service water and MP steam. MP steam connection to each
pass flow is provided to dislodge carbon deposit from inside the heater tubes. Local and
DCS panel mounted flow indications (11-FE-310 to 313) are provided on each steam
connection. Plant air is required to ignite the remaining coke fill deposit clinging on the
inner wall of tubes and achieve final cleaning. Local and DCS panel mounted flow
indications 11-FE-309 are provided on the main 4” plant air header. 11-FE-309 indicates
total plant air consumption during decoking operation.
Service water quench provision is given on 11-V-05 to quench the contents before letting
them to atmosphere. To carry out SAD, pass flow inlet and outlet of the furnace 11-F-01
are isolated from process network and connected by means of swing elbows with the
decoking network. Heater pass flow outlets are connected to the decoking pot 11-V-05.
While MP steam is introduced in the tubes it is fired from outside. Thermal shock caused
by the flame, cracks the coke scales inside the tubes and flowing steam dislodges them.
These coke particles are carried to 11-V-05 after being quenched in the decoking pot by
service water. When no more coke is removable as indicated by relatively clear colour of
the effluent, air along with steam is introduced into pass flow to blow out the coke inside
tube while firing is on in the heater. Oxygen burns coke at high temperature. Burning of the
coke is indicated by increased tube metal temp.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
PIGGING
Coke is removed from the heater tube by pumping a metal studded foam or plastic “pig” with
water and air. The metal studded “pig” rotates such that it scrapes the coke off the inside of
the heater tube.
Different size and abrasiveness “pigs”are used in the decoking process. “Pigs” are slightly
larger than the inside diameter of the heater tube.
Usually “pigs” are pumped through heater several times forward and backward until overall
differential pressure across the tube (inlet to outlet) is restored to its original “unfouled”
condition.
Typical decoking time is 18 to 24 hours per heater depending on setup time.
6.1.7 ATMOSPHERIC DISTILLATION COLUMN:

Crude oil after final heating in Atmospheric Heater is fed to the Atmospheric Distillation
Column. This Column has 40 valve type trays of SS410S material except the 37th to 40th
tray which are of SS316 material with monel lining. The column has a stripping section at
the bottom.
Description of entire column has been taken up zone wise.
1 Flash zone
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
2. Bottom section
3. Middle section
4. Overhead section
6.1.7.1 Flash Zone

Heated and partly vaporized crude oil enters the flash zone under the 7th tray. Hydrocarbon
vapours flash in this section and get liberated. Non-flashed liquid moves down which is
predominantly the bottom product called Reduced Crude Oil (RCO). Certain degree of over
flashing of crude is desirable for proper stabilization of RCO, and fractionation of gas oil
components.
Over-flashing is achieved by setting up COT at slightly higher temperature than what is
actually required. The required temperature of flash zone is 357 °C while that of feed is 360
°C. This over-flashed material mostly condenses at the 7th tray. The condensed liquid is
withdrawn from 7th tray and put back on the 6th tray. Overflash liquid travels down from 7th
tray to 1st tray. It strips off heavier components coming up from RCO stock collected at
column bottom which otherwise could move up and cause discolouration of Heavy Diesel
stream. Flow of overflashed liquid could be increased either by increasing the COT and
condensing more material on 7th tray or by reducing the Heavy Diesel draw-off rate.
However the second option will lead to less diesel yield and higher energy consumption
without any advantage. Too large flow of over flash liquid may result in the drop of bottom
temperature and lighter bottom product, i.e., RCO.
Over flash flow is indicated by 11- FI/ FR-402. This is a 6” line with a U-loop. 11-FE-402
is mounted in the liquid seal. This seal provides adequate liquid build up on upstream of FE
and ensures unflickering, steady flow through orifice. In addition, it provides some back
pressure which is required to prevent flashing just downstream of flow orifice due to
pressure drop.
MP steam is introduced in the column through 11-FRC-401, below tray 1 for stripping of
RCO. Stripping steam helps in removing lighter components from the heavier products by
reducing their partial pressures and vaporizing them without requiring additional heat.
Minimum 22 kg/h stripping stream per m3/h of RCO is to be used for effective stripping.
Hydrocarbon vapours liberated by flashing move upward along with steam in the column
for further mass transfer at the trays in the upper section. The Desalter pressure relief valve
and the Pre-flash Drum pressure relief valve discharges are connected to the flash zone.
6.1.7.2 Bottom Section

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Reduced Crude Oil (RCO) product is collected at the bottom of the column. The column
bottom level is indicated and controlled by 11-LRC-401. LRC-1401 goes to the ratio block
of vacuum heater. Manipulating the RCO flow to vacuum heater can do column bottom
level control. LRC is provided with software high / low level alarms. In Addition, 11-
LAL/LAH-401 are provided in DCS panel.11-TR-401 shows product RCO temperature.
RCO is pumped out from the bottom of the column at by RCO pumps 11-P-10 A/B to any
of the following destinations.
a) 10” line to Vacuum Furnace (12-F-01) as RCO feed. During normal operation, the RCO
flow (FX2100) is regulated by the column bottom level control. This total RCO flow in-
turn gives the set value to the vacuum furnace pass flow controllers.
b) Swing elbow has been provided at the inlet and outlet of the heater passes, therefore steam
and air decoking can be done either way.
c) There is a provision to route RCO in an 8” line to 12-E-06 A/B (i.e., VR lines) for
utilization of these exchangers during light crude processing. After exchanging the heat in
12-E-06 A/B, RCO goes to the vacuum furnace.
d) To SR manifold during start-up. This is a start-up line.
6.1.7.3 Middle Section

Middle section of the column has product withdrawal and circulating reflux network. In
order to maximize heat recovery and balance the column loading for maintaining proper
temperature profile across the column, three circulating refluxes (CR) are considered viz.,
Top Pump Around, Kerosene CR and Heavy Diesel CR. These circulating refluxes are
drawn from their draw-off seal boxes and are routed to preheat trains for recovery before
entering back to the column again.
a) Top Pump Around (TPA)

TPA is drawn from the 37th tray by the pump 11-P-09 A/B and is cooled by routing it
through 11-E-04 A/B. It enters the Atmospheric Column on the 39th tray. 11-TI-411 and 11-
TI-414 indicate its draw-off and return temperature respectively. TPA flow is indicated and
controlled by 11-FRC-406. The return temperature is to be maintained above 100 °C to
prevent the condensation of water vapour which may result in acid corrosion of the column
top.
b) Middle Pump Around (Kerosene Circulating Reflux)

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Kerosene CR is drawn from 20th tray by the pump 11-P-08 A/B and is cooled by routing it
through 11-E-09 and 11-E-25 in parallel and then through 11-E-11 (BH case). It is then
boosted by 11-P-08 C/D. In BH operation mode, it flows through 12-E-01 A/B/C and then
enters the Atmospheric Column on 22nd tray. 11-TI-403 and 11-TI-413 indicate its draw-off
and return temperature respectively. Kero CR flow is indicated and controlled by 11-FRC-
405. There is a pressure indication 11-PI-432 at the 20th tray in the Kerosene zone. There is
a provision to route hot Kerosene to the unit flushing oil header from the discharge of 11-P-
08 A/B.
c) Bottom Pump Around (Heavy Diesel (HD) Circulating Reflux)

HD is drawn from the 12th tray by pumps 11-P-07 C/D and is cooled by passing it through
11-E-15 A/B and 11-E-13. The seal flushing facility to these CR pumps is provided from
the outlet of 11-E-23, Diesel product cooler. The CR return enters the Atmospheric Column
on the 14th tray. 11-TI-402 and 11-TI-412 indicate its draw-off and return temperature
respectively. HD CR flow is indicated and controlled by 11-FRC-404.
Product Draw-Off
Heavy Naphtha (HN), Kerosene, and HD products flow by gravity from the 28th, 20th and
12th tray respectively to strippers 11-C-02, 03 and 04 under respective level control of
strippers (viz., 11-LIC-404, 403, 402 respectively). This draw-off from the draw-off boxes
includes the respective CR for Kerosene and Diesel cases. Vapour return lines from HN,
Kerosene, and HD strippers back to the fractionator column are provided just two tray
above the draw-off for HN and two trays above the draw-off for Kerosene, and HD. 11-TI-
403, 404, and 405 indicate the draw-off temperatures of HD, Kerosene and HN respectively
from the column in the in DCS panel. 11-TI-407, 408, 409 indicate the vapour return
temperature from HD, Kerosene and HN strippers respectively. 11-TI-206 indicates the
temperature at the 30th tray. An Elevation of 3m for HN and Kerosene and 4m for HD, from
draw off nozzle to each level control valve of the stripper has been provided to exert back
pressure necessary to prevent flashing just downstream of control valve. This also prevents
two phase flow in draw off piping.
6.1.7.4 Over Head Section

The overhead vapours of Atmospheric Column pass through the overhead condensers 11-E-
17 A to H (in 4 banks) and are totally condensed. The condensate gets collected in the
Overhead Naphtha Accumulator (reflux drum) 11-V-01. Any of this overhead condenser
banks can be isolated for maintenance. There is also a provision of service water connection
at the inlet of each condenser to occasionally wash away the deposits of ammonium salts in
the tubes.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Top pressure of Atmospheric Column is maintained by 11-PRC-409 A/B which

Manipulates 11-PV-409A on outgoing uncondensed gases from 11-V-01 and 11-PV-409B
on incoming fuel gas. Since isolation valve is provided in overhead line between
Atmospheric Column and overhead Naphtha accumulator, 11-PSV-401 A/B/C (set at 4.8
kg/cm2 g.) are provided at the top of column. Snuffing steam provision is given on the PSV
outlet header to quench the vapours in case of emergency or as a safety precaution to be
opened during thunder storms.
Condensed Hydrocarbons are allowed to settle in reflux drum where steam condensate
(water) settles in vessel boot and then flows to the Sour Water Stripper Unit on its pressure.
11-TI-410 indicates the temperature of the reflux drum in DCS panel. 11-PSV-403 on 11-
V-01 has also been provided for the safety of the Atmospheric Column top PSVs.
Uncondensed gases from 11-V-01 are routed to flare through 11-PV-409A and FX- 801
indicates the mass flow rate of the flare gases.
Water-Naphtha interface controller 11-LDIC-406 controls level of water in the boot and
operates 11-LV-406 on 3” sour water line. LIC-1406 has software high / low level alarm
(11-LAH/LAL-406) in DCS panel. 11-FI/FR-450 shows sour water flow in DCS panel
when Atmos sour water is routed to 11-V-04.
Accumulated hydrocarbon in 11-V-01 is pumped back to Atmospheric Distillation Column

as top reflux on the 40th tray by 11-P-06 A/B. Reflux flow is controlled by 11-FRC-403
which is cascaded to the Atmospheric Column top temperature controller 11-TRC-403.
Excess quantity of Naphtha in Reflux drum is pumped by 11-P-06 A/B to the Naphtha
Stabiliser as feed through a 6” line. The flow of Unstabilised Naphtha to the Stabiliser is
controlled by 11-FRC-503 which is cascaded to the Naphtha Accumulator (11-V-01) level
controller 11-LRC-405. LIC-1405 has software high / low level alarms (11-LAH/LAL-
405).
There is a ¾” provision for injection of Neutraliser and Corrosion Inhibitor on the

Atmospheric Distillation Column overhead vapour line and the reflux line to maintain the
desired pH.
Product Strippers
There are three side strippers for stripping out side draw-off products from Atmospheric
Column viz., Heavy Naphtha Stripper, Kerosene Stripper, and Heavy Diesel Stripper. The
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
flash point and the IBP of the distillate streams are controlled adjusting the stripping steam
flow in each of the strippers.
i) Heavy Naphtha Stripper (11-C-02)

Six valve type trays (SS410S) are provided in HN stripper of 1200 mm diameter. HN is
admitted on 6th tray under level control 11-LIC-404. The HN stripper is provided with
software low level alarm 11-LAL-404. Minimum 1.5m elevation is provided between 11-
LV-404 and feed in nozzle to provide back pressure and prevent flashing in the piping.
Superheated MP steam from the 11-F-01 is used for stripping. Steam flow is regulated by
11-FRC-409 which manipulates 11-FV-409 on the steam line. MP steam reduces the partial
pressure of hydrocarbon components inside the Stripper and helps them to get vaporised at
a lower temperature. Vapours move up the stripper column. Mass transfer between the
down coming Heavy Naphtha liquid from the 6th tray to bottom and uprising steam-
hydrocarbon vapours takes place on each tray. Stripped HN vapours enter the Atmospheric
Distillation Column at the 30th tray. Finally stripped HN from the bottom of the stripper is
drawn by Heavy Naphtha pumps (11-P-05 A/B) and sent to the product cooling section.
Minimum 16 kg/hr stripping steam per m3/h of product is to be used for effective
stripping
A temperature difference of maximum 12 °C between the stripper inlet and outlet

temperatures ensures proper stripping.
Temperatures of the incoming and outgoing HN from the stripper are indicated by 11-TI-
404 and 11-TI-409 respectively.
HN stream from 11-P-05 A/B discharge is cooled down in 11-E-01 by crude and further by
cooling water in 11-E-26. 11-TI-104 indicates final rundown temperature of HN.
HN can be routed as follows to

a) Heavy Diesel (sweet / sour) storage tanks, PG HN rundown (blending stream) and
Stabilised Naphtha rundown, through 11-FRC-103 in a 3” line
b) To Stabilised Naphtha rundown and ATP Diesel through 11-FRC-107 in a 3” line
c) To slops in a 3” line
d) To NHT-CCR in a 3” and a 4” (via 6” SRN) line as hot feed.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
ii) Kerosene Stripper (11-C-03)

Six valve trays (SS410S) are provided in the Kero Stripper of 2000 mm diameter. Kerosene
is admitted on 6th tray under1evel control 11-LIC-403. The Kerosene stripper is provided
with software low level alarm 11-LAL-403. Minimum 1.5m elevation is provided between
the inlet nozzle and 11-LV-403 to provide back pressure and prevent flashing in piping.
Superheated MP steam from 11-F-01 is used for stripping. Steam flow is regulated by 11-
FRC-408 on the steam line. MP steam reduces partial pressure of Hydrocarbon
Components inside stripper and helps them vaporise at lower temperature. Vapours move
up the stripper column. Mass transfer between the down coming Kerosene liquid from the
6th tray to bottom and uprising stream hydrocarbon vapours takes place on each tray.
Stripped Kerosene vapours enter the Atmospheric Column at the 22nd tray. Finally stripped
Kerosene is drawn by Kerosene product pumps (11-P-04 A/B) and sent to the product
cooling section.
stripping
Temperatures of the incoming and outgoing Kero from the stripper are indicated by 11-TI-

Kerosene stream from 11-P-04 A/B discharge is cooled down in 11-E-10, 05 & 02 by crude
and further by cooling water in 11-E-24 & 24A. 11-TI-203 indicates final rundown
temperature of Kerosene.
Kerosene can be routed as follows to
a) MEROX unit either as Kerosene / ATF through 11-FRC-203 in a 6” line (there is a 4”
branching to receive ATF from CDU-I from this line at the battery limit)
b) Diesel storage tanks (sweet / sour) through 11-FRC-204 in a 6” line
c) LDO pool with the flow indication11-FQ-205 in a 3” line (there is a 4” branching to route
Kerosene to VBU from this line)
d) FO pool with the flow indication 11-FQ-206 in a 3” line. (RFO and HFO lines)
e) Slops in a 4” header.
iii) Heavy Diesel (HD) Stripper (11-C-04)

Four valve trays (SS410S) are provided in the HD Stripper of 2200 mm diameter. HD to be
stripped is admitted on 4th tray under 1evel control 11-LIC-402. The HD stripper is
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
provided with software low level alarm 11-LAL-402. Minimum 1.5m elevation is provided
between the inlet nozzle and 11-LV-402 to provide back pressure and prevent flashing in
piping.
Superheated MP steam 11-F-01 is used for stripping. Steam flow is regulated by 11-FRC-
407 on the steam line. MP steam reduces partial pressure of Hydrocarbon Components
inside stripper and helps them vaporise at lower temperature. Vapours move up the stripper
column. Mass transfer between the down coming HD liquid from the 4th tray to bottom and
uprising stream hydrocarbon vapours takes place on each tray.
Stripped HD vapours enter the Atmospheric Column at the 14th tray. Finally stripped HD is
drawn by HD product pumps (11-P-03 A/B/C) and sent to the product cooling section.
stripping
Temperatures of the incoming and outgoing HD from the stripper are indicated by 11-TI-

HD stream from 11-P-03 A/B/C discharge is cooled down in 11-E-14, 12, 08, 06 & 03 by
crude and further by cooling water in 11-E-23 & 23A. 11-TI-202 indicates final rundown
temperature of HD.
HD can be routed as follows to

a) DHDS as hot feed in a 10” line through 11-FRC-3501 from the up-stream of 11-E-03
b) Diesel storage tanks (sweet / sour) in a 6” line through 11-FRC-202
c) LDO pool in a 4” line under the flow indication11-FI/FQ-207
d) A slip stream to flushing oil system from the upstream of 11-E-23 in a 2” line
e) A slip stream as seal flushing for 11-P-07 C/D from the downstream of 11-E-23
f) Slops in a 6” line from the down-stream of 11-FV-202
g) FCCU-II as hot diesel from the upstream of 11-E-23
6.2 NAPHTHA STABILISER

Unstabilised Naphtha obtained in Atmospheric Column overhead reflux drum 11-V-01
contains lighter ends like C3 and C4 which vaporize at normal Atmospheric conditions. This
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Naphtha if stored as such in storage tanks will release lot of Hydrocarbon vapours and can
create unsafe conditions and pressurization of the storage tank. To avoid this problem the
lighter components of Naphtha are removed in a column. This process is called Naphtha
stabilization.
Naphtha stabilization is carried out in Naphtha Stabiliser (11-C-05) where C3 and C4
hydrocarbons are removed from Naphtha. The Stabiliser is a distillation column which has
30 valve type trays (SS410S). It is provided with a PSV (11-PSV-501) set at 14.0 kg / cm2
g. The PSV outlet is routed to the flare header.
Unstabilized Naphtha from the Top Reflux Pump (11-P-06 A/B) discharge is first heated up
in Stabiliser feed / bottom exchanger (11-E-19 A/B) by exchanging heat with the outgoing
stabilized Naphtha product. There is a provision to route the CDU-I Unstabilised Naphtha
to 11-C-05, the flow of which is indicated by F1505. Feed enters the column on the 17th
tray under the flow control 11-FRC-503 which is normally cascaded with 11-LIC-405 of
11-V-01. 11-TI-501 indicates temperature pick up from 11-E-19 A/B before entering the
column.
Overhead vapours from Stabiliser (11-C-05) containing C3 and C4 components come out
from column top in a 12” overhead line. This line is routed through Stabiliser overhead
condensers 11-E-20 A/B/C/D. The condensed liquid, LPG, is collected in the reflux drum
(11-V-03) and consists of C3 and C4 components.
The Stabiliser overhead pressure is maintained by pressure controller 11-PRC-501 A/B.11-
PIC-501 acts as a split controller on 11-PV-501A mounted on the condensers bypass line
and 11-PV-501B mounted on the off-gas line from 11-V-03 to FCCU-II (14-V-11).
In case of decrease of Stabiliser top pressure below the set value, 11-PRC-501 opens 11-
PV-501A to allow hot vapours directly into 11-V-03, bypassing the condensers. If the
pressure in 11-C-05 increases above the set value, then 11-PV-501B would open to release
the excess pressure to the FCCU-II sweet fuel gas distribution network. There is a provision
to route the Off-gas through 11-PV-501B directly to the flare also.
LPG pumps 11-P-11A/B function as both LPG product and reflux pumps. Reflux flow
which is controlled by 11-FRC-501 can be cascaded with the column top temperature (30th
tray) indicator and controller 11-TI-510. A 2” minimum flow line (spill-back) from the
discharge header of 11-P-11 A/B is to the pump suction is also provided.
11-LIC-502 controls LPG product flow to maintain reflux drum level and it is cascaded to
11-FRC-502 on the LPG product flow line. LPG is sent to the Amine Treating Unit in
MEROX for the removal of H2S and Mercaptans. 11-V-03 also has level high / low alarms
in the DCS panel (11-LAH/LAL-502).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
A slip stream of LPG can also be sent to the LPG vaporiser of FCCU-II in a 2” line. Sour
water is collected in the boot of 11-V-03. The interface level of water and LPG is indicated
by DL-1503. High water level in boot may result in water carryover with LPG and it will
affect the Amine Treating Unit at MEROX. Hence it is drained at a controlled rate to OWS
periodically.
A technician should always be present during the draining of the water
11-PSV-502 set at 14.0 kg/cm2 g. is provided on the Stabiliser reflux drum whose discharge
is route to flare header. It prevents vessel from getting over pressurized in case of external
fire.
A 2" service water line connection is provided on 11-V-03 to fill the vessel and wash the
Stabiliser column with water during shut down.
A thermo siphon Stabiliser reboiler 11-E-25 is provided at Stabiliser bottom to supply the
necessary heat for boiling the Unstabilised Naphtha. Kerosene CR from the discharge of
11-P-08 A/B is used as heating medium. 11-TR-403 & 11-TI-507 indicate the Kerosene CR
supply and return temperature. The bottom temperature is indicated and controlled by 11-
TRC-501. The control is achieved by adjusting the flow of Kerosene CR through 11-FV-
504 which can be cascaded to the Stabiliser bottom temperature as indicated by 11-TRC-
501. 11-TI-506 & 505 indicate the stabiliser bottom reboiler shell-side (Naphtha-side) inlet
and outlet temperatures respectively.
Stabilised Naphtha gets collected at the bottom of the Stabiliser and the bottom level is
controlled by 11-LIC-501. There is also an indication of bottom level high and low alarms
as 11-LAH/LAL-501 in the DCS panel. This Stabilised Naphtha goes under the pressure of
the Stabiliser to 11-E-19 A/B where it exchanges heat with the feed and then it gets cooled
further in the salt water cooler 11-E-21.There are SRN hot feed provisions from the
upstream of 11-E-21.
• A 4” line to FCCU 2 (for FFCU 2 start up).
• An 8” line to NHT-CCR.
After 11-E-21, SRN goes to the Caustic & Water-wash system.
6.3 NAPHTHA CAUSTIC & WATER-WASH SYSTEM

The purpose of this section is to bring down the H2S and Mercaptans in the Stabilised
Naphtha below 10 ppm. The main equipment in this unit section are:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
a) Naphtha caustic wash drum (10-V-01)

b) Naphtha water wash drum (10-V-02)
c) Caustic circulation pumps (10-P-01 A/B)
d) Water make-up pumps (10-P-03 A/B)
Naphtha from 11-E-21 flows through a 6” line to the caustic wash drum (10-V-01).
Upstream to the 10-V-01, a vortex mixer 10-X-01 has been provided. Caustic solution is
injected into Naphtha upstream of this mixer. The mixer helps in the efficient mixing of
caustic solution with Naphtha with minimum pressure drop across it. Thorough mixing of
caustic solution and Naphtha enables the transfer of H2S / Mercaptans from the
Hydrocarbon phase to the caustic solution phase. Sufficient residence time is given in 10-
V-01 for the separation of the two phases: Hydrocarbon phase on top and caustic solution in
water phase at the bottom. The circulation rate is measured by 10-FI-101. The
concentration of circulating caustic diminishes gradually. This is replaced by fresh charge.
Make-up caustic solution is supplied from MEROX unit to the suction of Caustic
circulation pumps (10-P-01 A/B) which is diluted to a concentration of 5 Boumi. The spent
caustic is drained from the pump suction line to the Chemical Sewer at MEROX. Naphtha
goes out from the top of 10-V-01 to 10-V-02 for water wash. There is a continuous water
make-up (measured by 10-FI-103) to this drum from 10-P-03 A/B, from the service water
line. Equivalent amount of water is drained from the wash drum under the level control 10-
LIC-101. High level and low level alarms 10-LAH/LAL-101 have been provided for 10-V-
02.
After Caustic and Water Wash treatment, SRN can be routed to:
1. SRN storage tank in a 6” line, under the flow indication 11-FR/FQ-201. This flow is
controlled by the Stabiliser bottom level controller 11-LIC-501. Down-stream of 11-FV-
501, there is a provision to route the CDU-I Naphtha to the SRN storage tank
2. MS pool under the flow indication FR0104 in a 6” line. There is a selector switch to
cascade the Stabiliser bottom level controller on the SRN to MS pool also by operating the
software switch LI1501S1 in the DCS panel.
3. Slops in a 4” line.
6.4 VACUUM DISTILLATION UNIT

The Vacuum Distillation Unit is further classified into the following sub sections
1. Vacuum Heater
2. Vacuum Distillation Column (fractionation)
3. Product cooling and routing to storage tanks
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
6.4.1 VACUUM HEATER (12-F-01)

The major equipment of this section are Vacuum Furnace, Air Pre-heater, ID Fan, FD Fan
and Steam Decoking Pot.
The description of the Atmospheric Heater is divided into the following sub sections:
1) Process System
2) Fuel System
3) Air Preheating System
4) Trip and Interlock System
5) Steam Air Decoking
6.4.1.1 Process system

RCO from the 11-C-01 enters the vacuum furnace, where it is heated further so that it
reaches the required flashing temperature. This is a cabin type fired heater with a design
heat duty of 13.28 MM Kcal/h, which was increased to 15.24 MM Kcal/h. The RCO
coming to the heater gets split into 4 streams and enters the 4 passes of the furnace under
the flow recorders and controllers 12-FRC-101/102/103/104. Low flow alarms 12-FAL-
101/102/103/104 are provided on all the passes to protect the heater pass tubes in case of
low flow through each pass.
Steam connections are provided downstream of the FCV’s for purging the respective coils
in case of emergency. The isolation valve for the purging steam line is provided at a safe
distance from the heater.
RCO enters the convection zone of the heater first. It is located at the top of the furnace
above the radiation zone. This zone consists of 6 rows of tubes with 4 tubes per row. While
the top 4 rows of this zone are studded type, the bottom two rows are bare tubes. The
material of construction of the tubes is 9% Chromium+1% Molybdenum. The tubes are 6”
NB Sch. 40 type, during 2010 T&I additional convection zone was provided. This zone
consists of 8 rows of tubes with 4 tubes per row. In the additional zone, top 4 rows are
SPP16 studded tubes, next two rows are SPP9 studded tubes and bottom two rows are bare
tubes.
The convection section has a single row of 8 retractable pneumatic-operated soot-blowers

for the external cleaning of the convection tubes. During 2010 T&I soot blower provision
was given for additional convection zone (8 nos) and presently 4 number of soot blowers
from old setup (alternate) were shifted to additional convection zone. This was done to
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
carryout soot blowing of the new tubes installed during T&I. New soot blowers were under
procurement and will be fixed in the setup. They are operated at the convection zone
platform of the furnace. Pressure gauges are provided on the inlet and outlet of each pass in
the convection zone to indicate the pressure drop across each pass. Temperature indicators
12-TI-302, 307, 312 & 317 are provided on the outlet of the convection zone to measure the
temperature gain in this zone.
The coils come out from the bottom of the convection zone, and enter the radiation zone,
which is the combustion chamber. The radiation zone has 20 tubes per each pass. Each pass
has 34 tubes. These tubes are 4” NB, 6” NB & 8” NB Sch. 40 type. Each pass has provision
to monitor skin temperatures at three different levels in the furnace. They are used to
monitor the condition in the furnace and also give an indication of hotspots in the furnace.
There is also a provision of temperature indicators in the firebox 12-TI-125, 126, 127 &
128 near the floor level.
After gaining heat in the radiation zone, the outlets of the four passes combine and enter the
vacuum distillation column through the 52” transfer line. The outlet temperature of each
pass is measured by 12-TI-106, 111, 116, and 121. The common outlet transfer line
temperature is measured by 12-TI-122 and is controlled and recorded by 12-TRC-133 (coil
outlet temperature). The control is achieved by varying the quantity of fuel to the furnace.
There is also an alarm for high transfer line temperature as 12-TAH-133.
6.4.1.2 Fuel System

12-F-01 is a dual fired furnace i.e., either fuel oil or fuel gas or both can be used. It has 12
burners and were upgraded to 16 numbers during 2010 T&I.
i) Fuel Gas System

branched into a 3” header to the Vacuum Heater. This FG line is steam traced to avoid
FG to main burners passes through a mass flow meter F2406 and a shutdown valve 12-
SDV-105. This SDV is connected to interlock logic. 12-FR/FQ-107 records and integrates
the FG flow to 12-F-01. It is provided with FAL and FAH. Local PG and TG are provided
to indicate pressure and temperature at field.
12-PI-308 indicates FG pressure on the DCS panel. A low pressure alarm 12-PAL-108 is
also provided. Fuel gas pressure low trip is set at 0.2 kg/cm2 g. In case the fuel gas pressure
is low, only 12-SDV-105 will get closed. If fuel gas tip pressure falls below the set value,
chances of flame failure and subsequent accumulation of un-burnt hydrocarbons in the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
firebox is possible. This can lead to the possibility of explosion or back fire in the heater.
Hence the provision of FG pressure low trip. There is a provision to cascade the fuel gas
pressure to the 12-F-01 COT, 12-TRC-133 through a selector switch on the auxiliary panel
in the DCS room.
A 2” FG tapping upstream of 12-SDV-105 has been branched off for pilot burners. The
pilot gas pressure is normally adjusted manually and is maintained at a pressure of 0.7
kg/cm2 g. In case of low pilot gas pressure, 12-PAL-107 is provided to actuate an alarm.
Low pilot gas pressure will alert the operator when pilot gas pressure falls.
ii) Fuel Oil System

branched into a 2” header to the Vacuum heater. FO line is steam traced to maintain
temperature and avoid congealing. Flow recorder and integrator 12-FR/FQ-105 is provided
on main FO supply line and 12-FR/FQ-106 is provided on the main FO return line from
heater. Since this is a closed circuit through which FO circulation is maintained, the net
consumption of fuel oil is measured as the difference between FI-105 and FI-106.
temperature of FO supply. 12-PRC-101 indicates the Pressure of fuel oil on the DCS panel.
A low-pressure trip alarm has been provided on supply line. Actuation of this alarm shuts
12-SDV-102 A/B and cuts off only the fuel oil firing to the Furnace. Since FO is normally a
thick heavy liquid, it needs to be always maintained in circulating state. If it is left stagnant
and unused in burners and piping, it can get congealed despite the fact that tracing steam of
the FO circuit is on. Circulation in heater area (FO piping forming a closed circuit across all
passes called fuel oil ring) is maintained even when no fuel oil burner is in use. A ratio of
2:1 FO supply to return is normally maintained to obtain a good control on firing and
the heater, the circulation can be maintained. Purge steam connections are provided on each
oil burner. FO burners are to be kept steam purged when idle. When FO is fired, it is
atomised or sprayed as a fine mist for realising complete combustion. The spraying of FO is
done by de-superheated MP steam in FO burners.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0

FO supply and MP steam simultaneously. Atomising steam pressure is maintained about
2.0 kg/cm2 above the FO pressure. Atomising steam flow is recorded by 12-FR-108. Local
PG and TG are also provided on this line. 2” flushing oil connection is provided on FO
supply line up stream. CBD/OWS drain is provided on FO return line. These provisions are
to flush the line within Battery Limit after heater shut down. When furnace operates on
combination fuel-either Fuel Gas operates on PIC and Fuel Oil on PIC/TIC cascade or Fuel
Oil operates on PIC and Fuel Gas on PIC/TIC cascade mode. Selector switch is used to
select only one fuel for COT control by cascading.
6.4.1.3 Air Preheating System
12-F-01 is balanced draught furnace. It is a cabin-type heater. Both the convection and
radiation sections are used for heating crude. The combustion chamber houses the radiation
section of tubes. The convection section provided at the top of radiation section serves to
increase the thermal efficiency of the furnace by utilizing further heat from the flue gas.
Tubes are arranged horizontally both in the radiation and the convection zones. The
following are the major parts in the Air Preheating system of the furnace
a) Forced Draft Fan

This is a centrifugal type fan. It supplies the air required for combustion in the balanced and
forced draft operation of the furnace. The inlet of this fan is provided with variable guide
vanes to regulate the flow of air. The guide vanes are journalled in the fan shaft vicinity
with a spherical pivot in a hub ring with cylindrical drilling and at the outside with
cylindrical pivots. Sealing disc suction and discharge sides of the fan is effected via a soft
material compensator, which prevents the transfer of external forces, like the forces due to
thermal expansion, to the fan. The discharge side of the fan has a multi-vane damper in
between the fan casing and soft material compensator, which isolates the discharge duct of
the fan. The fan shaft with the impeller and guide vanes is seated in two oil-lubricated
sliding bearings. The fixed bearing is located on the motor-side and the mobile bearing is
situated opposite to it.
These bearings are lubricated by means of rotating lubrication rings and have Intermediate
chamber. The oil level is seen in the sight glass and the oil operating temperature should not
exceed 80 °C and brief peak temperatures up to 90 °C are sealed off by a labyrinth seal. The
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
fans are driven by polyphase induction motors via couplings, which are directly coupled to
the fan. The fans are dynamically balanced. This warrants a running performance which is
free of any vibration. In case of ID fans, an uneven caking on the impeller will create
unsteadiness of run.
b) Induced Draft Fan

This is a centrifugal type fan. It controls the flue gas flow from the furnace by the variable
inlet guide vane mechanism same as mentioned above. There is a provision to indicate the
wide open position of the suction vanes in the DCS room on the auxiliary panel.
c) Recuperative type Air Preheater

This is an assembly of rectangular cast tubes that have fins on either side at the hot end and
fins only on the flue side at the cold end. The tube lengths, size and pitch will vary as per
requirements in individual cases. Using the tubes as building block, air preheater of any
size can be made to suit heat duty and pressure drop. The entire tube assembly is built
inside a steel frame made by beams and fully insulated casings. Flue gas and air terminal
connections are made of rectangular flanges formed from rolled steel sections.
These flanges form an integral part of the air preheater frame and are sturdy and are capable
of carrying considerable external loads. The entire air preheater assembly forms part of the
ducting system. Because of the orientation of flat surfaces it is essential that flue gas flow is
always in the vertical direction.
The flue gas will be on single pass, vertically down and air can have a number of passes
depending upon allowable pressure drops. The pressure drop allowable is decided on a
case-to-case basis. Generally it is 50-100 mm WC on the air side and slightly lower side on
the flue-gas side. The tube is made of two half sections, cast independently and then bolted
together. To prevent air leakage in the longitudinal direction, two grooves have been
provided on the flanges on the either side. Asbestos ropes are placed in the grooves before
bolting. The flanges provide the necessary gap for the flue gas passage. The flanges also
have peripheral grooves on all four sides to accommodate asbestos rope to ensure air
tightness between adjacent tubes.
d) Drop-Out Doors
Drop-Out Doors are provided to supply combustion air in case of Natural Draft operation or
in case of emergency. The drop-out doors are double-flap isolator type, actuated
pneumatically by double-acting power cylinders and 4-way solenoid valves. The following
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
provisions are also made to operate them in case of Instrument air failure as extra safety
devices.
o Weight loading to open the DODs by the force of gravity.
o An air accumulator tank of sufficient capacity to operate the DODs.
are provided in the control room to open and close each drop out door. The open or close
position of the DOD’s is indicated by the lamps provided on the auxiliary panel. These are
actuated by the limit switches.
e) Stack Damper
Stack Damper is provided to prevent the flue gases from escaping directly without heat
exchange in the Air-Preheater. It also helps in the direct escape of flue gases when the
furnace is in Forced Draft or Natural Draft operation. The stack damper operates either full
open or full close. During 2010 T&I, the stack damper was replaced with full shut off
damper with controlled damper operation. The new stack Damper is a multi-Louver
isolation and control damper with pneumatic plus manual control. The damper is provided
with counter weight to the FAIL SAFE OPEN position.
The damper is designed as FAIL OPEN position and it shall attain FAIL OPEN position on
failure of:
1. Supply air failure with supply air pressure switch set at 2.5 Kg/Cm2 falling.
2. Electric Supply to the Control Panel by auto operation of solenoid valve.
3. The Signal failure i.e. signals pressure falling below 0.2 Kg/Cm2.
The damper shall open with decrease in signal air pressure and accordingly close with
increase in signal air pressure. It is provided with Pneumatic linear actuators for operation
and control of the damper. The damper is also provided with Winch and cable for manual
operation of the stack damper from grade. In auto operation, disconnect the winch by either
removing shackles from winch arm at damper level or by disengaging the worm wheel and
shaft provided on the winch machine by rotating the hand wheel in anti-clockwise direction
at grade level. The worm shaft can be locked by the lever below hand wheel in clockwise
direction.
are provided in the control room to open and close the Stack Damper.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
The open or close position of the Stack Damper is indicated by the lamps provided on the
auxiliary panel. These are actuated by the limit switches. There is a provision to open the
Stack Damper manually from the field by winch operation in case of emergencies.
Air is required for the combustion of fuels in a furnace. It is supplied by the FD fan (12-
FM-01). The air flow is regulated by adjusting the variable inlet guide vane mechanism to
maintain proper dP across the furnace and for maintaining the required excess air in the flue
gas. About 15 to 20% excess air in case of fuel oil and 10 to 15% in case of fuel gas is
found to give satisfactory performance of the furnace. An oxygen analyzer (AR-2501) is
also provided at the outlet of the flue gas to monitor the excess air regularly.
2.5% O2 on AR-2501 equals to 10-15% of excess air
Air preheating system helps in recovering the sensible heat from the flue gas further, after
the furnace convection zone, which is utilized to preheat the combustion air. This increases
the fuel economy and also the heater efficiency approximately by 10 %. There are separate
Air Preheating systems (APH) for Atmospheric and Vacuum Furnaces. Forced Draft fan
(12-FM-01) draws Atmospheric air and forces it through the APH. Induced Draft fan (12-
FM-02) draws the flue gas through the APH, and returns it to the stack above the stack
damper after recovering heat from it. Care should be taken to maintain the return
temperature of flue gas above its dew point (typically 175 °C) to avoid condensation which
otherwise would result in acid corrosion.
The design of the furnaces in CDU-II gives immense flexibility in their operation. There are
3 modes of operation as given under.
a) Balanced Draft operation

In this mode of operation, the FD and ID fans both function simultaneously and help in
recovering the heat from the flue gas. Flue gas is drawn by the ID fan through a duct
connection that is taken from the castable below the Stack Damper. This duct is lined with
refractory. Pressure and temperature gauges are provided to give local indication of the
pressure and temperature of flue gas entering the air pre-heater. PI and TI are also provided
to give the indication in the control room. A winch operated shut-off blade hand controller
is provided in the duct to isolate the flue gas duct. Hot flue gas enters the APH at the top
and exchanges the heat with combustion air. Flue gas exiting the APH is routed to the ID
fan suction. This fan draws the flue gas and conveys them back to the stack above the stack
damper through a duct. 12-TAL-503 (at the inlet of ID fan) is provided to give an alarm
when the flue gas temperature falls below the dew point temperature to avoid corrosion. In
case of low temperature, the air flow through the APH can be adjusted so that the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
temperature can be raised. In case there is an abnormal rise in temperature of flue gas
leaving the APH, TAH will give an alarm. 12-PAH-507B gives an alarm in case of high
furnace box pressure in the arch zone.
Combustion air under pressure from the FD fan is ducted through the bottom of the
APH.PG and TG give the local indication of the pressure and temperature of the cold air
entering the APH and a PI gives the cold air pressure indication in the control room. 12-
PAL-506 is provided on the discharge of the FD fan to give an indication in case of low
discharge pressure of the FD fan. After exchange of heat with the flue gas, hot air is sent
into the hot air distribution duct running west of the heater. This duct is provided with a TG
and PG to give a local indication of the temperature and pressure of the hot air. There is
also a TI and a PI to give an indication in the control room. A TAH (12-TAH-501) is
provided to give a high temperature alarm. This hot air duct branches into the plenum
chamber of the furnace, where the burners are mounted.
b) Forced Draft
In this mode of operation, the FD fan of the furnace will be running and the ID fan is
stopped and the stack damper is kept open. Flue gas escapes to the Atmosphere directly
without preheating the combustion air. This is done mainly when isolation of the APH or
ID fan is required to carry out maintenance activities.
c) Natural Draft
There is also a provision to operate the furnaces in natural draft, wherein there is no
requirement of FD and ID fans. There is a provision of 2 Drop out Doors (DOD’s) on the
combustion air duct of 12-F-01.
To operate the furnace in Natural Draft, DOD’s and stack damper are opened. Atmospheric
air goes inside the furnace by the action of the draft in the furnace and aids in combustion.
The flue gas escapes directly through the Stack Damper without preheating the combustion
air.
6.4.1.4 Trip and Interlock System
Trip values of 12-F-01:

Trip Unit Value
FD fan discharge pressure (low) mm Aq. +15
ID fan suction pressure (High) mm Aq. -45
Furnace pressure (high) mm Aq. +2.95
Fuel oil pressure (low) Kg/cm2g. +2.77
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Fuel gas pressure (low) Kg/cm2g. 0.20

Furnace pass flow (low) m3/h 14
The following trips are provided on 12-F-01

DOD – SD Check Trip: This trip opens stack damper under the following conditions
c) ID fan trips
FD Fan Trip: This trip opens the DOD’s under the following conditions
c) FD fan motor amps low (Annunciator alarm)
d) Any of the DOD’s is not closed completely
f) ESD is activated.
ID Fan Trip: This trip opens the SD under the following conditions
c) ID fan motor amps low (Annunciator alarm)
f) ESD is activated
g) Stack damper opens when in Balanced Draft
Fuel Oil Trip: This trip closes the fuel oil supply and return SDV’s under the following
conditions:
a) Fuel oil pressure low (Annunciator alarm)
c) ESD is activated
Fuel Gas Trip: This trip closes the fuel gas SDV under the following conditions
a) Fuel gas pressure low (Annunciator alarm)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
c) ESD is activated
Timers: Three timers are provided in the furnace trip circuit, which will start counting
when their respective alarms are activated. If the alarm is not brought back to normal value
within 30 seconds (as counted by the timer), the timer relay will activate the fuel oil and
fuel gas trips. If the alarm is brought back to normal value within 30 seconds (as counted by
the timer), the timer will
a. Furnace Pressure High Timer: It gets activated when furnace pressure high alarm
comes on the annunciator panel and gets reset when the alarm is normalized.
b. FD Fan Trip Timer: It gets activated when the FD fan is not running, and gets reset
when FD fan is running or the FD fan trip is bypassed.
c. ID Fan Trip Timer: It gets activated when the ID fan is not running, and gets reset
when ID fan is running or the ID fan trip is bypassed.
Interlock system: Interlocks are provided to ensure safe operation of the equipment. They
ensure that corrective action is taken automatically whenever unsafe operating conditions
arise due to process upsets, mal-operation etc. But the interlocks can be made ineffective /
inactive by bypassing the trip switches provided on the DCS panel.
Interlocks on furnace operation: The following interlocks ensure the safe operation of
furnace. The following description is valid only when the trips described above are in auto-
interlock mode.
a) Drop out doors opening or closing
b) Stack damper opening or closing
c) FD fan starting or stopping
d) ID fan starting or stopping
e) Fuel SDV’s opening or closing
f) Low Pass Flow
Interlock 1: DOD Operation

i) When the furnace is in natural draft mode, all the DOD’s have to be in fully open
position. If any one DOD leaves the fully open position (either by operation or by
instrumentation malfunction), then the fuel to the furnace is cut off.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
ii) When the furnace is in forced draft mode, DOD’s are in fully closed position and if any
of the DOD’s is not in fully closed position, FD fan is tripped. As get reset i.e., the timer
indication will become zero.
In case the FD fan is tripped, all the DOD’s will open automatically.
iii) When the furnace is in balanced draft mode, DOD’s are in fully closed position. They
get opened automatically if the
a. FD fan trips
b. Arch pressure high gets activated
Interlock 2: SD Operation
a) When the furnace is in natural draft mode, the SD has to be in fully open position. If the SD
b) When the furnace is in forced draft mode, the SD has to be in fully open position. If the SD
c) When the furnace is in the balanced draft mode, the SD has to be in fully closed position. If
it leaves this position, the ID fan is tripped. The SD gets opened if
d) ID fan gets tripped
e) Arch pressure high gets activated
f) FD fan trips /any DOD leaves fully closed position
Interlock 3: FD Fan Operation

a) When the furnace is in natural draft mode, the FD cannot run as long as the DOD’s are in
open position.
b) When the furnace is in forced draft mode, FD fan gets tripped if any DOD leaves fully
closed position or the furnace pressure is too high.
c) When the furnace is in the balanced draft mode, the FD gets tripped if any DOD leaves
fully closed position.
Interlock 4: ID Fan Operation

a) When the furnace is in natural draft mode, the ID cannot run if FD fan is not running.
b) When the furnace is in forced draft mode, the ID is in stopped condition. No interlock.
c) When the furnace is in the balanced draft mode, the ID fan gets tripped if
d) SD is not fully closed
e) any DOD leaves fully closed position
f) FD fan is tripped
g) Furnace pressure is high
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Interlock 5: Fuel SDV’s Operation

The fuel SDV’s get closed by operating the ESD on the auxiliary panel. Individual ESD’s
are also provided for fuel oil and fuel gas. The fuel SDV’s get opened only after the
individual “SDV Reset” push button on the auxiliary panel is operated. The following are
the interlocks on the Fuel SDV’s
a) When the furnace is in natural draft mode, fuel is cut off if any DOD or stack damper
leaves the fully open position.
b) When the furnace is in forced draft mode, fuel is cut off if any DOD leaves fully open
position / FD fan trips
c) When the furnace is in the balanced draft mode, the fuel is cut off in case any of the three
timers gets activated.
Interlock 6: Low Flow in the Furnace Passes

This interlock shuts down the fuel SDV’s to the furnace whenever the furnace pass flow in
any coil is low. The trip value set for the low pass flow for 12-F- 01 is 14 m3/h.
6.4.1.5 Steam Air Decoking

Steam air decoking (SAD) of vacuum heater tubes is done to remove coke deposit from
inside heater tubes with the help of steam and air. Removal of coke results in clean heater
tube internals and improves heater performance by better heat transfer to process fluid.
SAD† also achieves low pressure drop through heater tubes and reduces chances of hot spot
on heater tubes. Need for steam air coking of heater tubes is indicated by increased pressure
drop and harder firing.
This dedicated SAD arrangement comprises decoking pot (11-V-05) (which is common for
11-F-01 and 12-F-01), piping and instrumentation for plant air, service water and MP
Steam. MP steam connection to each pass flow is provided to dislodge carbon deposit from
inside the heater tube. Local and DCS room mounted flow indications (12-FE-111 to 113)
are provided on each steam connection plant air is required to ignite the remaining coke
film deposit cleaning inner wall of tubes and achieve final cleaning for each 4” size plant
air connections. 12-FE-110 indicates the total plant air consumption.
Service water quench provision is given on 11-V-05 as well as on decoking line to quench
the contents before letting out to atmosphere. To carry out SAD, pass flow inlet and outlet
of the furnace 12-F-01 are isolated from process network and connected by means of swing
elbows with the decoking network.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Heater pass flow outlets are connected to the decoking pot (11-V-05). While MP steam is
introduced in the tubes it is fired from outside, thermal shock caused by the flame cracks
the coke scales inside tube and flowing steam dislodges them. These coke particles are
carried to 11-V-05 after being quenched in the line as well as in the decoking pot by service
water. This operation is called spalling. When no more coke is removable by spalling as
indicated by relatively clear colour of effluent, air along with steam is introduced into pass
flow to burn out the coke inside tube while firing is on in the heater, oxygen burns coke at
high temperature, burning of the smoke is indicated by increased tube metal temperature
and same should not be allowed to go beyond 625 °C Number of passes selected for
spalling and coke burning is largely dependent on limitations posed by steam availability
and piping network. Sudden release of coke during spalling may result in choking of the
piping handling effluent or may cause hot spots of the tube during burning. SAD of only
one pass at a time should be done if limitations in steam and SAD piping are experienced.
6.4.2 VACUUM DISTILLATION COLUMN
The vacuum column (12-C-01) has three sections of different diameters. Top section is of
5000 mm diameter. Middle section is of 6600 mm diameter and bottom section is of 5000
mm diameter. As the Vacuum Column operates under vacuum, the vapour velocities are
high. Sections where the vapour load is low are smaller in diameter for cost saving. The
upper portion of the column has 3 packed beds of SS410S material. During 2010 T&I the
LVGO packing (Existing : 25 M3 M-PaK1.5+7.5M3 MPak2.0+ 17M3 Hy-Pak 1.5) and
HVGO packing (52M3 Hy-Pak 3.0 + 52M3 M-Pak 3.0) were replaced with IMTP-40 and
IMTP-70 respectively with SS316 2.5% Mo metallurgy. There are 3 side draw-off trays
(chimney type) for slop cut, HVGO and LVGO, one each below the three packed beds. The
bottom portion has 3 disc and doughnut type heat transfer trays. Short residue is drawn as
bottom product.
Description of Vacuum Column has been taken up zone wise starting from bottom.
6.4.2.1 Vacuum Column Bottom Section:

The partially vaporised RCO feed stock coming from the Vacuum Heater enters the column
in the flash zone below the slop draw-off chimney tray. The vaporised portion rises up in
the tower and is fractionated into 3 side stream products. The liquid portion of the feed
drops into the bottom section of the tower and is withdrawn as Short residue (VR). 12-TR-
203 and 12-PR-202 indicate the Column flash zone temperature and vacuum respectively
on the DCS panel.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
The Column bottom level is maintained by 12-LIC-202’s action on 12-LV-202 on VR

rundown line. LI-2201 also indicates level on DCS panel. Both LIC and LI have software
high level and low level alarms 12-LAH/LAL-201. 12-TI-201 indicates temperature of the
column bottom on the DCS panel. LAH-2108 and LAL-2109 are also provided for column
bottom on the DCS panel.
A tangential vapour horn is provided for flash zone inlet, which minimises entrainment of
heavier hydrocarbon liquid droplets. There is a 3 inch LP steam line provision to column
bottom below tray 1 for steaming out purpose.
Vents of all pumps taking suction from Vacuum Column are connected back to Vacuum
Column above flash zone through a common vacuum line. With this arrangement all pumps
connected with Vacuum Column can be vented to the column.
Temperature at the bottom section is normally quenched to about 350 oC at a vacuum of -

735 mm Hg (g.). RCO is fed to the flash zone at 390 oC.
6.4.2.2 Short Residue Draw-off

Short residue (VR) is drawn by VR + Quench pumps (12-P-01 A/B) from the Vacuum
Column (12-C-01) bottom. VR pump discharge can be routed to following destinations:
a) To Vacuum Heater (12-F-01) through 8” start-up line which joins the RCO feed line
to 12-F-01. This is used during start-up only.
b) A slip stream of the pump discharge can also be routed to the pumps suction in a 2”
line as spill-back.
c) The pump discharge from 12-P-01 A/B exchanges heat with crude in 11-E-16, 12-E-
06 A/B and 12-E-03. The outlet of 12-E-03 at a temperature of 250 °C can be routed as
follows.
• It is partly sent to the 12-C-01 bottom in a 6” line for quenching and maintaining
the bottom temperature at 350 °C to prevent cracking of SR and lead to other
problems like deterioration of vacuum, plugging or suction strainers of 12-P-01
A/B leading to loss of suction. The quench flow is recorded and controlled by 12-
FRC-204.
• It can be partly sent as feed to the Bitumen Blowing Unit in a 3” line.
• The rest of it can either be sent to 12-E-01 A/B/C and then to 12-E-09 A/B/C/D or
can be routed directly to the 12-E-09 A/B/C/D where it is cooled. TIC-2103 located
on VR product rundown header to tanks controls TV-2103 on the tempered water
line to 12-E-09 A/B/C/D.
d) Downstream of the coolers, SR can be routed to

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
• IFO pool partially in a 6” line.

• Storage via the three-way FCV 12-FRC-405 through an 8” RFO line, or to the HFO
pool by adjusting 12-FV-405. The HFO flow is measured by 12-FR-406.
• LDO pool partially, in a 4” line, measured by 12-FI-407.
• VBU as hot feed from the upstream of 12-E-09 A/B/C/D or to VBU storage tanks in
10” line. (TIC-2420 on rundown line maintains VR temperature by bypassing a
certain amount of hot VR to the rundown line)
• BBU storage tanks via HFO line (at unit limit tie-in).
6.4.2.3 Vacuum Slop Draw-off:
The zone immediately above the flash zone is known as Wash Zone. It consists of a packed
bed (Hipack type). Above this there is a 150 mm thick SS410 Glitsch Grid packing to
remove the entrained asphaltenes. Spray nozzles are provided above the packing for proper
distribution of the internal reflux. The spray nozzles were replaced with Lechler’s spray
nozzles (designed by Shell) were fitted (28nos). The Wash zone also has a demister pad
above the spray nozzles of the wash zone packing. The vapours rising from the wash zone
pass through a demister pad provided to trap the entrained droplets of Heavy hydrocarbons
which could otherwise adversely affect the HVGO/LVGO quality. Slop-cut is drawn by
slop distillate and recycle pumps (12-P-02 A/B). The draw-off temperature is indicated by
12-TI-204. The level on the chimney tray is regulated by 12-LI-203 by operating 12-LV-
203 on the slop-cut rundown line to the VR line. Slop + Recycle pump (12-P-02 A/B)
discharge has following destinations.
One part of slop distillate goes to the furnace under flow control 12-FRC-109 through a 3”
line. The purpose of the recycle stream to vacuum furnace is to maximise HVGO recovery
from the slop cut. The slop-cut recycle from slop pump is mixed with RCO from
Atmospheric column before getting heated in vacuum furnace. Additional provision was
given during 2010 T&I for routing the slop-cut to FCCU-II from the downstream of slop-
cut recycle control valve.
A slip stream of the pump discharge can also be routed to the pumps suction in a 2” line as
spill-back.
As product rundown, a part of Slop Distillate pump discharge gets mixed VR product up
stream to 12-E-01 A/B/C. 12-LV-203 on slop line maintains slop level on the chimney tray
of slop section.
The product stream can also be routed to the storage tanks through the CDU-I cooler box.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
6.4.2.4 Heavy Vacuum Gas Oil (HVGO) Draw-off:
The majority of rising hydrocarbon vapours from slop zone wash section are condensed in
HVGO section by circulating reflux to yield the side draw-off product. HVGO product,
Internal Reflux (IR) + Circulating Reflux (CR) is withdrawn as the second side stream.
12-TI-205 indicates the draw-off temperature. HVGO draw-off from the Column is routed
to HVGO product + CR pumps (12-P-03 A/B). There is a provision to route SR to these
pump suction (during flushing of the Vacuum Column bottom). The HVGO discharge from
the pumps is routed as
a) HVGO Internal Reflux: One part goes as Internal Reflux (IR) for packing washing
of Wash zone of vacuum column without any heat exchange. HVGO IR (Wash Oil) is
regulated by 12-FRC-202 in such a way that proper washing of the packing is always
achieved for all throughputs. One distributor is provided for proper distribution of HVGO
IR over the entire cross section area of the column packing. Strainers (12-X-01 A/B) are
provided to arrest the carryover of foreign materials back into column. Pressure gauges
across the filters indicate the pressure drop across the filters and its rise would indicate the
need to change over of the filter in line. 12-TI-206 shows HVGO IR temperature.
b) HVGO Circulating Reflux: HVGO CR + product from 12-P-03 A/B discharge is

split into two steams. One stream goes through 12-E-05 A/B and 12-E-02 and the other
through 12-E-04. Here, it exchanges its sensible heat with the crude. The two streams are
then combined and routed to the MP steam generators 12-E-10/10A parallely. The stream
coming out of the steam generators is routed partly as HVGO CR back to column at
through the CR strainer 12-X-02 A/B. This flow is controlled and recorded by 12-FRC-203.
The CR return temperature is indicated by 12-TI-208. The remaining volume is either
routed as hot feed to FCCU-II or to product rundown line or both at the same time.
HVGO Products:
The HVGO can be routed to the following:
a) To the 6” Hot feed line, under the flow controller 12-FRC-402. The temperature of this
stream is indicated by TX-2402.
b) To 12-E-12 A/B where it gets cooled down to 80 °C and goes to the product storage tanks
in a 4” line under the control of 12-LIC-204, which controls the HVGO level in the
Column. The product can also be routed to LDO pool, whose flow is recorded by 12-
FR/FQ-408.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
c) A slip stream of HVGO is routed as quench to 13-PV-402 under the flow controller 13-
FRC-404.
d) To slops in a 6” line
6.4.2.5 Light Vacuum Gas Oil Draw-off (LVGO):
The rising uncondensed hydrocarbon vapours from HVGO zone are condensed in LVGO
section by circulating reflux to yield the side draw product LVGO product + Internal
Reflux (IR) + Circulating Reflux (CR) is withdrawn through 10” line from the third
chimney tray. 12-TI-207 indicates draw-off temperature on the DCS panel. LVGO draw-off
from the column is routed to LVGO product + CR + IR pumps (12-P-04 A/B), whose
discharge is routed as
a) LVGO Internal Reflux: This stream joins the HVGO CR stream and goes as a reflux
over the HVGO packing without any heat exchange. The flow of this stream is controlled
by 12-FRC-201. This stream joins the cold HVGO CR stream upstream of the strainers 12-
X-02 A/B.
b) LVGO Circulating Reflux: This stream splits further into two streams. One stream goes
11-E-07 to exchange its sensible heat with the crude and then goes to 11-E-22 for cooling.
The other stream goes to 11-E-22A directly for cooling. The outlet of 22 & 22A combine
and go through the LVGO CR strainer 12-X-03 A/B to the top of the LVGO packing as top
reflux. The CR flow is controlled by 12-FRC-205 and the return temperature is indicated by
12-TI-210.
c) LVGO Product: A part of 12-P-04 A/B discharge stream gets cooled in 12-E-11 and can
be routed to HVGO storage tanks or FCCU-II. The flow of this stream is controlled by 12-
LRC-205 and is recorded / integrated by 12-FR/FQ-403. The product can also be routed to
Diesel or LDO pool controlled by 12-FRC-404.
LVGO product is routed as follows:

• As hot feed to FCCU-II along with hot HVGO through 12-LV-205
• To VGO storage tanks along with HVGO through 12-LV-205
• Either to Diesel/LDO/SR or HVGO (at battery limit) storage tanks through 12-FV-404
in a 3” line. There is a provision to cascade the level controller on the LDO FCV
• To flushing oil system in a 2” line
• To slops along with HVGO.
6.4.2.6 Vacuum Column Overhead System:

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
Steam and small amount of light hydrocarbons produced as a result of cracking, pass out of
the vacuum column top through a 36” size line. The uncondensed vapours flow through a
demister pad provided in the column top vapour space to set of steam ejectors. Demister
pad prevents carry over of liquid droplets to ejectors and condenser system. The Vacuum
Column top temperature is indicated by 12-TI-209. The overhead pressure is indicated and
controlled by 12-PRC-206 on DCS panel. 12-PSV-202/ 202B set at 3.5 kg/cm g. are
mounted on top of the Vacuum Column to protect the column from over pressurisation.
Column top vacuum is normally operated at -751 mm Hg (g.).
Vacuum is created and maintained in the column by 3-stage ejector system with
condensers.
The 1st stage ejectors (12-J-01 A/B/C), 2nd stage ejectors (12-J-02 A/B/C) and the 3rd stage
ejectors (12-J-03 A/B/C) are designed for a capacity factor of 1/7, 2/7 and 4/7 totalling
150% of normal capacity. If required each ejector element can be isolated by cutting off
steam and isolating suction inlet valves.
The vapours from the Vacuum Column top are sent to the primary condenser 12-E-07A.
The non-condensable from the primary condenser are drawn by the 2nd stage ejectors,
which is again routed to the secondary condenser (12-E-07B). The non-condensable from
the secondary condenser are drawn by the 3rd stage ejectors and routed to the after
condenser (12-E-07D). The non-condensables from this stage are routed to the hotwell
drum through a dip leg. The non-condensables from here enters to knock out pot and then
are either routed to 11-F-01 Hot well off gas burners 17,18,19 and 20 or it has to be routed
to atmosphere (vent the non-condensable into atmosphere). The condensate from all the
three condensers drops to the Hotwell drum (12-V-01) through the barometric legs. Cooling
water is supplied to the primary condenser in an 18” header. The water outlet from the
primary condenser is bifurcated into two parts. One part feeds the cooling water to the
secondary condenser and the next part feeds the after-condenser. There is a provision to
back flush the primary condenser. A draining provision is provided in the up-stream of the
after-condenser. 12-PRC-206 is mounted on the non-condensable line from 12-E-07D,
controls the Vacuum Column overhead pressure by routing a part of the non-condensable
vapours (before letting them into the Hotwell drum) to the inlet of the 1st stage ejectors. A
3” fuel gas line is provided near the inlet of the 1st stage ejectors, for backing-in of fuel gas
during the start-up and shut-down to maintain the column in positive pressure.
MP steam to all ejectors is supplied in parallel by 6” header. Ejector steam consumption is

indicated by 12-FR-207. Strainers are provided on the MP steam line to arrest line scales
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
etc. from reaching into ejectors and adversely effecting performance of overhead system.
Ejector steam pressure is controlled by 12-PRC-207. This should be maintained constant as
far as possible for smooth operation of the Vacuum Column. Corrosion Inhibitor and
Neutraliser injection facility into overhead vapours have been provided both on Vacuum
column top overhead.
Hotwell (12-V-01) is a horizontal vessel provided to separate out condensed hydrocarbons

from vacuum column overhead stream and provide effective sealing of the system
operating under vacuum from Atmosphere. Hotwell is provided with 3 compartments
created by two internal baffles of 400 mm and 800 mm height. The process lines called
barometric legs carrying the condensate from all ejector condensers are kept dipped into
water in the left side of the compartment (left of 400 mm baffle). Dip legs are provided so
that no air ingress is possible. An overflow line with a U-loop seal and valve (called as
siphoning loop) is provided on the water side of the Hotwell Drum. This siphoning loop
ensures that a minimum water level in the water compartment of the drum is maintained, so
that water doesn’t rise back into the barometric legs, thereby bringing down the vacuum. At
the crest of this siphon U-loop, a 1” vent having an opening downwards is provided to
break the siphoning effect, and hence called, the siphon breaker.
The water-hydrocarbon interphase is formed in the middle compartment from where

hydrocarbon overflows to its higher baffle height (800 mm) compartment (slop oil
compartment) and water remains in the middle sour water compartment. The sour water
from the middle compartment is pumped out by sour water pumps (12-P-06 A/B) to the
Sour Water Stripping unit.
12-LDIC-201 controls the Hotwell interface level acting on 12-LV-201 which is mounted
on the sour water line. 12-FI/FR-650 shows sour water flow on DCS panel when Hotwell
sour water is routed to 11-V-04. 12-LT-201 is mounted in the middle section of the hotwell
to monitor the oil-water interphase. Condensed and separated hydrocarbon components
(Hotwell oil) are collected in oil compartment. Hotwell oil is pumped out by Hotwell oil
pump (12-P-05 A/B) to Hotwell oil storage tank or to slop. Hotwell oil pumps are
interlocked with Hotwell oil high level alarm (12-LAH-205) and low oil level alarm (12-
LAL-205) for auto cut-in and cut-off respectively. These high and low level switches
automatically start and stop the Hotwell oil pumps. This flow is recorded by 12-FI/FR-206.
Vapours from 12-V-01 are routed to the hot well knock-out pot where entrained liquid is
knocked off and routed to OWS periodically. Vapours from the knock-out pot are either
routed to 11-F-01 Hot well off gas burners 17,18,19 and 20 or it has to be routed to
atmosphere (vent the non-condensable into atmosphere). Steam connection is provided on
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
this vent line to Atmosphere for dilution of hydrocarbon vapours which are vented. Hot
well off gas flame arresters (2 no’s) are provided on the off gas line to 11-F-01.
6.4.2.7 Vacuum Pumps Priming

The pumps in the Vacuum section that take suction from the Vacuum Column are served by
a vacuum vent system. The vents from the various Vacuum section pumps are connected to
a header which enters below the first tray of the Vacuum Column. The vent system is
necessary so that vacuum can be pulled in a pump casing before the suction valve is
opened. This facility ensures proper priming of pumps operating under vacuum. The
following pumps are served by the system.
11-P-10 A/B RCO pumps
12-P-01 A/B Short Residue pumps
12-P-02 A/B Slop Distillate and Recycle pumps
12-P-03 A/B HVGO pumps
12-P-04 A/B LVGO pumps
6.5 MP STEAM GENERATION

MP steam is generated from BFW in the unit by recovering heat from HVGO CR + Product
stream. BFW is received from off-sites through a 4” header taken from which a 2” tapping
is for steam generation. Steam is generated in kettle type steam generators 12-E-10 / 10A
by exchanging heat with HVGO. The level of the BFW in the steam gen is controlled by
12-LIC-301/302 by operating 12-LV-301/302 on the BFW lines to 12-E-10/ 10A
respectively. The temperature of HVGO from the steam generators is controlled by 12-
TRC-302/303 by operating the three-way control valves 12-TV-302/303 respectively on
12-E-10/10A respectively. Saturated MP-steam is generated in this system at 10.5 kg/cm2 g.
pressure and 190.7 oC. Two PSV’s (set at 13.5 kg/cm2 g.) have been provided on each
steam generator to protect the steam generators from over-pressurisation in the event of
external fire. A 2” vent line is provided to vent out the steam from the PSV’s to
atmosphere.
In order to depressurise and blow down steam safely, 12-V-03 (steam blow down drum) has
been considered. Blow down from steam generators 12-E-10 and 12-E-10A enters the blow
down drum (12-V-03) and gets quenched by service water and then routed to OWS. This
drum has a vent at safe height. Its drain connection has water seal provision.
6.6 TEMPERED WATER AND DM WATER SYSTEM

DM water at 60 oC is used in a closed circuit to cool Short Residue and Bitumen product
streams. This is used as these products should not be cooled below their pour points. Salt
water or service water are also not used to prevent scale formation in the exchanger tubes at
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
high operating temperatures, which would otherwise lead to severe loss in heat transfer
efficiency.
This system consists of 12-V-01 (tempered water drum), 12-P-07 A/B (tempered water
pumps), 12-E-08 A/B (tempered water coolers), 12-E-09 A/B/C/D (Short Residue coolers)
and 13-E-02 A/B/C (Bitumen product trim coolers). 12-V-02 is a vertical cylindrical vessel
of Height Diameter, 5400 1800 mm. The vessel is elevated 6000 mm above the ground,
so as to provide the necessary NPSHR to the tempered water pumps and avoid cavitation. It
is provided with a level indicator (12-LI-401), low level alarm (12-LAL-401), high level
alarm (12-LAH-401) and a temperature gauge (12-TG-401). DM water makeup line has
been provided to make up for evaporation loss. For heating the tempered water during the
start-up, a 1½” LP steam line is provided to admit open steam into the tempered water
drum. Tempered water at 60 °C drawn by tempered water pump is routed to 12-E-09
A/B/C/D and 13-E-02 A/B/C located in the plant. The hot tempered water is maintained by
adjusting the bypass globe valve across the cooler 12-E-08 A/B. The outlet temperature is
indicated by 12-TI-405.
Tempered water is also used as bearing cooling water for 12-P-01 A/B (Short Residue
pumps)
6.7 CHEMICAL INJECTION FACILITIES

Crude oil contains salts such as chlorides of Magnesium and Calcium. These salts if not
removed, hydrolyse in the system to form Hydrochloric acid. There is also a possibility of
formation of acidic Hydrogen Sulphide (formed from dissociation of heavy sulphur
compounds present in crude) which is then dissolved in the crude. Both of these concentrate
in the overhead system and form acid solutions, which are corrosive. Measures must be
taken to overcome their harmful effects.
The overhead system including condensers and reflux drum is made of carbon steel. In
order to protect this section, caustic solution, ammonia solution and corrosion inhibitors are
added at various points. The purpose of injecting caustic at the outlet of Desalter is to
achieve better mixing of these chemicals with crude and neutralise the acids/salts mainly
HCl and H2S as soon as they formed (at a temperature of 120oC and above). The reaction
products i.e. Sodium and Ammonium salts go along with reduced crude (RCO). The
balance acids and acid gases if any will go up to the overhead system where ammonia is
injected in the overhead vapour line for neutralisation. Amount of ammonia should be
controlled in such a way that pH of reflux drum water remains at around 6.5 Injection of
caustic at the outlet of Desalter should be maintained in such a way that the salt formation
should be low in the overhead circuit which might form scales in the overhead condensers
tubes.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
A slightly acidic condition of the overhead system is desirable to keep ammonium salts in
solution, which if precipitate, would foul and plug the condensers. Corrosion against
slightly acidic (pH 6.5) condition is minimized by adding corrosion inhibitors in the
overhead vapour line. The inhibitor is also added in reflux line. Top section of the column
is also benefited from the injection of corrosion inhibitors mainly in the reflux line. These
inhibitors are high boiling point compounds and can perform satisfactorily at higher column
top temperature also. The amount of inhibitor injected depends upon the type of inhibitor
used and is generally specified by vendor. Adjustment is made by operating personnel
depending upon iron contents in the reflux drum water. Inhibitors are filling organic
compounds which cover entire metal surface of the system with a thin film. This prevents
contact of corrosive water with metal surface.
Demulsifier is added to the crude to break the water-crude emulsion. Water-crude emulsion
behaves like a single phase and does not get separated easily. Demulsifier helps the process
and ultimately in Desalter vessel water is separated out. Demulsifiers are surface activating
agents and acts on interface surface tension of crude and water emulsion.
6.7.1 CAUSTIC INJECTION SYSTEM
Caustic is received at unit battery limit either from MEROX or from Power Plant-I. There
are two caustic solution vessels in the unit 11-V-07 A/B. Concentrated solution is received
in these vessels from unit battery limit and then diluted to 5 Beo. Each vessel is provided
with service water connection for dilution and 2” plant air connection through spargers for
agitation and mixing. Vent, level gauge and overflow lines are also provided on each tank.
There is also a provision of sample point on each drum. Caustic solution is pumped by 11-
P-13 A/B/C to the following destinations
1. Crude charge pump suction
2. Downstream of Desalter through a vortex mixer 11-X-01.
The injection pumps are metering pumps which give a maximum discharge pressure of 15
kg/cm2 g. Caustic injection rates can be varied from 0 to 75 lph, by varying the stroke of
the pump. The rate of injection can be measured by using the graduated cylinder provided
on the pumps
6.7.2 DEMULSIFIER INJECTION SYSTEM
The chemicals that are used as DMF come under the trademark names EC2040A and
Embreak. De-emulsifier chemical is received in drums and is pumped into the De-
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
emulsifier vessel using a pneumatic pump. This is further diluted with water in the De-
emulsifier vessel in the ratio of 1:3. De-emulsifier injection pumps (11-P-16 A/B) takes
suction from the de-emulsifier vessel and is injected to the suction header of the crude
charge pumps 11-P-01 A/B. The injection pumps are metering pumps which give a
maximum discharge pressure of 15 kg/cm2 g. De-emulsifier injection rates can be varied
from 0 to 16 lph, by varying the stroke of the pump. The rate of injection can be measured
by using the graduated drawdown cylinder provided on the pumps.
6.7.3 NEUTRALISER INJECTION SYSTEM
A battery of liquid Ammonia cylinders is provided for meeting Neutraliser requirement.

Ammonia gas is drawn from cylinders at reduced pressure into Ammonia solution vessel
(11-V-06 A/B). A rotameter 11-FI-601 indicates Ammonia gas consumption. The
cylinders are connected to a common manifold. A pressure gauge (11-PG-601) and a PSV
(11-PSV-601) are provided on the Ammonia collection common manifold. Ammonia
solution vessel is a vertical vessel with a water seal on its vent to prevent escaping of
Ammonia while preparing solution. Water seal will blow off during excess pressure build
up in the vessel indicating the saturation of Ammonia in the solution. The Ammonia
solution prepared is injected by ammonia solution dosing pumps 11-P-14 A/B/C to
following destinations:
To Atmospheric Column Top (Vapour line) through rotameter 11-FI-602
To Atmospheric Column Top Reflux line through rotameter 11-FI-603
Ammonia (10% soln) dosing rate is normally 10 lph for both the sections. The injection
pumps are metering pumps which give a maximum discharge pressure of 15 kg/cm2 g.
Ammonia injection rates can be varied from 0 to 20 lph, by varying the stroke of the pump.
The rate of injection can be measured by using the graduated cylinder provided on the
pumps
The neutralizer to the Vacuum Column overhead lines is supplied by 12-P-08 A/B, at rates
varying from 0 to 20 lph to the Vacuum Column overhead vapour line.
6.7.4 CORROSION INHIBITOR INJECTION SYSTEM
Corrosion Inhibitor is received in drums and is pumped into the corrosion inhibitor vessels.
NALCO 5186 or equivalent filming amine solution (1% conc.) is prepared by diluting it in
Kerosene in 1:3 ratio in the Corrosion Inhibitor solution vessels. The solution is pumped by
11-P-15 A/B to the following destinations
Atmospheric Column overhead
Vacuum Column overhead system
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 6
PLANT NAME: CDU II
Chapter Rev No: 0
The injection pumps are metering pumps which give a maximum discharge pressure of 15
kg/cm2 g. Corrosion inhibitor injection rates can be varied from 0 to 10 lph, by varying the
stroke of the pump. The rate of injection can be measured by using the graduated cylinder
provided on the pump
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
CRITICAL CONTROL SCHEMES
7.1 ATMOSPHERIC SECTION:
It is important that the operation of crude distillation unit be conducted to produce products
of desired quality. At the same time appropriate controls should be exercised on certain
parameters to prolong the life of the equipment. The following discussion gives guidelines
about affect of the variables and measures to be taken to achieve desired results.
7.1.1 Desalter Operating Variables:
Only operating experience with desalter can determine optimum operating conditions. No
two crudes behave alike at the same desalting conditions. But, all are affected similarly by
change in desalting conditions.
i) Water Injection and Pressure Drop:
Water injection should be started only after the crude temperature reaches specified level and
power is switched on to the grid. Initially the injection rate should be limited between 2 to 6%
of crude flow rate and point of injection should be just ahead of the emulsifying valve.
The pressure drop across emulsifying valve should be adjusted to give the required degree of
desalting. The higher the pressure drop the more efficient the contact between the salt in the
crude and the injection water. Too high pressure drop will result in excessive emulsification
and poor separation of oil water, resulting in carry-over of water in the desalted crude. A
pressure drop between 0.2- 1.0 kg/cm2 is normally sufficient and the value has to be decided
based on oil content in effluent and desalter inlet and outlet salt content.
Additional emulsification can be obtained by injection of water before the feed pump suction
(11-PM-01A/B). Injection at this point results in maximum contact and also prevents the
sediments from settling in the exchanger tubes and fouling them. But care should be taken
such that the intense shearing agitation in the preheat train does not create so tight an
emulsion that cannot be resolved in the Desalter. The severe shearing effect due to the crude
pump impellers should also be considered here. The quality of water is a very important
aspect.
Optimum water injection rate and pressure drop across mixing valve should be established to
get the desired desalting of crude. Once this is done the conditions should be maintained
steady and should be varied only for changes in feed rate and feed qualities.
ii) Oil/ Water Interface level:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
The Oil water interface level should be kept below the centre line of the vessel. Incorrect
operation of the interface level controller can result in more water in desalted crude due to
less hold up time available for oil (high interface level) and more oil carry-over in brine-
water due to less hold up time available for water (low water level). Also too high an
interface level may put watery mixture up between the electrodes and cause them to short out.
iii) Desalter Vessel Pressure:
The pressure in the vessel should be maintained at about 10 to 11 kg/cm2g. A low pressure
will cause vaporization of crude and high pressure will result in chances of lifting of the
safety valve on the desalter. Sudden variation in the operating pressure may cause hunting of
the desalter level control valve with consequent fluctuation of the interface level. If there is
vaporization in desalter, it results in hazardous condition, erratic operation and loss of
desalting efficiency.
iv) Desalter Temperature:
Temperature is another important variable which affects oil water separation in Desalter.
Most crude oils have an optimum operating temperature range of 120 to 130°C. Lower the
temperature higher the viscosities of the oil which slows down the separation rate. As
conductivity of crude increases with temperature, operating temperature beyond the range
will lead to drop in grid voltage and high amperage which imposes limitation on good
separation. Excessive amperage will eventually cause the circuit breaker to open removing
the grid voltage and rendering the electrical system inoperable until the thermal relay is
closed. Moreover very high temperature may lead to vaporization of crude in the desalter.
v) Demulsifier injection:
Stable emulsions can also be broken by use of demulsifying chemicals. The amount of
chemicals required depends on the nature of the emulsion, type of crude and other operating
conditions like residence time, temperatures etc. Tests should be made to ascertain the
required chemicals injection rate for optimum operation of desalting unit.
vi) Voltage and Amperage:
The electrical panel houses pilot lights, a voltmeter and ammeter. The voltmeter gives the
voltage across the primary circuit of the transformer. The ammeter gives the current flow.
These meters give an indication of the performance of the grids inside the desalter. In case, if
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
crude/water emulsion is too tightly bound or if the interface level is too high there will be
increase in the amperage and the voltage will drop. Take corrective action to break the
emulsion or reduce the interface level.
For more details about the operation of desalter the vendors operating and maintenance
manual should be referred.
7.1.2 Heater Outlet Temperature and Column Pressure:
The quantity of crude oil vaporized during its passage through the heater depends on transfer
temperature and pressure at the flash zone of the column. In order to achieve proper recovery
of distillates little over flash is maintained, by keeping the transfer temperature slightly
higher. This flow is about 6% volume of crude flow rate. This also indicates the presence of
liquid levels in the trays down below the diesel draw off for avoiding dry operations of these
trays (nos. 7 to 11). Maintaining high over flash rate will result in more consumption of
energy. Heater outlet temperature is controlled by 11-TRC-301.lower temperature will not
give desired distillate recovery, bottom product RCO will be lighter and all side draw offs
will also be proportionate to lighter. Higher than normal temperature enhances cracking
possibility and at the same time specification of every product may not be met.
The pressure in the column is maintained by split range pressure controller11-PRC-409 A/B.
A low pressure aids in greater vaporization. All products will be heavier and there will be gas
loss from reflux drum. Higher than normal pressure will result in reverse effects. Efforts
should be made to operate the column at the designed pressure of 0.6 kg/cm2g at the reflux
drum. Adjust cooling water flow in the cooler 11-E-17 A/B/C/D/E/F/G/H in such a way that
there is total condensation and both the control valves (11-PV-409 A/B) of split range
controller remain shut.
7.1.3 Crude Column Top Temperature:
The column top temperature is controlled by regulating amount if overhead reflux through
11-FRC-403. Top temperature is continuously recorded by the recorder. Lowering of top
temperature will reduce FBP of naphtha and flash point of Heavy Naphtha. Too low a
temperature will start steam condensation at the top section of the column (as the dew point
will be reached), which may likely to increase rate of corrosion at the top. Raising the
temperature will increase FBP of overhead naphtha and IBP (flash) of Heavy Naphtha as well
as the product and CR draw off temperatures. In some cases, the temperature may go to such
a value that pumps design limit might be violated.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
Increasing the top temperature also increases the naphtha yield. For lighter crudes where
naphtha yield is high, increasing top temperature will increases naphtha yield further and
overhead drum 11-V-01 level may increase.
7.1.4 Pump around Flows (Circulating Reflux):
The pump around/ circulating reflux serve mainly in withdrawal of heat from the column and
to reduce the vapor liquid traffic in the appropriate section of the distillation column. There
are three circulating flows- Top Pump Around (TPA), KERO circulating reflux and diesel
circulating reflux. These flows are respectively controlled by flow meters 11-FRC-
404/405/408. The return temperature is maintained by operating the respective exchangers.
Return temperature are indicated by 11-TI -414(TPA), 11-TI-413 (KERO CR) and 11-TI-
412(Diesel CR). A high TPA flow will result in decrease of overhead reflux and affect the
quality of light naphtha. The overhead condenser duty will come down as there will be
correspondingly less O/H product. Similarly a high KERO CR flow will tend to lower the
plate temperature of heavy naphtha and kerosene draw off resulting in lighter product in these
trays. The gap between naphtha and kerosene will decrease.
Likewise a high diesel CR will tend to lower the draw off temperature of kerosene and diesel.
Increase of circulating reflux will result in higher crude preheat temperatures by greater
recovery in heat exchanger train.
7.1.5 Product Withdrawal Temperature:
The withdrawal temperature of a product from the column influences the end point of the
product. This is determined by quantity of the product withdrawn from the stripper. An
increase in withdrawal rate of the side stream increases the withdrawal temperatures and the
end point of all side stream lower down the column unless withdrawal rate lower down the
column are reduced correspondingly. For example, if kerosene withdrawal rate is increased,
the internal reflux in the trays below the draw off tray will be reduced which will lead to flow
of heavier vapors above the tray. This increases the end point of kerosene. If diesel
withdrawal rate is not reduced to maintain its plate temperature, its initial boiling point (flash)
will go up.
Similar reverse action takes place when withdrawal temperature is lowered by reducing the
quantity of withdrawal.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
7.1.6 Stripping Steam:
i) Atmospheric tower stripping steam:
At 10.5 kg/cm2g pressure and 350 °C, superheated steam is used to strip lighter fraction from
the reduced crude in the lower part of the crude tower. Design steam rate is about 4585 kg/hr
for Basrah crude. This is assumed to be optimum rate for economical stripping and should not
be varied much. Lowering the rate below the optimum may leave some lighter component in
the reduced crude and is undesirable. Exceeding the design rate might cause entrainment of
reduced crude into the diesel because of excessive vapor velocity and also will overload the
over head condenser system. The flow of steam controlled by 11-FRC-401
ii) Stripping steam in Heavy Naphtha, Kerosene and Diesel strippers:
The initial boiling points and flash points of heavy Naphtha, Kerosene and Diesel products
are controlled to some extent by varying the stripping steam rate to stripper 11-C-02/03/05
respectively. Steam at 10.5 kg/cm2g and 350 °C used for these strippers. Steam flows are
indicated by 11-FI409/11-FI-408/ 11-FI-407 and regulated by respective control valves.
It is advisable not to exceed the steam flow rate of its designed value viz. Heavy naphtha
stripper 444 kg/hr. kerosene stripper 1496 kg/hr and diesel stripper 1906 kg/hr, as this will
tend to lift some of the high boiling materials. In case if the desired flash point could not be
reached by designing rate of stripping steam, the draw off temperature at the product just
above it to be increased to enhance its flash.
7.1.7 Corrosion Control of Overhead System of Distillation Column:
Hydrochloric acid formed from the hydrolysis of salt present in the crude and hydrogen
sulphide formed dissolved in the crude (formed from the dissociation of heavy sulphur
compounds present in crude), goes to the overhead system. Both form acid solutions which
are very corrosive. Measures must be taken to overcome their effects.
The overhead system including condensers and reflux drum are made of carbon steel. Only to
protect this section caustic ammonia solution and corrosion inhibitors are added at the
following points:
Caustic injection:
1. Suction of crude booster pump i.e. ahead of desalted crude preheat trains.
2. After the preheat trains before booster pump 11-PM-02A/B suction
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
Ammonia injection:
1. Suction of crude booster pump ahead of desalted crude preheat train.
2. Column top reflux line.
3. Crude column overhead vapor line.
Corrosion inhibitor injection

The idea of injecting caustic and ammonia at the outlet of Desalter is for better mixing of
these chemicals with crude and neutralizes the acids/acid salts mainly HCl and H2S as soon
as it is formed(120 °C and above). Chance of H2S formation at this temperature is remote.
The reaction product is sodium and ammonium salts goes along with the reduced crude. The
balance acids and acids gases if any will go up to the overhead system where ammonia or
ammonium solution is injected either along with reflux or in the overhead vapor line fro
neutralization. Amount of ammonia should be controlled in such a way that pH of reflux
drum sour water remains around 6.0 to 6.5. Injection of caustic and ammonia at the outlet of
Desalter should be maintained in such a way that the salt formation should be low in the
overhead which might scale up the overhead condensers tubes.
A slightly acidic condition of the overhead system is desirably to keep ammonium salts in
solution, which if precipitates would foul and plug the condensers.
Corrosion against slightly acidic condition is minimized by adding corrosion inhibitors in the
overhead line. The inhibitor is also added in reflux line. The amount of inhibitor injected
depends upon the type of inhibitor used and generally specified by vendor. However, slight
adjustment is made by operating personnel depending upon from content in the reflux drum
water. These inhibitors are filming organic compounds (amines) which covers entire metal
surface of the system with a thin film. This prevents contact of corrosive water with metal.
Top section of the column is also benefited from the injection of inhibitors mainly in the
reflux line/ these inhibitors are high boiling compounds and can perform satisfactorily at
higher tower temperatures.
7.2 STABILIZER TEMPERATURE AND PRESSURE:
Stabilizer removes the majority of butane and lighter hydrocarbons from the naphtha stream.
These are recovered as overhead LPG product. High top temperature will make overhead
product heavier, even pentanes may be carried into LPG, making it off-spec. Lower
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
temperature will reduce LPG, make. Vapor pressure of LPG may go beyond the specified
limit if top temperature is too low.
Bottom temperature if too low will result in higher than allowable vapor pressure (RVP) of
naphtha and at the same time it will reduces LPG make.
Low pressure in the column will cause higher amount of hydrocarbon compounds (propane
and butanes) to escape into fuel gas system. This has got similar affect as that of higher
temperature in the column. The RVP of naphtha has to be controlled by the re-boiling and the
LPG spec has to be obtained by varying the top pressure and reflux.
The stabilizer pressure has to be maintained at constant value and there should not be drastic
changes in the parameters affecting the stabilizer pressure. It has to be ensured that gas
generation does not fluctuate drastically because that will yield in disturbance of fuel gas
header pressure and may result in flaring and vaporization.
7.3 VACUUM SECTION:

The following variables of the vacuum column influence the quality of the products and
should be controlled to meet the product specifications.
7.3.1 Transfer Line Temperature:
The transfer line temperature is controlled by 12-TRC-133 on the outlet of the vacuum
heater, and should be adjusted to maintain the flash zone temperature around 395 °C, this
temperature determines the degree of vaporization and the level of heat in the liquid vapor
mixture, entering the vacuum tower for fabrication. This temperature will be varied
depending on the quantities of the desired distillates. But the furnace outlet temperature
should not be allowed to go beyond the designed limit of 415 °C after which the degree of
cracking increases rapidly. Detrimental effect of cracking or coke deposition on heater tubes,
transfer line and bottom line sections. It also increases quantity of non-condensable going to
the overhead system. The cracking can also have a detrimental effect in the curing qualities of
asphalt. Too low a transfer temperature will result in lower yields of vacuum distillates and
also the vacuum residue from the column becomes lighter.
7.3.2 Vacuum Column Pressure:
The column top pressure is controlled by 12-PRC-306 which recycles some non-
condensables to the ejector 12-J-01 A/B/C inlet line. The top pressure should be maintained
around 7-9 mm Hg absolute. Increase in pressure will result in reduced yield of vacuum
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
distillates and may lead to cracking of the feed. Reduction in top pressure further may result
in carryover of LVGO into the overhead system. The lower the pressure, the higher is the
feed vaporization and higher is the distillates yield.
7.3.3 flash zone pressure and temperature:
It is of paramount importance to maintain a high vacuum and temperature at the flash zone
with in the prescribed limit to obtain maximum yield distillates. The designed flash zone
pressure is 24 mm Hg and temperature 395 °C. Fluctuation of vacuum will affect the product
quality adversely besides producing mechanical stress on column internals. Increasing the
flash zone temperature will result in greater yield distillates but cracking possibility is
enhanced. If for any reason, vacuum starts falling sharply, firing in the heater should be
reduced to bring down temperature of feed.
7.3.4 LVGO system:
The LVGO system is a combination of LVGO product, LVGO circulating reflux and internal
reflux for HVGO packing. The circulating reflux is sprayed over the LVGO packing through
a distributor. This stream is taken from the column and a part of LVGO after exchanging its
sensible heat with crude in 11-E-07 and cooled in coolers 11-E-22/22A in parallel, it is then
returned at a temperature of 65 °C to the column (12-C-01) under flow controller 12-FRC-
205 to maintain column to temperature of 80 °C, Because of crude throughput maximization,
it was observed that the Vac. Column temperature was frequently crossing the desired
temperature ultimately resulting in under control, LVGO CR from 11-E-07 outlet is modified
accordingly and routed to 12-E-12 A (top cooler), the outlet of 12-E-12 A routed to 11-E-
22/22A in parallel. Increasing the reflux will reduce the top temperature which will simply
increase the energy consumption. Reduction in reflux rate will increase the top temperature
that will overload the ejector and increase the slop production thereby losing LVGO yield.
The internal reflux to HVGO packings from LVGO draw off tray is maintained by diverting a
part of the LVGO from 12-PM-04 A/B pump discharge. This flow is regulated by 12-FRC-
201. The LVGO product withdrawal rate is regulated by 12-LIC-205, which controls the
LVGO level. LVGO rundown flow is indicated by F2403R. LVGO draw off temperature is
213 °C. the draw off temperature as well as LVGO product rate can be varied by increasing
or decreasing either LVGO internal reflux or HVGO circulating reflux. Increase in reflux
means reduction of LVGO draw off temperature and LVGO product flow rate and vice-versa.
A software switch is provided fro LVGO system when it is being routed to either
HVGO/LDO. When the switch is kept in position 1, LVGO level will be controlled by its
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 7
PLANT NAME: CDU II
Chapter Rev No: 0
own LVC (LI2205). When the switch is kept in position 2, LVGO level i.e. LI2205 will be
cascaded with FR2404 (i.e. LVGO to LDO/diesel).
7.3.5 HVGO Draw off:
The HVGO system is a combination of Wash liquid for wash zone packing, circulating reflux
(HVGO packing) and HVGO product. Heat transfer requirement is met through HVGO pump
around flow. A higher than the design pump around rate will result in overloading of packing
in HVGO. A pump around flow rate lower than the requirement will result in carry-over of
heavier ends to LVGO section.
If the withdrawal rate is lower than the design it will result in lower draw off temperature,
reducing recovery of HVGO. Higher rate of withdrawal will result in increased tray
temperature. This may lead to carry-over of asphaltenes to HVGO. The wash liquid is given
to the wash zone packing for avoiding chocking of the packing area because of heavy
asphaltenes. The chocking of the packing zone would result in higher differential pressure
across this zone and this will adversely affect the column performance. About 45 m3/hr of
HVGO is normally supplied as wash oil, the flow of which is regulated by 12-FRC-202. An
increase in wash oil flow will reduce the carryover of asphaltenes in HVGO stream. More the
desired quantity of this stream may adversely affect the quality/yield of Vacuum residue.
Less quantity of Wash Oil may result in the carryover of heavy asphaltenes into HVGO
stream.
7.3.6 Slop Distillate & Recycle:
The object to provide slop recycle to furnace flow is to get desired over flash so as to ensure
proper recovery of distillates. A higher recycle rate will unnecessarily increase the energy
consumption. Recycle + slop distillates are draw from the chimney tray below the wash zone
packing. The draw-off rate of slop distillate product is regulated by 12-LIC-203 which
controls the level in the draw off tray. The recycle stream flow rate is controlled by 12-FRC-
102. Recycle rate at normal throughput is about 12.0 m3/hr.
7.3.7 Quench:
Quench flow is a slip of vacuum residue at 250 °C obtained after exchanger 12-E-03 and the
flow is regulated by 12FRC-204. Its temperature is indicated by 12-TI-202. The purpose of
providing quench is to prevent, coke formation at the bottom of the column by quickly
cooling Vacuum Residue from 395 °C to 350 °C. A lower temperature than this, i.e. higher
quench is not wanted because of disproportionate increase of energy loss, whereas lower
quench flow may lead to coke formation due to cracking.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 8
PLANT NAME: CDU II
Chapter Rev No: 0
DESCRIPTION OF DCS
NOTE: Manual copy not yet provided by Instrumentation.
Standing Instruction for Improving Aesthetics of MOI Control Room : SI 30
1.0 Objective:
DCS Stations of CDU-I/II/III, FCCU-I/II, MEROX, PP-II,TPH,DHDS,DHDS-SRU

are in MOI Control room. To improve and maintain MOI Control room Aesthetics, Standing
Instructions have been developed.
2.0 Background:
VIP’s frequently visit the MOI Control room where DCS stations of CDU-
I/II/III,FCCU-I/II,MEROX,PP-II,TPH,DHDS,DHDS-SRU exist. The MOI control room
needs to be clean and maintained properly. The standing Instructions have been prepared to
improve and maintain the aesthetics of the MOI Control room.
3.0 Responsibility:
The overall responsibility to implement these guidelines rests with the unit Shift-in-
charges at DCS stations of CDU-I/II/III, FCCU-I/II,MEROX,DHDS,DHDS-SRU,TPH,DCS
–Instrumentation group. Section Head of respective locations to ensure compliance of the
guidelines.
4.0 A) The following guidelines to be followed by Operations for improving the aesthetics
of MOI Control room:
a) Eatables are not allowed inside the MOI Control room.

b) Footwear are not allowed inside the MOI Control room.
c) One month old TOB’s only are to be kept in MOI Control room. Old documents, files
etc are not allowed inside.
d) 2 chairs are to be kept at each DCS Station.
e) The following Registers only need to be kept in MOI Control room at DCS Stations.
i) DCS TOB
ii) Summary book
iii) C/V Parameter data bank
iv) Shift Event review register
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 8
PLANT NAME: CDU II
Chapter Rev No: 0
DESCRIPTION OF DCS
v) Stack Analyzer register

vi) Trip interlock bypass register
vii) DCS Alarms setting register
viii) Tracking register for ensuring all control valves remain in ‘AUTO’ or
‘Cascade’
ix) Permits entry register
f) Important telephone nos, Trips data, Standing Instructions etc need to be kept in a file
properly.
B) The following guidelines are to be followed by Maintenance-Instrumentation for

improving the aesthetics of MOI Control room:
a) Instrumentation group to ensure proper cleanliness at DCS Panels and in the entire MOI
control room.
b) While laying new cables/new fittings inside MOI control room, it should be in proper
way without affecting the aesthetics of the room.
c) For any new addition of items, review is to be carried out and permission to be taken
from Division Head –Production block.
All unused/old items belonging to Instrument group are to be removed from MOI after
replacement with new items.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
DESCRIPTION OF ADVANCED PROCESS CONTROLS

In a process plant the basic operating parameters measured in the field are flow, temperature,
pressure, level etc. Plant operators depend on these measured parameters for achieving
control on plant performance. However, qualitative control cannot be directly achieved to the
fullest potential by the operator as there is no online indication for product quality. Operator
has to necessarily rely on feedback from quality control laboratory and individual operating
experience. Operators with different levels of experience operate the plant differently, at
times resulting in a possible loss of optimum plant performance.
Safety of plant personnel and equipment is paramount in a running plant. Yet the plant must
not run under ‘over safe condition’ which results in the loss of certain achievable benefits. In
a plant, various constraints appear for short durations and practically it is not possible for the
operators to keep track of each and every constraint and take action on a real time basis. APC
takes care of such a situation by taking small actions at a time and keeping strict control on
various constraints to ensure they are not violated while optimizing the plant performance.
With the advent of high powered computers it has become possible to make available, critical
calculated parameters using empirical equations, scientific relations and basic plant
parameters on a real time basis. Calculated parameters such as Reflux ratio, Dew point
margin etc., and inferential like SRN RVP, HVGO 95%, HD Flash etc., can be used directly
as controlled variables for improving the plant performance.
Advanced Process Controllers maximize or minimize a given variable for attaining the
defined benefits in the plant. Variables to be maximized and minimized are identified and
limits are set for each variable. A limit is the maximum or minimum value of a variable
beyond which it becomes unacceptable for ensuring favorable unit conditions. Predictions are
made for each variable and the controller downloads the desired move to the DCS. APC
control encompasses the benefits of feed maximization, better and sustained product quality,
reduced energy consumption, safety and less of manual intervention from DCS operating
personnel.
9.1 PROFIT CONTROLLER APPLICATIONS:
Profit controller improves production performance while promoting operational flexibility.

The generic structure of Profit controller supports its application to solve the following
problems in process plants:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.1.1 Feed maximization:

Many times process constraints can be better managed to result in higher production rates.
DCS operators typically do not have time to closely monitor the symptoms leading to a
constraint. Profit controller being a multivariable controller, monitors the process frequently
and makes small adjustments to compensate for any changes in feed rate due to a constraint.
Extent of increase in feed rate depends on how conservatively the process was originally
operated.
9.1.2 Real time quality control:

Profit controller includes Profit Sensor Pro, a comprehensive easy-to-use data analysis and
inferential model development application. It simplifies the task of identifying and
developing relationships among process variables offering online capability that allows for
real-time quality control (Lab inferential). This allows tighter product quality control without
the long delays associated with lab analyses.
Accuracy of lab inferential is effectively maintained through the use of online model
updation with periodic laboratory feedback information. Improvement in quality is derived
from improved process stability, fewer process upsets and more consistent control across
operator shifts.
9.1.3 Optimization:
Profit controller provides a perfect framework for implementation of desired optimization
objectives. The built in model calculates the desired target conditions of the process and the
controller moves the process to the optimal resting conditions while still controlling the
process within the specified constraints. Lab inferential of products quality when included as
a controlled variable in the process model allows for optimization objectives, such as feed
maximization or product value optimization to occur.
9.2 APC NOMENCLATURE:
9.2.1 Controlled Variable (CV):

The process variables that must be maintained at some value or within certain limits, and
should be optimized are called as CVs. CV limits are defined by the operator and can be a
measured or calculated value. RMPCT controller tries to control and maintain the CVs within
the operator specified limits (HI & LO).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.2.2 Manipulated Variable (MV):

The “handles” that are adjusted to keep the CVs within limits (or at set points), and to
optimize the process. The controller always honors MV limits specified by the operator.
Manipulated variables can be a regulatory controller’s set point (SP) or output (OP). With the
help of MVs, RMPCT controller maintains the CV within limits.
9.2.3 Disturbance Variable (DV):

These are measured variables not under the control of RMPCT controller but have an effect
on the controller’s CVs. By predicting the future effects of the DVs on the CVs, the controller
can take action to prevent CV excursions before they occur. The DV’s provide information
for feed-forward control. RMPCT Controller only takes the PV of the DVs and takes
necessary action on the MVs so that the CVs are within limits.
Controller status (displayed on RMPCT graphics):
STATUS DESCRIPTION
INACTIVE Controller point is inactive. RMPCT is not tracking the CV’s, it is not executing
calculations and it is not controlling the MVs.
CONTROL OK Controller is running (without optimization)
INITIALIZING Controller is aligning itself with the current process conditions and running
integrity checks on points.
BLANK (Nothing Controller is receiving input from the process and making prediction
displayed) calculations, but there is no controller output.
SHEDDING Controller has been shut off and is shedding control to the configured regulatory
CONNECTIONS PID loops.
WAIT FOR Controller is waiting for background calculations to complete. Background
EXECUTION calculations are lower priority calculations.
HANDLING The controller is indicating that it has encountered competing control objectives
CONSTRAINTS and that bringing all variables within the constraints cannot be managed at the
current execution or cannot be managed within the prescribed horizon.
Caution: Competing constraints are usually temporary conditions, provided that
operating conditions have not changed since the controller was tuned.
OPTIMIZING Controller is running and the control objectives at the current execution have
been met. Controller is now attempting to optimize the process based upon
economic objectives.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
Understanding CV summary (displayed on RMPCT graphics)

In the controller graphic, when the CV summary is clicked on the graphics, certain CV
related fields appear whose significance is as follows:
Field Field type Default Description User notes

Access
CV # Read Only No Access The index of the
variable
CV Read Only Operator Description that Click the field to display the CV detail
Descripti characterizes the display.
on variable’s function
or location
Status Editable Operator Status of this Selecting the status allows you to drop a
variable GOOD, CV under control or take dropped CV
DROP, PRED, under control. The controlled can
CRIT, INIT, automatically drop a CV. Dropping a CV
WDUP or INAC. in DROP status means the CV will not
be used once the condition causing
DROP state clears.
Value Read Only No Access The value of the Dash displays when the source value is
CV at the current bad or unavailable for longer than the
execution. This can number of bad values allowed. Values
be the measured display in color:
process value or a Cyan= Displayed value within the limits
predicted value Yellow= Displayed value near the limits
Red = Displayed value violating the
limits
Future Read Only No Access Displays the future Values display in color:
predicted value Cyan= Displayed value within the limits
after three Yellow= Displayed value near the limits
measurement Red = Displayed value violating the
cycles plus delay limits
SS value - - Predicted steady
state value.
Lo limit Editable Operator Lowest end of Green up arrow displays when CV is
operating range. ramped up.
♦◊-Solid or hollow yellow diamonds
display when hard or soft limit constraint
is reached for a CV.
High Editable Operator Highest end of Green down arrow displays when CV is
limit operating range. ramped down.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
♦◊-Solid or hollow yellow diamonds

display when hard or soft limit constraint
is reached for a CV.
Set point Editable Operator The operating field Click in set point column to make entry.
of the CV Setting same Hi and low limits also
establishes a set point. Value is grey
when set point is in use.
Understanding MV summary (displayed on RMPCT graphics)

In the controller graphic, when the MV summary is clicked on the graphics, certain MV
Field Field Default Description User notes

type Access
MV # Read No The index of the variable
Only Access
MV Read OPER Description that Click the field to call the MV
Description Only characterizes variable’s detail display.
function or location
Status Read No Status ON, FFWD, HIGH, Whether the MV is dropped or
Only Access LOW, SERV, INIT, INAC. used as the feed forward value is
set on the MV process tuning
display or on the MV detail display
Value Read No Value of the MV at current Value shown is the OP or SP when
Only Access execution. status is ON. Otherwise it is the
PV.
Move Read No The size and direction of
Only Access change made to the
immediate downstream
controller at the last
execution
Future Read No Displays the future predicted Values display in color:
Only Access value after three Cyan=Displayed value within limit
measurement cycles plus Yellow=Displayed value near limit
delay Red=Displayed value violating
SS value Read No Predicted steady state value. limit
Only Access
Lo limit Editable OPER Lowest end of operating ▲Arrow displays when MV is
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
range. ramped up.

♦◊-Solid or hollow yellow
diamonds display when hard or
soft limit constraint is reached for a
MV.
High limit Editable OPER Highest end of operating ▼Arrow displays when CV is
range. ramped up.
Mode Editable OPER Control Mode: Either In operator mode, profit controller
RMPCT or Operator stops outputting changes to the
downstream controller.
Field is locked if the MV is
critical.
Critical or non critical is set on
MV tuning display or MV detail
display.
Critical Read No This column displays a “C”
Only Access if the value is critical
Understanding DV summary (displayed on RMPCT graphics)

In the controller graphic, when the DV summary is clicked on the graphics, certain DV
Field Field Default Description User notes

type Access
DV # Read No The index of the
Only Access variable
DV Read OPER Description that Click the field to call the MV detail display.
Description Only characterizes
variable’s function
or location
RMPCT Editable OPER Status GOOD, A critical DV has –C on its suffix. The
Status CRITIC, DROP or controller shuts down (OFF) when a critical
INAC DV goes bad. Selecting the status allows to
drop a DV in use or put in use a dropped DV.
Critical DV’s cannot be dropped. Non-
critical DV’s can be dropped if they go bad
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.3 CONTROL OBJECTIVES AND STRATEGIES
The advanced process control applications are designed to reduce variations of key unit
operating variables through model based predictive control, which includes feed forward
disturbance rejection. The prime objective of increasing overall unit profitability is achieved
by utilizing RMPCT in conjunction with supporting calculations and intermediate regulatory
controls. Supporting calculations are provided to supplement existing process measurements.
The intermediate regulatory controls provide a more stable foundation for implementation of
the multivariable control applications.
9.3.1 General Control Objectives:

• Provide stable operation of entire unit
• Maximize unit throughput
• Maintain product quality
• Increase run length of equipments by maintaining its guiding parameters
within limits
• Minimize energy & utility consumption (Fuel gas, Fuel oil and steam)
• Maximize the yield of valuable products
• Avoid extra safe operations and operate close to the safer limits.
9.3.2 Overall Control Strategy:
Based on the level of interaction among the variables and their respective settling time, four
different RMPCT controllers have been configured for the entire CDU-II unit. The variables
for the RMPCT controllers have been chosen to achieve the control and LP optimization
objectives as mentioned in the respective sections. The four controllers are as follows:
1. Atmospheric Section Controller- ADU2

2. Vacuum Section Controller- VDU2
3. Naphtha Stabilizer Controller- NSU2
9.3.2.1 ADU2 Control Strategies:

Atmospheric section controller has a total of 30 CVs, 21 MVs and 1 DV. The variables for
the Atmospheric section controller have been chosen to achieve the following optimization
strategies:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
• Atmos Heater Pass balancing:

The regulatory level control of the individual passes in cascade with the master flow
controller is broken and the individual pass flows are manipulated through the RMPCT
controller for achieving pass outlet temps balancing even while maximizing thruput.
• Throughput Maximization:
Total feed will be maximized subject to Heater Skin temperatures and desalter pressure
control valve opening. Ex-PFD crude flow FR1804.PV will be used as the tag for
maximization.
• SRN Maximization:
Un-stabilized Naphtha flow to Stabilizer will be maximized, subject to the SRN 95%.
• Heavy Naphtha Maximization:

Heavy Naphtha flow will be maximized, subject to Kero / ATF Flash point.
• Kero / ATF Maximization:

Kerosene will be maximized, subject to draw temp and Kero/ATF FBP (not a direct CV).
• HD Maximization:
The HD rundown will be maximized, subject to 95% Point and minimum over flash flow.
9.3.2.2 VDU2 Control Strategies:
Vacuum section controller has a total of 18 CVs, 9 MVs and 1 DV. VDU2 controller has the
following optimization strategies:
• Vacuum Heater Pass balancing:
The regulatory level control of the individual passes in cascade with the Atmos column
bottom level controller is broken and the individual pass flows are manipulated through the
RMPCT controller for achieving pass outlet temps balancing while maintaining atmos
column bottom level.
. Vacuum column top temperature Minimization:

Vacuum column top temperature will be minimized by regulating LVGO CR flow (FR2205).
• HVGO Maximization
HVGO will be maximized subject to HVGO 95% by regulating HVGO IR & CR flow
(FR2202 / 3).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.3.3.3 NSU2 Control Strategies:
The NSU2 controller has a total of 3 CVs, 3 MVs and 1 DV. NSU2 controller optimization
strategies include the following:
• LPG Maximization:
LPG will be maximized subjected to its C5 specification based on field weathering and
Stabilizer top PCT while maintaining control on SRN RVP.
9.4 APC START UP, SHUTDOWN & HANDLING PROCEDURE:
9.4.1 Putting the APC Controller ON:
i. Switch on the power to the Profit Viewer machine beside DCS. To login use User
name “administrator” and password for this user is “password” and press Enter.
ii. In the Profit Viewer machine open the ‘Profit Viewer’ Application, i.e. go to
Start>Programs>Honeywell HiSpec Solution>Profit Viewer (One can also use the
Shortcut of the same available in the ‘Profit’ folder on the Desktop)
iii. Ensure that the Controller Application is present in that window and its status is
“ACTIVE” (Controller status is there at the right end of the Profit Viewer Screen).
iv. If the Controller Application is not present, then click the drop down button in the
Program Applications & select Add Profit Viewer Remote Application. You will
see a window like this:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
a. Click on the drop down button ‘Select / Type The Name of the Computer where the
Application Runs’ and select the ‘CDU2APCSERVER’.
b. Then select the Controller (e.g. ADU2, VDU2 & NSU2) & then click Add, repeat this
for rest of the controllers to be able to view all in the Profit Viewer Window.
c. After the Controller Applications are added in the Profit Viewer machine, select one of
the controller (say ADU2) & click ‘View’, you will see a face plate like this:
d. Click Yes to view this Application .

If the Controller Application is present but its status is displayed as ‘Inactive’ then contact
APC Engineer. Controller can be placed in service only after it is made ‘Active’ by the APC
engineer.
e. Click WARM. This will change colour of WARM button to yellow & a face plate will
come. Click Yes to put the controller in WARM mode.
Why to put in WARM mode?

In WARM mode controller works like a simulated controller and the limits of all MVs &
CVs can be checked and set right before putting the controller ‘ON’. In Warm mode, move
size and steady state values can also be checked. Then each MV, CV, DV (one by one) can
be placed in RMPCT mode or DROP mode as desired by the operator.
In Warm mode, it is recommended to check whether controller is giving proper ‘Moves’ or
not and the future / steady state value is desirable or not.
f. After one minute the colour will change to cyan & the status appears as “WARM”
disclosing the SS Value (Steady State Value) and Moves.
g. Set carefully HI & LO Limits for each CV & MV and then observe the MV Moves.
h. Put the MVs (which show permissible moves) in RMPC mode from OPR mode (in the
extreme right hand side column). When MV1 is put on RMPC mode, following face
plate will appear:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
Click Yes; you will see the RMPC mode getting selected on the right hand side against MV1.
Note: At least one MV is required to be in RMPC mode before putting the total controller in
ON Mode. Otherwise the controller gets put off automatically.
i. Put the controller ‘ON’ (after carefully examining that all CVs & MVs high and low
limits are set properly, the ‘MOVE’ size as indicated by the controller against each MV
is acceptable and taking the CVs & MVs online).
j. Confirm that for all MVs, which have been taken into RMPCT, the status has become
ON in Profit Viewer and have gone to SPC mode in DCS.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
SHED MODES (required mode for placing in RMPCT):
• ADU2 – MV SHED MODEs:

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
VDU2 – MV SHED MODES:
No Tag Number Descriptions SHED MODE

1. FR2101.SV 12F01 PASS-A FLOW AUTO
2. FR2102.SV 12F01 PASS-B FLOW AUTO
3. FR2103.SV 12F01 PASS-C FLOW AUTO
4. FR2104.SV 12F01 PASS-D FLOW AUTO
5. TR2133.SV 12F01 COT AUTO
6. FR2201.SV LVGO IR FLOW AUTO
7. FR2202.SV WASH OIL FLOW AUTO
8. FR2205.SV LVGO CIRCULATING REFLUX FLOW AUTO
9. FR2203.SV HVGO CIRCULATING REFLUX FLOW AUTO
NSU2 – MV SHED MODES:
No Tag Number Descriptions SHED MODE

1. PR1501.SV STABILISER TOP PRESSURE AUTO
2. FR1501.SV STABILISER REFLUX FLOW AUTO
3. TR1501.SV STABILISER 3RD TRAY TEMP AUTO
Note: Before taking any MV on RMPCT mode, at the DCS level the same need to be in the
correct (SHED) mode of operation (either Manual / Auto / Cascade mode). If any MV is not
in its pre-defined shed mode while taking in RMPCT mode, the MV’s status in the controller
graphics would appear as ‘INIT’ (initialization).
9.4.2 Putting the APC Controller OFF: Any controller can be put ‘OFF’ from the
‘Profit
Viewer Graphics’ as well as from DCS control panel.
• From Profit Viewer Graphics:
a) Click on the OFF tab (at top row). A face plate will appear:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
b) Click “Yes” to switch the controller OFF. It will take few seconds to get switched off.
• From DCS (using Master Switch):

In case of any communication failure between APC server and client, a master switch is
configured in the DCS to put OFF individual APC controllers as well as all 3 together.
Under normal circumstances, it is always recommended to switch off APC controllers
from APC client PC. However, this master switch can be used to put OFF all the three
controllers at a time (like in case of emergency or any process upset when Operator
wants to take control in his hands).
1) The Master switch schematic name in DCS is GR0293.

2) To switch OFF the controllers, go to the above schematic page & click on fields as
required by the DCS supervisor.
DCS schematic page showing the master switch is given below.

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
APC SCHEMATIC IN DCS GRAPHIC PAGE GR0293:
9.4.3 Crude Switch Program:
HPCL CDU – II handles Crude Switch once in 2-3 days. During this, operator has to reduce
the feed and then switch tanks. Whenever crude switch is taking place from Low Sulfur type
to High Sulfur type and vice versa, main operating parameters which gets changed are the
feed rate and 11F1 COT. In order to facilitate automatic change / shift in these important
operating parameters, an APC level program has been developed. This Crude Switch utility
(program name is CR_SWITCH) will help the DCS Panel operators in changing the Feed and
11F1 COT in a timely and smooth manner. DCS graphic (GR0293) is prepared to help panel
operators to change the limits according to requirement.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
• Handling the crude switch program:
Procedure:
a) First check the new limits (Low and High) one wants the Feed and 11F1 COT set
values to go in the DCS graphic page GR0293. If required, change the limits, by
clicking on the targets provided.
b) Prior to feed tank switch, to reduce the feed rate, start the program exactly 60 minutes
ahead of tank switch. Program will reduce the feed rate gradually within that period
keeping atmospheric column operation smooth.
c) COT will start changing after a time lag of 10 minutes (after the crude switch program
was made active) and will be changed gradually to the new limit in the next 50
minutes by the program.
d) Once the plant is stabilized at the lower feed rate, feed rate shall be raised upto the
potential available, either through APC in the normal way or by Crude Switch
program once again by setting proper target values as explained above
e) If the panel operator wants to intervene in-between (in case of any process upset
during the crude switch program run) he may do so by stopping the program.
f) Keep wide limits for all MVs in controllers, as controller has to take action
accordingly to maintain column profile as much as possible.
g) Specially, pass flows need to be made wide in controller limits all the time, as 11F1
pass flows control the Feed and 12F1 pass flows are controlling Atmospheric column
bottom level.
h) Don’t change any of the limits of Feed and 11F1 COT when this program is active. If
any of these limits are changed in between, program will take it as an OFF request
and set itself off.
i) Don’t set the program active for less than 30 M3/hr feed change, as program will take
60 minutes irrespective of the amount of change. This level of change can very well
be done from controller limits directly.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
UNDERSTANDINGMANUAL LAB-UPDATE:
Lab-Update has to be done for validating the inferential. This can improve the quality of
future predictions.
9.5.1 How to do Lab-Update?
i. In the Profit Viewer machine open the Profit Viewer Application and then open the
“Lab update”, i.e. go to Start>Programs>Honeywell HiSpec Solution>Lab Update
(One can use the Shortcut of the same available in the Desktop in the Profit folder).
ii. Type “CDU2INF” in the “Connect to Application” field & click Connect.
iii. Enter the Date and time of actual lab sampling for each individual inferential.
iv. Click the corresponding cell under Lab Value and a face plate will appear. Enter the
lab reported value correctly & click Enter.
v. After few seconds, it updates and returns with Average at Sampling Time
(inferential predicted value) and Calculated Bias, press Enter.
vi. After this again a Face plate will come & will show the Delta Bias. Click Enter to
update the bias.
Notes:
• For lab bias updation it is important to enter exact sample collection time (Do not
round off) and correct lab value.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
• If Operator feels LAB value is not correct then better not to enter. Wrong data entry /
unreliable values will eventually drift the calculation from the actual and future
predictions will deteriorate affecting the controller’s performance. If by mistake
wrong value was entered, do not update the bias.
vii. For continued better prediction it is advisable to do the lab update in the order of time.
For example, Nov 28th 1100 hrs sample should be entered first, Nov 28th 2300 hrs
sample second, Nov 29th 1100 hrs sample third etc.
9.5.2 Automatic Lab-Update:
Timely lab updation helps in improving the accuracy level of inferential predictions which
are used as Controlled variables in APC for meeting the desired objectives. To improve the
inferential predictions, automatic lab updation feature has been enabled through an APC level
program. Every 5 minutes, CDU-II APC server checks for any new value being entered in
LIMS by QC Lab crew and automatically updates the corresponding inferential.
The normally expected values (low and high) for each of the product property have
been defined and values in violation of these limits will not be updated. Similarly non-
numeric values will not be considered for updation.
9.6 PROCESS PARAMETERS TRENDING:

i. Trending & plotting- There are various parameters related to MV/CV/DV/Controller
being historized in the Embedded PHD archive files. To plot a particular
MV/CV/DV/Controller parameter one has to open Process Trend Application
(Start>Programs>Honeywell Uniformance Desktop> Process Trend).
ii. For trending in the client machine it will ask for, Server name. The server name in
the client machine is IP address “10.6.0.92”.
iii. To add the Tag or plot definitions, press F12 or go to Plot> add/modify Tag or plot
definition. Now importing of the Tags for trending can be done from tag explorer or
by manual entry. Maximum eight parameters can be plotted in a file, the file can be
saved with the “.plt” extension.
iv. Once a “.plt” file is saved, all its settings (Tag name, HI, LO limits Plot format) will
remain as it is, which can be used at any moment.
v. To change the plot definition or to add / remove tags, press F12 or by right click and
select appropriate option. The plots characteristics can be customized by pressing F9
key or by right click. Hair line can also be introduced by pressing F11 key or by right
click.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.7 OPERATING INSTRUCTIONS:

9.7.1 General:
• Before making a controller ON check whether the controller is Active or not.
• Check HI / LO Limits of all MVs & CVs. It is recommended to put MV limits relaxed
and CV limits as per specifications & requirements.
• It is always recommended to make the controller WARM before making it ON.
• For taking any MV in RMPCT mode, ensure that it is in desired DCS (Shed) mode of
operation (Auto / Manual / Cascade). When any of the four controllers is put OFF by an
operator, all the MVs in that controller will go back to their normal DCS mode (Shed
Mode) of operation.
• At least one MV has to be in RMPC mode to make the controller ON. If not the
controller will automatically get switched OFF and all the MVs in that controller will
go back to their normal DCS mode (Shed Mode).
• Value of any parameter on the RMPCT graphic page in CYAN color means that
parameter is within the low & high limit (Normal).
• Value of any parameter on the RMPCT graphic page in YELLOW color means that
parameter is touching the low or high limit including its soft/ hard limits.
• Value of any parameter on the RMPCT graphic page in RED color means that
parameter is violating the set low or high limit.
• In the event of failure of any instrument or requirement for checking any instrument:
Check whether that instrument is contributing (directly or indirectly) to any MV / CV
/ DV in any of the controller (ADU2 / VDU2 / NSU2). This can be checked from the
‘Gain Delay’ graphics page or MV / CV/ DV tags list.
Check whether that instrument is contributing (directly or indirectly) to any calculated
or inferential variable. This can be checked from the list of input tags for calculated &
inferential variables (chapter: 6.0).
Accordingly, all the related MV, CV, DV, Inferential & Calculated tag need to be
taken out from RMPCT mode. After restoration of normalcy of the instrument, the
concerned variables can be placed in RMPCT mode again.
• If any of the CV including calculated tag & inferential tags and DV value goes bad (No
value; ------) the controller drops that CV / DV automatically. If any of the source tag
becomes bad, the calculated / inferential value also goes bad and gets dropped
automatically. However if any of the CV or DV shows erratic / random values, then it
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
does not get dropped automatically and it is advisable to drop that CV / DV manually
immediately.
• When a MV is dropped from RMPC mode, operator has to decide whether he wants to
put that MV in Service mode or in Feed forward mode. Feed forward mode is useful for
prediction purpose provided the indication is healthy, whereas keeping in Service mode
will not give any information of that MV to the controller for any calculation. However
for safety reasons the default mode for "When MV In Manual" option has been
configured as “DROP” to avoid unnecessary moves (when the MV is checked by
Instrumentation without putting in drop mode) based on FFWD.
• During communication failure or to put off all three APC controllers at a time use the
Master Switch configured in the DCS. Operator can call the schematic GR0293 to
access the master switch.
• When any of the three APC controllers is Switched OFF due to any reason, an alarm
will come on the DCS panel saying the respective APC controller is switched OFF.
• Never put the APC controllers ON from the DCS Schematic page. This is to avoid
possible upset / disturbance in the unit. Instead operator must check the MV / CV limits
on the profit viewer before putting controller ON.
• Periodically check for automatic lab updation of inferential. In case of discrepancy,

inform Technical-APC group.
• If any of the CV has status as WDUP, it means that the CV cannot be controlled within
the set limits as its MV’s set low / high values are limiting.
• If any of the MV shows status as HIGH or LOW, check its output at the DCS level for
locks if any & take proper actions to bring its output into the floating range.
• When any MV is taken into APC, it will go to SPC mode in DCS. There will not be any
mode change for CVs & DVs.
• If the communication between APC machine and DCS gets broken, all MVs in the
RMPCT controllers will go back to their Shed Mode.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
9.7.2 Controller Specific:
• ADU2 Controller:
a) For taking feed maximization and pass temp balancing strategies under APC control,
ensure that FR1804 is in manual and pass flows are in Auto. Under APC control,
furnace pass flows (in SPC mode at DCS) will be manipulated for achieving these
objectives. When APC controller is switched off, pass flows will go to AUTO (shed)
mode and FR1804 will remain in manual. DCS supervisor to ensure that FR1804 is
taken back into Auto with pass flows in Cascade mode (normal regulatory control).
b) Product flows in each rundown line are considered as individual MV. Make sure that
Product lines, which are not in operation are kept out of APC (i.e., MVs are made
OFF). e.g., when only Kero rundown, FR1203, is in line, then keep the other MV
FR1204 (Kero to Diesel) OFF from APC Controller and set proper limits for FR1203.
In general, if there are more than one r/d MV for the same product, ensure that the one
that can be manipulated is in APC. Keep the other MV in Auto.
c) In the controller, along with product inferential like 95% points, Draw Temperatures
are also considered as CVs. Whenever inferential is predicting better, make limits for
draw temperature relaxed, so that these CVs does not have any conflict with the
inferential limits.
d) If 95% inferential value is showing bad or wrong value, then make that CV off and
make draw temperature limits tight. One can control the product quality with draw
temperature in such a situation.
e) Dew point inferential is based on empirical equation and hence it is not always
perfect. Keep limits considering 4-5 degree positive offset.
f) If any of the skin (or Arch) temperatures are showing bad or wrong values, the
maximum skin (or Arch) temp CV shall be kept dropped and inform APC group. The
particular tag will be dropped from the calculation and the CV can be taken back
inline. The maximum skin (or Arch) temperature will be calculated based on
remaining indications. Make sure, that the tag is taken back inline by APC group
when the indication is attended and value returned to normal range.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
• VDU2Controller:
a) For taking pass temp balancing strategy under APC control, ensure that LR1401 is in
manual and pass flows are in Auto. Under APC control, furnace pass flows (in SPC
mode at DCS) will be manipulated for achieving this objective. When APC controller
is switched off, pass flows will go to AUTO (shed) mode and LR1401 will remain in
manual. DCS supervisor to ensure that LR1401 is taken back into Auto with pass
flows in Cascade mode (normal regulatory control) and Atmospheric column bottom
level under control.
b) In the controller, along with product inferential like 95% points, Draw Temperatures
are also considered as CVs. Whenever inferential is predicting better, make limits for
draw temperature relaxed, so that these CVs does not have any conflict with the
inferential limits.
c) If 95% inferential value is showing bad or wrong value, then make that CV off and
make draw temperature limits tight. One can control the product quality with draw
temperature in such a situation.
d) If any of the skin (or Arch) temperatures are showing bad or wrong values, the
maximum skin (or Arch) temp CV shall be kept dropped and inform APC group. The
particular tag will be dropped from the calculation and the CV can be taken back
inline. The maximum skin (or Arch) temperature will be calculated based on
remaining indications. Make sure, that the tag is taken back inline by APC group
when the indication is attended and value returned to normal range.
e) As vacuum column is normally faced with instrumentation problems because of
viscous fluid, get the maintenance and instrument rectification on time for better and
reliable APC
• NSU2 Controller:
a) In the column, both Top Temperature and bottom temperature are controlled. For
column stability and LPG yield / quality, keep the bottom temperature relaxed and
control top parameters tight.
9.8 APC MONITORING & MANAGEMENT:
9.8.1 Role of DCS supervisor :

1. Strictly follow the APC startup, shutdown and operating instructions given in
Section 7.0 & 8.0.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 9
PLANT NAME: CDU II
Chapter Rev No: 0
2. When APC is ON, the RMPCT controllers will be downloading the set point for
MVs to DCS in order to keep the CVs within limits. DCS supervisor needs to
monitor the condition of all variables in all the controllers and functionality of
RMPCT. Following the color coding (Cyan for normal; Yellow for operation on
limits & red for operation beyond limits) will make it easier for real time
monitoring.
3. Check for periodic automatic lab updates of inferentials and if it is not done, do it
manually.
4. The profit viewer computer kept at the DCS is directly used for controlling the plant
operation. From system security point of view following points need to be ensured:
- The computer should not be used for purposes other than APC.
- No other software should be downloaded on to this computer.
- Floppy, CD and USB drives should not be used.
Any disturbance / virus attack in this computer would make the APC unavailable.
5. To ensure proper flow of information with respect to functioning of RMPCT
controller on round the clock basis, relevant observations need to be mentioned in
shift TOB.
Role of APC group:
1. Technical APC group shall oversee the service factor of all APC controllers and
circulate performance reports for individual RMPCT controllers on a daily and
monthly basis and carry out trouble shooting as and when required.
NOTE: Assets related to APC like server, Profit viewer computer and associated
accessories will be monitored and managed by Technical-APC group.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
PRE-COMMISSIONING ACTIVITIES
There is a large amount of preparatory work which should be performed by the operating
crew before starting of the unit after completion of mechanical jobs. A planned check of the
unit will not only set the foundation of a smooth start-up but will also provide a firm basis for
acquainting operators with the equipment. Start-up is a critical period and the operators must
know the operation of equipments.
Some of the pre-commissioning works can be carried out simultaneously along with
construction. But care in the organization of this work is necessary so that it will not interfere
with construction work. It is most important to plan schedule and record with check-lists and
test schedules all the preliminary operation and to co-ordinate he construction program.
10.1 INSPECTION:
Inspection of the following items is primarily contractors’ responsibility. Nevertheless, it is

important for operating crew to participate in the inspection to the fullest extent since for
many of them this may be the only opportunity before start -up to examine the internals of
some of the equipment.
10.1.1 Inspection of Vessels and Columns:
Inspection of the interior of the vessels, columns, heaters and other equipments that are not
normally accessible during operation will be made to ensure that they are completed clean
and correctly installed.
10.1.2 Piping and Accessories:
Piping and accessories will be checked against drawings and specifications. Piping support
and hangers will be inspected to ensure that all anchorages are firm. Valves will be checked
for proper packing and mounting. Spring supports are to be checked for the cold settings and
later for hot settings while the plant is in operation.
10.1.3 Instruments:
Instruments will be checked, starting from the controller and proceeding logically through the
control loop. Cascade control system will be checked from the impulse point of primary loop.
Operating crew should check proper mounting of control valves.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
10.1.4 Relief Valves:
Relief valves will be set in the shop and mounted before the system pressure test. Block
valves ahead and after relief valves will be checked for lock open or lock close position as
per P&ID. Relief valves will be checked against specifications. Rupture discs should not be
mounted during tightness test.
10.2 PREPARATION OF UNIT:
• Check the unit for completion of mechanical work against P&ID.

• Remove all construction debris lying around in the unit and clean up the area.
• Install blinds as per master blind list.
• Safety valves should be kept blinded during flushing and re-installed
afterwards. These should be shop tested and set at the stipulated values.
• Ensure that underground sewerage system is in working condition. Clear
plugging, if any. Check by flushing with water.
• Check that communication between units, control room, offsites and utilities
are complete and in working condition.
• Ensure that the required lube oil, grease and other consumable are available in
the unit.
10.3 COMMISSIONING OF UTILITIES:
Commissioning of various utilities in the DC unit is described below. Prior to commissioning

of each utility system, the utility section should be informed about it and the load which is
expected.
10.3.1 Steam Network:

Network shall be blown through completely from battery limit with a strong steam flow in
order to clean the lines. The following steps are recommended.
• Check network, all equipment will be disconnected to avoid entry of flushed
material.
• Drain all the low points. If necessary open steam trap inlet flanges.
• Open slowly battery limit valve and let the temperature rise in the header,
slowly and steadily.
• Check support of fixed points and expansion loops.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
• When line is hot blow it through completely with a strong steam flow.
• Close battery limit valve and prepare another network. When the blowing is
satisfactory, reconnect all equipment and remount steam traps. Recharge header as
above.
Note: The following precautions are to be taken while blowing/commissioning steam
header:
• To drain the low points of the lines before and during heating period in order
to avoid water accumulation, which leads to hammering.
• To open drain/vent during cooling period to prevent vacuum formation
• To isolate the instruments, remove orifice plates and control valves; to re-
install the orifice plates and control valves blowing is over.
10.3.2 Cooling Water and Service Water:
Network shall be cleaned from battery limit with a strong water flow. All equipment will be
disconnected at the inlet and reconnected when lines are cleaned. Control valves and orifice
plates will be removed and re-installed after the lines become clean. When system has been
flushed charge the lines to the operating pressure.
The following precautions to be taken:
• To open vents at high points in order to expel air from equipment and piping
• To open the battery limit valve, slowly and steadily.
10.3.3 Boiler Feed Water:
Flanges are to be opened at the inlet of the connected equipment and at any convenient low
point. Network shall be first cleaned with raw water from battery limit with a strong water
flow. The net work shall then be drained and rinsed with boiler feed water. Open flanges will
be made up and header charged after the network is clean. Usual precautions for instruments
like isolation, removal etc. are to be taken as mentioned above in case of steam network.
10.3.4 Instrument and Plant Air:
Network shall be blown through completely from battery limit with strong flow of air in
order to clean and dry the lines. All joints and connection shall be checked for tightness with
soap solution. Header and branch lines will be blown through with a high flow rate of air.
During all tests, the instruments and control valve shall be carefully isolated from the system.
10.3.5 Fuel Gas and Fuel Oil Networks:

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
Networks shall be blown through from battery limit with a strong steam flow for fuel oil and
a strong air flow for fuel gas in order to clean the lines. During this operation, orifice plates
and control valves shall be removed. Special care shall be taken to prevent water from
entering the furnace. The fuel gas headers will be commissioned before firing the Coker
furnace.
10.4 WATER FLUSHING OF PROCESS LINES:
To clean scales and foreign matters etc. from inside, lines and equipment are flushed with
water wherever possible. Temporary water connections should be provided at convenient
locations in the system for carrying out water flushing. The following points should be
remembered during water flushing.
• Low point drains and high point vents should be flushed.
• All instruments connection should be isolated, orifice plates removed. Control
valves isolated and by-passed. In case there is no bypass, remove control valve and
flush the line. The valve will be installed after clean water starts coming out and
further flushing may be continued.
• If there is any heat exchanger in the line flushing should be done upto and
around the exchanger using by-pass line. It should be ensured that dirty water from
initial flushing does not get into he exchanger. Wherever by-passes are not available,
the flanged joints at the inlet of heat exchanger should be first opened and the line
flushed till clear water starts coming out. Then reconnect flange and flush through the
exchanger.
• At each opening of the flanged joints, a thin metallic sheet should be inserted
to prevent dirty water from entering the equipment or piping.
• The flow of water should preferably be from top to bottom for flushing of heat
exchanger coolers. The bottom flange of the equipment should be opened to permit
proper flushing.
• The flushing should be carried out with maximum possible flow of water till
clear water starts coming out
• Vertical lines which are long and rather big (say over 100 mm dia.) should
preferably be flushed from top to bottom. This will ensure better flushing. Filling the
lines and releasing from bottom is also helpful. The rundown lines can also be flushed
conveniently to the respective tanks.
• It should be ensured in all flushing operation that design pressure of lines and
equipment are never exceeded. After flushing of lines and equipment, water should be
thoroughly drained from all low points. Lines and equipment containing pockets of
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
water should not be left idle for a long time. It is preferable to dry these lines and
equipment with air after water flushing.
• For flushing of stainless steel lines and equipments DM water shall be used.
10.5 FUNCTIONING TEST:

All rotary equipment (including dosing pumps) will undergo functional test to check
their performance.
10.5.1 Motors:
Each motor should be checked and started to ensure that it has the correct direction of
rotation. The motor speed should be checked with tachometer to ensure that RPM is correct.
The manufacturer’s lubrication schedule should be used to ensure that all lubrication points
have been serviced. After a short run each bearing should be felt to ensure that it is free and
not overheated.
10.5.2 Pumps:
Generally the pump casing is opened and checked to ensure that it contains no foreign
material. Pump casing need not be opened up in case the pump had been stored carefully and
the blinds covering suction and discharge nozzles were not removed in storage or in transit.
Cleanliness of suction line and installation of line mesh strainer should be ensured. Pumps
and motor will be aligned and then tried on water. Temporary connections may have to made,
if required. When running a pump designed for hydrocarbons on water the discharge valve
may have to be throttled so that the rated amperage is not exceeded. Ensure that the vents and
drains of the pumps are clear. Pressure gauge tapping will be flushed and filled with sealing
fluid wherever necessary.
10.5.3 Turbines:
Turbines should be de-coupled and run using steam as per manufacturer’s

instructions.
10.5.4 Compressors:
It is important to make sure that the inside of piping (especially suction piping) around the
compressor has been cleaned. The compressor cylinder should have no stress of piping. The
lube oil lines and compressor suction lines downstream of the suction filter should be acid
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
cleaned and pickled. Vendor's instructions may be followed in this regard. A fine mesh
strainer (about 100 mesh) should be inserted in the suction line. Lube oil should be used as
per manufacturer's recommendation. The compressor should be run for a few hours following
the manufacturer's instructions regarding media and mode of trial operation. A close watch
should be kept on critical parameters like bearing temperature, discharge pressure and
temperature, lube oil temperature and pressure, etc. When the compressor is found to function
satisfactorily, it should be connected to the rest of the system.
Note: Vendor's instructions shall be followed as far as the testing medium for pumps and
compressors is concerned. In general, casing design pressures and rated motor amperes shall
not be exceeded.
10.6 CALIBRATION OF INSTRUMENTS:

The following guidelines may be adopted for checking and calibration of all instruments.
10.6.1 Orifice Plates:
Before each orifice plate is installed the orifice taps should be blown clear. The orifice plate
should be callipered to check, if the correct size orifice plate is installed. The plate should
then be installed after checking for the correct direction.
10.6.2 Differential pressure Transmitters and Receivers:
Ordinarily these should be calibrated locally against a manometer. The calibration should be
checked at the receiver which may be board or locally mounted recorder or indictor.
10.6.3 Pressure Transmitters and Receivers:
This should be checked in place. The calibration of the receiver should be checked at the
same time.
10.6.4 Alarms:
All alarms auto start and cut off systems should be checked by simulating the conditions.
Check the sequence of start-up/ shut down interlocks by simulation.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 10
PLANT NAME: CDU II
Chapter Rev No: 0
10.7 FURNACE DRYING:

The furnace refractory must be thoroughly dried out so that it does not crack when the Heater
is brought into operation. The drying should be done by gradual heating of the refractory so
that no spalling or cracking takes place due to sudden vaporization of moisture from the
refractory. The drying procedure for heater refractory is given separately.
10.8 TIGHTNESS TEST:
The purpose of this test is to check the tightness of flanges, joints, manholes etc. (except
pumps and control instruments). This operation can be integrated with steam purging activity
aimed at expelling air prior to introducing hydrocarbon into the unit.
• Drains at low points will be opened and after draining is over, these will be
closed. Vents will be opened; pressure gauges will be installed on each circuit.
• Steam is progressively admitted where connections are available. Circuits
which do not have direct admission of steam will be supplied through hoses.
• The temperature of the whole installation is increased slowly and free
expansion of lines is checked. The condensed water is drained while the temperature
of the circuit rises.
• When temperature is steady, vents are progressively closed in order to get the
desired pressure by keeping a vent slightly opened. A steam make-up is maintained.
All joints will be checked for leaks. If leaks are detected system will be depressurized
and leaks will be attended and the system retested.
• For vacuum system perform vacuum test if tightness test is satisfactory.
10.9 CHARGING OF CHEMICALS:
Small quantity of the corrosion inhibitor, ammonia & demulsifier are required for use in the
CDU/VDU unit (no chemical is used in BBU). It is important that these chemicals should be
available for use from the time the unit is put on stream.
Corrosion inhibitor is received in drums and is used directly from the drums. Proceed as
follows:
• Receive two full drums of corrosion inhibitor.
• Open the two bungs on each drum and install vent connection on one
opening and valve connection on the other in each drum.
• Load the two drums on the rack.
• Hook up the outlet of drums one each to the suction of the corrosion inhibitor
pumps respectively with hoses.
• Check for leaks and keep ready for starting the pump.
• Similarly keep ready ammonia & demulsifier dosing system for use.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 11
PLANT NAME: CDU II
Chapter Rev No: 0
PREPARATORY OPERATIONS & ACTIVITIES FOR COMMISSIONING
PREPARATORY OPERATIONS & ACTIVITIES FOR

COMMISSIONING
Start up and normal operating procedures are described in this section. Start up and shutdown
are the most critical periods in operation. It is then that the hazardous possibilities for fire and
explosion are greatest.
The hazards encountered most frequently in start up and shut down of units are accidental
mixing of air and hydrocarbons and contacting of water with hot oil. Other hazards primarily
associated with startup are pressure, vacuum, thermal and mechanical shocks. These can
result in fires, explosions, destructive pressure surges and other damages to unit as well as
injury to personnel.
Fires occur when oxygen and fuel vapor or mists are mixed in flammable proportions and
come in contact with an ignition. They may run out of control or touch off devastating
explosion. Pressure surge from unplanned mixing of water and hot oil may cause damage of
equipment and / or loss of valuable production. This may result in expensive, costly down
time on process unit. Fires usually follow if the explosion bursts lines or vessels.
Preparation for start - up begins with a complete review of the start up procedure by the
operating crew. Activities of CDU/VDU should be coordinated with OMS and other units
and utilities section. Start up of the unit involves the following consecutive phases:
• Preparation of the unit.

• Removal of air from the unit by steaming.
• Tightness testing under steam pressure.
11.1 PREPARATION:
Prior to actual commissioning of the plant it should be established that all preparatory works
have been successfully completed and all equipment are ready to function. Ensure that:
• Blinds are installed as per master blind list. Each removal and insertion of a blind
should be noted and installed by the operator in charge.
• All vessels, piping, equipment are pressure tested, flushed and ready for service.
• All rotating equipment such as pumps motors etc. have undergone functional test
successfully.
• All instruments have been checked and calibrated. Control should be on manual.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 11
PLANT NAME: CDU II
Chapter Rev No: 0
• All safety valves are in position after setting and testing. Isolating valves will be left
in lock open position. Spare valves should be kept isolated.
• All utility headers are charged.
• Flare, closed blow down, sewer and flushing oil systems are in operable condition.
• All related units are informed of the start - up plan.
• All pre-commissioning activities are completed.
• Fuel oil and fuel gas blinds are removed and both headers charged.
• Refractory dry out for heater is carried out.
• Tracing steam to the lines in opened.
Tightness and vacuum test will from part of pre-commissioning activities for the first start up.
For subsequent start ups the tightness test and vacuum test can be done in conjunction with
the step of elimination of air.
11.2 STEAM PURGING AND TIGHTNESS TESTING:
For this purpose, Unit is divided into following sections.

CDU/VDU
1. Desalter and crude preheat system and PFD.
2. Atmospheric column, top, middle and bottom pump around systems and product
circuits up to battery limit
3. Stabilizer and stabilizer reflux drum
4. Naphtha caustic wash
5. Vac column for vacuum test.
6. Vac products and Vac reflux systems.
Steam connection is given at appropriate places to remove air from equipment and pipes.
Water to coolers and condensers is isolated. Low point drains of pipes and equipment are
opened to remove condensate. High point vents are opened for air removal. Steaming is done
till O2 content of the system reduces to less than 1%. For leak testing vents and drains are
throttled, pressure is built up to 1kg/cm2g for atmos column and for stabilizer pressure to be
build up to 5 kg/cm2g and all product systems pressure to be build up to 7 kg/cm2g and
system checked for any leaks. Leaks are attended after depressurizing.
In vacuum section, vacuum is pulled in the vacuum column and the system checked for
holding the vacuum. Air will be removed from vacuum section during vacuum pulling.
Equipment and lines will be included during this activity.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 11
PLANT NAME: CDU II
Chapter Rev No: 0
Low point drains of pipes and equipment are opened to remove condensate. High
point vents are opened for air removal. Steaming is done till O2 content of the system
reduces to less than 1%. For leak testing vents and drains are throttled, pressure is
built up to 5 kg/cm2g for product system and system is checked for any leaks. Leaks
are attended after depressurizing.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
NORMAL START-UP PROCEDURE
NORMAL START -UP PROCEDURE

12.1 Introduction
Start up and normal operating procedures are described in this section. Start up and shutdown
are the most critical periods in operation. It is then that the hazardous possibilities for fire and
explosion are the greatest.
The hazards encountered most frequently in start up and shut down of units are accidental
mixing of air and hydrocarbons and contacting of water with hot oil. Other hazards primarily
associated with start up are pressure, vacuum, thermal and mechanical shocks. These can
result in fires, explosions, destructive pressure surges and other damages to unit as well as
injury to personnel.
Fires occur when oxygen and fuel vapor or mists are mixed in flammable proportions and
come in contact with a source of ignition. They may run out of control or touch off
devastating explosion. Pressure surge from unplanned mixing of water and hot oil may cause
damage of equipment and loss of valuable production. Extensive costly down-time on the
process unit may result. Fires usually follow if the explosion bursts lines or vessels.
Preparation for start-up begins with a complete review of the start-up procedure by the
operating crew. Activities of CDU / VDU and BBU should be coordinated with OMS, other
units and utilities section. Start-up of the unit involves the following consecutive phases:
• Preparation of the unit

• Removal of air from the unit by steaming
• Tightness testing under steam pressure
• Backing in fuel gas
• Cold oil circulation and removal of water
• Hot oil circulation
• Bringing the unit on stream
12.2 Summary of Start-up
Normally both CDU and VDU will be running. However in case of some problem in VDU,
CDU above can be kept running for some time by diverting RCO to fuel oil tanks.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
Two types of start-up are envisaged.

• Start-up of both CDU and VDU simultaneously
• Start-up of only CDU
Start-up of the unit will be done by taking crude oil in Atmospheric section and gas oil in
vacuum section.
12.2.1. Preparation
Prior to actual commissioning of the plant it should be established that all the preparatory
works have been successfully completed and all equipment are ready to function. Ensure that:
1. Blinds are removed as per the master blind list. Each removal and insertion of a blind
should be noted and installed by the operator in-charge.
2. All vessels, piping and equipment are pressure tested, flushed and ready for service.
3. All rotating equipment such as pumps motors etc., have undergone functional test
successfully.
4. All instruments have been checked and calibrated. Control should be on manual.
5. All safety valves are in position, after setting and testing Isolating valves will be left in
lock open position.
6. All utility headers are charged.
7. Flare, closed blow-down (CBD), sewer and flushing oil systems are in operable
condition.
8. All related units are informed of the start-up plan.
9. All pre-commissioning activities are completed.
10. Fuel oil and fuel gas blinds are removed and both headers charged.
11. Refractory dry-out for heater is carried out.
12. Tracing steam to the lines is opened.
Tightness and vacuum test will from part of pre-commissioning activities for the first
start-up. For subsequent start-ups the tightness test and vacuum test can be done in
conjunction with the step of elimination of air.
12.2.2. Steam Purging and Tightness Testing
For this purpose, the unit is divided into following sections:
i. Desalter and crude preheat system.

ii. Atmospheric column, top, middle and bottom pump around systems and product
circuits up to the battery limit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
iii. Stabilizer and stabilizer reflux drum.

iv. Naphtha and caustic wash.
Steam connections are given at appropriate places to remove air from equipment and
pipes. Water to coolers and condensers is isolated. Low point drains of pipes and equipment
are opened to remove condensate. High point vents are opened for air removal. Steaming is
done till O2 content of the system reduces to less than 1%. For leak testing, vents and drains
are throttled, pressure is built up to 1 kg/cm2 g and the system is checked for leaks. Leaks are
attended on, after depressurizing.
In vacuum section, vacuum is pulled in the vacuum column and the system is checked for
holding the vacuum. Air will be removed from vacuum section during vacuum pulling.
Equipment and connected lines will be included during this activity.
12.2.3. Backing in Fuel Gas
Steam is cut off slowly and fuel gas is backed in, for which, provision has been made in the
design. Avoid pulling in vacuum during this period. This may cause entry of air in the system
and damage of vessels which are not designed for vacuum. It is advisable to back in fuel gas
section wise. After all the sections have been floated on fuel gas, water is drained from low
point drains, and draining should be recorded. In vacuum section, after system tightness is
proven, maximum vacuum is pulled. This vacuum will be broken by fuel gas admission (0.5
Kg/cm2 g. pressure). Positive pressure in the system will facilitate draining of residual water.
Removal of water from the system is an important step for smooth start-up.
12.2.4. Cold oil Circulation
Atmospheric Unit: For Atmospheric unit, crude oil is used during cold oil circulation. The
purpose of cold oil circulation is to try out pumps and control system and for better water
removal. Crude oil is pumped at about 50% of design rate by crude charge pumps 11-P-01
A/B. Crude oil passes through crude preheat system. Two trains of desalted crude preheat
system, Atmospheric furnace and into Atmospheric distillation column 11-C-01. Reduced
crude oil pump 11-P-10A/B takes suction from column bottom. The discharge of this pump
bypasses vacuum heater 12-F-01 and flows through the Short Residue circuit to the slop
header circuit through start-up line and then to the crude tanks. The cold circulation is then
established. During cold oil circulation one of the crude oil tanks will remain floating with
the system. After establishing cold oil circulation for an hour, stop the pumps and circulation
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
and allow water to settle at the lowest points. Drain water from all low points and restart cold
circulation. Repeat the procedure till all the water in the system is removed.
Vacuum Unit: In vacuum unit, gas oil is used for cold circulation. Gas oil is charged in the
vacuum column through flushing oil connection provided for the purpose. This oil is put in
the vacuum heaters. LVGO system, HVGO system, slop distillate and quench system and
these systems are circulated individually.
After establishing cold oil circulation for an hour, stop the pumps and circulation and allow
water to settle at the lowest points. Drain water from all low points and restart cold
circulation. Repeat the procedure till all the water in the system is removed.
Systematically, the cold oil circulation for both CDU & VDU can be done as per the
following sequence:
a) Line up 11-P-01A/B suction and fill Desalter at a slow rate, using feed pump turbine.
Open 1½” relief valve bypass and displace fuel gas to fractionators (11-C-01). Control
Desalter pressure manually by 11-PV-105 at 7 kg/cm2 then close unit limit feed valve.
b) Line up the unit as per the following circuit
CRUDE 11-P-01A/B 11-E-01 to 11-E-07
Startup Line
11-V-02
SR Circuit
11-PM-10A/B 11-E-08 to 11-E-16 11-PM-02A
11-C-01
11-F-01 11-E-40A/B 12-E-01 to 12-E-06

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
Take flushing oil to 11-C-01 bottom through flushing oil tie-in and bring up level.
Start 11-PM-10A/B, 12-LV-202 bypass open and fill SR exchanger up to feed pump
suction.
c) Isolate Desalter. Switch control level switches to startup mode. Start feed pump
turbine and control Desalter downstream pressure at 9.0 kg/cm2 by operating 11-PV-
105 manually. Keep heater pass flows wide open and fill all exchangers. Add flushing
oil at 11-C-01 bottom to make up level
d) Maintain column (11-C-01) pressure at 1.0 kg/cm2 and release displaced gas to flare.
Shut off fuel gas and commission surface condenser to check any pressure buildup in
12-C-01. Open hot well vent.
e) When the system is filled with flushing oil, start cold oil circulation by running 11-
PM-10A/B.
f) By circulating cold oil, water in the system will settle at low points. Stop circulation
after one hour, allow water to settle, drain water from all low points. Restart
circulation and repeat this operation until no water drains out.
g) Commission tempered water system by taking DM water to 12-V-02.
h) Take flushing oil to 12-C-01 top, through flushing oil tie-in at 12-P-01 discharge
manifold under 12-FRC-205. After getting LVGO level, start reflux to HVGO
packing at 30m3/hr. through FRC-201 and build up HVGO level. Similarly, build up
level in slop cut, running 12-PM-3A/B and routing through 12-FRC-202
i) Take flushing oil to 12-F-01 passes and build up 12-C-01 bottom level and establish
internal circulation as shown below.
12-F-01 12-C-01
12-P-01A/B
j) Circulate cold oil through all circuits i.e. bottom, slop cut, HVGO, LVGO, for about
an hour. Drain water after settling and repeat until systems are completely water free.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
k) Operate all control valve bypasses and exchanger bypasses to remove water from
these points
12.2.5. Heater Firing and Hot Oil Circulation
Atmospheric Unit: When cold-oil circulation has been well established and water in the
system has been thoroughly drained out, heater firing will be done. About 50% of normal
flow will be maintained through heater coils. Transfer temperature is raised to 120 °C at a
rate of 20 °C/h, (MAX). This temperature is maintained for about four hours to remove
residual water from the system. The transfer temperature will be further raised to 250 °C at
30 °C /h. Top temperature of the column will gradually rise. When it reaches more than 100
°C, steam will escape from the column and condense in overhead Naphtha accumulator.
Drain condensate at regular intervals. As top temperature rises further, column pressure is
slowly raised to its normal value. Higher pressure will help in better condensation of vapors.
As level starts building up in overhead Naphtha accumulator 11-V-01, refluxing is started to
maintain desired top temperature. Complete hot bolting at 250 °C.
System temperature will be further raised to 365/385 (BH/AM). Top temperature and
pressure are maintained. Admit stripping steam to crude column at a transfer temperature of
about 300 °C. When Naphtha production increase, which is indicated by rising oil level in
crude column overhead Naphtha accumulator, it is routed to Stabilizer column 11-C- 05.
Naphtha is diverted directly to Stabilizer column and build up level slowly at the column
bottom. When levels appear in the crude column side stream strippers, maintain these levels
at about 50% and line up BPA (Bottom Pump Around –DCR), MPA (Middle Pump Around –
KCR) and TPA (Top Pump Around-TPA) reflux circuits. Water is drained before starting
BPA, MPA and TPA pumps. Flow and temperature of top pump around, middle pump
around and bottom pump around are adjusted to maintain temperature profile in the column.
Line up all product circuits up to battery limit. Start respective product pumps when level
appears in the strippers. Route all products to slop header. Once sufficient level (70%) is built
up at Stabilizer column bottom, Stabilizer column will be brought on stream by gradually
cutting in the heating medium i.e., KCR in re-boiler. As the temperature of the Stabilizer
column rises, pressure will increase and level will appear in the Stabilizer reflux drum.
Stabilized Naphtha will be routed to storage tanks. When level appears in the Stabilizer reflux
drum refluxing will be started. When LPG quality is on-spec, it will be sent to the Amine
Treating Unit. Reduced Crude Oil at the outlet of Atmospheric column bottom will be routed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
to fuel oil tanks till vacuum section is ready to receive RCO. When the normal transfer
temperature of 365/385 (BH/AM) has been attained, make necessary adjustments and
normalize the operating conditions.
Vacuum Unit: Once cold oil circulation has been established and water in the system is
drained out burners are lit in the vacuum heater 12-F-01. Transfer line temperature is slowly
raised to 90 °C at 30 °C /h. Hold this temperature for 2 hours. Activate all the circuits in the
system using start-up lines. Transfer line temperature is then raised to 120 °C and held for 4
hours. During this period, water in the system will be removed as steam in the overhead
system. After removing water completely from the system, transfer line temperature is raised
to 230 °C at the rate of 30 °C /h. Any level build up on trays is pumped to slop. When RCO
from Atmospheric unit is available, it is lined up to the vacuum unit. Establish once through
flow in the unit by gradually displacing the flushing oil in the unit. Transfer line temperature
is raised to 300 °C at the rate of 30 °C/h. Hot bolting is done by holding the transfer line
temperature at 300 °C. After hot bolting is completed, increase the transfer line temperature
to 360 °C @ 30 °C/h. Light fractions will be collected on the upper trays as transfer line
temperature is increased. Pump around and internal refluxes should be maintained
continuously Tray levels are maintained by adjusting the product routing to slop. At this stage
recycle stream from column bottom to heater inlet is commissioned. Gradually vacuum is
pulled. Transfer temperature is then gradually increased to 395 / 402 °C (BH/AM) at 30 °C/h.
Quench rates, draw-off rates etc., are adjusted and steady conditions are maintained. When
products are on spec. they are routed to the respective tanks.
Systematically, hot oil circulation for both CDU/VDU can be as per the following plan:
a) Fire both heaters and bring up coil outlet temperature at 30°C/hr rate.
b) When transfer line temperature reaches 120°C hold firing rate and maintain
circulation in both heaters for about 4 hrs, to remove final traces of water.
c) Closely follow 12-C-01 pressure, commissioning 3rd stage ejector if required to
contain pressure build up
d) Admit small amount of steam into 11-F-01 superheating coil and vent through
silencer. Outlet temperature should not exceed 350°C.
e) Slowly raise furnace COTs to 220°C/hr rate
f) Check all the equipments and pumps during this period.
g) When 11-C-01 top temperature crosses 100°C, steam will escape from column and
condensate collects in reflux drum keep interface controlling service.
h) Hot bolt at 200-250°C and cap off all bleeders.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
12.3 DETAILED PROCEDURE
12.3.1 ATMOS SECTION
Elimination of Air
Air from various equipment, piping etc. is eliminated by steaming. Steaming of various
Sections of the unit to expel air can be carried out simultaneously or in a convenient
Sequence. The following basic things should be taken care of during steaming of the
equipments / systems:
1. Cooling water to the condensers and product coolers to be isolated and water should
be drained out from the condensers, coolers etc.
2. Keep water side vents and drains of condensers / coolers opened
3. Keep all pumps isolated
4. Keep instruments like PT, FT etc., isolated
5. Power supply to the Desalter is cut off
i) Admit steam into the system by opening the valve on 3” steam line joining the discharge
header of crude charge pump 11-P-01 A/B.
ii) Prior to this activity, isolate Desalter and introduce LP steam. Keep watch on Desalter
pressure which should be maintained around 0.5 kg/cm2 g. If necessary, throttle steam.
Allow steam to vent from Desalter top. Purge Desalter safety valve inlet line. Air will be
purged from both inlet and outlet lines of safety valve. MP steam should not enter
Desalter.
iii) Open steam slowly into the system and allow piping and equipment to gradually warm
up. Drain condensate frequently from low points.
iv) Keep booster pump suction and discharge valves closed
v) Line up overhead condensers 11-E-17 A-H, and overhead Naphtha accumulator 11-V-01
with the column. Ensure cooling water to Condensers is isolated and water is drained out.
vi) Open vents of overhead Naphtha accumulator and crude column.
vii) Line up strippers, product circuits and circulating reflux circuits up to the respective
pumps. Keep pump suction and discharge valves closed.
viii) Commission fuel gas header to furnace, after removing the battery limit blind. Fire the
heater at a small rate. Heater is fired to avoid condensation in tubes and subsequent
hammering if steam is introduced in cold tubes. Please refer vendor Operating Manual
for heater start up procedures. Maintain heater Arch temperature at about 250°C. Pilot
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
burners will be lighted initially. Main burners can be lighted afterwards, if required.
Keep open the vents at crude column top and overhead Naphtha accumulator.
ix) Slowly open steam into all passes of the heater coils through emergency steam purging
connections. Also open steam to the crude column bottom via stripping steam line.
x) Drain condensate from low points and allow system to warm up. Regulate the steam flow
to heat up the system gradually. Continue purging till steam comes out from the top of
the crude column and overhead Naphtha accumulator.
xi) Back up steam up to the Booster Pump discharge. Wedge open discharge valve upstream
flange to release air and condensate. Drain condensate from exchangers and lines from
all low points. Steam the bypass lines of the exchangers.
xii) Purge product and pump around circuits by backing up steam from crude column. Steam
the product circuit up to the battery limit and vent through sample points or any
convenient high and low point drains. It may be necessary to augment steam supply at
the discharge of product pump by connecting temporary hoses to vent or drain points in
the lines. B/L flange may be wedge opened for good steaming. Box up the flange under
slight steam pressure.
xiii) Steam out RCO and VR circuit up to isolation valve at the B/L. Eliminate air through all
exchanger vent points and drain out condensate from all exchanger drain points.
xiv) Back up steam into the top reflux line and vent from the bleeder valve upstream of the
Stabilizer feed control valve 11-FV-501.
xv) Vigorously steam for about 2 hours and then shut off crude column vent. Allow steam to
vent from overhead Naphtha accumulator and other points as mentioned above.
xvi) Maintain 1.0 kg/cm2 g. pressure in column flash zone (11-PI-401) by regulating the
quantity of steam being introduced into the system.
xvii) Line up the Stabilizer overhead condenser 11-E-20 A to D and reflux drum 11-V-03 to
Stabilizer column. See that vents in the cooling water side of condenser are kept open.
Open vent valves of Stabilizer column and its reflux drum.
xviii) Remove blind on the utility steam connection at the Stabilizer column bottom and admit
steam slowly. Drain condensate from low points and allow the system to warm up.
xix) When steam comes out from Stabilizer top, vigorously steam for about half an hour.
Then shut off this vent and allow steam to come out of reflux drum vent.
xx) Maintain Stabilizer column pressure at 1.0 kg/cm2 g. (11-PIC-501) by regulating the
quantity of steam. Open the pressure control valve 11-PV-501 and globe valve on its
bypass line. Steam for about half an hour then shut off the control valve and the globe
valve.
xxi) Purge feed line by backing up steam from the Stabilizer column.
xxii) Purge Stabilizer bottom outlet circuit up to the battery limit along with caustic wash
system. Vigorous steam venting from various points of the unit as described above will
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
be continued for about 4 hours. It is estimated that oxygen will be eliminated at the end
of this period. Samples may be checked from different location to check that O2 content
is less than 0.5%.
xxiii) During the period of steaming, systems should be checked for leaks. Attend the leaks by
depressurizing the system. Retest and purge. When sufficient steam comes out from all
the vents and drains, reduce steam inlet to maintain positive pressure.
Backing in Fuel Gas
Before admitting fuel gas into the system, all vents and drains are to be closed. Admit
fuel gas through fuel gas make-up control valve. Steam entering the system is throttled
slowly. Rate of fuel gas backing is adjusted in such a way that operation of the refinery gas
system is not adversely affected. During gas backing, ensure that vacuum is not formed in the
system due to condensation of steam. Furnace fires are cut off. Cooling water is
commissioned to the overhead condensers and coolers. Maintain the pressure in the system
around 0.5 – 1.0 kg/cm2 g. As the system cools, condensate will accumulate. The drain at
each low point must be opened and the condensate be drained. Never leave open drains
unattended. Each drain which is opened and checked should be listed in the start-up check
list. A log should be kept for the draining activities showing time of check and absence of
condensate. Each drain must be closed as soon as gas issues from it. When the draining is
complete the system is ready to take crude oil.
Steps in backing fuel gas into the systems are given below:
i) Reduce steam to the various points in the crude column and furnace coils. Close all
drains and vents except any one vent at a convenient point to vent steam to maintain
system pressure.
ii) Close all the vents one by one. Adjust steam inlet rate to maintain system pressure
about 0.5 kg/cm2 g. Cap off all vents properly to avoid leakage of gas through these
points. Throttle the drain valves to allow only condensate to flow to keep the system
hot. Keep watch on the system pressure. Adjust steam inlet if necessary.
iii) Open the pressure control valve 11-PCV-409B very slowly to admit fuel gas into the
system. Close the vent valve which was kept open at a convenient point to maintain
the steam pressure. Slowly reduce and finally shut off steam inlet to the system.
Watch system pressure which should not be allowed to cross 1.0 kg/cm2 g. Fuel gas
inlet is to be regulated such that other running units are not affected by this operation.
Ensure that all the vents and drains are fully closed.
iv) Cut off furnace fires when steam to the unit is shut off.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
v) Commission water to the overhead condensers and coolers after venting air from
water side. Open suction and discharge valves of pumps.
vi) As the system cools, drain condensate that collects at all low points in the system.
Always shut off drains after gas starts issuing from it.
vii) Reduce steaming in Stabilizer section and close all vent and drain valves and admit
fuel gas into the Stabilizer by gradually opening the control valve 11-PV- 501.
viii) As Stabilizer pressure tends to increase, cut off steam and maintain Stabilizer pressure
around 1.0 kg/cm2 g. Check for leaks, if any.
ix) Purge flare header with fuel gas and open B/L isolation valve. This flare header
should now be lined up to various equipments.
x) As the system cools, the steam in the systems will condense and collect at low points
in the unit. Repeat draining operation every half an hour till no more condensate is
drained. Most of the problems in unit start-up can be avoided if condensate draining is
done thoroughly at this stage. When all condensate has been drained and the unit is
under fuel gas pressure of about 1.0 kg/cm2 g, crude oil can be taken into the unit.
xi) Take all instruments on line which were kept isolated during steaming.
Receiving crude in the Unit
The crude tank that will feed the unit will be prepared in advance by thorough draining of
water. Sample will be analyzed and dips will taken. It will then be lined up to the unit.
a. Open suction valves of crude charge pumps 11-P-01 A/B and crude booster pumps 11-
P-02 A/B.
b. Slowly charge crude from the crude tanks. Crude will begin to flow by gravity into the
line and displaces air. This air is vented from the crude pump vents. In subsequent
start-ups this operation may not be required as off-site’s line up to the battery limit
will remain full.
c. Make sure that electrical supply to Desalter is cut-off. Open the discharge value of
crude pump and allow the crude to flow to the Desalter. Alternatively, Desalter can be
kept filled with Crude oil and by-passed.
d. Release displaced fuel gas into the flare system from overhead Naphtha accumulator
11-V-01, and do not exceed column pressure beyond 1.0 kg/cm2 g.
e. When gravity flow of crude oil stops start crude charge pump 11-P-01 A/B. Continue
charging crude oil at a slow rate. Preferably start turbine for low flow rates.
Note: Before warming up the stand-by pump of any hot pump through the 1” warm-up
line across NRV of stand-by pump, it is to be ensured that suction valve of the stand-by
pump is kept open. This is to avoid pressurization of the pump and its suction line to the
discharge pressure of running pump.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
Establishing cold oil circulation

Circulating cold oil will carry liquid water in the system to low points in the unit. Stop
circulation after about an hour, allow water to settle. Drain water from all low points. All
plugged drains must be cleared. When draining water, be careful to prevent unnecessary loss
of oil to the sewer. Restart circulation once draining from all low points is over. This
operation of circulation, stopping, settling and draining will be repeated till no further water
separates out. The steps involved to establish cold oil circulation are detailed below:
a) With crude charge pump 11-P-01 A/B running, carefully operate the Desalter 11- V-
02 pressure controller PIC-1105 manually and build up a pressure of 8.0 to 9.0 kg/cm2
g. in the Desalter. Keep the bypass of booster pump open for continuing circulation.
Crude oil flow rate should be kept at the minimum, limited by FG venting capacity
from overhead Naphtha accumulator to flare.
b) Start Booster Pump 11-P-02 A/B and close the bypass valve gradually. Regulate the
coil flow through FIC-1301 to 1304 of 11-F-01 such that crude flow to unit records
about 225 m3/h (about 50% of normal throughput). Also divide the flow equally
through two crude preheat exchanger trains by operating FRC – 1101.
c) Stabilize the Desalter pressure at 9.5 kg/cm2 g and put PIC-1105 on auto. Observe the
performance. Crude oil will gradually displace fuel gas and build up level in crude
column.
d) Keep watch on crude column level (LI-1401)
e) Maintain column pressure at 1.0 kg/cm2 g by operating PIC-1409. Displaced gas will
be released to flare.
f) When sufficient level is built up in the column bottom, start RCO pump 11-P-10 A/B
and route the crude to Crude tank through VR circuit to slop for about 1 hour to
displace free water. Check that there is no flow of crude oil to vacuum furnace.
g) Keep the crude feed tanks floating with crude charge pump suction.
h) Vent the exchangers in RCO circuit to CBD, so that these become full of crude.
Activate exchanger by passes; Bleed residual fuel gas from the RCO circuit.
i) Stop all pumps every one hour and allow settling for one hour. Carry out water
draining from all the low points in the system including column and exchangers.
Restart circulation. Repeat this operation till no further water separates out. A check
for water content of circulating crude oil is useful information.
Firing the Heater
When cold circulation has been well established and water in the system has been thoroughly
drained out, heater firing will be done. Ensure the following before firing the heater:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
1. Cooling water flow is established in all overhead condensers and product coolers.
2. Tempered water system is activated.
3. Tracing steam is commissioned.
4. Set level controllers (LIC-1404, 1403, 1402) of strippers 11-C-02/03/04 at 50% level
(auto mode). Check that valves remain opened as there is no level in the strippers.
5. All safety isolation valves are left lock opened.
Raising Temperature to 120°C
a) Charge atomizing steam header to the heater. Commission fuel oil supply and return
lines and establish circulation. Fire the burners one by one. The rate of increase of
transfer line temperature will be restricted to 20 °C per hour. When the transfer line
temperature reaches 120 °C at heater outlet hold firing rate to maintain this
temperature for four hours.
b) Lower column pressure to 0.5 kg/cm2 g. or less to facilitate water removal as water-
vapor to the column overhead. Keep watch on the column pressure. The excess
pressure will be released to flare.
c) Monitor all temperature and pressure reading of column and heater.
d) While raising the temperature it will be observed that crude passing through preheat
trains will be gaining heat from the RCO. Check for presence of water in product and
circulating pumps’ suction and drain out.
e) Watch performance of RCO pump as it may tend to lose suction with rise in crude oil
temperature. If required, increase column pressure to 1.0 Kg/cm2
f) Maintain temperature of crude at the outlet of Vac. Residue cooler 12-E-09 A/B/C/D
about 40°C to avoid cavitation due to hot RCO going back to the crude charge pump
(11-P-01 A/B) suction.
g) Maintain crude column level by matching RCO pump discharge rate with crude intake
to the unit. Flow is to be maintained at about 50% of the normal throughput.
h) At the end of 4 hours, carry out test for water content in circulating oil. Water content
equal to or less than that of tank sample is indication of good water removal. A value
of about 0.2 wt% of water is often obtained.
i) After holding the temperature at 120°C for 4 hours, transfer temperature will be
further raised at a rate of 30°C/h to 250°C and held at this temperature.
ii) Closely watch all instrument readings and check their performance.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
iii) Hold crude column at about 50% level. Manipulate, if necessary, the RCO pump
discharge rate.
iv) Top temperature (11-TI-403) of the column will rise gradually. When it crosses
100°C, steam will escape from column and condense in the overhead Naphtha
accumulator.
v) When level appears in the accumulator 11-V-01, check and drain it out. Local checks
for levels are to be made.
vi) As top temperature rises further, slowly raise column pressure a little at a time to its
normal value of (BH/AM) 2.5/2.4 kg/cm2 g. at accumulator. After steadying out, put
pressure controller 11-PIC-409 on auto to hold this pressure. Higher pressure will
help in condensation of vapors which would otherwise escape.
vii) Check for appearance of oil level in crude column overhead Naphtha accumulator.
Start refluxing when oil level builds up. Care will be taken so that water does not go
in the reflux stream. Refluxing will be started at a small rate. No overhead product
will be withdrawn at this stage.
viii) Start hot bolting in the transfer line, RCO circuit, column bottom manholes and
other flanges in hot service where temperature exceeds 200°C.
ix) Cap off all drains that were used to drain water.
i) When hot bolting of the portion where temperature reaches 200°C is over, start
raising the transfer temperature at 30°C/h and continue hot bolting in other areas
where temperature touches 200°C.
ii) Watch water and oil levels in overhead Naphtha accumulator 11-V-01.
Commission water and oil level controllers 11-LDIC-406 and 11-LIC-406 and put
them on auto to hold about 50% level respectively. Watch the instrument
performance.
iii) Regulate top refluxing to maintain the column top temperature (11-TI-403) of
(BH/AM) say 118/110°C.
iv) When Naphtha make increases as indicated by rising oil level in crude column
overhead Naphtha accumulator, route this product to Stabilizer column.
v) Maintain about 50% oil level in overhead Naphtha accumulator by regulating the
quantity of Naphtha withdrawn.
vi) In case RCO product temperature at the outlet of 12-E-09 A/B/C/D goes beyond
45°C, Receiving slop crude tank may experience high temperature which should be
taken care of.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
vii) When column top temperature and pressure reaches its normal value, line up
Bottom (HSD CR), middle (KERO CR) and top pump around circuit. Always drain
water before activating the circuits. Start refluxing at minimum flow rate after
draining water from pump casing drain.
viii) When level appears in side strippers, drain water from pump suction and line up
product discharge (heavy Naphtha, kerosene, & HD) to slop header. Heating
medium to Stabilizer reboiler 11-E-25 should not be commissioned which will be
commissioned at a later stage when continuous feed to Stabilizer will be available.
The control valve 11-TV-504 will remain 100% open on manual. When sufficient
level is built up in the side strippers (about 40%) start withdrawing off-spec.
products to slop header which is lined up to crude storage tank.
ix) Check performance of level controllers of Heavy Naphtha stripper 11-LIC-404,
Kerosene stripper 11-LIC-403, and HD stripper 11-LIC-402.
x) Activate stripping steam header by draining Condensate from drain points provided
near crude column and strippers.
xi) When crude column bottom temperature reaches 300°C, admit stripping steam step
by step about 250 kg/h (11-FRC-401) in each step. With introduction of stripping
steam, amount of vapour flowing to the upper section will go up.
xii) Divert RCO to vacuum furnace, provided vacuum section is ready to receive RCO.
Otherwise divert to slop. Divert other side products to Fuel oil tanks / slop tanks.
xiii) Watch column top pressure and temperature. Adjust circulating refluxes and top
reflux if necessary. Raise the circulating reflux flow to suit conditions.
xiv) When transfer temperature reaches (BH/AM) 365 / 385°C put TIC-1409 on auto
and steady out the conditions. Introduce stripping steam to side strippers. Ensure
that condensate is drained before allowing steam flow to the strippers.
xv) Adjust cooling water, if necessary, to all product coolers to maintain run-down
temperature of Heavy Naphtha, Kerosene and HD around 45°C.
Bringing up Naphtha Stabilizer System
i) Start taking Naphtha from crude column overhead Naphtha accumulator by

maintaining its level (11-LIC-405) at about 50%
ii) Take about 75% level (11-LT-501) in Stabilizer bottom through 11-FIC-503.
iii) Commission 11-PIC-501 on auto setting at about 10.0 kg/cm2 g. Initially the
control valve 11-PV-501 will remain fully closed.
iv) Keep 11-FIC-502 (LPG product to ATU) manually closed.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
v) Divert KERO CR through Stabilizer reboiler 11-E-25 partially by adjusting to rise

stabilize bottom temperature gradually. Restrict rise in temperature to about 25
°C/h.
vi) Stabilizer pressure will tend to rise along with the bottom being heated by KERO
CR. PIC-1501 should be manually operated to gradually open 11-PV-501 towards
fuel gas system to maintain the pressure of the column. Condensable accumulated
in condensers should be periodically released to reflux drum 11-V-03. When
normal pressure (8.0 kg/cm2 g. at 11-PIC501) is reached normal working of the
column will be established. During the process of heating up, Stabilizer bottom
level will fail if rate of heating is too fast. Divert column bottom to caustic wash
unit through feed / Stabilizer bottom exchanger 11-E-19 A/B.
vii) Raise gradually Stabilizer tray temperature by adjusting 11-TV-501. When
temperature stabilizes at around 180 °C put 11-TIC-501 on auto. Sudden increase
of temperature and pressure will destabilize the column making heavy fraction to
go to the top. Then it will take longer time to stabilize. So increase or decrease of
temperature or pressure of Stabilizer shall be done gradually.
viii) When level appears in reflux drum, drain water from boot and pumps 11-P-11
A/B. Start refluxing to the column keeping 11-FRC-501 on manual control.
Maintain top temperature about 60 / 70 °C (BH/AM). When reflux drum pressure
reaches around 10.0 kg/cm2 g., open 11-PV-501 manually put 11PIC-501 on auto.
ix) Stabilizer column will remain on total reflux. Check sample of LPG for weathering
test. If it is found to be on-spec, route this product slowly to Amine Treating Unit
under flow control 11-FIC-502 cascaded with reflux drum level control 11-LIC-
501. Any abrupt operation in temperature, flow or pressure is likely to make LPG
off-spec.
Normalizing the Operating Conditions
When the normal transfer line temperature 365/385 °C (BH/AM) has been attained maintain
temperature and make further adjustments.
i. Adjust heater firing to maintain 365/385°C (BH/AM) at heater outlet.

ii. Check for normal product run down temperatures.
iii. When conditions have become steady take all remaining controls on auto one-by one.
Particular care should be taken in case of heaters control. Safety shutdown system for
low fuel gas pressure (which was on bypass initially) should be made operative.
iv. Take product samples. Make adjustment on operating parameters to bring the
products on-spec.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
v. When products are on-spec., route them to respective tank / down-stream units.
vi. When vacuum unit is ready to receive RCO, RCO will be diverted to vacuum furnace
inlet.
vii. Check locally temperature, pressure, flow and level of different equipment and
streams. Also check for normal functioning of pumps, heaters and other equipment.
Commissioning of Desalter
Desalter will be brought into service at this stage before commissioning vacuum section.
i. Stabilize Desalter 11-V-02 pressure at about 10.5 kg/cm2 g. by PIC-1105. Control the
Desalter temperature at about 120°C. Check oil water interface level through the try
lines and check for any presence of vapor.
ii. Switch on the power supply to Desalter. High voltage and low amperage should be
indicated by voltmeter and ammeter respectively.
iii. Line up for water injection at Desalter inlet and start injection at about 4% (by
volume) of crude throughput. Also line up effluent water circuit.
iv. Start caustic injection pump 11-PM-13 A/B/C and inject caustic solution into suction
of crude charge pump 11-P-01 A/B and crude booster pump 11-P-02 A/B to maintain
the effluent brine pH at about 10.0
v. Start Demulsifier pump 11-P-16 A/B and inject Demulsifier at crude charge pump
suction at the rate of about 1.5 to 2 ppm on crude charged.
vi. Commission LP steam and water in the wash water heater 11-E-18. Commission level
controller LIC-1102 and route Desalter water to waste water treatment plant.
vii. Take samples of crude before and after Desalter and readjust operating condition for
getting following performance.
i. Salt content as NaCl at the outlet should be 3.0 mg/1 or 5% of salt content of raw
crude whichever is greater.
ii. The insoluble water content in desalted crude should be less than 0.15% (Max) by
volume and the effluent brine should have oil content less than 100 ppm (Max).
12.3.2 Vacuum Section
While start-up in Atmospheric section is in progress, vacuum section should be made ready
systematically as per the following sequence:
1. Elimination of air and vacuum test

2. Fuel Gas backing in and water draining
3. Cold circulation with gas oil
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
4. Hot circulation
5. Feed cut-in
6. Bringing up the unit
7. Stabilization
It is to be ensured that RCO does not enter the vacuum section while it is still not ready.
Blinding at the appropriate places may be necessary if valves are suspected to be passing. It
becomes mandatory if maintenance work is planned in the vacuum column while
Atmospheric section is on-stream.
Elimination of air
Air will be eliminated from the system by pulling vacuum.

i. Commission water to ejector condensers 12-E-07 A/B/C.
ii. Ensure normal level in hot well with vent open to Atmosphere from hot well catch pot
12V03. Ensure that hot well seal compartment is filled with water and the seal is
maintained.
iii. Slowly start pulling vacuum in the system. Commission one of the third stage
ejectors, to be followed by second and first stage. Vacuum pulling should be done
slowly. 12-PRC-206 may be used for this.
iv. Air will be gradually drawn out from the system including furnace coil and other
connected piping and equipment.
v. Watch pressure in the system. Gradually lower the pressure to the maximum possible
extent. Operate control valves and exchanger bypass to subject all equipment and
pipes to vacuum for pulling out air.
vi. When there is no further lowering of pressure, block off the system. Isolate at ejector
inlet and outlet and simultaneously shut off steam. Isolate 12-PV-206.
vii. Observe the rate of fall of vacuum. Initially there may be rapid drop during the
process of blocking off. If the rate of fall of vacuum does not exceed 0.05 kg/cm2 g
per hour (approximately 40 mm Hg per hour), the system is assumed fairly tight.
Otherwise thorough leak checking has to be carried out by pressurizing the system to
about 1 kg/cm2 g. with air and applying soap solution on every flange / joint.
Backing in Gas
1. Ensure all vents are closed and properly capped.

2. Slowly admit fuel gas through fuel gas back up line and break the vacuum. Adjust gas
backing such that fuel gas system is not disturbed during this operation. Pressure
surges during fuel gas backing in should be avoided.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
3. Isolate the liquid seal at the hot well during fuel gas backing. Valves in hot well vent,
drain and overflow line are to be closed.
4. Maintain the pressure in the system at 0.5 kg/cm2 g. by regulating the fuel gas inlet
valve or by opening the vent to Atmosphere on the hot well.
5. Open the low point drain one by one and drain out condensate completely. Check list
is to be prepared to ensure that all drains are made free of condensate. A log should
be kept for drain check showing the time of check, absence of condensate and initials
of the person who made the final check on the drain. Each drain must be closed as
soon as gas issues from it.
6. Back up gas from column to the heater up to feed inlet flow control valves and then to
the short residue pump discharge through start up line.
7. Back up gas from column to all pump around reflux and internal reflux circuits.
8. Back up gas from column to all the product run-down lines through internal and
circulating reflux lines from the column.
9. Drain out water from the following points:
Preheat Exchangers
Transfer line
Pump around and reflux lines
All product circuits up to B/L
Quench line through control valve bleeders
All pumps
All exchangers and coolers
10. Repeat draining operation every half an hour till no more condensate is drained.
Maintain the whole system at 0.5 kg/cm2 g. fuel gas pressure. Ensure all vents and
drain points are closed and capped off.
Cold oil circulation
Commission cooling water to surface condensers 12-E-07 A/B/C (three-stage ejector

condensers).
i. Commission tempered water system if not commissioned already by taking DM water
to 12-V-02. Establish the system by running 12-P-07 A/B.
ii. Admit flushing oil into the column through the 4" gas oil (cutter) line through the
connection provided for this purpose.
iii. Build up level in vacuum column up to 70%. Settle and drain water.
iv. Start the pump 12-P-01 A/B and keep gas oil flow of about 25 m3/h through each coil
of 12-F-01 keeping FRC-101/102/103/104 on manual.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
v. Maintain the column bottom level at by making up, if required, with gas oil. Stop
circulation after 1 hour. Allow water to settle and drain out from all low points. Repeat
the operation till no water appears through the drains.
vi. Route about 15 m3/h of start up gas oil to the top of the column through the 4'' start-up
line connected to LVGO CR return header. Regulate the flow by 12-FRC- 205.
vii. When level appears in LVGO draw-off tray, start refluxing in the HVGO packing at a
rate of around 20 m3/h through 12-FRC-201. Through LVGO CR circuit, maintain a
flow of around 50 m3/h by controlling 12-FRC-205
viii. Similarly activate HVGO pump and reflux the wash zone packing. Control the flow @
20 m3/h by keeping 12-FRC-202 in manual control. Put around 200 m3/h through
HVGO CR circuit to maintain the minimum pump capacity though 12- FRC-203.
ix. When level appears in the slop distillate draw-off tray, start 12-P-02 A/B after draining
water. Recycle about 20 m3/h of slop distillate to the furnace inlet though 12-FRC-
109. Raise the furnace feed flow appropriately to accommodate this quantity.
x. Maintain column and tray levels around 50%. Now circulation is established through
all circuits except quench line.
xi. Operate all control valve bypasses and exchanger bypasses to remove water from these
points.
xii. Stop all pumps every one hour and allow a settling time of one hour. Drain water from
all low points in the system. Restart circulation. Repeat this operation till no further
water issue out of the drains.
xiii. In case level tends to increase due to too much flushing oil drawn into the system,
some of it can be routed to slop.
xiv. Drain-out water from the quench line through all low points. Divert RCO from VR
circuit to Vacuum column through quench line c/v for about 10 minutes to flush out
water / condensate from the quench line c/v and bypass circuit. Care should be taken to
close the quench line c/v and bypass immediately after flushing to avoid vacuum
column build-up.
xv. During the circulation care should be taken to maintain the system pressure at 0.5
kg/cm2 g. by FG back-up. Release the excess gas to Atmosphere from the hot well in
case pressure goes beyond 1 kg/cm2 g.
Hot Oil Circulation
When cold oil circulation has been well established and water in the system has been
thoroughly drained out, the system is ready for hot oil circulation. Utmost care should be
taken in de-watering the system completely to prevent water shot and damage to the column
internals.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
After ensuring that atomizing, snuffing and emergency steam headers to the vacuum furnace
are commissioned, hot oil circulation is established as follows
i. Establish fuel oil circulation through the Fuel Oil circuit of 12-F-01.
ii. Restart pump 12-P-01 A/B and establish flow through each furnace coil of 12-F-01 at
about 25 m3/h. Put all the four flow controllers 12-FRC- 101/102/103/104 on auto
control and observe the performance.
iii. Continue tray to tray circulation including pump around as mentioned earlier.
iv. Maintain column bottom level around 50%
v. Fire the furnace as per the normal procedure. Light 1 or 2 burners initially and
increase the number of burners as the temperature is raised gradually taking care that
the burners are equally spread in the fire box. When steady flame condition is
established, increase transfer line temperature to 120°C at 30°C/h rate with the help of
TRC-2133. Hold the temperature for about 4 hours. Ensure that entire column is
heated up to about 110°C. This will ensure that the water accumulated in the trays will
be removed as steam in the overhead system.
vi. After holding transfer temperature at 120°C and removing water completely from the
entire system, transfer line temperature is to be raised further. Any oil level build-up
in the hot well and trays may be pumped out to slop.
vii. Before raising temperature beyond 120°C shut off 4” start-up line connection to
LVGO circulating reflux. Also stop flow of internal reflux from tray to tray (FRC-201
/ 202). Stop LVGO, HVGO and slop distillate pumps as and when they lose suction.
viii. Continue gas oil circulation in the bottom section of column.
Cutting in Feed
When the system temperature is 120°C it is assumed to be dry. Raise the transfer temperature
to 220°C at the rate of 30°C/h. Reduce the column level to minimum operating level, confirm
with second level transmitter and route excess gas oil to slop.
i. Maintain the system pressure around 0.5 kg/cm2 g. (make-up fuel gas if necessary or
release the pressure through hot-well vent at controlled rate)
ii. Hold the temperature until hot-bolting is completed in the column, transfer lines,
exchangers etc.
iii. Divert RCO slowly from 11-P-01 A/B discharge to 12-F-01. Line up 12-P-01 A/B
discharge to VR circuit which in-turn is lined up to the slop tank. Change level control
of crude column bottom to vac. Furnace flows once these are steady. Vacuum column
bottom level controller should be connected to 12-LV-202 and put on auto control.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
iv. Close 12-P-01 A/B to 12-F-01 and RCO to VR circuit. Monitor 12-F-01 firing. As
RCO temperature is 300°C firing in 12-F-01 requires to be reduced to keep the
temperature around 300°C..
v. Hold the temperature at 300°C and carryout hot bolting of flanges, heater coil plugs,
manholes, etc. Activate quench oil circuit and maintain about 10 m3/h flow. With
diversion of RCO to 12-F-01, once-through flow will be established and gas oil will
be displaced by RCO to slop tank. After displacing gas-oil, flow can be re-routed to
the appropriate tank. Normal capacity of 12-P-01 A/B is about 133 m3/h.
vi. Maintain system pressure at 0.5 kg/cm2 g. by backing-up fuel gas if necessary.
vii. During this period ensure the following:
Tempered water circulation is established
All coolers are commissioned
All product tanks are lined up
Slop tank has enough ullage to cater to the requirements of unit start-up.
viii. The hot well water side has to be maintained at 50 % water level. If sufficient water is
not available, fill up with fresh water through utility connection. Ensure that the seal
compartment drain line is blinded down stream of block valve to prevent mal-
operation of drain valve and losing of seal level.
ix. After completing hot bolting at 300 °C, bring the unit on stream by raising transfer
temperature at the rate of 30 °C/h.
x. Light fractions will be collected in the upper trays as transfer temperature is increased.
Tray pump-arounds and internal refluxes should be commissioned. Adjust product
routing to slop to hold tray levels. Watch run-down temperature while routing
products to tank.
xi. Commission slop-recycle stream from the discharge of 12-P-02 A/B to RCO feed line
of the heater. Adjust flow to about 6-7 m3/h through 12-FRC-109.
xii. Shut off FG to 12-C-01 overhead, if open.
xiii. Adjust quench flow to keep 12-C-01 bottom temperature at 350°C.
xiv. Commission steam to third-stage ejectors 12-J-03 A/B/C after thorough draining of
condensate from the steam header. Before that ensure that hot well catch pot vent is
opened to Atmosphere.
xv. Commission 12-PRC-07 and maintain the steam pressure at desired level.
xvi. Pull vacuum by increasing the steam flow rate gradually. Care should be taken so that
the pumps connected to the system are not affected. Activate pressure controller 12-
PRC-206 manually to avoid pressure system surge in the column
xvii. Activate sour water pump at hot well bottom and route water to sour water stripper.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
xviii. Anticipate lifting of light oil from trays into hot well when vacuum is pulled. Pump
out the oil from hot well through slop oil pump 12-P-05 A/B to slop. Check the
operation of interface level controller 12-LDIC-201.
xix. Once the system is normalized i.e., all pumps are working satisfactorily, commission
the 2nd stage ejector 12-J-02 A/B/C and increase the system vacuum gradually.
Watch the performance of the pumps.
xx. Once system is stabilized with 2nd ejectors on operation, commission 1st stage ejector
12-J-01 A/B/C gradually. Pull vacuum to about 7mm of Hg absolute pressure at the
top of the column. Put pressure controller 12-PIC-206 on auto and set the top pressure
in such a way that flash zone pressure reads 24 mm Hg absolute.
xxi. Raise the transfer line temperature to 395 – 400°C as required based on the crude in
slow intervals. Adjust quench rate, draw off rates etc., on pro-rata basis and steady out
conditions.
xxii. Send samples of LVGO, HVGO and Short residue. Route them to respective tanks
when they are on-spec.
Raising to Normal Throughput
At this stage normal operating conditions are established for both Atmospheric
section as well as vacuum section with 50% of normal capacity of the plant. All products are
routed to their respective storage tanks / down-stream plants.
Feed rate of the plant is to be raised to its normal capacity in steps as outlined below:
Raise the feed to Atmospheric furnaces by 50 – 60 m3/h.
Steady out transfer temperature at (BH/AM) 365/385°C. Check all furnace controls
for proper functioning.
Adjust draw-off of Heavy Naphtha, Kerosene, LVGO and HVGO to maintain
respective draw off temperatures.
Make adjustment to the stripping steam in the main column bottom and side strippers.
Raise circulating refluxes proportionately to maintain column temperature profile.
Adjust RCO draw off to maintain main column bottom level and adjust draw off of
LVGO, HVGO and Slop Distillate in the Vacuum Column. Raise the circulating
refluxes of vacuum column proportionately.
Steady out all parameters including vacuum furnace controls.
Check samples of all products. If any product goes off spec. divert it to slop tank and
make adjustment as detailed under operating variables to bring the product to
specification.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 12
PLANT NAME: CDU II
Chapter Rev No: 0
Raise the throughput further only when all products are on-spec. Raise the throughput
to maximum by steps with the procedure outlined above. Establish operating
conditions in each step.
Keep watch on the running equipment, heaters etc. Look for leaks and any
abnormalities.
Take hourly log readings and report any abnormal conditions to the supervisor
immediately.
Keep watch on ejector performance. Adjust water flow to the condensers, and product
coolers to achieve required temperature, pressure, vacuum etc.
Refer to section which shows the normal operating conditions and make necessary
adjustment on operating parameters.
Chemical Injection to Atmospheric Section
Start caustic injection pumps 11-P-13 A/B/C and inject caustic (about 5% solution in
water) at the suction of crude charge pumps 11-P-01 A/B and crude booster pumps 11-PM-02
A/B. Rate of caustic injection should be limited to a maximum to avoid caustic embrittlement
of downstream equipment and process lines at higher temperatures. Line up ammonia
cylinders and inject ammonia gas in to the crude column overhead vapor line. Adjust the rate
of injection of ammonia to such an extent that the crude column overhead reflux drum water
pH is around 6.5 + 0.2. Start corrosion inhibitor dosing simultaneously and adjust the rate of
injection as per requirement.
12.3.3 CDU/VDU Startup Procedure after Short Shutdown
a) Pre startup checks
i)Check all the pump couplings, direction of rotation, lube oil levels and BCW flow to
all pumps.
ii) Check all the utilities and inform the respective units/sections about their
consumption
iii) Check then proper functioning of fire fighting equipment in unit
iv) Check all the line-ups
b) Startup
The startup procedure is similar to that discussed in feed cut in and stabilization section with
slight modifications. The modifications are
i)The 11-F-01 COT can be raised at the rate of 120°C/hr

ii) Hot bolting is not required in the vacuum section.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 13
PLANT NAME: CDU II
Chapter Rev No: 0
START UP AFTER T&I
START UP AFTER T&I
During T&I normally many agencies from various departments like projects, maintenance
electrical, instrumentation, rotary, onsite, off-site, civil, Technical (PAD, Inspection, MES)
and minor projects carry out their respective jobs in parallel such that the down time of the
unit / equipment is optimally used for completing various planned jobs in time.
Normally towards the end of the T&I under pressure of time to meet planned
schedules, situations do occur with chances of improper completion of jobs as per standard
practice. If these gaps are not corrected through a proper system of checking, it induces
unintended and unknown amount of risk into the startup process which could lead to major
accidents or costly down time.
Thus need exists to do a comprehensive check from various angles by respective

disciplines, when the unit is getting ready for startup. In the recent past, there were instances
in so many refineries, in which the unit had to be immediately shut down due to the need to
change improper gaskets which remained in position without proper checking.
Start-up clearance procedure to be followed to ensure safe, smooth and incident free
startup of the Unit after planned Turnaround & Inspection (T&I). The start-up clearance
procedure is intended to ensure that the plant equipment is properly closed as per checklist
and restored to normalcy for a safe start-up and operation after T&I. In other words, it
ensures that no additional risk is induced into the whole system due to improper work during
T&I. This start up clearance is a prerequisite for unit / equipment start-up and shall be
completed before introducing any hydrocarbon.
13.1 DEFINITION OF ‘START-UP CLEARANCE’:
“Startup clearance” is a formal means of assurance by various functional disciplines about the
satisfactory and proper completion of their planed respective functional activities during the
T & I. This clearance serves as assurance of non-addition of any safety risk and also
authorization for the commencement of startup activity. This clearance is normally issued
after thorough checking for proper completion of all planned activities as per work procedure.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 13
PLANT NAME: CDU II
Chapter Rev No: 0
START UP AFTER T&I
Steps for unit start-up post T&I consists of the following:
1. Reviewing and assessment of T&I jobs completion status.

2. Seeking ‘start-up clearance’ from each section of concerned dept.
3. Receiving the ‘‘start-up clearance’ and ‘exception job’s list’ (if any)
4. Obtaining approval from HOD (Maint. & Opns.) For start-up, pending ‘exception jobs’.
5. Obtaining ‘final start-up clearance’ from division head - operations.
6. Proceeding for start-up.
1. Reviewing and assessment of T&I jobs completion status:
The unit Manager (Operations) shall take assessment of the readiness of the unit for start-up
and intimate concerned sections of Maint. / Tech. / Projects seeking “Start-up clearance”.
Keeping in mind the nature of jobs carried out in the unit during the period of shut down, he
would originate-
a. Letter of Request for “Start-up Clearance” for obtaining full-fledged start up clearance
from all concerned sections (4 days prior to start-up date).
b. “Waiver for Start-up Clearance”, if any, for obtaining ‘Waiver’ for some sections whose
activities were minor / nil during the S/D. The waiver shall be adjudged and approved by
Division Head - Operations. Letter to be initiated 4 days prior to start-up date (parallel to
case- a.)
2. Seeking ‘start-up clearance’ from each section of concerned dept.
All the concerned sections (Maintenance / Tech. / Projects) should be notified 96 hours in
advance by UAT Leader (Manager - Operations), indicating clearly the date and time of the
proposed commencement of start-up activities and indicating the time by which this
‘clearance’ should reach him back.
3. Receiving the ‘‘start-up clearance’ and ‘exception job’s list’ (if any)
After receiving the intimation about startup plan the concerned Section Head (Maint. / Tech. /
Projects) should immediately assign the respective UAT member (or alternate designated
person) for thorough & systematic checking (through check list) of relevant activities carried
out by them. They shall ensure internally that proper and detailed system of checking is put in
place for thorough checking prior to issuance of 'Start up clearance'
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 13
PLANT NAME: CDU II
Chapter Rev No: 0
START UP AFTER T&I
4. Obtaining approval from HOD (Maint. & Opns.) For startup, pending ‘exception jobs’ (if
any).
The 'Startup Clearance' from individual sections of Maint. / Tech. / Projects to be taken. Each
of the respective section head has to develop detailed / elaborate internal check list (which
need not be sent to operations) using which a detailed checking should precede the issuance
of 'Start up clearance'. Developing and implementing the required 'internal checking system'
is the responsibility of respective functional section heads of Maint. / Tech. / Projects. It is
expected that the 'Start up clearance' shall reach the Unit Area Team leader (Oprns) within 24
~ 36 hours of receipt of intimation (at least 48 hours before commencement of startup.
5. Obtaining ‘final start-up clearance’ from division head – operation

The final 'Startup Clearance' to be taken from the Division Head-Operations. After obtaining
clearance only actual field activities for startup are to be started.
6. Proceeding for start-up :
Check the unit for completion of mechanical work against P&ID with new changes.
1. Remove all construction debris lying around in the unit and clean up the area.
2. Install blinds as per master blind list. Each blind removal and insertion of blind should be
entered in the blind register.
3. Safety valves should be kept blinded during flushing and re-installed afterwards. These
should be shop tested and set at the stipulated values.
4. Ensure that underground sewerage system is in working condition. Clear plugging, if any.
Check by flushing with water.
5. Check that communication between units, control room, Offsite and utilities are complete and
in working condition.
6. Ensure that the required lube oil, grease and other consumable are available in the unit.
7. The proceedings for startup activities are as below
a. COMMISSIONING OF UTILITIES
b. WATER FLUSHING OF PROCESS LINES
c. FUNCTIONING TEST
d. CALIBRATION OF INSTRUMENTS
e. FURNACE DRYING
f. TIGHTNESS TEST
g. CHARGING OF CHEMICALS
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 13
PLANT NAME: CDU II
Chapter Rev No: 0
START UP AFTER T&I
The explanations of above activities are mentioned in chapter number 10. Please refer chapter
number 10.
8. After these preliminary activities are completed the startup procedure is same as the normal
startup procedure. The steps to be followed as below
a. Removal of air from the unit by steaming
b. Tightness testing under steam purge
c. Backing in fuel gas
d. Cold oil circulation and removal of water.
e. Hot oil circulation.
f. Bringing the unit on stream.
The explanations of above activities are mentioned in chapter number 12. Please refer chapter
number 12.
Note: Before going for the start up the startup check list to be filled by respective
person as mentioned in the document. The startup check list document is available
in chapter number 34.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 14
PLANT NAME: CDU II
Chapter Rev No: 0
OPERATING LIMITS AND CONSEQUENCES OF DEVIATIONS
All the equipment used in the unit has some operating limits. The limits of any
equipment, line, etc should always be respected. The limiting parameter for all equipments
will be different and the values should always be kept in mind to follow them. The deviation
will result in severe consequences like unit upsets as well as equipment damage. This may
also result in unsafe working conditions. The values can be obtained from the design package
of the unit or the soft copy present in form MS- Excel sheets.
14.1 PUMPS:
The pumps have their operating parameters provided by the vendor. Every machine is
designed to work at some optimum condition and also the maximum deviation it can handle
from its optimum value. For pumps, the operating parameters are maximum and minimum
flow, suction pressure and discharge pressure, differential head and net positive suction head.
For a pump, the vendor provides the value of normal flow as well as maximum and minimum
flow. If the pump flow is within the limits of maximum and minimum flow, then it will be
healthy. If the pump flow is beyond its maximum limit, it means that the pump is overloaded
and it is pumping liquid more than what it has been deigned. So there is a chance of the pump
tripping on overload. In such conditions, pump amperes has to be continuously monitored
and compared with full load current. The pump flow has to be more than the minimum flow
so otherwise the pump starts loosing suction and will suffer more vibrations. This damages
the pump bearings, seal as well as can harm the pump impellers.
The pump suction pressure also has to be more than its minimum suction pressure. If the
pump doesn’t get suction at the desired pressure, it will also damage the pump bearings, as
well as the mechanical seal and if the problem is not attended and the pump is kept running,
the impellors will also get damaged. The pump discharge pressure also cannot be violated as
it will overload the pump in trying to increase the discharge pressure.
The pump differential head and NPSH are required to know the exact pumping capacity of
the pump and if the pump is not able to meet them, it is an indication that something is wrong
with pumping capacity.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 14
PLANT NAME: CDU II
Chapter Rev No: 0
14.2 HEATERS:
Operating temperatures and pressures of the heater is the temperature and pressure at which
the process liquid enters and leaves the heater. If the inlet temperature of the process liquid in
the heater is low, the energy required to raise it to required temperature will be very high.
Sometimes it will not even be possible for the operator to bring the COT to the desired value
due to limiting parameters like arch and skin temperatures. The operating pressure also has to
be between the limits because high pressure will develop chances of tube rupture and leaks.
Low inlet pressure means the velocity of process fluids in the line will be slow and that will
lead to higher cracking and coking of heater tubes. Outlet pressure also need to be maintained
at a desired value and drop in the outlet pressure when inlet pressure is normal, is an
indication of heater tubes getting coked up.
Heater TURNDOWN value is 50%. It means that if the heater feed is less than 50% of its
operating value, then it cannot be kept in service and has to be shutdown. This is for meeting
minimum flow requirements of pass flows. The fuel gas pressure has to be maintained
between its maximum and minimum values. If it goes below its minimum value then the gas
flow will experience back pressure and the supply will get stopped creating unsafe
conditions. If the pressure is very high, it will damage the gas rings and the tip size will also
get enlarged or the opening will get eroded. The same is for fuel oil because very high steam
pressure will erode the oil gun tips. Very less fuel oil pressure will congeal the fuel oil lines
and thus will stop the fuel oil flow completely.
Fuel oil viscosity should also meet the desired specifications because a very high fuel oil
viscosity again will stop the flow of oil in the lines. Atomizing steam pressure also has to be
maintained because a high steam pressure will erode the tip of the gun and a very low steam
pressure means that atomizing will not take place. There has to be a minimum amount of
difference between the pressure of oil and steam so that it can atomize fuel oil. The fuel oil
will not ignite until it is in atomized form. So the atomizing steam has to be properly used for
best results in the heater.
14.3 HEAT EXCHANGERS:
Heat exchangers are used as preheat exchangers, coolers and condensers in the unit. Even
though the usage may be different, operating parameters for all of them are mostly same.
They have inlet and outlet temperatures which need to be maintained. Every preheat
exchanger needs to maintain the outlet temperature because the outlet of the exchanger will
be the inlet stream to some other equipment. If the outlet doesn’t meet the operating value i.e.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 14
PLANT NAME: CDU II
Chapter Rev No: 0
the deviation is very high, the temperature of the stream will be very less or very high for the
next equipment. If the temperature of the inlet is very less, it becomes very difficult to attain
the outlet temperature because the requirement of temperature raise will exceed the duty that
exchanger can provide. Also if the temperatures are very high at the inlet and outlet, they may
result in channel section leaks, and also gasket may give up resulting into emergencies.
The pressure on the shell side and tube sides are also monitored as the operating procedures.
If the pressure is too high on either side, it may result into leaks and thus creating
unnecessary emergencies and equipment damage. A very less pressure on either side means
sufficient flow will not be established and the heat transfer will not be effective. Thus the
operating pressure should be maintained as mentioned in the design manual to get maximum
output from every exchanger under safe limits.
14.4 COLUMNS:
The column limits on the conditions like the column DP and the product draw-off
temperatures. The parameters like DP are indicators for column internal condition like vapour
load and flooding. High column DP is indicative that the column is flooding or the vapour
load in the column is very high. For the total height of 11-C-01, the column DP should not
exceed 0.40 kg/cm2. More column DP will result in the colour of products going off spec as
the heavier ends will contaminate the lighter products by rising up in the column. Also a very
high vapour velocity may erode the internal surfaces of the column and also cause damage to
the trays.
Column draw-off temperature for every products draw-off is specified in the design package.
The draw-off temperatures affect the qualities of the products. A very high draw-off
temperature of a product will make it heavier. The product may become off on distillation.
Also if the temperature at a particular tray is high, the CR pumps design suction temperature
may be violated and the pump may get damaged. A very low draw-off temperature means the
product will become lighter and the IBP and the flash of it may go down.
14.5 CDU-II ALARM VALUES:
TAG NO. DESCRIPTION SETTING

LL1401 Atmos column bottom level low 40
LH1401 Atmos column bottom level high 70
LL2201 Vac bottom low switch 40
LH2201 Vac. Column bottom high 70
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 14
PLANT NAME: CDU II
Chapter Rev No: 0
LL2203 Vac. Column HVGO level low 30

LL2204 Vac. Column LVGO level low 30
LL1501 Stabilizer bottom level low 30
LH1501 Stabiliser bottom level high 75
LL1902 PFD level low 30
LH1902 PFD level high 80
LL2202 Vac. Slopcut level low 30
LL2401 Tempered water low 30
LH2401 Tempered water high 80
LL11P11A LPG pump seal level switch A -
LL11P11B LPG pump seal level switch B -
PH1807 11F01 ID Fan Suction Pr. Indication -60
PH1807A 11F01IDFan Suc. Pr.high -40
PH2507 ID fan suction Pr.high -60
PH2507A ID fan suction Pr.high -40
PL1806 11F01FDFan dis.Pr.Low 15(18)
PL2506 FD fan Discharge Pr.Low 8(14)
PR1808 11F01 Pr. Control +1.0
PR1809 11F01Pr.Control(switch) +2.95
PR2508 12F1 Pr.Control +1.0
PO2509 12F1 Arch Pr trip +2.95
11-PAL-301 11F1 fuel oil pressure low 2.77
11-PAL-303 11F1 fuel gas pressure low 0.2
12-PAL-106 12F1 fuel oil pressure low 2.77
12-PAL-108 12F1 fuel gas pressure low 0.2
11FR301 Crude to Pass A 42
11FR302 Crude to Pass B 42
11FR303 Crude to Pass C 42
11FR304 Crude to Pass D 42
12FR101 RCO to Pass A 14
12FR102 RCO to Pass B 14
12FR103 RCO to Pass C 14
12FR104 RCO to Pass D 14
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
NORMAL OPERATION OF THE PLANT
15.1 OPERATING VARIABLES OF ATMOSPHERIC SECTION:
It is important that operation of CDU be conducted to produce products of desired quality. At

the same time appropriate controls should be exercised on certain parameters to prolong the
life of the equipment. The following discussion will give the guidelines about affect of the
variables and measures to be taken to achieve the desired result.
15.1.1 Desalter Operating Variables:
Only operating experience with desalter can determine optimum operating conditions.
No two crudes behave alike at the same desalting conditions, but all are affected similarly by
change in desalting conditions.
a) Water Injection and Pressure Drop:
Water injection should be started only after crude reaches a specified level and power is
switched on to the grid. Initially the injection rate should be limited between 2-6% of crude
flow rate and point of injection should be just ahead of the emulsifying valve. Pressure drop
across the emulsifying valve should be 0.3-1.0 kg/cm2. Higher pressure drop ensures more
efficient contact between the salt n the crude and the injection water. Too high pressure drop
will result in excessive emulsification and poor separation of oil and water, resulting in carry-
over of water in desalted crude. Injection of water can also be done before feed pump suction.
Injection at feed pump suction point results in maximum contact and also prevents the
sediments from settling in the exchanger tubes and fouling them. But care should be taken
such that the intense shearing agitation in the preheat train does not create so tight an
emulsion that cannot be resolved in the Desalter. The severe shearing effect due to the crude
pump impellers should also be considered here. The quality of water is a very important
aspect.
b) Oil water Interface:
The oil water interface level should be kept below the centre line of the vessel. Incorrect
operation of the interface level controller can result in more water in the desalted crude due to
less hold up time available for oil (high interface level) and more oil carryover in brine due to
less hold up time available for water (low water level). Also too high interface level may put
watery mixture up between the electrodes and cause them to short out.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
c) Desalter Vessel Pressure:
The pressure in the vessel should be maintained about 10.5 kg/cm2. A low pressure
will cause vaporization of the crude and high pressure will result in lifting of the safety valve
on desalter.
d) Desalter Temperature:
Temperature is another important variable which affects oil water separation in desalter.
Most crudes have an optimum operating temperature range of 120-130 °C. Lower the
temperature higher the viscosities of the oil which slows down the separation rate. As
conductivity of crude increases with temperature, operating temperature beyond the range
will lead to drop in grid voltage and high amperage which imposes limitation on good
separation. Excessive amperage will eventually cause the circuit breaker to open, removing
the grid voltage and rendering the electrical system inoperable until the thermal delay is
closed. Moreover very high temperature may lead to vaporization of crude in desalter.
e) Demulsifier Injection:
Stable emulsions can also be broken by use of demulsifying agents. The amount of chemicals
required depends on the nature of emulsion, type of crude and other operating conditions like
residence time, temperature, etc. tests should be made to ascertain the required chemical
injection rate for optimum operation of desalting unit.
f) Voltage and Amperage:
The electrical panel houses 3numbers of voltmeters and ammeters. The voltmeter gives the
voltage across the primary circuit of the transformer. The ammeter gives the current flow.
These meters give an indication of the performance of the grids inside the desalter. Incase, if
crude/water emulsion is too tightly bound or if the interface level is too high the amperage
will increase and voltage will drop. Take corrective action to break the emulsion or reduce
the interface level.
15.1.2 Heater Outlet Temperature and Column Pressure:
The quantity of crude oil vaporized during its passage through the heater depends on transfer
temperature and pressure at the flash zone of the column. In order to achieve proper recovery
of distillates little over flash is maintained, by keeping the transfer temperature slightly
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
higher. This flow is about 6% volume of crude chare. This also indicates the presence of
liquid levels in the trays down below the diesel draw off for avoiding dry operations of these
trays (nos. 7 to 11). Maintaining high over flash rate will result in more consumption of
energy. Heater outlet temperature is controlled by 11-TRC-301.lower temperature will not
give desired distillate recovery, bottom product RCO will be lighter and all side draw offs
will also be proportionate to lighter. Higher than normal temperature enhances cracking
possibility and at the same time specification of every product may not be met.
The pressure in the column is maintained by split range pressure controller11-PRC-409 A/B.
A low pressure aids in greater vaporization. All products will be heavier and there will be gas
loss from reflux drum. Higher than normal pressure will have reverse effects. Efforts should
be made to operate the column at the designed pressure of 0.6 kg/cm2g at the reflux drum.
Adjust cooling water flow in the cooler 11-E-17 A/B/C/D/E/F/G/H in such a way that there
is total condensation and both the control valves (11-PV-409 A/B) of split range controller
remain shut.
15.1.3 Crude Column Top Temperature:
The column top temperature is controlled by regulating amount of overhead reflux through
11-FRC-403. Top temperature is continuously recorded by the recorder. Lowering of top
temperature will reduce FBP of naphtha and flash point of heavy naphtha. Too low a
temperature will start stem condensation at the top section of the column which may likely to
increase rate of corrosion at the top. Raising the temperature will increase FBP of overhead
naphtha and IBP (flash) of Heavy Naphtha.
15.1.4 Pump Around Flows:
The pump around/ circulating reflux serve mainly in withdrawal of heat from the column and
to reduce the vapor liquid traffic in the appropriate section of the distillation column. There
are three circulating flows- Top Pump Around (TPA), KERO circulating reflux and diesel
circulating reflux. These flows are respectively controlled by flow meters. 11-FRC-
404/405/408. The return temperature is maintained by operating the respective exchangers.
Return temperature are indicated by 11-TI -414(TPA). 11-TI-413 (KERO CR) and 11-TI-
412(Diesel CR). A high TPA flow will result in decrease requirement of overhead reflux and
affect the quality of light naphtha. The overhead condenser duty will come down as there will
be correspondingly less O/H product. Similarly a high Kero CR flow will tend to lower the
plate temperature of heavy naphtha and kerosene draw off resulting in lighter product in these
trays. The gap between naphtha and kerosene will decrease.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
Likewise a high diesel CR will tend to lower the draw off temperature of kerosene and diesel.
Increase of circulating reflux will result in higher crude preheat temperatures by greater
recovery in heat exchanger train.
15.1.5 Product Withdrawal Temperatures:
The withdrawal temperature of a product from the column influences the end product of the
product. This is determined by quantity of the product withdrawn from the stripper. An
increase in withdrawal rate of the side stream increases the withdrawal temperatures and the
end point of all side stream lower down the column unless withdrawal rate lower down the
column are reduced correspondingly. For example, if kerosene withdrawal rate is increased,
the internal reflux in the trays below the draw off tray will be reduced which will lead to flow
of heavier vapors above the tray. This increases the end point of kerosene. If diesel
withdrawal rate is not reduced to maintain its plate temperature, its initial boiling point (flash)
will go up.
Similar reverse action takes place when withdrawal temperature is lowered by

reducing the quantity of withdrawal.
15.1.6 Stripping Steam:
a. Atmospheric Column Stripping Steam:
At 10.5 kg/cm2g pressure and 350 °C, superheated steam is used to strip lighter fraction from
the reduced crude in the lower part of the crude tower. Design steam rate is about 4585 kg/hr
for Basrah crude. This is assumed to be optimum rate for economical stripping and should not
be varied much. Lowering the rate below the optimum may leave some lighter component in
the reduced crude and is undesirable. Exceeding the design rate might cause entrainment of
reduced crude into the diesel because of excessive vapor velocity and also will overload the
over head condenser system. The flow of steam controlled by 11-FRC-401.
b. Stripping steam in heavy naphtha, kerosene and diesel stripper:
The initial boiling points and flash points of heavy Naphtha, Kerosene and Diesel products
are controlled to some extent by varying the stripping steam rate to stripper 11-C-02/03/04
respectively. Steam at 10.5 kg/cm2g and 350 °C used for these strippers. Steam flows are
indicated by 11-FI409/11-FI-408/ 11-FI-407 and regulated by respective control valves.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
It is advisable not to exceed the steam flow rate of its designed value viz. Heavy naphtha
stripper -444 kg/hr. kerosene stripper-1496 kg/hr and diesel stripper-1906 kg/hr, as this will
tend to lift some of the high boiling materials. In case if the desired flash point could not be
reached by designing rate of stripping steam, the draw off temperature at the product just
above it to be increased to enhance its flash.
15.1.7 Corrosion Control of Overhead system of Distillation Column:
Hydrochloric acid formed from the hydrolysis of salt present in the crude and hydrogen
sulphide formed dissolved in the crude (formed from the dissociation of heavy sulphur
compounds present in crude), goes to the overhead system. Both form acid solutions which
are very corrosive. Measures must be taken to overcome their effects.
The overhead system including condensers and reflux drum are made of carbon steel.
Only to protect this section caustic ammonia solution and corrosion inhibitors are added at
the following points:
Caustic injection:
3. Suction of crude booster pump i.e. ahead of desalted crude preheat trains.
4. After the preheat trains before booster pump 11-PM-02A/B suction
Ammonia injection:
4. Suction of crude booster pump ahead of desalted crude preheat train
Corrosion inhibitor injection

The idea of injecting caustic and ammonia at the outlet of Desalter is for better mixing
of these chemicals with crude and neutralizes the acids/acid salts mainly HCl and H2s as
soon as it is formed(120 °C and above). Chance of H2S formation at this temperature is
remote. The reaction product is sodium and ammonium salts goes along with the educed
crude. The balance acids and acids gases if any will go up to the overhead system where
ammonia or ammonium solution is injected either along with reflux or in the overhead vapor
line fro neutralization. Amount of ammonia should be controlled in such a way that Ph of
reflux drum sour water remains around 6.0 to 6.5. Injection of caustic and ammonia at the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
outlet of Desalter should be maintained in such a way that the salt formation should be low in
the overhead which might scale up the overhead condensers tubes.
A slightly acidic condition of the overhead system is desirably to keep ammonium

salts in solution, which if precipitates would foul and plug the condensers.
Corrosion against slightly acidic condition is minimized by a adding corrosion

inhibitors in the overhead line. The inhibitor is also added in reflux line. The amount of
inhibitor injected depends upon the type of inhibitor used, and generally specified by vendor.
However, slight adjustment is made by operating personnel depending upon from content in
the reflux drum water. These inhibitors are filming organic compounds (amines) which
covers entire metal surface of the system with a thin film. This prevents contact of corrosive
water with metal.
Top section of the column is also benefited from the injection of inhibitors mainly in
the reflux line/ these inhibitors are high boiling compounds and can perform satisfactorily at
upper tower temperatures.
15.1.8 Stabilizer Temperature and Pressure:
Stabilizer removes the majority of butane and lighter hydrocarbons from the naphtha stream.
These are recovered as overhead LPG product. High top temperature will make overhead
product heavier, even pentanes may be carried into LPG, making it off-spec. Lower
temperature will reduce LPG, make. Vapor pressure of LPG may go beyond the specified
limit if top temperature is too low.
Bottom temperature if too low will result in higher than allowable vapor pressure
(RVP) of naphtha and at the same time it will reduces LPG make. Low pressure in the
column will cause higher amount of hydrocarbons (propane and butanes) to escape into fuel
gas system. This has got similar effect as that of higher temperature in the column.
15.2 OPERATING VARIABLES OF VACUUM SECTION:
The following variables of the vacuum column influence the quality of the products and
should be controlled to meet the product specification.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.2.1 Transfer Line Temperature:
The transfer line temperature is controlled by 12-TRC-133 on the outlet of the vacuum
heater, and should be adjusted to maintain the flash zone temperature around 395 °C. this
temperature determines the degree of vaporization and the level of heat in the liquid vapor
mixture, entering the vacuum tower for fabrication. This temperature will be varied
depending on the quantities of the desired distillates. But the furnace outlet temperature
should not be allowed to go beyond the designed limit of 415 °C after which the degree of
cracking increases rapidly. Detrimental effect of cracking or coke deposition on heater tubes,
transfer line and bottom line sections. It also increases quantity of non-condensable going to
the overhead system. The cracking can also have a detrimental effect in the curing qualities of
asphalt. Too low a transfer temperature will result in lower yields of vacuum distillates and
flash point of distillate cut may be lower.
15.2.2 Vacuum Column Pressure:
The column top pressure is controlled by 12-PRC-306 which recycles some non-
condensables to the ejector 12-J-01 A/B/C inlet line. The top pressure should be maintained
around 7-9 mm Hg absolute. Increase in pressure will result in reduced yield of vacuum
distillates and may lead to cracking of the feed. Reduction in top pressure further may result
in carryover of LVGO into the ejector system.
15.2.3 Flash zone pressure and temperature:
It is of paramount importance to maintain a high vacuum and temperature at the flash

zone with in the prescribed limit to obtain maximum yield distillates. The designed flash zone
pressure is 24 mmHg and temperature 395 °C. Fluctuation of vacuum will affect the product
quality adversely besides producing mechanical stress on column internals. Increasing the
flash zone temperature will result in greater yield distillates but cracking possibility is
enhanced. If for any reason, vacuum starts falling sharply, firing in the heater should be
reduced to bring down temperature of feed.
15.2.4 LVGO system:
The LVGO system is a combination of LVGO product, LVGO circulating reflux and internal
reflux for HVGO packing. The circulating reflux is sprayed over the LVGO packing through
a distributor. This stream is taken from the column and a part of LVGO after exchanging its
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
sensible heat with crude in 11-E-07 and cooled in coolers 11-E-22/22A in parallel, it is then
returned at a temperature of 65 °C to the column (12-C-01) under flow controller 12-FRC-
205 to maintain column to temperature of 80 °C. Because of crude throughput maximization,
it was observed that the Vac. Column temperature was frequently crossing the desired
temperature ultimately resulting in under control, LVGO CR from 11-E-07 outlet is modified
accordingly and routed to 12-E-12 A (top cooler), the outlet of 12-E-12 A routed to 11-E-
22/22A in parallel. Increasing the reflux will reduce the top temperature which will simply
increase the energy consumption. Reduction in reflux rate will increase the top temperature
that will overload the ejector and increase the slop production thereby losing LVGO yield.
The internal reflux to HVGO packing’s from LVGO draw off tray is maintained by
diverting a part of the LVGO from 12-PM-04 A/B pump discharge. This flow is regulated by
12-FRC-201. The LVGO product withdrawal rate is regulated by 12-LIC-205, which controls
the LVGO level. LVGO rundown flow is indicated by F2403R. LVGO draw off temperature
is 213 °C. the draw off temperature as well as LVGO product rate can be varied by increasing
or decreasing either LVGO internal reflux or HVGO circulating reflux. Increase in reflux
means reduction of LVGO draw off temperature and LVGO product flow rate and vice-versa.
A software switch is provided fro LVGO system when it is being routed to either
HVGO/LDO. When the switch is kept in position 1, LVGO level will be controlled by its
own LVC (LI2205). When the switch is kept in position 2, LVGO level i.e. LI2205 will be
cascaded with FR2404 (i.e. LVGO to LDO/diesel).
15.2.5 HVGO system:
The HVGO system is a combination of Wash liquid for wash zone packing, circulating reflux
(HVGO packing) and HVGO product. There wash liquid is given to the wash zone packing
for avoiding chocking of the packing area because of heavy asphaltenes. The chocking of the
packing zone would result in higher differential pressure across this zone and this will
adversely affect the column performance. About 80 m3/hr of HVGO is normally supplied as
wash oil, the flow of which is regulated by 12-FRC-202. An increase in wash oil flow will
reduce the carry over of asphaltenes in HVGO stream. More the desired quantity of this
stream may adversely affect the quality/yield of Vacuum residue. Less quantity of Wash Oil
may result in the carry over of heavy asphaltenes into HVGO stream.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.2.6 Slop Distillate and Recycle:
The object to provide slop recycle to furnace flow is to get desired over flash so as to ensure
proper recovery of distillates. A higher recycle rate will unnecessarily increase the energy
consumption. Recycle + slop distillates are draw from the chimney tray below the wash zone
packing. The draw-off rate of slop distillate product is regulated by 12-LIC-203 which
controls the level in the draw off tray. The recycle stream flow rate is controlled by 12-FRC-
102. Recycle rate at normal throughput is about 12.0 M3/hr.
15.2.8 Quench:
Quench flow is a slip of vacuum residue at 250 °C obtained after exchanger 12-E-03 and the
flow is regulated by 12FRC-204. Its temperature is indicated by 12-TI-202. The purpose of
providing quench is to prevent, coke formation at the bottom of the column by quickly
cooling Vacuum Residue from 395 °C to 350 °C. A lower temperature than this, i.e. higher
quench is not wanted because of disproportionate increase of energy loss, whereas lower
quench flow may lead to coke formation due to cracking.
15.3 FEED TANK SWITCH OVER IN CDU.
15.3.1 LOW SULPHUR TO HIGH SULPHUR
Feed tank changeover Standing Instructions: SI20

Following procedural steps are to be adopted before change-over of feed tank:
a. Reduce feed rate to 440 m3/hr

b. Suspend water injection to desalter.
c. Desalter try-cock levels to be set between 70-75% and to be confirmed with try-cock
levels (2&3). In case of any Desalter grid voltage / amperes fluctuations, level can
reduce to suit. But it should be informed to the unit manager.
d. Wait for an hour after tank switch over to make changes in feed rate.
e. Adjust CRs and yields accordingly.
f. Inform FCCU /MEROX/DHDS/YSF.
Preflash Drum
a. Slowly decrease the vaporization watching product colors in general and diesel color
in particular.
b. Increase the flow through the furnace keeping a watch on PFD level.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
Atmospheric Section
a. Increase the Furnace COT gradually as per technical data.

b. Make changes in reflux rates to attain design column pressure and vapor line
temperature.
c. Keep watch on bottom level and adjust Vac feed accordingly.
d. Stop additional reflux and product pumps.
Vacuum section
a. Increase Furnace COT as per technical data.

b. Adjust refluxes to maintain column temperature profile.
c. Reduce SR pump spillback to the minimum and wide open the discharge valve.
d. Adjust slop cut pump spillback also.
e. Stop additional LVGO pump.
f. Place additional tempered water pump if required.
g. Take into service additional SR/Tempered water coolers.
h. Change SR quench flow rate to suit the column bottom temperature
i. Route Slop cut to SR/HVGO via CDU 1 cooler box to decrease load on SR/Tempered
water coolers.
Chemical injection
a. Introduce caustic solution injection

b. Adjust Atmos and Vac neutralizer rates to attain designed pH values of sour waters.
Product routing
a. Route Diesel R/D to sour DSL storage/DHDS in coordination with OM&S/DHDS

b. Route SR to FO/VBU storage or BBU in coordination with OM&S.
Sampling
a. Send product & crude (both FC &DC)samples after four hours after tank change over
b. Samples to be tested for Sulphur also as per OM&S requirement.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.3.2 HIGH SULPHUR TO LOW SULPHUR
Follow standing instructions for Feed tank changeover SI20.
Pre-flash Drum
a. Slowly increase the vaporization watching product colors in general and diesel
color in particular.
b. Decrease the flow through the furnace keeping a watch on PFD level.
Atmospheric Section
a. Decrease the Furnace COT gradually as per technical data.

b. Make changes in reflux rates to attain design column pressure and vapor line
temperature.
c. Keep watch on bottom level and adjust Vac feed accordingly.
d. Start additional reflux pump and product pumps.
Vacuum section
1) Decrease Furnace COT as per technical data.

2) Adjust refluxes to maintain Column temperature profile.
3) Increase SR pump spillback to the maximum and adjust the discharge valve.
4) Adjust slop cut pump spillback also.
5) Stop additional tempered water pump if required.
6) Take out additional SR/Tempered water coolers service.
7) Change SR quench flow rate to suit the column bottom temperature.
8) Route Slop cut to SR to maintain SR level.
Chemical injection
1) Caustic solution injection.

2) Adjust Atmos and Vac neutralizer rates to attain designed pH values of sour
waters.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
Product routing
1) Route Diesel R/D to sour DSL storage/DHDS in coordination with

OM&S/DHDS.
2) Route SR to FO/VBU storage or BBU in coordination with OM&S.
Sampling
1) Send product & crude (both FC &DC) samples after four hours after tank change
over.
2) Samples to be tested for Sulphur also as per OM&S requirement.
15.4 Standing Instruction on Heater fuel oil gun cleaning (SI 38):
15.4.1 Fuel Oil burners are required to be cleaned / repaired, if
a) Fuel oil fires to burners pressure is holding on higher side even for lesser flow
b) Fire pattern is not good – Sooty, flickering and impingement in spite of adjustment.
c) Fuel Oil dripping from the burner.
d) Coke formation on the fuel oil burners.
e) Leaks on the Fuel oil or steam hoses of the oil burners.
15.4.2 REQUIREMENTS FOR OIL GUN DROPPING:

a. Asbestos Gloves
b. Face shield / Goggles.
c. Bench Vice with necessary arrangements.
d. Proper sized pipe wrenches.
e. Two number of lead gaskets
f. DCS shift in charge clearance(after stack damper opening)
15.4.3 STANDING INSTRUCTIONS:
o Inform DCS shift in charge before going to start oil gun dropping activity and
ensure that stack damper is in open condition, during oil gun dropping & placing
back the oil fire.
o Remove the oil fire and ensure that gas fire and pilot are there in the particular
burner. Adjust The firing in other burners.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
o Open the purge steam valve fully to purge the oil gun. (Ensure only dry steam is
admitted)
o When all signs of flame disappear, close the purge steam & atomizing steam valve.
o Open burner drain to drain the oil present inside the burner assembly.
o Ensure that no oil accumulation inside burner by viewing through burner view
Ports.
o Do not allow oil gun more time without steam purging when gas fire is in-side as
the oil burner tip will get damaged.
o If oil accumulation is not there, drop the oil gun by wearing face shield & asbestos
Gloves, after ensuring that the steam valves (Atomizing & purge steam) are not
passing. After removing the gun, fix the sealing plate.
o If oil accumulation is there then remove all fires and close air registers for cooling
before dropping.
o After dropping the gun soak it in the soaking pit for 1 hour (after cooling).
o After soaking, fix the oil gun in the bench vice and open the gun parts one by one,
clean them and compare them with the new spare parts.
o Replace the worn out or damaged parts of oil gun (Oil tip, atomiser etc).
o After cleaning the oil gun, care should be taken to reassemble the oil gun in the
reverse order of dismantling.
o Assemble the parts of the burner slowly by taking care of the threaded nipples and
gaskets.
• Over tightening and wrong threading can damage the parts.
o After assembling the parts check for leaks if any by using steam.
o Fix the oil gun with new lead gaskets & Inform DCS shift in charge before light up
of the cleaned burner.
o Purge the gun with steam for testing leaks, if any.
o If no leaks are present, then slowly open the fuel oil block valves after ensuring gas
fire &Atomising steam is present in the particular burner.
o Carry out fine adjustments, so that proper flame is there without any impingement.
o Update the burner spares register.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.5 Standing Instruction to apprise Merox DCS shift in charge in case of sudden
fluctuation in unit sour water flow to SWSU(SI 37):
15.5.1. OBJECTIVE:
To appraise Merox DCS shift in charge in case of sudden fluctuation in unit sour water flow
to SWSU (say ≥ 2m3/hr), so that corrective actions can be taken and the following can be
avoided.
a. Disturbances in unit & stripper conditions, leads to poor stripping operation.
b. Carryovers of sour water with oil into Acid Gas flare KOD (280V05) due to sudden rise in
level of surge drum.
c. Sudden rise in Acid Gas flare KOD level, resulting in spillage of oil around the flare,
with consequent fires in the flare vicinity.
15.5.2.BACKGROUND:
1. Sour water from FCCU-I, FCCU-II and VBU goes into the sour water Surge
Drum(16V-05) in SWSU-I.
2. Rich Sour water surge drum (16V-05) is a horizontal vessel provided with baffle
plates which divide the drum into three compartments.
3. Sour water enters the middle compartment, where phase separation takes place.
Water, being heavier, underflows to the third compartment. Oil overflows from the
top of the baffle to the first compartment. From first compartment oil drains to
OWS continuously through siphon loop arrangement.
4. The drum is connected to the Acid Gas Flare header so as to vent any disengaged
5. Hydrocarbon vapors coming along with the sour water. The drum is provided with
PSV-1106 and PSV-1107 which discharge to the Acid Gas Flare header.
6. From the third compartment, Stripper Feed pumps 16P-06 A/B transfer the sour
water from 16V-05 to the I Stripper Column (16C-04) through preheat exchanger
16E-05A/B/C under flow control FIC-ll03.
7. Sour waters from CDU-I. VDU-I, CDU-II, VDU-II, CDU-III and VDU-III goes in
to the Lean Sour water Surge Drum (16V-12) in SWSU-2. This drum works
identical to 16V05.
8. The drum is connected to the Acid Gas Flare header so as to vent any disengaged
9. Hydrocarbon vapors coming along with the sour water. The drum is provided with
PSV-1201 and PSV-1202 which discharge to the Acid Gas Flare header.
10. From the third compartment, lean sour water is pumped by 16P-15 A/B to II
Stripper Column (16C-05) through a preheating system.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
11. There is an option available in Merox to route sour waters from FCCU-1, FCCU-2
&VBU to lean oil surge drum (16V-12) in SWSU-2.
12. There is an additional option available for FCCU-1/ FCCU-2 to route sour water to
MS block SWSU.
15.5.3. STANDING INSTRUCTIONS:
1. Always maintain steady sour water flow to SWSU and apprise Merox DCS shift in
charge (4454), when sour water flow fluctuation is greater than 2m3/hr.
2. During unit normal operation, check the sour water samples for any oil carryover at
every 2 hours frequency, in case any abnormality is noticed, inform Merox DCS shift
in charge and discontinue sour water routing to SWSU immediately. Resume water
intake after reconfirming there is no oil carry over.
3. During plant upsets and during boot LT’s failure, check the sour water samples for
any oil carry over at 15 minutes frequency and in case any abnormality is noticed,
inform Merox DCS shift in charge and discontinue sour water routing to SWSU
immediately.
4. Resume after reconfirming no oil carryover is there.
5. The above instruction is equally applicable in case of sour water routing from FCCU-I
/II to MS block, in that case information should be given to MS block DCS shift in
charge (4504).
15.6 Standing Instruction on Car seal Management (SI42):
15.6.1. OBJECTIVE:
• To ensure car seals on the inlet and outlet isolation valves in open position for the
PSV’s in service.
• To ensure car seals on all the First Aid Fire Hose reels, TSV’s, Sour water drain to
OWS valves, Critical Utility lines at Battery limits as per the identified list, chemical
system drain valves and other important valves as per process requirement.
• To ensure the car seals are maintained on the all the specified valves and their
condition is monitored on a regular basis.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.6.2 BACKGROUND:
• In the past some shift incidents/upsets were experienced due to inadvertent
isolation of some critical valves in the unit. To avoid such incident/upsets, car
seals to be provided at the following equipment isolation valves.
• PSV’s: The pressure safety valve (PSV) is a type of valve used to limit the
pressure in a system or vessel which can build up by a process upset,
instrument or equipment failure or fire. Inadvertent isolation of a PSV will
defeat its purpose and therefore periodic checks are to be carried out
.Upstream and downstream isolation valves are to be car sealed in open
position to prevent such inadvertent closure.
• Utilities: Utilities such as Bearing Cooling water supply & return, DM water,
Instrument Air, Fuel oil supply & return, Fuel Gas and Nitrogen form an
integral part of the Unit Operation. Continuous supply of these utilities is very
important and failure of any one of these utilities can lead to partial or total
shutdown of the Unit. In advertent isolation of these utilities can be prevented
by car sealing these utility lines valves in open condition at the Unit Battery
limits.
• FAFHR: First aid fire hose reels are provided in the Unit to aid in firefighting
at times of emergencies. Usage of fire water for other activities like lines
flushing and floor cleaning will lead to overloading of ETP’s as well as
hampering the treatment of the effluents at ETP. Car seals are provided to
ensure usage of FAFHR only for the firefighting purposes.
• Chemical system drain Valves: Chemicals often require different treatment
steps than oily water streams before final disposal, therefore Chemical should
not be drained to OWS. Car seals to be fixed on chemical system drain valves
to avoid chemicals draining to OWS.
• Sour water system drain Valves: Sour water draining to OWS will increase
the load on ETP’s, therefore Sour should not be drained to OWS. Car seals to
be fixed on Sour water system drain valves to avoid Sour water draining to
OWS.
• Other Specified valves as per PDI: There are some critical equipment or
lines in the Unit for which the valves to be either to remain open or in close
condition as per the existing process conditions. Car seals are to be provided to
valves on such lines or equipment as per PDI instructions.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
15.6.3. STANDING INSTRUCTIONS:
.1. Car seals to be provided and periodic checks to be carried out as mentioned
below:
Car Seals Monitoring Standing Instructions

provision to duratio
n
Monthly Provide car seals to the inlet and outlet valves in
PSV’in Service
DRJ open condition.
Car Seals to the following utility lines with
valves at Battery limits in open conditions
Weekly a. Instrument Air b. BCW Supply
Utility lines
DRJ c. BCW Return d. IFO Supply
e. IFO Return f. Fuel Gas Supply
g. Nitrogen
Monthly Car Seals to all the FAFHR lines with valves in
FAFHR’s
DRJ closed conditions.
Chemical
Car Seals to all the chemical system & Sour
system & Sour Weekly
water drain valves to OWS in closed
water drain DRJ
conditions.
Valves
Other Specified Weekly Car seals to only those specified valves either in
valves as per DRJ open condition or in closed condition as per
PDI the requirements advised through PDI.
.2. Car seals can be broken in case of any process requirement by intimating concerned
shift supervisor, same to be entered in car seal register and in FIELD/DCS TOB.
.3. After meeting the process requirement the broken car seals to be restored to their
normal position as early as possible after taking clearance from concerned shift
supervisor, same to be entered in car seal register and in FIELD/DCS TOB.
15.7 Standing Instruction on Refinery Fuel gas system Management and control
(SI 16):
1. Maintain constant pressure in VBU fractionator (11PR-1501). Other variables

affecting the gas generation rate and under operational control( viz. Feed rate, Heater
COT, Stabilizer re boiling etc.) should not be varied drastically.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
2. Sudden variation in feed quality, cooling water pressure/ Temperature also affects the
Fuel gas generation rate in the unit. As those variations are not under the operational
control, immediately information to be given to YSF when such variations are
observed.
3. During startup consume minimum quantity of F.G. Inform to F.G. controlling unit in
advance.
4. During normal run of the plant maintain constant consumption of fuel gas.
5. In case of any change in FG consumption, prior permission from FG controlling unit
needs to be obtained in coordination with YSF.
6. Always follow the instructions from FG controlling unit for increase/decrease in FG
consumption.
7. Record the summation value of total gas released from unit to flare in TOB in every
shift.
15.8 Standing Instructions to avoid congealing of heavy oil rundown lines from the
unit. SI 35
4. OBJECTIVE:
To avoid congealing of heavy oil rundown lines from the unit.
5. BACKGROUND:
SR obtained from vac. Column bottom is routed to various specified rundowns

like RFO, HFO, VBU feed tanks and as BBU hot feed. Due to various planner
requirements, different specs of SR having different viscosity grades V-10, V-30 and V50
grade bitumen and are routed to designated tanks. SR being a heavy product, during the
change over of SR from one tank to another, it is required to flush the previous lines with
cutter after changeover in case of RFO and HFO tanks. This prevents congealing of the
lines. Heat tracing and steam tracing is provided along the length of the line from the unit
to tank farms to prevent congealing.
Feed to BBU is obtained from CDU-I/II/III VAC bottom short residue (SR).
Bitumen product from BBU is being routed to RFO, HFO and VBU tanks during ullage
problem or due to off-spec bitumen. As the product being heavier, line has to be flushed
with cutter after change over. This prevents congealing of the lines.
6. SCOPE:
This “Standing Instruction” is generated for routing of the bitumen product due to off
spec. or ullage problem. In such cases, the product has to be routed to VBU tank line in
CDU-II.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
7. RESPONSIBILITY:
The overall responsibility to implement these guidelines rests with the unit shift-in
charges (Field &DCS) and technicians.
A. The following are different cases for routing of Bitumen product to RFO, HFO, VBU
tank lines:
i. BBU start up: During BBU start-up, initially cutter will be taken and displaced
with the SR from CDU’s. During the process, air to reactor is introduced and off
spec product is being routed to HFO or VBU tank. In that process, initially the
product having viscosity of SR is being routed to rundown and after a period of time
the viscosity increases and product (spec. near to the V30 or V50 grade) still flows
through the HFO or VBU line. The off spec bitumen having higher viscosity and
pen should have higher EHT temperature than that of SR rundown in off-sites.
ii. BBU feed change over: whenever Feed to reactor changes, the rundown will be
routed to VBU tank or HFO line till the product is on spec. The product routed till
the time is highly viscous and proper heat tracing till the tank is to be ensured. After
completion of routing the line to be flushed with cutter.
iii. Production of V30 grade: During production of V30 grade, viscosity has to be
more than 2500 cst and if the product doesn’t meet the requirement it has to be
routed to HFO or VBU tank line. During this time, the product obtained will be
highly viscous and hence the product has to be routed at a minimum temp of 140 °C
to prevent congealing.
iv. Direct bitumen from vac column: whenever high sulfur crudes like IM, UM are
processed, direct bitumen is obtained from vac column bottom. During that period
SR obtained has high viscosity and till the product is on spec. (if pen is above 100
m) SR has to be routed to RFO, HFO or VBU tanks. During these conditions the
heat tracing has to be maintained above 140 °C and as per the technical advice the
line temperatures are to maintain around 90 °C. So chances of congealing of line are
more when there is sudden stoppage of pump (or due to suction loss) or slower rates
of flow.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
As per Technical,
a. The minimum temperature to be maintained for the SR which has to be routed to
RFO or HFO is 90-95 deg C. (line design 120 deg C)
b. The minimum temperature to be maintained for the bitumen which has to be routed
to Tank 35 or Tk34 via new or old rundown line is 140-150 deg C. (line design 170
deg C)
c. The minimum temperature to be maintained for routing SR or bitumen to VBU tank
is 90- 160 deg C (line design 266 deg C)
The above said temperatures are the operating temperatures of the lines which are to
be maintained in the offsite area. Hence, when ever the bitumen is being routed to RFO
or HFO the heat tracing temperature is not sufficient in case of sudden stoppage of
Bitumen product or slower rates of flow and may cause plugging. During the above
activities, the off spec. bitumen product has to be routed via VBU line to respective tanks
only.
Note: while processing high sulfur crudes like IM, UM or bituminous crudes
(bituminous crudes list to be provided by technical) even though vac column conditions
are not adjusted for direct bitumen, it has to be ensured that the SR to be routed to VBU
tanks only as the product SR may have bitumen product qualities.
B. Due to potential hazard, Bitumen cannot be routed to RFO or HFO lines as the design
temperature of the lines are 120 deg C and the EHT for RFO and HFO lines are 90 -110
deg C and for bitumen, minimum temperature has to be maintained is 140 deg C.
C. During processing of bituminous crudes in CDU and even though vac column conditions
are not adjusted for direct bitumen, it has to be ensured that the SR to be routed to VBU
tanks only as the product SR may have bitumen product qualities. Flushing of RFO and
HFO to be done after changeover of the rundown. Considering 1000 m length of the line
then total HFO/RFO line content to be displaced is around 50m3. At a cutter flow rate of
50 m3/hr, it has to be flushed for one hour. If cutter rate at 25 m3/hr means at least 2 hrs
lines has to be flushed.
D. The bitumen product due to off spec. or ullage problem, product has to be routed to VBU
tank line, as its line temperature is maintained in the bitumen range with MP steam
tracing.
E. Old and new bitumen lines cannot be flushed with cutter as the lines are floating on the
bitumen tanks and will off spec. the bitumen product.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 15
PLANT NAME: CDU II
Chapter Rev No: 0
9. THE FOLLOWING ACTION ARE TO BE FOLLOWED BY CDU-II

PERSONNEL:
i.Route Bitumen from BBU or vac column bottom through designated bitumen rundown
lines only.
ii.Do not route bitumen product via HFO/RFO lines, as the line temperatures are limiting.
iii.Route off-spec bitumen from BBU or SR of bituminous crudes from vac. bottom to VBU
tanks only.
iv.After tank switch, flushing of HFO or RFO are to be done to avoid congealing, as
advised in the above instructions.
v.Bitumen cannot be flushed with cutter as the lines are floating on the rundown tanks.
Due to planner requirement, if product is to be routed against the above instructions,
permission has to be taken from the division head operations.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
MAJOR EQUIPMENT DESCRIPTION AND
OPERATING PROCEDURES

The major equipments of the units are as follows:

16.1 Crude Charge Pump
16.2 Crude Booster Pump
16.3 Desalter
16.4 Pre-Flash Drum
16.5 Atmospheric Heater
16.6 Atmospheric Column
16.7 Naphtha stabilizer
16.8 RCO pumps
16.9 Vacuum Heater
16.10 Vacuum Column
16.11 Ejectors
16.12 HVGO pumps
16.13 SR pumps
16.14 Condensate recovery unit
16.1 CRUDE CHARGE PUMP 11-PM- 01A/B:
It is a motor and turbine driven centrifugal pump. The pumping temperature is 30°C and
viscosity at pumping temperature should be 7.5 cst. Vapor pressure at pumping temperature
has to be 0.5 kg/cm2 absolute. Density of the fluid has to be 840 kg/m3. It has a design
pressure of 31.7 kg/cm2A and temperature of 65°C. The casing and the impellor are made of
carbon steel. It has a mechanical seal to protect out flow of liquid from the casing.
Operating Conditions:
Normal flow rate 482 m3/hr

Minimum flow rate 219 m3/hr
Suction Pressure 2.0 kg/cm2A
Discharge Pressure 24.45 kg/cm2A
Differential Head 367.3 meters
NPSH available 6 meters
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Pump Change over Procedure: (motor to turbine)
• First take clearance from CPP and also from PP-II for consumption of HP steam.
• Ensure all the utilities like BCW, seal steam and self coolant are open. Suction valve is open
and discharge valve is in closed position. Casing has to be thoroughly drained.
• Check the pump basement and remove any foreign materials present.
• Drain the condensate from turbine and vent some steam to get dry steam.
• Check the pump freeness and ensure all the vents and bleeders are capped up.
• Check the auxiliary oil system:
Lube oil level
Lube oil pressure
Trip lever pressure
Cooling water system is commissioned
Check DP gauge of filters.
• Engage trip lever and start rolling of turbine.
• Place AOP (auxiliary oil pump) in AUTO mode.
• Increase the RPM of turbine and slowly close motor discharge valve against the feed
discharge pressure and adjust the discharge pressure to the value required by DCS supervisor
by increasing the turbine RPM (speed) and simultaneously closing the running pump
discharge valve. This activity has to be done very slowly, ensuring there are no jerks in feed
pump discharge pressure. Continuous watch has to be kept on the pump discharge pressure.
• Switch over seal flushing to 11-PM-02A from motor to turbine.
• When the running pump discharge is fully closed and amps become low, confirm the flow
with DCS supervisor. Check the healthiness of turbine and with his consent stop the idle
running pump. Check for leaks after changeover of the pumps.
Pump Change over Procedure: (turbine to motor)

• First take clearance from CPP for placing an HT motor and also from PP-II for reduction
of HP steam.
• Ensure all the utilities like BCW, seal steam and self coolant are open. Suction valve is
open and discharge valve is in closed position. Casing has to be thoroughly drained.
• Check the pump freeness.
• Ensure all drains and vents are capped up.
• Inform the field person to start the motor.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
• Start the pump and adjust the discharge pressure to the value required by DCS supervisor by
opening the discharge and simultaneously reduce the turbine RPM while watching the feed
discharge pressure. This activity has to be done very slowly, ensuring there are no jerks in
feed pump discharge pressure. Continuous watch has to be kept on the pump discharge
pressure.
• Switchover seal flushing to motor.
• Check the motor amperage and healthiness of pumps and then stop the turbine.
16.2 CRUDE BOOSTER PUMP 11PM 02A/B:
It is a motor as well as turbine driven centrifugal pump. The pumping temperature is 120°C
and viscosity at pumping temperature should be 1.85 cst. Vapor pressure at pumping
temperature has to be 9.5 kg/cm2 absolute. Density of the fluid has to be 789 kg/m3. It has a
design pressure of 41.0 kg/cm2A and temperature of 145 °C. The casing and the impellor
both are made of carbon steel. It has a mechanical seal to protect out flow of liquid from the
casing.
Operating conditions:

Maximum flow rate 515 m3/hr
Discharge Pressure 34.6 kg/cm2A
NPSH available 6 meters
Pump Change over Procedure: (motor to turbine) when PFD not in service.
• First take clearance from CPP and also from PP-II for consumption of HP steam.
• Ensure all the utilities like BCW, seal steam and self coolant are open. Suction valve is open
and discharge valve is in closed position. Casing has to be thoroughly drained.
• Drain the condensate from turbine and vent some steam to get dry steam.
• Check the pump freeness and ensure all the vents and bleeders are capped up.
• Engage trip lever and start rolling of turbine.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
• Reduce Desalter pressure to 09.50 Kg\Cm2.

• Increase the RPM of turbine and slowly close motor discharge valve against the booster
discharge pressure and adjust the discharge pressure to the value required by DCS supervisor
by increasing the turbine RPM (speed) and simultaneously closing the running pump
discharge valve. This activity has to be done very slowly so that the booster discharge
pressure and flow, as well as the Desalter pressure do not fluctuate. Continuous watch has to
be kept on the pump discharge pressure.
with DCS supervisor and with his consent stop the idle running pump. Check for leaks after
changeover of the pumps.
• Keep the stand by booster pump in warm up condition.
• Place necessary trips online after the activity.
16.3 DESALTER (11-V-02):
Desalter handles crude and water together. The desalter receives thoroughly mixed crude oil
and water.
The operating conditions of desalter are as follows:
Normal Flow rate 367647 kg/hr

Pressure 9.0 – 11 kg/cm2A
Temperature 120-130 °C
Material of Construction Carbon Steel
Corrosion Allowance 3 mm
Insulation 100 mm (hot)
Design Pressure 13.5 kg/ cm2A
Oil Content in Water 100 ppm (max)
Inlet chlorides as NaCl 85.601 mg/l
Outlet chlorides as NaCl 5.0 mg/l
Desalting is the accepted industry term for the electrostatic process for removing
contaminants such as salts, solids and water from crude oil at a refinery.
Crude oil brings along with it salts, particularly those of Sodium, Magnesium etc. metals like
Arsenic, Vanadium etc. In addition crude oil contains solids such as finely divided sand
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
particles, clay, drilling mud and rust and scale. Most of the contaminants are present in crude
as it is produced from oil wells and accumulated during the transportation by tankers.
Although these are present only in small amount, their presence can result in serious
problems in down stream equipment viz, heat exchangers, heaters and columns. Hence the
need for their removal is important before processing.
When crude oil enters a refinery, it typically contains a small amount of water, approximately
0.1 to 0.5 % by volume. The water in the crude oil contains water-soluble salts, and the crude
oil contains insoluble particulate matter. To lower the level of impurities, water must be
added first to the crude.
A mix valve mixes the wash water in to crude by dispersing water in to extremely small
droplets. This intimate mixing of water and oil causes fresh water to contact brine droplets
and various water soluble impurities in the oil. The water and oil mixture is then piped in to
the Desalter vessel where the mixture is metered out at a low velocity in to an electrical field.
The electrical field causes the oil and water to separate. The droplets of wash water (now
combined with droplets of brine) form large drops that are separated from the crude oil by
high voltage electricity and force of gravity. This process is called electrostatic coalescence.
Application of strong electric field hastens the process of coalescing and therefore settling of
all unwanted material. When the mixture of crude and water is subjected high potential
electric field, the tiny water droplets get distributed between the electrodes forming dipoles.
This makes it possible for the tiny particles to coalesce and form bigger particles of sufficient
weight to settle down. The force of attraction between two droplets must be of sufficient
magnitude to break through the oil film.
Desalter employs electrostatic elements operating at 415 volts to coalesce and separate water
from oil for reducing the salts contents in crude oil so that it is within acceptable and
specified limits in desalted crude. When oil water mixture enters the high voltage electric
field, it separates into two phases in desalter. The oil phase floats on top and overflows, while
water with its dissolved salts, metals, mud and iron oxides settles down at the bottom.
At a level below the electrodes an interface is formed between Hydrocarbons and water.
Regulating desalted water withdrawal from the vessel controls this inter-phase level.
If the wash water is not added, the total population of water droplets in crude oil would not be
sufficient for much coalescence (combining) of water droplets to occur. The addition of wash
water to the crude oil increases the total water volume in crude and permits removal of
contaminants.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Caustic injection upstream of desalter in crude is done to neutralize acids present in crude and
convert them into salts. These salts are then removed by desalter water in desalter. Caustic
injection down stream of desalter is provided to neutralize any other acid traces formed at
desalter operating conditions.
Brine in associated with crude both as a fine suspension of droplets and more permanent
emulsion. To break these light emulsions demulsifier is added. This improves the
effectiveness of desalter. Demulsifier is injected into crude upstream of desalter. Provision
also exists for injection of demulsifier into the crude line at battery limit.
Caustic solution and demulsifier can also be added into the crude before the first exchanger in
the preheat train-l.
Stripped water from Sour water stripper (SWSU) and MAB condensate from FCCU-II will
be used as desalting water. Also, sour water from Atmos. overhead drum (11V01) and hot
well water drum (12V01) are recycled to wash water drum. This helps in reducing the load on
SWSU. Provision is there to make up fresh water using service water or DM water.
Following is a general description of crude desalting system of CDU given under three
subsections viz. desalter description, desalter water system & desalter operation. Major
equipments of this section are desalter, desalter water pumps and desalter water vessel.
16.3.1 Standing instructions for Desalter Online Desludging: SI 10
The Desalter is located in 1st stage PHT-1 after successive preheat exchangers i.e., (11-E-01,
11-E-02, 11-E-03, 11-E-04A/B, 11-E-05, 11-E-06 & 11-E-07) utilizing relatively low
temperature fluids such as HN, Kero, diesel, TPA, Kero, diesel and LVGO respectively. The
outlet temperature of this preheat train is between 120-130°C. Service water/DM
water/stripped water (sour water from MEROX) is used for desalting which will be stored in
vessel (11V04). The water will be preheated to 90°C in 11E18 using LP steam before
injecting to desalter through 11PM 12A/B pumps.
In normal desalting process, water will be mixed with crude u/s of mix valve upstream of the
desalter (provision is there for injecting a part of wash water into crude line suction also
upstream of 11P01). On mixing, the undesirable salts present in the crude get dissolved in the
wash water and hence get separated from crude. The electrostatic field applied in the desalter
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
helps in breaking the oil water emulsion and thus the two liquid phases separate out. The hot
brine from the desalter is routed to sour water stripper unit ( merox for heat recovery and
subsequently transfer to ETPs ( effluent treatment plant).
1.0 Important checks during desludging.

1. Desludging operation has to be carried out once in three days for 1/2hour.
2. The important watch should be on interphase level that is to be maintained at about 40
to 45%.
3. Interphase level should not be dropped during process of desludging.
4. Continuous checking & confirmation through trycocks is a must.
5. Desalter LT /Agar probe must be checked by instrumentation befor carrying out
desludging operation.
2.0 Steps to be followed during desludging.

1. Inform all concerned Units and YSF before Desludging Operation.
2. Water injection to desalter via mix valve to be suspended by closing the field block
valve located west of the desalter.
3. Resume wash water through a 3” line u/s of wash water isolation valve (with 4 lateral
tie ins ) and which is going to desalter ( at bottom shell) directly with a check valve
and a block valve located at north of desalter,
4. The water rate can be controlled from MOI ( FI1102).
5. Route effluent through normal effluent line up. The wash water entry to desalter is
from the bottom where the sludge and emulsion that is present separates out of the
desalter through the normal effluent water outlet.
6. Maintain all process conditions of desalter normal, including power , pressure,
temperature & interphase and desludging to be continued until the sludge is removed
from the desalter by time to time check of trycock from 1to 5 nos.
Once the sludge is removed and effluent water is clear the online desludging process can
be stopped by closing the block valve in the field and desalter normal wash water
injection can be resumed. The routing of clear effluent water should be restored as earlier.
When routinely done once in three days it is supposed to take about half an hour for
desludging.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.4 PRE-FLASH DRUM:
Crude enters the PFD approximately in the middle of the vessel. There is a provision
to record the crude inlet pressure and temperature on DCS panel as P1901R and T1901R
respectively. Crude that flashes in the PFD exits in the form of vapours from the top of the
PFD and enters the 12th tray of the Atmos Column. A demister pad is provided on the vapour
line to knock off any liquid droplets entrained in the vapour. The amount of flashing depends
on the pressure in the PFD, which is controlled by PR1902. The crude level in the PFD is
controlled by LR1902. Level gauge glasses are also provided on the shell of the PFD for
physical verification of the level. There is also a high-level and low level switch provision.
The un-flashed heavier crude goes to the PFD turbine 11-PT-02B from where it is boosted to
25 kg/cm2 g. and sent to the PFD manifold through 11-E-40 A/B. The crude outlet flow from
the PFD and its temperature are indicated on the DCS panel by F1902R and T1902R
(provided on the outlet of crude from PFD) respectively. The PFD has two pressure safety
valves (120-PSV-1201 A&B) set at 25.5 kg/cm2 g. The discharge of the PSV is connected to
the flash zone of the Atmospheric Distillation Column (down stream of Desalter RV).
There is a provision to bypass crude flow to PFD in case of emergency, from the DCS
panel. This is done by operating the ROV switch on the auxiliary panel. There is an interlock
on this ROV operation. When ROV is opened, the LCV-1902 gets closed. This interlock is
provided to prevent the crude entry into the PFD when it is bypassed. A switch is provided on
the auxiliary panel to trip the turbine (11-P-02B) from the DCS panel. Operating this switch
on the auxiliary panel will close the steam shut off valve on the steam inlet to the turbine,
thereby cutting off steam to the turbine. There is a provision to reset the SDV manually in the
field, by which the SDV can be reset to open position
Standing instructions for commissioning of PFD : SI 34
10. OBJECTIVE:
To have safe commissioning of PFD without effecting the unit operation.
11. SCOPE:
This “Standing Instruction” is generated for commissioning of PFD in a smooth
manner and to reduce the risk factor in CDU-II.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
12. RESPONSIBILITY:
The overall responsibility to implement these guidelines rests with the unit shift-in-
charges (Field &DCS) and technicians.
The following are the changes to be made before commissioning the PFD.
i. Feed rate to be reduced to 440 m3/hr and adjust the parameters accordingly.
ii. Drain the cold stock from the PFD to suction and discharge of 11-PT-02B
turbine to CBD.
iii. Trip check the 11-PT-02B turbine steam SDV.
iv. Trip check the ROV with PDF level control valve (LR1902) and close the
ROV after ensuring the bypass valve in wide open position.
v. Stroke check the PFD pressure control valve (PR1902).
vi. Ensure PFD ROV in closed position and PFD bypass valve in wide open
position.
vii. Close the block valve of level control valve (LR1902) and stroke check the
control valve.
viii. Bypass 11-E-40A/B in co-ordination with FCCU-2.
After completion of the above activities build up PFD level initially by opening
turbine warm up line up to ~10-15%. After that PFD drum filling to be done by opening the
level control valve block valve and by opening the level control valve by 5 %.
Note: 1. Ensure the PFD inlet pressure P1901R is maintained less than (or around) 17
kg/cm2.g
2. Take clearance from TPH, to route KERO to DSL as a precaution against
discoloration during commissioning of PFD.
3. Take clearance from Power plant for consumption of HP steam around 7 tons for
placing PFD turbine (11-PT-02B).
The steps are to be followed for placing the PFD into service.
1. Drain the crude from the PFD to suction and discharge lines at pump to CBD.
2. Keep a close watch on the CBD drum temperature and level. Ensure level is under
control and CBD pump AUTO cut-in is working.( ensure CBD drum temperature is
maintained below 80 °C and continuous supply of cooling water is provided to the
coil of the CBD drum to ensure temperature under control).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
3. After attaining temperature above 150 °C at PFD draw off temperature (T1902R) and
PFD level around 50% and pressure above 5 kg/cm2, start rolling of turbine 11-PT-
02B.
4. When F1902R starts sensing the flow, Increase the speed of the turbine and
simultaneously reduce the PFD bypass valve. Ensure no starvation of the flow
towards the heater pass flows.
5. If the flow from turbine not developing then
i.) Increase the speed of turbine to get the turbine to heater (F1902R) flow.
ii.) Ensure that the PFD pressure is above 5 Kg/cm2g and if not, increase PFD level
/ hot feed to PFD to increase the pressure. Open the PFD LCV further to reduce
the back pressure on the turbine (the flow through turbine will get established /
increase.)
iii.) Reduce the PFD inlet pressure (P1901R) by reducing the booster pump
discharge.
iv.) If still flow is not developing then stop the turbine, as there is a chance of seal
failure due to vapor lock. (If turbine was stopped due to no flow then again the
pump content has to be drained and again it has to be tried as mentioned
earlier).
6. After ensuring the flow from F1902R, slowly close the PFD bypass valve and speed
up the turbine in steps.
7. While closing the PFD bypass valve ensure PFD inlet pressure P1901R should not
increase drastically. (Maintain less or around18 kg/cm2). If the pressure is crossing
23 Kg/cm2g, immediately open the PFD level control valve (LR1902) by keeping a
close watch on the PFD level. If the pressure doesn’t come down then open the PFD
bypass valve and stop the PFD turbine and check the system for any abnormalities.
This is done to avoid the popping of the downstream Relief valves present on the
exchangers (11-E-16, 12-E-01 to 05A/B with a set valve of 35.2 Kg/cm2g ).
8. Slowly increase the speed of the PFD turbine in steps (PFD outlet flow = F1902R)
and simultaneously reduce the PFD bypass valve and finally close it after full flow is
ensured from the turbine.
9. After attaining the flow from PFD to heater the feed selectors switch has to be
changed over to PFD mode (FR1804S1 position 1- controls 11-F-01 pass flows with
respect to F1902R and position 2- controls 11-F-01 pass flows with respect to
F1104R).
10. Route turbine outlet steam to system (to LP header) after ensuring dry steam from
the turbine.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Schematic of PFD:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.4.1 Standing instructions on 11E40A/B commissioning procedure : SI 17
1. Objective : To have safe commissioning of 11E40A/B without effecting unit operations.

2. Background : 11E40 A/B ( crude /Circulating oil) exchanger was introduced to recover
sensible heat from FCCU-II circulating oil and to increase the preheat of the crude in
CDU II to give heat relief to heater. Inlet of 11E40A/B is taken from 14PM06A/B (
circulating oil pumps) discharge and outlet is joined to 14E07( MP steam generator)
upstream. A bypass facility at 14E07 and isolation facility at unit limit is provided for
this scheme.
3 Scope: Commissioning of 11E40A/B is a crucial operation inview of light oil/ cold stock
entry to column and reactor especially after cold startup of the unit. standing instructions
are generated based on the past experiences.
4. Responsibility: FCCU-II field/DCS officers/Operations technicians.
5 Commissioning of 11E40A/B when CDU II online
1. Keep Crude side is in bypassed condition at CDU-II( it should be floating).

2. Displace condensate in the circuit /drain at low points.
• CBD/OWS near 11E40A/B bypass valve.
• Unit limit circulating oil inlet and outlet drains.
• CBD/OWS on 11E40 inlet and outlet at CDU-II.
3. Displace cutter with feed in the 11E40A/B circuit to the column .
4. Circulate feed in the 11E40A/B circuit for at least 5hrs with 11E40A/B bypass in
close condition and 1hr in open condition.
5. Check for feed in the circuit at the following locations.
• 11E40A/B circulating outlet to CBD/OWS at CDU-II
• FR406 control valve downstream drain to CBD/OWS.
• Circulating oil to 11E40A/B drains to OWSat unit limit.
• Circulating oil pumps suction to CBD/OWS.
• 11E40A/B bypass loop.
6. Flush with feed @ 35M3/Hr for 4hrs to eliminate lighter oil in the circuit to main
column and pump out column tray 12 stock to slop.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
7. During hot oil circulation (MC flash zone temp of 170- 180DegC), take feed to
tray 12 and flush out for 4 hrs through CDU-II circuit.
8. Check periodically drain points at the loops mentioned in item No 5.
9. Monitor circulating oil supply and return temperatures.
10. After ensuring flow thorough flushing, open circulating oil bypass valve to about
8turns.
6 Commissioning of 11E40A/B during FCCU-II on line and CDU-II startup in progress

In this case FCCU-II unit is on line and CDU-II is under shutdown is considered. Whenever
CDU-II is under shutdown, circulating oil from FCCU-II to CDU-II bypass will be kept open
condition and inlet will be isolated at unit limit , outlet will be in floating condition. Once the
CDU-II comes on line and stabilized, follow the below procedure for re-commissioning of
11E40A/B with circulating oil.
1. Coordinate with CDU-II and ensure the unit is stabilized and crude is through
11E40A/B.
2. Keep open unit limit inlet block v/v by 2turns and wait for 2hrs. this is to ensure
complete filling of the loop. Ensure FR405 flow is not reduced.
3. Inform CDU-II to drain inlet and outlet to CBD till the outlet temperature on
circulating oil reached 100degC.
4. After ensuring hot liquid in the circulating oil inlet and outlet loop, keep wide open
11E40A/B inlet valve at unit limit in slow steps.
7 Activity during placing of CDU-II Pre-flash Drum
The circulating oil temperature may fall down due to low temperature crude entry into
11E40A/B during commissioning of CDU-II PFD.
1. Prior to commissioning of CDU-II PFD , bypass 11E40 circulating oil at FCCU-I
2. Once the PFD commissioning is completed and stabilized, ensure circulating oil
11E40A/B outlet temperature is at normal condition.
3. Close the 11E40A/B bypass in slow steps.
16.5 ATMOSPHERIC HEATER:
Crude enters at the top of the convection zone or the fired heater. From the bottom of the
convection zone, the coils are routed to the radiation zone. From radiation zone crude comes
out of the heater and enters atmospheric column 11-C-01. Crude oil is heated from 280 °C to
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
375 °C and 260 °C to 367 °C in PG and BH case respectively before entering 11-C-01 for
fractionation.
The heater 11-F-01 is a cylindrical, cabin type fired heater having four passes. The radiant
section of the heater is provided with 22 tubes each of 19090mm (weld to weld). These tubes
are 6” NB Sch 40 type. The convection section has 12 rows of tubes with 8 tubes per row.
These 12 rows are arranged in 3 bundles with 4 rows per bundle. While the top 2 rows of this
zone are finned type the bottom two are bare tubes. All the others are studded type. The
effective length of each tube in this zone is 9058mm. The material of construction of the
tubes is 5% Chromium + 0.5% Molybdenum. Additional convection zone was provided
during 2010 T&I to increase the heater efficiency and heat duty. The additional convection
zone consists of 8 rows of tubes with 8 tubes per row. In these 8 rows, top 4 rows of this zone
are 24 SPP studded tubes, below it 2 rows of 12 SPP studded tubes and the bottom two are
bare tubes. The crude passes are numbered as pass A to pass D. Skin thermocouples have
been provided on heater pass tubes to know the metal temperatures at convection zone outlet,
middle of the radiation zone and outlet of the radiation zone.
Flow in each pass is regulated by individual pass flow controllers namely 11-FRC-
301/302/303/304. These controllers get input signal from respective flow transmitters (FT-
1301 to FT-1304) and set point signal from a ratio controller. Controllers generate output
signal and manipulates respective flow valves (FR1301 to FR1304). And Low flow alarms
11-FAL-301/302/303/304 for each pass respectively.
A ratio controller or pass balancer maintains ratio of crude flow in a particular pass to total
crude flow. The ratio controller/pass balancer functions in such a way that the weighted
average temperature at the outlet of each pass is maintained almost the same. The pass
balancer receives software input signal from FR1804 (feed selector switch. Total crude flow
or PFD bottom flow), 11-TRC-301 (Crude oil Temperature exit Atmospheric heater), 11- FI/
FR-402 (Crude over flash flow), 11-TI-306, 311, 316, and 321 (Outlet temperature of
individual passes) and FR1301 to FR1304 (Current values of all crude heater pass flows).
The output from the pass balancer regulates individual crude flow through the individual
passes by manipulating the Flow control valves (11-FRC-301/302/303/304) located on the
individual passes.
The distribution of crude through each pass should be adjusted in such a way that the heat
duties and hence COT (Coil outlet temperature) of all the passes are more or less same.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Depending on heat duty variation, pass flow will vary. In equality of flow through each pass
to the extent of 10% can be tolerated while operating on manual mode or with pass balancer.
All the 4 passes join together at the outlet of radiation zone. 11-TI-302, 307, 312, and 317
shows the intermediate heating of crude in the convection zone.
To avoid repetitive description, features of only pass-A have been taken up. For other passes
identical arrangements exist.
11-FRC-301 controls and indicates crude flow through pass-A. Through the transmitter FT -
1301 from the same element, one flow low-low alarm 11-FAL-301 has been provided in
DCS. Actuation of this alarm will trip fuel supply to all burners of the heater excluding pilots.
A local PI indicates field pressure and DCS bound 11-TI-302 indicates temperature of crude
at radiation zone inlet. 11-TI-306 indicates temperature in DCS of crude of pass-A at heater
outlet. Software alarm TAH and TAL on the COT has been provided to alert the operator
against inadequate flow or inadequate firing in that particular pass. Finally, heated crude
enters a common manifold of 24” size called transfer line before entering atmospheric
column.
The common outlet transfer line temperature is measured by the 11-TI-322 and is controlled
and recorded by the COT (coil outlet temperature) 11-TRC-301, which regulates quantity of
fuel to the furnace. Typical COT values are 375 o C (IM) and 365 o C (BH).
Pressure drop across the heater coil is a measure of internal tube condition and increase in
pressure drop indicates tube fouling due to coke formation in the tubes.
Emergency coil MP steam connections are given in each pass, down stream of pass flow
control valves to displace crude from the coil to the column during an emergency or after
normal shut down operation.
Soot blowers, using MP steam are provided in convection zone of the heater. Need of soot
blowing will be indicated by poor heat pick-up in convection zone and increase in flue gas
temperature. The soot blowers can be operated from grade level also.
Emergency steam, soot blower steam and decoking steam connections are taken from MP
steam header.
Snuffing steam (furnace purging steam) is connected to convection zone and heater box in
order to extinguish fire by steam blanketing. LP steam is used for this purpose.
To facilitate safe approach to emergency steam/snuffing steam during an emergency scenario
isolation valve on steam line needs to be provided at a safe distance of at least 15 meters from
heater.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Fuel System:
11-F-01 is a balanced draught furnace (and can be operated in natural draught at 70%
efficiency). Both the convection and radiation sections are used for heating crude. The
combustion chamber houses the radiation section of tubes. The convection section provided
at the top of radiation section serves to increase the thermal efficiency of the furnace by
utilizing further heat from the flue gas. Tubes in radiation and convection zone are arranged
horizontally.
atmospheric heater has a total of 12 burners. Of late, 3 burners (No. 2, No. 5 & No. 8) have
been dedicated to utilize off gases from the vacuum distillation column’s hot well drum as the
burning fuel. During 2010 T&I, all the burners were replaced with 20 new burners ZEECO
make (16 are combined firing and 4 are hot well off gas burners (number 16 to 20)).
a) Fuel Gas System:
branched into a 6” header to the Atmospheric heater. This FG line is steam traced to avoid
FG to main burners passes through a mass flow meter (F1315) and shutdown valve
11-SDV-303. This SDV is connected to interlock logic. 11-FR/FQ-308 indicates FG flow in
DCS room. It is provided with FAL and FAH. A local PG and a TG are provided to indicate
pressure and temperature at field. 11-PI-308 indicates FG pressure in the DCS room. A low
pressure alarm 11-PAL-303 is also provided. Fuel gas pressure low trip is set at 0.2 kg/cm 2g.
In case the fuel gas pressure goes below the trip value, only 11-SDV-303 will get
closed. If fuel gas tip pressure falls below the set value, chances of flame failure and
subsequent accumulation of un-burnt hydrocarbons in the firebox is possible. This can lead to
the possibility of explosion or back fire in the heater. Hence the provision of “FG pressure
low” trip was provided. There is a provision to cascade the fuel gas pressure to the 11-F-01
COT, 11-TRC-301 through a selector switch on the auxiliary panel on the DCS panel. A 2”
FG tapping upstream of 11-SDV-303 has been branched off for pilot burners. The pilot gas
pressure is normally adjusted manually and is maintained at a pressure of 0.7 kg/cm2 g. In
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
case of low pilot gas pressure, 11-PAL-302 is provided to actuate an alarm. Low pilot gas
pressure will alert the operator when pilot gas pressure falls.
b) Fuel Oil System
branched into a 3” header to the Atmospheric heater. FO line is steam traced to maintain
temperature and avoid congealing. Mass flow recorder and integrator 11-FR/FQ-305 are
provided on main FO supply line and 11-FR/FQ-306 is provided on the main FO return line
from heater. Since this is a closed circuit through which FO circulation is maintained, the net
consumption of fuel oil is measured as the difference between FI-305 and FI-306.
temperature of FO supply. 11-PRC-301 indicates the pressure of fuel oil on the DCS panel.
A low-pressure trip alarm has been provided on supply line. Actuation of this alarm
shuts 11-SDV-301 A/B and cuts off only the fuel oil firing in the Furnace. Since FO is
normally a thick heavy liquid, it needs to be always maintained in circulating state. If it is left
stagnant and unused in burners and piping, it can get congealed despite the fact that tracing
steam of the FO circuit is on. Circulation in heater area (FO piping forming a closed circuit
across all passes called fuel oil ring) is maintained even when no fuel oil burner is in use. A
ratio of 2:1 FO supply to return is normally maintained to obtain a good control on firing and
the heater, circulation can be maintained. Purge steam connections are provided on each oil
burner. FO burners are to be kept steam purged when idle.
When FO is fired, it is atomised or sprayed as a fine mist for realising complete

combustion. The spraying of FO is done by de-superheated MP steam in FO burners.
FO supply and MP steam simultaneously. Atomising steam pressure is maintained about 2.0
kg/cm2 above the FO pressure. Atomising steam flow is recorded by 11-FR-307. Local PG
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
and TG are also provided on this line.2” flushing oil connection is provided on FO supply
line up stream CBD/OWS drain is provided on FO return line. These provisions are to flush
the line within Battery Limit during heater shut down. When furnace operates on combination
fuel-either Fuel Gas operates on PIC and Fuel Oil on PIC/TIC cascade or Fuel Oil operates
on PIC and Fuel Gas on PIC/TIC cascade mode. Selector switch is used to select only one
fuel for COT control by cascading.
c) Off Gas System
Vapors from Hot well drum (12-V-01) are routed to the Atmospheric heater burner
through flame arresters. Off gases from the hot well are burnt in Atmos heater. An SDV (ZS-
2901) is provided on this line, which will close in the event of Atmospheric heater (11-F-01)
trip. Provision for routing the off gases from 12-V-01 to atmosphere exists to route gases to
atmosphere in the event routing of off gases to Atmos. furnace is not possible. An SDV (ZS-
2900) is provided on the vent line, which can be opened from DCS. Steam connection is
provided on this vent line to atmosphere for dilution of hydrocarbon vapors, which are
vented. Three burners are provided in Atmos. heater for burning off gas. Fuel gas connection
also is provided for these burners. During 2010 T&I number of burners were increased to 4
ZEECO burners.
When furnace operates on combination fuel, either fuel gas operates on auto mode and Fuel
Oil on cascade or fuel oil operates on auto mode and Fuel Gas on cascade mode. Selector
switch is used to select only one fuel for COT control by cascading.
Heater operating conditions:
Operating Temperature (°C) 270 (IN) 380(OUT)
2
Operating Pressure (kg/cm -a) 17.5 4.5
Heater Section:
Design Pressure 30 kg/cm2-a
Material of Construction 5 Cr + 0.5 Mo (A335 Gr P5)
Desired efficiency 88 %( LHV)
Stack height 71412 mm above grade
Note: For further details, please refer to furnace improvements of CDU-II crude heater,
Volume-I, page 21.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.6 ATMOSPHERIC COLUMN:
Crude oil after final heating in atmospheric heater is fed to the atmospheric column at 375°C
(IM) and 367°C (BH). This column has 40 valve type trays including baffle trays and three
chimney trays for side stream withdrawal. The column has a stripping section at the bottom.
Description of entire column has been taken up zone wise.

a. Flash zone
b. Bottom section
c. Middle section
d. Over head section
16.6.1 Flash Zone:
Heated and partly vaporized crude oil enters the flash zone. Hydrocarbon vapors flash in this
section and get liberated. Non flashed liquid moves down, which is largely the bottom
product called RCO (Reduced Crude oil). Certain degree of over flashing of crude is
desirable for proper stabilization of RCO and fractionation of gas oil (diesel) components.
Over flashing is achieved by setting up COT at slightly higher temperature than actually
required. Required temperature of flash zone is 357 °C while that of feed is 360 °C. This over
flashed material mostly condenses at 7th tray. The condensed liquid is withdrawn from 7th tray
and put back on 6th tray. Over flash liquid travels down from 7th tray to 1st tray. It strips off
heavier component coming up from RCO stock collected at column bottom which otherwise
could move up and cause coloration of heavy diesel stream. Flow of over flashed liquid could
be increased either by increasing COT and condensing more material on 7th tray or by
reducing heavy diesel draw off. However the second option will lead to less diesel yield and
higher energy consumption without any advantage. Too large flow of over flash liquid may
result in drop in bottom temperature and lighter bottom product RCO.
Over flash flow is indicated by 11- FI/ FR-402. This is a 6” line with a U-loop. 11-FE-
402 is mounted in the liquid seal. This seal provides adequate liquid build up on upstream of
FE and ensures no flickering, steady flow through orifice. In addition, it provides some back
pressure which is required to prevent flashing just downstream of flow orifice due to pressure
drop.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
MP steam is introduced in the column through 11-FRC-401, below tray 1 for

stripping of RCO. Stripping steam helps in removing lighter components from the heavier
products by reducing their partial pressures and vaporizing them without requiring additional
heat.Hydrocarbon vapors liberated by flashing move upward along with steam in the column
for further mass transfer at trays in upper section.
Pressure relief valve discharge from Desalter and PFD are routed to the flash zone.
16.6.2 Bottom Section:
Reduced Crude Oil (RCO) product is collected at the bottom of the column. The
column bottom level is indicated and controlled by 11-LRC-401. LRC-1401 goes to the ratio
block of vacuum heater. Manipulating the RCO flow to vacuum heater can do column bottom
level control. LRC is provided with software high / low level alarms. In Addition, 11-
LAL/LAH-401 are provided in DCS panel.11-TR-401 shows product RCO temperature.
RCO at a temperature of 340 to 370°C is pumped out from the bottom of the column
at by RCO pumps 11-P-10 A/B to any of the following destinations.
a) 10” line to Vacuum Furnace (12-F-01) as RCO feed. During normal operation, the
RCO flow (FX2100) is regulated by the column bottom level control. This total RCO
flow in-turn gives the set value to the vacuum furnace pass flow controllers.
b) Swing elbow has been provided at the inlet and outlet of the heater passes, therefore
steam and air decoking can be done either way.
c) There is a provision to route RCO in an 8” line to 12-E-06 A/B (i.e., VR lines) for
utilization of these exchangers during light crude processing. After exchanging the heat
in 12-E-06 A/B, RCO goes to the vacuum furnace.
d) To SR manifold during start-up. This is a start-up line.
16.6.3 Middle Section:
Middle section of the column has product withdrawal and circulating reflux network. In order
to maximize heat recovery and balance the column loading for maintaining proper
temperature profile across the column, three circulating refluxes (CR) are considered viz.,
Top Pump Around, Kerosene CR and Heavy Diesel CR. These circulating refluxes are drawn
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
from their draw-off seal boxes and are routed to preheat trains for recovery before entering
back to the column again
Duty controllers are provided on CR circuits to control CR flow rates to column. These duty
controllers take corrective action based on actual CR duty and desired CR duty. For a
particular type of crude and crude throughput, the CR under reference will have certain duty.
This will be governed by total crude flow and specific heat of CR and is called CR duty.
Actual CR duty is also computed by duty controller based on real time measurement of a)
temperature difference between CR draw off and CR return stream b) CR flow rate and c)
specific heat of CR. While total crude flow, CR temperature difference and CR flow are
measured by various instruments, specific heat of CR is fixed by operator in software for
computation purpose and no on line measurement for this parameter is available. Actual and
desired CR duty is calculated in the duty controller as under:
Actual CR duty = Measured CR flow * CR temperature difference * Sp. heat of CR

stream.
Desired CR duty= (Desired CR duty/desired total crude flow)* Actual crude flow.
The CR draw off and the CR return stream to the atmospheric column temperature
difference is achieved by routing the respective streams through the preheat trains and
exchanging heat with crude oil in the preheat exchangers.
Inputs that are to be manually provided by operator are i) Sp. heat CR stream and ii)
the ratio (Desired CR duty/desired total crude flow) for each crude. Desired CR duty should
be estimated on prorate feed basis to CDU. This is typical to all such duty controllers on CR
lines. Desired CR duty is compared with actual CR duty and flow of CR is varied to achieve
desired CR duty.
a) Top Pump Around (TPA)

TPA is drawn from the 37th tray by the pump 11-P-09 A/B and is cooled by routing it
through 11-E-04 A/B. It enters the Atmospheric Column on the 39th tray. 11-TI-411 and 11-
TI-414 indicate its draw-off and return temperature respectively. TPA flow is indicated and
controlled by 11-FRC-406. The return temperature is to be maintained above 100 °C to
prevent the condensation of water vapour which may result in acid corrosion of the column
top.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
b) Kerosene Circulating Reflux:

Kerosene CR is drawn from 20th tray by the pump 11-P-08 A/B and is cooled by routing
it through 11-E-09 and 11-E-25 in parallel and then through 11-E-11 (BH case). It is then
boosted by 11-P-08 C/D. In BH operation mode, it flows through 12-E-01 A/B/C and then
enters the Atmospheric Column on 22nd tray. 11-TI-403 and 11-TI-413 indicate its draw-off
and return temperature respectively. KERO CR flow is indicated and controlled by 11-FRC-
405. There is a pressure indication 11-PI-432 at the 20th tray in the Kerosene zone. There is a
provision to route hot Kerosene to the unit flushing oil header from the discharge of 11-P-08
A/B
c) Diesel Circulating Reflux:

HD is drawn from the 12th tray by pumps 11-P-07 C/D and is cooled by passing it
through 11-E-15 A/B and 11-E-13. The seal flushing facility to these CR pumps is provided
from the outlet of 11-E-23, Diesel product cooler. The CR return enters the Atmospheric
Column on the 14th tray. 11-TI-402 and 11-TI-412 indicate its draw-off and return
temperature respectively. HD CR flow is indicated and controlled by 11-FRC-404.
d) Product draw-off:
Heavy Naphtha (HN), Kerosene, and HD products flow by gravity from the 28th, 20th
and 12th tray respectively to strippers 11-C-02, 03 and 04 under respective level control of
strippers (viz., 11-LIC-404, 403, 402 respectively). This draw-off from the draw-off boxes
includes the respective CR for Kerosene and Diesel cases. Vapour return lines from HN,
Kerosene, and Diesel strippers back to the fractionator column are provided just two tray
above the draw-off for HN and two trays above the draw-off for Kerosene, and HD. 11-TI-
403, 404, and 405 indicate the draw-off temperatures of HD, Kerosene and HN respectively
from the column in the in DCS panel. 11-TI-407, 408, 409 indicate the vapour return
temperature from HD, Kerosene and HN strippers respectively. 11-TI-206 indicates the
temperature at the 30th tray. An Elevation of 3m for HN and Kerosene and 4m for HD, from
draw off nozzle to each level control valve of the stripper has been provided to exert back
pressure necessary to prevent flashing just down stream of control valve. This also prevents
two phase flow in draw off piping.
16.6.4 Over Head Section:
The overhead vapours of Atmospheric Column pass through the overhead condensers
11-E-17 A to H (in 4 banks) and are totally condensed. The condensate gets collected in the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Overhead Naphtha Accumulator (reflux drum) 11-V-01. Any of this overhead condenser
banks can be isolated for maintenance. There is also a provision of service water connection
at the inlet of each condenser to occasionally wash away the deposits of ammonium salts in
the tubes.
Top pressure of Atmospheric Column is maintained by 11-PRC-409 A/B which

manipulates 11-PV-409A on outgoing uncondensed gases from 11-V-01 and 11-PV-409B on
incoming fuel gas. Since isolation valve is provided in overhead line between Atmospheric
Column and overhead Naphtha accumulator, 11-PSV-401 A/B/C (set at 4.8 kg/cm2 g.) are
provided at the top of column. Snuffing steam provision is given on the PSV outlet header to
quench the vapours in case of emergency or as a safety precaution to be opened during
thunder storms.
Condensed Hydrocarbons are allowed to settle in reflux drum where steam

condensate (water) settles in vessel boot and then flows to the Sour Water Stripper Unit on its
pressure. 11-TI-410 indicates the temperature of the reflux drum in DCS panel. 11-PSV-403
on 11-V-01 has also been provided for the safety of the Atmospheric Column top PSVs.
Uncondensed gases from 11-V-01 are routed to flare through 11-PV-409A and FX- 801
indicates the mass flow rate of the flare gases.
Water-Naphtha interface controller 11-LDIC-406 controls level of water in the boot

and operates 11-LV-406 on 3” sour water line. LIC-1406 has software high / low level alarm
(11-LAH/LAL-406) in DCS panel. 11-FI/FR-450 shows sour water flow in DCS panel when
Atmos sour water is routed to 11-V-04.
Accumulated hydrocarbon in 11-V-01 is pumped back to Atmospheric Distillation

Column as top reflux on the 40th tray by 11-P-06 A/B. Reflux flow is controlled by 11-FRC-
403 which is cascaded to the Atmospheric Column top temperature controller 11-TRC-403.
Excess quantity of Naphtha in Reflux drum is pumped by 11-P-06 A/B to the Naphtha
Stabiliser as feed through a 6” line. The flow of Un-stabilized Naphtha to the Stabiliser is
controlled by 11-FRC-503 which is cascaded to the Naphtha Accumulator (11-V-01) level
controller 11-LRC-405. LIC-1405 has software high / low level alarms (11-LAH/LAL-405).
There is a ¾” provision for injection of Neutraliser and Corrosion Inhibitor on the

Atmospheric Distillation Column overhead vapour line and the reflux line to maintain the
desired pH.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.7 NAPHTHA STABILIZER:
Unstabilised Naphtha obtained in Atmospheric Column overhead reflux drum 11-V-

01 contains lighter ends like C3 and C4 which vaporize at normal Atmospheric conditions.
This Naphtha if stored as such in storage tanks will release lot of Hydrocarbon vapours and
can create unsafe conditions and pressurization of the storage tank. To avoid this problem the
lighter components of Naphtha are removed in a column. This process is called Naphtha
stabilization.
Naphtha stabilization is carried out in Naphtha Stabiliser (11-C-05) where C3 and C4

hydrocarbons are removed from Naphtha. The Stabiliser is a distillation column which has 30
valve type trays (SS410S). It is provided with a PSV (11-PSV-501) set at 14.0 kg / cm2 g.
The PSV outlet is routed to the flare header.
Unstabilized Naphtha from the Top Reflux Pump (11-P-06 A/B) discharge is first
heated up in Stabiliser feed / bottom exchanger (11-E-19 A/B) by exchanging heat with the
outgoing stabilized Naphtha product. There is a provision to route the CDU-I Unstabilised
Naphtha to 11-C-05, the flow of which is indicated by F1505. Feed enters the column on the
17th tray under the flow control 11-FRC-503 which is normally cascaded with 11-LIC-405 of
11-V-01. 11-TI-501 indicates temperature pick up from 11-E-19 A/B before entering the
column.
Overhead vapours from Stabiliser (11-C-05) containing C3 and C4 components come

out from column top in a 12” overhead line. This line is routed through Stabiliser overhead
condensers 11-E-20 A/B/C/D. The condensed liquid, LPG, is collected in the reflux drum
(11-V-03) and consists of C3 and C4 components.
The Stabiliser overhead pressure is maintained by pressure controller 11-PRC-501

A/B.11-PIC-501 acts as a split controller on 11-PV-501A mounted on the condensers bypass
line and 11-PV-501B mounted on the off-gas line from 11-V-03 to FCCU-II (14-V-11).
In case of decrease of Stabiliser top pressure below the set value, 11-PRC-501 opens
11-PV-501A to allow hot vapours directly into 11-V-03, bypassing the condensers. If the
pressure in 11-C-05 increases above the set value, then 11-PV-501B would open to release
the excess pressure to the FCCU-II sweet fuel gas distribution network. There is a provision
to route the Off-gas through 11-PV-501B directly to the flare also.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
LPG pumps 11-P-11A/B function as both LPG product and reflux pumps. Reflux
flow which is controlled by 11-FRC-501 can be cascaded with the column top temperature
(30th tray) indicator and controller 11-TI-510. A 2” minimum flow line (spill-back) from the
discharge header of 11-P-11 A/B is to the pump suction is also provided.
11-LIC-502 controls LPG product flow to maintain reflux drum level and it is
cascaded to 11-FRC-502 on the LPG product flow line. LPG is sent to the Amine Treating
Unit in MEROX for the removal of H2S and Mercaptans. 11-V-03 also has level high / low
alarms in the DCS panel (11-LAH/LAL-502).
A slip stream of LPG can also be sent to the LPG vaporiser of FCCU-II in a 2” line.
Sour water is collected in the boot of 11-V-03. The interface level of water and LPG is
indicated by DL-1503. High water level in boot may result in water carryover with LPG and
it will affect the Amine Treating Unit at MEROX. Hence it is drained at a controlled rate to
OWS periodically.
11-PSV-502 set at 14.0 kg/cm2 g. is provided on the Stabiliser reflux drum whose
discharge is route to flare header. It prevents vessel from getting over pressurized in case of
external fire.
A 2" service water line connection is provided on 11-V-03 to fill the vessel and wash
the Stabiliser column with water during shut down.
A thermo siphon Stabiliser reboiler 11-E-25 is provided at Stabiliser bottom to supply

the necessary heat for boiling the Unstabilised Naphtha. Kerosene CR from the discharge of
11-P-08 A/B is used as heating medium. 11-TR-403 & 11-TI-507 indicate the Kerosene CR
supply and return temperature. The bottom temperature is indicated and controlled by 11-
TRC-501. The control is achieved by adjusting the flow of Kerosene CR through 11-FV-504
which can be cascaded to the Stabiliser bottom temperature as indicated by 11-TRC-501. 11-
TI-506 & 505 indicate the stabiliser bottom reboiler shell-side (Naphtha-side) inlet and outlet
temperatures respectively.
Stabilised Naphtha gets collected at the bottom of the Stabiliser and the bottom
level is controlled by 11-LIC-501 down stream of caustic and water wash sections. There is
also an indication of bottom level high and low alarms as 11-LAH/LAL-501 in the DCS
panel. This Stabilised Naphtha goes under the pressure of the Stabiliser to 11-E-19 A/B
where it exchanges heat with the feed and then it gets cooled further in the salt water cooler
11-E-21. Naphtha from 11-E-21 flows through a 6” line to the caustic and water wash drums
(10-V-01 and 10-V-02).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.8 RCO PUMPS:
It is a motor driven centrifugal pump. The pumping temperature is 343°C and viscosity at
pumping temperature should be 1.25 cst. Vapor pressure at pumping temperature has to be
3.76 kg/cm2 absolute. Density of the fluid has to be 780 kg/m3. It has a design pressure of
15.3 kg/cm2A and temperature of 380°C. The casing and the impellor are made of 11-13%
Cr-steel. It has a mechanical seal to protect out flow of liquid from the casing.

Maximum flow rate 232 m3/hr
Discharge Pressure 12 kg/cm2A
NPSH available 3.0 meters
Pump Change over Procedure:
• Ensure all the utilities like BCW, seal steam and self coolant are open, suction valve is open
and discharge valve is closed. Drain the standby pump casing for removal of any entrapped
water.
• Ensure the discharge is fully closed and warm-up is open.
• Close warm up after ensuring the readiness of pump.
opening the discharge and simultaneously closing the running pump discharge valve. This
activity has to be done very slowly so that the flow does not fluctuate heavily. During this
activity, amps of both the pumps have to be checked and ensure that it doesn’t go beyond
FLC for either of the pump.
• Keep the stand by pump in warm up condition.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.9 VACUUM HEATER:
Major equipments of this section are Vacuum heater, air pre-heater, ID fan, FD fan and steam
decoking pot (Common for Atmospheric and vacuum heater), separate APH including ID and
FD fans have been provided for the crude and vacuum heaters.
RCO enters at the top of the convection zone of the fired heater. Part of the slop distillate
produced from vacuum column is also routed along with RCO for the purpose of providing
over flashing. From the bottom of the convection zone the coils are routed to the radiation
zone. From radiation zone, RCO comes out of the heater and enters Vacuum column 12-C-
01. Reduced Crude oil is heated 405 0 C (IM)/398 0 C (BH) before entering the 12-C-01 for
fractionation.
The heater 12-F-01 is a single cell, cabin type fired heater having four parallel passes.
The radiant section of the heater is provided with 20 bare tube/pass of 9% Chromium+1%
Molybdenum grade 4” NB Sch. 40 size except the last two tubes of each pass which are of 8”
NB Sc 40 and 6” NB Sch 40 from outlet. The convection section has 4 tubes per row and
consists of 6 rows of tubes with 4 tubes per row. While the top 4 rows of this zone are
studded type, the bottom two rows are bare tubes. The material of construction of the tubes is
9% Chromium+1% Molybdenum. The tubes are 6” NB Sch. 40 type, during 2010 T&I
additional convection zone was provided. This zone consists of 8 rows of tubes with 4 tubes
per row. In the additional zone, top 4 rows are SPP16 studded tubes, next two rows are SPP9
studded tubes and bottom two rows are bare tubes. The RCO passes are numbered as pass A
to pass D. Skin thermocouples have been provided on heater pass tubes to know the metal
temperatures at convection zone outlet, middle of the radiation zone and outlet of the
radiation zone.
Individual pass flow controllers namely 12-FRC-101/102/103/104 regulate flow in

each pass. These controllers get input signal from respective flow transmitters (FT2101 to
FT2104) and set point signal from a ratio controller. Controllers generate output signal and
manipulates respective flow valves (FV -2101 to FV-2104).
The ratio of RCO in a particular pass to the total crude flow is maintained by a ratio
controller or passes balancer. The ratio controller/pass balancer functions such a way that the
weighted average temperature at the outlet of each pass is maintained almost the same, Ratio
controller receives software input signal from 11-LRC-401 (Through a selector switch) which
is responsible for Atmospheric column bottom level, Pass balancer gets input from each pass
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
flow (12-FRC-101/102/103/104) and each coil outlet temperature (12-TI-106, 111, 116, and
121) and then controls individual pass flow in order to maintain heat balance of all the passes.
Pass balancer is an advanced control feature conceived for better furnace control.
The distribution of RCO through each pass should be adjusted in such a way that the heat
duties and hence COT (Coil out let temperature) of all the passes are more or less same.
Depending on heat duty variation pass flow will vary. In equality of flow through each pass
to the extent of 10% can be tolerated, while operating on manual mode or without pass
balancer. 12-FAL-101/102/103/104 are provided on all the passes to protect the heater pass
tubes in case of low flow through each pass.
All the four passes join together at the outlet of radiation zone. DCS indication of
temperature for each pass is provided (12-TI-106, 111, 116, and 121) and there is also an
alarm for high transfer line temperature as 12-TAH-133. Temperature indicators 12-TI-302,
307, 312 & 317 are provided on the outlet of the convection zone to measure the temperature
gain in this zone.
To avoid repetitive description features of only pass-A have been taken up. For other
passes identical arrangements exists.
FIC-2101 controls and indicates RCO flow through pass-A, through transmitter FT-2101 has
been provided. 12-FAL-101 actuation of this alarm will trip fuel supply to all burners of the
heater, excluding pilots. A local PI indicates field pressure and DCS bound 12-TI-302
indicates temperature of RCO at radiation zone inlet. 12-TI-106 indicates temperature in DCS
and a local PI shows pressure of RCO of pass-A at heater outlet, software alarm TAH and
TAL on the COT has been provided to alert the operator against inadequate flow or
inadequate firing in that particular pass. Prolonged high temperature may lead to coking up of
that particular pass, Finally heated RCO enters a common manifold 52” size called transfer
line before entering Vacuum column.
The common outlet transfer line temperature is measured by 12-TI-122 and is controlled
and recorded by 12-TRC-133 (coil outlet temperature), which regulates quantity of fuel to the
furnace.
Pressure drop across the heater coil is a measure of internal tube condition and increase in
pressure drop indicates tube fouling due to coke formation in the tubes. Emergency coil MP
steam connections are given in each pass, down stream of pass flow control valves to displace
RCO from the coil to the column during an emergency or after normal shut down operation.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Soot blowers, using MP steam are provided in convection zone of the heater. Need of
soot blowing will be indicated by poor heat pick-up in convection zone and increase in flue
gas temperature. The soot blowers can be operated from grade level also.
Emergency steam, soot blower steam and decoking steam connections are taken from 8“MP
steam header.
Snuffing steam (furnace purging steam) is connected to convection zone and heater box in
order to extinguish fire by steam blanketing. LP steam is used for this purpose.
To facilitate safe approach to emergency team/snuffing steam during an emergency scenario

isolation valve on steam line needs to be provided at a safe distance of at least 15 meters from
heater.
ii) Fuel System:

12-F-01 is a balanced draught furnace (and can be operated in natural draught at 70%
efficiency). Both the convection and radiation sections are used for heating crude. The
combustion chamber houses the radiation section of tubes. The convection section provided
at the top of radiation section serves to increase the thermal efficiency of the furnace by
utilizing further heat from the flue gas. Tubes in radiation and convection zone are arranged
horizontally.
vacuum heater has a total of 12 burners. During 2010 T&I, all the burners were replaced with
16 new burners ZEECO make.
a) Fuel Gas System:
branched into a 3” header to the Vacuum Heater. This FG line is steam traced to avoid
FG to main burners passes through a mass flow meter F2406 and a shutdown valve
12-SDV-105. This SDV is connected to interlock logic. 12-FR/FQ-107 records and integrates
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
the FG flow to 12-F-01. It is provided with FAL and FAH. Local PG and TG are provided to
indicate pressure and temperature at field.
12-PI-308 indicates FG pressure on the DCS panel. A low pressure alarm 12-PAL-
108 is also provided. Fuel gas pressure low trip is set at 0.2 kg/cm2 g. In case the fuel gas
pressure is low, only 12-SDV-105 will get closed. If fuel gas tip pressure falls below the set
value, chances of flame failure and subsequent accumulation of un-burnt hydrocarbons in the
firebox is possible. This can lead to the possibility of explosion or back fire in the heater.
Hence the provision of FG pressure low trip. There is a provision to cascade the fuel gas
pressure to the 12-F-01 COT, 12-TRC-133 through a selector switch on the auxiliary panel in
the DCS room.
A 2” FG tapping upstream of 12-SDV-105 has been branched off for pilot burners.
The pilot gas pressure is normally adjusted manually and is maintained at a pressure of 0.7
kg/cm2 g. In case of low pilot gas pressure, 12-PAL-107 is provided to actuate an alarm. Low
pilot gas pressure will alert the operator when pilot gas pressure falls.
b) Fuel Oil System:
branched into a 2” header to the Vacuum heater. FO line is steam traced to maintain
temperature and avoid congealing. Flow recorder and integrator 12-FR/FQ-105 is provided
on main FO supply line and 12-FR/FQ-106 is provided on the main FO return line from
heater. Since this is a closed circuit through which FO circulation is maintained, the net
consumption of fuel oil is measured as the difference between FI-105 and FI-106. Shutdown
valves 12-SDV-102 A/B are provided on the FO supply and return headers respectively.
Local PG’s and TG’s are provided on the supply line to show pressure and temperature of FO
supply. 12-PRC-101 indicates the Pressure of fuel oil on the DCS panel. Pressure is
maintained by 12-PRC-101, which regulates 12-PV-101 on the fuel oil supply line. There is a
provision to cascade the fuel oil pressure 12-PRC-101 to the 12-F-01 COT, 12-TRC-133
through selector switch, on the auxiliary panel.
A low-pressure trip alarm has been provided on supply line. Actuation of this alarm
shuts 12-SDV-102 A/B and cuts off only the fuel oil firing to the Furnace. Since FO is
normally a thick heavy liquid, it needs to be always maintained in circulating state. If it is left
stagnant and unused in burners and piping, it can get congealed despite the fact that tracing
steam of the FO circuit is on. Circulation in heater area (FO piping forming a closed circuit
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
across all passes called fuel oil ring) is maintained even when no fuel oil burner is in use. A
ratio of 2:1 FO supply to return is normally maintained to obtain a good control on firing and
the heater, the circulation can be maintained. Purge steam connections are provided on each
oil burner. FO burners are to be kept steam purged when idle. When FO is fired, it is
atomised or sprayed as a fine mist for realising complete combustion. The spraying of FO is
done by de-superheated MP steam in FO burners.

FO supply and MP steam simultaneously. Atomising steam pressure is maintained about 2.0
kg/cm2 above the FO pressure. Atomising steam flow is recorded by 12-FR-108. Local PG
and TG are also provided on this line. 2” flushing oil connection is provided on FO supply
line up stream. CBD/OWS drain is provided on FO return line. These provisions are to flush
the line within Battery Limit after heater shut down. When furnace operates on combination
fuel-either Fuel Gas operates on PIC and Fuel Oil on PIC/TIC cascade or Fuel Oil operates
on PIC and Fuel Gas on PIC/TIC cascade mode. Selector switch is used to select only one
fuel for COT control by cascading.
Heater operating conditions:
Operating Temperature (°C) 340 (IN) 405(OUT)

Operating Pressure (kg/cm2-a) 3.57 0.07
Heater Section:
Design Pressure 18 kg/cm2 g
Material of Construction 9 Cr + 1 Mo (A335 Gr P9)
Desired efficiency 88% (LHV)
Minimum stack height 60 meters.
Note: For further data, please refer to furnace improvements of CDU-II vacuum heater,
Volume-I, page 20.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.10 VACUUM COLUMN:
The vacuum column (12-C-01) has three sections of different diameters. Top section is of
5000 mm diameter. Middle section is of 6600 mm diameter and bottom section is of 5000
mm diameter. The column has 3 packed sections. It is provided with 3 total draw-off trays for
LVGO, HVGO and Slop cut. Vacuum Residue is drawn as bottom product. Chimney trays
are provided for all side draw off products. The vacuum column is designed to operate in dry
vacuum mode. Vacuum indicators are provided at top and flash zone of the column.
Description of Vacuum column has been taken up zone wise starting from bottom.
16.10.1 Vacuum Column Bottom Section:
The partly vaporized RCO feed stock coming from the vacuum heater enters the column in
the flash zone below the slop draw off chimney tray. The vaporized portion rises up in the
tower and is fractionated into 3 side stream products. The liquid portion of the feed drops into
the bottom section of the tower and is withdrawn as Vacuum Residue (VR). Vacuum Residue
is also called as Short Residue (SR). Column bottom has 3 disc and donut type trays.
The Column bottom level is maintained by 12-LIC-202’s action on 12-LV-202 on VR

rundown line. LI-2201 also indicates level on DCS panel. Both LIC and LI have software
high level and low level alarms 12-LAH/LAL-201. 12-TI-201 indicates temperature of the
column bottom on the DCS panel. LAH-2108 and LAL-2109 are also provided for column
bottom on the DCS panel.
A tangential vapour horn is provided for flash zone inlet, which minimises
entrainment of heavier hydrocarbon liquid droplets. There is a 3 inch LP steam line provision
to column bottom below tray 1 for steaming out purpose.
Vents of all pumps taking suction from Vacuum Column are connected back to
Vacuum Column above flash zone through a common vacuum line. With this arrangement all
pumps connected with Vacuum Column can be vented to the column.
Temperature at the bottom section is normally quenched to about 350 °C at a vacuum

of -735 mm Hg (g.). RCO is fed to the flash zone at 390 °C.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.10.2 Vacuum Residue Draw-off:
Vacuum Residue (VR) is drawn by VR + Quench pumps (12-P-01A/B SR pumps) at 350 o C

from the column (12-C-01) bottom. VR pump discharge can be routed to following
destinations:
a) To Vacuum Heater (12-F-01) through 8” start-up line which joins the RCO feed line to
12-F-01. This is used during start-up only.
b) A slip stream of the pump discharge can also be routed to the pumps suction in a 2” line
as spill-back.
c) The pump discharge from 12-P-01 A/B exchanges heat with crude in 11-E-16, 12-E-06
A/B and 12-E-03. The outlet of 12-E-03 at a temperature of 250 °C can be routed as
follows.
i. It is partly sent to the 12-C-01 bottom in a 6” line for quenching and maintaining the
bottom temperature at 350 °C to prevent cracking of SR and lead to other problems
like deterioration of vacuum, plugging or suction strainers of 12-P-01 A/B leading to
loss of suction. The quench flow is recorded and controlled by 12-FRC-204.
ii. It can be partly sent as feed to the Bitumen Blowing Unit in a 3” line.
iii. The rest of it can either be sent to 12-E-01 A/B/C and then to 12-E-09 A/B/C/D or can
be routed directly to the 12-E-09 A/B/C/D where it is cooled. TIC-2103 located on VR
product rundown header to tanks controls TV-2103 on the tempered water line to 12-
E-09 A/B/C/D.
d) Down stream of the coolers, SR can be routed to

i. IFO pool partially in a 6” line.
ii. Storage via the three-way FCV 12-FRC-405 through an 8” RFO line, or to the HFO
pool by adjusting 12-FV-405. The HFO flow is measured by 12-FR-406.
iii. LDO pool partially, in a 4” line, measured by 12-FI-407.
iv. VBU as hot feed from the upstream of 12-E-09 A/B/C/D or to VBU storage tanks in
10” line. (TIC-2420 on rundown line maintains VR temperature by bypassing a certain
amount of hot VR to the rundown line)
v. BBU storage tanks via HFO line (at unit limit tie-in).
16.10.3 Vacuum Slop-Cut Draw Off:
Immediately above flash zone, a wash zone consisting of one section packed bed is provided.
Slop section is a bed with a demister pad above the zone packing. The vapors rising from the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
wash zone pass through a demister pad provided above the wash section to trap entrained
droplets of heavy hydrocarbons, which could otherwise adversely affect HVGO/LVGO
quality.
Slop is drawn by slop distillate pumps (12-P-02 A/B) at 350 o C. This is first side draw off
from the bottom.
The draw-off temperature is indicated by 12-TI-204. The level on the chimney tray is
regulated by 12-LI-203 by operating 12-LV-203 on the slop-cut rundown line to the VR line.
Slop + Recycle pump (12-P-02 A/B) discharge has following destinations.
• As recycle stream to vacuum furnace along with RCO. One part of slop distillate goes to the
furnace under flow control 12-FRC-109 through a 3” line. The purpose of maintaining slop
recycle is to provide necessary over flash in the vacuum column. The slop recycle from slop
pump is mixed with RCO from atmospheric column before getting heated in vacuum furnace.
However if any premature coking is observed, the slop recycle may be reduced accordingly.
Additional provision was given during 2010 T&I for routing the slop-cut to FCCU-II from
the downstream of slop-cut recycle control valve.
• As product rundown, a part of Slop Distillate pump discharge gets mixed VR product up
stream to 12-E-01 A/B/C. 12-LV-203 on slop line maintains slop level on the chimney tray of
slop section
16.10.4 Heavy Vacuum Gas Oil Draw off:
The majority of rising hydrocarbon vapors from slop zone wash section is condensed in
HVGO section by circulating reflux to yield the side draw product. HVGO product internal
reflux (IR) + circulating reflux (CR) is withdrawn as a second side steam.
12-TI-205 indicates draw off temperature. HVGO after draw off is pumped by HVGO
product +CR pump (12-P-03 A/B) at 314 o C and splits in to two streams.
One part goes as internal reflux for packing washing of slop section of vacuum column
without any heat exchange. HVGO IR is regulated by 12-FRC-202 in such a way that proper
washing of the packing is always achieved for all throughputs. Height of packing is fixed and
dependent on heat withdrawal requirement by slop quench stream. One distributor is
provided for proper distribution of HVGO IR over entire cross section area of the column
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
packing. Strainers (12-X-01 A/B) are provided to arrest carry over of foreign materials back
into column. Pressure gauges across the filters indicate the pressure drop across the filters and
its rise would indicate the need to change over of the filter in line. 12-TI-206 shows HVGO
IR temperature.
The other part is routed to preheat exchanger trains as HVGO CR + product.
HVGO CR + product from 12-P-03 A/B discharge is split into two steams. One stream goes
through 12-E-05 A/B and 12-E-02 and the other through 12-E-04. Here, it exchanges its
sensible heat with the crude. The two streams are then combined and routed to the MP steam
generators 12-E-10/10A parallel. The stream coming out of the steam generators is routed
partly as HVGO CR back to column at through the CR strainer 12-X-02 A/B. This flow is
controlled and recorded by 12-FRC-203. The CR return temperature is indicated by 12-TI-
208. The remaining volume is either routed as hot feed to FCCU-II or to product rundown
line or both at the same time.
16.10.5 Light Vacuum Gas Oil Draw off (LVGO):
The rising uncondensed hydrocarbon vapors from HVGO zone packing are condensed
in LVGO section by circulating reflux to yield the side draw product. LVGO product+
internal reflux (IR) + circulating reflux (CR) is withdrawn through 10” line from the third
chimney tray. 12-TI-207 indicates draw-off temperature on the DCS panel. LVGO draw-off
from the column is routed to LVGO product + CR + IR pumps (12-P-04 A/B), whose
discharge is routed as
LVGO IR stream: The packed bed in HVGO zone below the LVGO zone is washed by
LVGO internal reflux stream. This stream enters the column without any heat exchange.
LVGO IR is regulated by 12-FRC-201 in such a way that proper washing of packing is
achieved for all throughputs. One distributor is provided for proper distribution of LVGO IR
stream over entire cross sectional area of the column packing. Strainers (12-X-02 A/B) are
provided on LVGO IR return to arrest carry over of any foreign materials back into column.
LVGO Circulating Reflux: This stream splits further into two streams. One stream goes 11-
E-07 to exchange its sensible heat with the crude and then goes to 11-E-22 for cooling. The
other stream goes to 11-E-22A directly for cooling. The outlet of 22 & 22A combine and go
through the LVGO CR strainer 12-X-03 A/B to the top of the LVGO packing as top reflux.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
The CR flow is controlled by 12-FRC-205 and the return temperature is indicated by 12-TI-
210.
LVGO Product: A part of 12-P-04 A/B discharge stream gets cooled in 12-E-11 and can be
routed to HVGO storage tanks or FCCU-II. The flow of this stream is controlled by 12-LRC-
205 and is recorded / integrated by 12-FR/FQ-403. The product can also be routed to Diesel
or LDO pool controlled by 12-FRC-404.
LVGO product is routed as follows:

1 As hot feed to FCCU-II along with hot HVGO through 12-LV-205
2 To VGO storage tanks along with HVGO through 12-LV-205
3 Either to Diesel/LDO/SR or HVGO (at battery limit) storage tanks through 12-FV-
404 in a 3” line. There is a provision to cascade the level controller on the LDO FCV
4 To flushing oil system in a 2” line
5 To slops along with HVGO.
16.11 Ejectors:
Fluid handled: Composition
Component Kg/hr MW Moles/hr ° API

Non condensable 840 33.7 24.93 -
Oil vapor (condensable) 500 250 2.0 30.31
Vapor pressure data of condensable oil vapors:
Temperature, °C Vapor pressure, mm Hg abs

40 0.011
50 0.025
60 0.056
70 0.120
80 0.23
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Operating conditions:
Temperature, °C Pressure
Maximum Normal Maximum Normal
Inlet 95 80 - 5.0 mm Hg abs
Outlet - - - 1.1 kg/cm2.a
Mechanical design:
Design temperature 340 °C
Design pressure kg/cm2.abs 14 /full vac.
Material of construction:
Ejector nozzle SS
Ejector steam chest steel
Suction chamber and diffuser cast iron and steel plate
Steam condenser tubes 70:30 Cu-Ni
Valves steel bodies
Description:
In Vacuum column overhead system, three stage ejectors with condensers are
provided to maintain the desired vacuum. MP Steam is used as a motive fluid in ejectors.
Vacuum column overhead vapor line (36”) is routed to first stage ejectors (12-J-01 A/B/C).
First stage ejectors outlets are joining a common header and which is routed to shell side of
1st stage inter condensers (12-E-07A). Uncondensed vapors from inter condensers (12-E-
07A) are joining a common header and then routed to second stage ejectors (12-J-02 A/B/C).
Second stage ejectors outlets are joining a common header, which is routed to shell side of
second stage inter condenser (12-E-07B). Uncondensed vapors from inter condensers (12-E-
07B) are routed to third stage ejectors (12-J-03 A/B/C). Third stage Ejectors (12-J-03 A/B/C)
outlets are joining a common header which is routed to surface condenser (12-E-07D).
Condensate streams from surface condensers (12-E-07A, 12-E-07B and 12-E-07D) are routed
through barometric legs to Receiver Vessel called hot well drum (12-V-01). These barometric
legs are dipped in water the ejector condensate receiver (12-V-01) for sealing purposes.
Uncondensed vapors from third stage ejectors (12-J-03 A/B/C) are routed to the Hot Well
Drum through a dip leg. 12-PRC-206 is mounted on the non-condensable line from 12-E-
07D, controls the Vacuum Column overhead pressure by routing a part of the non-
condensable vapours (before letting them into the Hotwell drum) to the inlet of the 1st stage
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
ejectors. A 3” fuel gas line is provided near the inlet of the 1st stage ejectors, for backing-in of
fuel gas during the start-up and shut-down to maintain the column in positive pressure.
The 1st stage ejectors (12-J-01 A/B/C), 2nd stage ejectors (12-J-02 A/B/C) and the 3rd
stage ejectors (12-J-03 A/B/C) are designed for a capacity factor of 1/7, 2/7 and 4/7 totalling
150% of normal capacity. If required each ejector element can be isolated by cutting off
steam and isolating suction inlet valves.
Cooling water is supplied to the primary condenser in an 18” header. The water outlet
from the primary condenser is bifurcated into two parts. One part feeds the cooling water to
the secondary condenser and the next part feeds the after-condenser. There is a provision to
back flush the primary condenser. A draining provision is provided in the up-stream of the
after-condenser.
MP steam to all ejectors is supplied in parallel by 6” header. Ejector steam

consumption is indicated by 12-FR-207. Strainers are provided on the MP steam line to arrest
line scales etc. from reaching into ejectors and adversely effecting performance of overhead
system. Ejector steam pressure is controlled by 12-PRC-207. This should be maintained
constant as far as possible for smooth operation of the Vacuum Column. Corrosion Inhibitor
and Neutraliser injection facility into overhead vapours have been provided both on Vacuum
column top overhead.
Operation procedure:
1. Commissioning:
a. Ensure all the mechanical jobs are completed on the ejectors with all accessories.
b. Check all the blinds have been removed or not.
c. Check Hot well is properly filled of water or not. If not fill it up and commission Hot
well overflow loop.
d. Charge steam header to the ejector. Drain condensate from the low point drains.
Ensure steam is clear before it is charged to the ejectors.
e. Open cooling water to all the surface condensers.
f. Before opening steam to the ejectors, open the strainer bleeder and purge the strainer.
g. Open all the isolating valves of the ejectors to be placed in service on the first and
subsequent stages of the ejectors.
h. Open upstream and downstream valves of the pressure controller for controlling
vacuum.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
i. Open steam slowly to the ejectors to the last stage. Wait till the vacuum stabilises.
Next open steam to the preceding stage ejectors and so on until the required vacuum
is obtained.
Note: when an ejector in a stage is in service, the other ejectors in that stage should be
positively isolated, if they are not in service to avoid circulation of the non-condensables in
that stage. If any of the ejector is out of service, is to be placed in service, the following is the
sequence of steps to be followed.
Open the ejector outlet valve.
Open steam to the ejector
Open hydrocarbon inlet valve to the ejector.
If an ejector in service has to be taken out, then the alternative ejector has to be first
placed in service.
j. When the hot well level starts increasing commission hot well oil and water pumps.
When the hot well oil rate becomes steady put the oil pump on AUTO.
2. De-commissioning:
a) Close the hydrocarbon inlet valve to ejectors.
b) Close steam to the ejector
c) Close the outlet valve to the ejector.
The above sequence of operation is for shut down of an ejector. And for total shut down of all
the ejectors, the above sequence of operation should be carryout from the last stage to first
stage and followed by
Opening make up water to the hot well drum
Closing cooling water to surface condensers
For total shut down of all ejectors, take out steam from first stage ejectors to last stage
ejector in that order and isolate steam header to ejectors.
Open make up water to hot well and maintain level
Isolate all ejectors upstream and downstream valves
Close cooling water to all surface condensers.
Trouble shooting:
If vacuum starts falling, the reason may be:
Insufficient inlet steam pressure
Inlet water temperature to the condensers higher then normal temperature
Air leaks in the tail pipe of inter condensers
Flooding of the inter condensers by excessive water flow (direct cooling water
condensers).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Starving of any inter stage condensers by insufficient water flow.

Plugging of water distribution system in the condensers.
Plugging of the tail pipe.
Plugging of the steam nozzle and jets due to pipe scale.
Steam leak at nozzle throat.
The defects mentioned are to be located and rectified for proper operation.
16.12 HVGO PUMPS:
pumping temperature should be 0.7 cst. Vapor pressure at pumping temperature has to be
17 kg/cm2A and temperature of 340°C. The casing and the impellor are made of 11-13% Cr-
steel. It has a mechanical seal to protect out flow of liquid from the casing.
Normal flow rate. 333 m3/hr

Maximum flow rate. 400 m3/hr
Minimum flow rate. 211 m3/hr
Discharge Pressure 12.22 kg/ cm2A
Differential Head 144 meters
NPSH available >6 meters
• First take clearance from CPP as it is a HT pump.

• Ensure all the utilities like BCW (supply and return), seal steam are open, suction valve is
open and discharge valve is closed. Drain the standby pump casing for removal of any
entrapped water.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.13 SR PUMPS:
pumping temperature should be 3 cst. Vapor pressure at pumping temperature has to be
29.7 kg/cm2A and temperature of 415°C. The casing and the impellor are made of 11-13%
Cr-steel. It has a mechanical seal to protect out flow of liquid from the casing.
Normal flow rate. 133 m3/hr

Maximum flow rate. 174 m3/hr
Minimum flow rate. 80 m3/hr
Discharge Pressure 21.3 kg/ cm2A
NPSH available 3.5 meters
• First take clearance from CPP as it is a HT pump.

• Ensure all the utilities like tempered water, seal steam are open, suction valve is open and
discharge valve is closed. Drain the standby pump casing for removal of any entrapped water.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
16.16 Condensate recovery unit: (CRS)
The condensate recovery unit was commissioned in the 2010 T&I. The main aim is
to recover the condensate obtained from the steam traps of various steam tracings. The steam
trap outlets are joined together and same were routed to flash vessel located at CRS skid (at
south of BBU compressors). In the flash vessel the steam and condensate were separated and
condensate was routed through bucket trap to the collector drum and when the collector
drum reaches 5 kg.cm2 pressure the content will be routed to condensate tanks located at
FCCU-II. The top uncondensed steam from flash vessel is routed to seal steam header with a
check valve.
Total no. of steam traps connected to CRS: 233
List of critical steam traps connected to CRS:
1. Steam tracing of Bitumen product take off from reactor- North of 13PM-03A
2. Steam tracing of bitumen R/D at pump discharge- North of 13E-03A
3. Steam tracing of CDU-II SR to BBU C/V loop- East of BBU off gas KOD
4. Steam tracing of BBU Long circulation loop-South of 13E-01A/B
5. Steam tracing of SR to HFO, RFO, IFO, LDO, and start up circulation loop at SR
manifold- North of Preheat train-II block v/v.
6. Steam tracing of SR to VBU R/D at SR manifold- North of 12PM-07B
7. Steam tracing of SR LCV manifold- West of SR LCV
8. Steam tracing of SR pump spill back- North of 12PM-02B
9. Steam tracing of CDU-III SR to BBU- North of 12PM-01B
10. Steam tracing of SR pump discharge- North of 12PM-01A
11. Steam tracing of SR to HFO, IFO, and LDO at B/L- South of BBU off gas KOD-2
12. Steam tracing of 12F-01 FO Supply & Return- North of pillar no. N26
13. Steam tracing of HVGO to slop & slop header- South of slop manifold
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
14. Steam tracing of HVGO hot feed- West of 11PM-03C

15. Steam tracing of SR quench C/V loop- South of 11PM-04B
16. Steam tracing of HVGO R/D, RFO, and Bitumen R/D at B/L- North of 11F-01 MP steam
manifold
17. Steam tracing of HW off gas flame arrestor loop- North of flame arrestor
18. Steam tracing of 11F-01 FO Supply & return- West of inst. air KOD
19. Steam tracing of SR to VBU at B/L- South of EBL
Flash Drum & Pump:
Flash drum pressure is holding at 2 kg/cm2g. Condensate from flash drum is pumped out by a
Pressured Powered Pump for which MP steam acts as a motivator. Pump is Operating at a
temp. 75 deg C & pressure 4.5 bar.
Condensate Drum:
Condensate drum at FCCU-II is commissioned which is having a LT, & LOW & HIGH level
switches. FCCU-II CRS condensate header joins to 4” header before connecting to
condensate drum. A TG & PG provided at the drum inlet condensate header.
PROCEDURE:
Pressured Powered Pump Package Unit:

1. Slowly open supply to provide pressure at the PP pump inlet valve.
2. Check that trap is operational. Open gate valves in the condensate inlet and discharge
line.
3. Open valves ahead of the unit allowing condensate to enter the receiver and fill the PP
pump body. Pump will discharge when full. PP pumps should cycle periodically
cycle.
4. Set the motive pressure about 2 kg above total back pressure including frictional
losses.
5. If the condensate to the pump is slow. The pump will not operate till it is full. The
strokes will be intermittent.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
Do’s:
1. Before attempting any maintenance, be sure that the unit is completely isolated and
relieved of any internal pressure. Motive supply, exhaust, condensate inlet and
discharge lines should all be closed.
2. Check whether condensate reaches pump.
3. Check the vent is open to atmosphere, check strainers weekly for chokes and clean.
4. Check motive pressure. It must be 2 bar above the back pressure.
5. When the available motive steam or air pressure exceeds 8.7 kg/cm2, a pressure
reducing arrangement is required to reduce pressure going to pump.
6. The discharge line should rise vertically up immediately after outlet DCV to cover the
entire head and then it should discharge to the tank by a sloping line. This is necessary
so that frictional losses are kept to minimum and realize maximum advantage of
gravity.
Don’ts:
1. Do not close the vent under any circumstances
2. Do not allow the motive pressure to fluctuate
3. Do not install crooked delivery line.
4. The discharge line should never be smaller than the bore of the outlet valve, it should
be properly sized to handle the quality of condensate.
5. Do not hammer the pump if it does not work. Go to the trouble shooting schedule.
6. Do not allow steam in the condensate to enter the pump body. Steam must be separated
before hand by providing proper trap.
Trouble shooting of Pressured Powered Pump:
S no Symptom Cause Check and cure

1. Pump fails to a. Motive supply closed. 1. Open valves to supply motive pressure to
operate on start up pump
b. Condensate inlet line 2. Open condensate valve, check upstream
closed or flow is strainers and clean. Wait till sufficient
inadequate condensate flows to the drum and fill the
pump.
c. Condensate discharge 3. Open all discharge lines to allow free
line closed. discharge from pump to destination.
d. Motive pressure 4. Check motive pressure and static back
insufficient to overcome pressure. Adjust motive pressure to 1 to 2 bar
back pressure more than total back pressure.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
2. Supply line/ a. Pump under sized. a. Verify the rated capacity as per the TIS
equipment flooded, capacity table. Increase check valve size or
but pump appears to install additional pump as required.
cycle normally. b. Insufficient motive b. Check motive pressure setting and maximum
pressure to achieve rated back pressure during operation. Compare
capacity. with capacity table of TIS increase motive
pressure as required to meet the load
requirements.
c. Restriction in c. Clean the strainer and check that all valves
condensate inlet line are fully open.
d. Inlet or outlet check d. Isolate check valves and relieve line
valve stuck open pressure. Clean the DCV’s
(debris)
Pressure reducing valve (DP143):
i) Ensure that all connections are properly made and that all valves are closed.
ii) Close all valves at reducing valve station, including valves on by pass line if fitted.
iii) Check that adjustment screw is turned fully anti-clockwise until spring is slack.
iv) Open small valve in pressure control line.
v) Blow through the approach pipe work by removing the cap and screen from the strainer
protecting the steam trap draining the upstream pipe work. Replace upon completion. Do
not remove the screen from the main line strainer during this operation. Although this
should remove most of the dirt which is present, it may be necessary to examine and
clean the main line strainer at regular intervals.
vi) Slowly open the upstream isolation valve until it is fully open.
vii) Using a suitable spanner slowly turn adjustment screw in a clockwise direction until
desired downstream pressure reading is obtained.
viii) Holding the adjustment screw in position with the spanner tighten down the locknut to
secure the setting of the adjustment spring, making sure that the “C” washer stays in
position.
ix) Slowly open the downstream valve until it is fully open.
Maintenance of the valve:
It is recommended that the valve is dismantled once in every twelve to eight months for a
complete overhaul and ideally this is to be carried out with the valve removed from the line.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 16
PLANT NAME: CDU II
Chapter Rev No: 0
The parts that may require replacing or refurbishing are listed below. Main valve (22) and
valve head (21), pilot valve assembly (14), pilot diaphragms (10), main diaphragms (28).
Diaphragms and cleaning:
If the valve is dismantled and either the main diaphragms or the pilot diaphragms are not
renewed care must be taken not to turn the diaphragms over- refit them in exactly the same
position as and when dismantled. The control orifice in the adapters (17) and (27a) and the
interconnecting pipe assembly (18) as well as the pressure sensing pipe work (16) or (15)
must be kept clear of dirt. Blow through with compressed air if necessary- do not use a drill
on either of the control orifice, one of which contains a split pin, as enlargement of the
orifices might upset the operation of the valve.
Pressure reducing valve (DP143)

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
UPSET CONDITIONS & STABILIZATION
In any running unit, upsets are bound to happen. Sometimes they can be avoided and
sometimes the conditions are unavoidable. The upsets can be of any type, nature. It can be a
situation encountered earlier or a totally new situation. The dealing with upset conditions
needs a blend of knowledge and experience for successful handling. Some unit upsets which
have been observed earlier are discussed here. The probable reasons for upset and the
stabilization methods are also discussed here.
17.1 FEED PUMP LOSING SUCTION:
• This can be confirmed by the feed pump suction pressure gauge. If it is low, immediately
ask TPH to check the offsite booster pump and check line-ups and make corrections
immediately.
• If the upset is not from offsite, then check the feed pump condition and immediately
change the pump if any abnormality is found. Check DP of the running pump suction
strainer for any plugging due to which the pump may be loosing suction. Take clearance
from CPP and PP-II before change over of the pump as this is an HT motor and stand by
pump is turbine driven.
Two different upset conditions are observed based upon the status of PFD in the unit:
When PFD in service:

PFD level gives some cushion and unit can be sustained for some time and during that time
reduce heater feed flow (for sustaining PFD level) and heater firing. If the feed flow does not
increase to maintain PFD level and thereby feed to heater cannot be sustained at even lower
feed rate, unit has to go for shut down.
When PFD not in service:

Keep a check on heater COT as it will shoot up very quickly. If it cannot be controlled
by pressure of FO and FG then remove fires from the heater. If the feed has failed totally and
there is no resumption immediately, unit has to go for emergency shut down
17.2 DESALTER PRESSURE FLUCTUATION:

1. Following control valves to be checked for faults/fluctuations:
i) Desalter PCV
ii) FCV1101
iii) PFD LCV (If it is in AUTO mode, level to be checked for fluctuations)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
iv) Wash water FCV to Desalter

v) Effluent water / Desalter Interface LCV (If it is in AUTO mode, level to be checked for
fluctuations)
vi) Pass flow control valves (When PFD is not in service)
2. Feed pump discharge pressure to be checked for fluctuations
3. Water carryover from desalter and probable loss of suction of booster pump
4. Desalter PCV malfunctioning
In brief:
• This will happen if the feed pump discharge pressure is varying vigorously. Here the feed
pump pressure has to be stabilized and if necessary, the desalter pressure control valve has to
be operated manually for sometime to stabilize it.
• The same will also happen if there in any sudden fluctuation in desalting water inlet flow rate
or the effluent flow rate. Also if there is any problem in the desalter LCV, the pressure will
start swinging badly. In such cases, the fluctuation in water flow should be avoided as much
as possible. The root cause has to be analyzed immediately and the problem to be sorted out.
If there is a problem with level control valve, desalter water injection has to be removed after
permission from Unit Manager/YSF.
• The desalter interface level also has to be kept at a stable value and any changes required
have to be done very slowly. Any sudden change in set point will give a jerk to effluent water
flow and thus result in a fluctuation in desalter pressure.
• If the Desalter mixing valve DP is high and proper separation is not there then carryover of
water from Desalter to next preheat exchangers, Desalter pressure will start to swing
vigorously.
• If the Desalter pressure control valve gets opened more on its own, the feed to the unit will
suddenly increase. Also the Desalter pressure will shoot up very quickly. In this case, the
pressure control valve has to be bypassed immediately and rectified on priority.
• In case the Desalter pressure transmitter is malfunctioning, the Desalter pressure will not be
displayed correctly but the control valve will operate depending upon the value transmitter is
showing. In that case immediately the control valve has to be taken in manual control and
transmitter to be rectified on priority.
• If the PFD level control valve fluctuating badly, this will give back pressure on Desalter and
pressure will start to fluctuate drastically. If this happens then that control valve has to be
immediately taken in manual and rectified on priority.
• When PFD not in service and if the heater pass flows control valve gets wide opened or
closed in one or more passes, it will give sudden jerks to Desalter pressure and the pressure
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
will start to fluctuate drastically. If this happens then that control valve has to be immediately
bypassed and rectified on priority.
• Also check the heater pass flows and the preheat train –II split control valve position. Any
problem in the control valve like getting stuck suddenly at wide open or full close condition
will also result in booster pump pressure and flow fluctuations
• If all the above said conditions are Ok, Desalter RV to be checked for passing. Passing in
Desalter RV may lead to pressure fluctuation. Same can be confirmed by reducing atmos.
Colum Flash zone temperature but if the passing is very low, drop in temperature will be
minimum to identify
17.3 BOOSTER PUMP SUCTION PRESSURE FLUCTUATION:
• This will happen when the desalter pressure is fluctuating. Since the booster takes direct
suction from the desalter, to ensure steady booster suction and hence discharge pressure, it is
very important to keep desalter pressure at a steady value.
• Check the feed booster pump condition and if any abnormality is found, immediately bypass
PFD and change the turbine line up to booster line up and change the pump. Check the
suction strainer of the pump for any plugging due to which the pump may be loosing suction.
Take clearance from CPP and PP-II before changeover of the pump as this is HT motor and
other is turbine.
• Check the PFD level control valve position. Any problem in the control valve like getting
stuck suddenly at wide open or full close condition will also result in booster pump pressure
and flow fluctuations.
• Also check the heater pass flows (when PFD not in service) and the preheat train –II split
control valve position. Any problem in the control valve like getting stuck suddenly at wide
open or full close condition will also result in booster pump pressure and flow fluctuations.
17.4 FUEL OIL PRESSURE FLUCTUATIONS:
• This may happen due to upsets in FO supply pressure from IFO. In that case, the pressure
will fluctuate heavily and accordingly control valves will respond. Take control valve in
manual and keep the pressure at some steady value by operating control valve manually.
Once the control valve becomes unsteady, it becomes very difficult for it to stabilize on its
own in AUTO-CASCADE mode. Also the COT has to be monitored because FO fluctuations
mean that COT is bound to fluctuate. Check the COT and vary FO control valve opening or
gas consumption accordingly as per the situation. FO header pressure fluctuation from IFO
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
can be confirmed as this will cause FO pressure fluctuations in both the heaters and can be
ruled out if the fluctuations are observed in only one heater.
• The other reason can also be a problem in the FO pressure control valve. It may get stuck and
will result in no response from control valve. The graphics will show it to be operating but
actual control valve will not be operating in the field. In this case, first the reason of the
pressure fluctuation has to be confirmed as non-operation of the valve and the same has to be
rectified by maintenance.
• The problem will also arise if the transmitter is malfunctioning. In that case, take control
valve on manual control and transmitter steam tracing needs to be checked for being
effective. If the steam tracing is effective then the transmitter needs to be checked by
maintenance.
• Passing of steam purge line to any of the FO guns will cause FO pressure fluctuations. Check
for each purge to be tightly shut.
• COT fluctuation when FO is in CASCADE mode.
• SDV malfluctuating
17.5 FUEL GAS PRESSURE FLUCTUATIONS:
• This may happen when the fuel gas header pressure is varying very quickly. In that case, the
pressure will fluctuate heavily and accordingly flow fluctuates and leads to heater COT to
fluctuate. Take FG flow control valve in manual and keep the pressure at some steady value
by operating control valve manually. Once the control valve becomes unsteady, it becomes
very difficult for it to stabilize on its own. Also the COT has to be monitored because FG
fluctuations mean that COT is bound to fluctuate. Check the COT and vary FG control valve
opening or gas consumption accordingly as per the situation. (To be observed in both heaters,
same as FO pressure fluctuations)
• The other reason can also be a problem in the FG control valve. It may get stuck and will
result in no response from control valve. The graphics will show it to be operating but actual
control valve will not be operating in the field. In this case, first the reason of the pressure
fluctuation has to be confirmed as non-operation of the valve and the same has to be rectified
by maintenance.
• The problem will also arise if the transmitter is malfunctioning. In that case, take control
valve on manual control and transmitter steam tracing needs to be checked for being
effective. If the steam tracing is effective then the transmitter needs to be checked by
maintenance.
• Liquid carryover in FG, the best way to confirm is to see the FG fire. The flame will be
smoky with fire flies.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
• Abnormal increase in flow and drop in pressure will be observed if a FG tip gets disengaged.
• SDV malfluctuationing.
17.6 11-F-01 PASS FLOWS FLUCTUATIONS:
• This can be a result of booster or PFD turbine discharge pressure fluctuations. If the booster
or PFD turbine flow is fluctuating, then the feed to heater pass flows will vary, resulting in
heavy variations in the control valve opening to counter the effect. The variations will affect
the flow through the pass flows. In this case (PFD not in service), the booster discharge has to
be stabilized first because that is the root cause of the problem. After stabilizing the booster
discharge pressure, if the control valves do not get stabilized, then operate them manually and
stabilize the feed flow. In case of PFD in service, check the healthiness of turbine and proper
steam consumption of turbine. Due to HP steam fluctuation turbine speed will varies vary and
lead to pass flow fluctuations.
• The feed flows can also fluctuate if a pass flow transmitter fails. For example, if Pass A FT
starts showing “0” value then the control valve will open further to normalize the value. But
the actual flow is not zero in the tube. But on the opening of control valve, flow will start to
increase (in case PFD in service, PFD level will decrease and level control valve will open)
and thus the total feed going to the unit will start increasing, thus upsetting the unit. The only
solution here is to watch the outlet temperature and analyze if the flow has really reduced or
is it transmitter problem. In case of transmitter problem, the control valve has to be taken on
manual immediately and output should be given around the value before upset. Then monitor
the pass outlet temperature and accordingly operate the control valve. Transmitter has to be
rectified on priority basis. Also check for the steam tracings of the transmitter lead lines to be
effective.
• If PFD not in service and the pass flows are also fluctuate if there is a restriction of flow from
upstream like too much closing of 11-FRC-101 (PHT II split valve). In this case, the control
valves get wide opened but then also the sufficient feed flow cannot be established. Here, 11-
FRC-101 needs to be opened further to establish sufficient flow in the heater.
17.7 ATMOSPHERIC COLUMN PRESSURE SHOOTING UP:
• The column pressure can shoot up if there is excess vaporization in the column. This can be
seen and concluded from the column conditions. If the case is of excessive vaporization, the
COT needs to be reduced. Sometimes crude layers may get formed and the instead of a blend
of crudes coming to a unit, the case may happen that the lighter component of the blend is
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
coming to the column. Thus this lighter crude will vaporize to a larger extent increasing the
column pressure. CR’s to be increased to maximum possible extent.
• In some cases, it may happen that 11V01 may get full of liquid and start exerting back
pressure on the vapor coming from column to 11V01. In this case, column pressure will shoot
up very quickly. If the level is observed to be very high in gauge glass, it has to be reduced to
approximately 50% immediately. Once the level comes down, column pressure will also get
reduced. During such situations, column top temperature and COT can be temporarily
reduced to reduce the yield of naphtha.
• Again if the boot level of 11V01 is full, water will come to HC section of the drum and this
water will go back to column as reflux stream. This reflux stream will contain water and thus
water will return to column by this path, causing the top pressure to shoot up. Here, the top
temperature and pressure will come down for some time and then start shooting up.
• If the column bottom stripping steam control valve gets opened more and the steam flow
starts going high, the column top pressure will rise. In this case, the problem has to be
identified and then flow to be reduced to normalize column conditions.
• The column top pressure will also shoot up if there is a reduction in the cooling water
pressure or if the cooling water fails totally. The situation has to be handled depending on the
extent of water failure.
• The column pressure may also shoot up and stay at higher value if there is any vapor lock in
the column. This can only be reduced by releasing the vapor lock from the column.
• Pressure also shoots-up if water is entering the column in high volumes. This happens when
water is present in crude and proper separation of water from crude is not done at the desalter
outlet. The carried over water will create upsets in the column.
• If the control valve of fuel gas make up to column gets wide open, then the pressure will start
shooting and will result in high column pressure. In that situation the control valve upstream
or downstream block valve needs to be pinched down and adjusted depending on the value of
column pressure.
• If any of the CR flow fails then that will also result in shooting up of the column pressure.
Immediately the CR flow has to be restored. If that is not possible, other CR to be maximized
and feed rate may be needed to reduce after clearance from Manager/YSF.
• If the top reflux flow control valve gets more or wide opened, the pressure of the column will
shoot up. The control valve in that case needs to be bypassed and rectified on priority.
• If the column bottom level is abnormally more, the column pressure will swing and hold at a
high value. In that case, level to be cross checked by column DP value as well as by checking
the levels in the gauge glass.
• If the column top pressure transmitter fails, the value shown by it will be wrong.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
• If column DP increases and causes flooding. This will lead to flaring from the column due to
sudden release of lighter fractions.
• Water carryover from 12E10/10A
• If overhead condensers salt water valves drop seated during back flushing of condensers,
column pressure will shoot up. Same can be confirmed by checking the individual salt water
valves and same has to be reverted back.
17.8 11-V-01 LEVEL HIGH:

• Sudden increase in level at same operating conditions indicates naphtha yield has
increased. In such cases, the lighter end content of the crude may have increased. So
reduce the top temperature of the column but do not go below dew point. Both the
reflux pumps are to be placed in service in this case to bring down the level.
Reduction of COT may also help in this situation.
• In case where the stabilizer feed control valve is having a problem, 11-V-01 level will
increase. If the control valve got stuck and not opening beyond some value the control
valve has to be by passed and rectified on priority basis.
• The drum level can also go up if there is a problem with top reflux pumps. In that
case, if sufficient flow is not obtained which is required to maintain the top
temperature, the top temperature will shoot up and naphtha yield will rise. Also the
pump will have to take more load for level reduction as reflux flow has come down.
• Level to be cross checked with gauge glass if increase is instantaneous
17.9 COLUMN BOTTOM LEVEL HIGH:

• The main reason of the column level going suddenly high will be failure of RCO
pumps. In that case, try to place the standby immediately. If the standby pump is not
starting immediately then feed rate has to be reduced till the time the pump is
available. If the problem continues for a longer time then follow the procedure
discussed in chapter 19.
• If the column level is slowly building up and the overflash is high, increase the diesel
yield so that the overflash comes down to normal value and the level increasing is
stopped. But while doing this, ensure that the diesel color is ok and not going off-
spec.
• If vacuum heater pass flows control valves encounter a problem, 11-C-01 bottom
level will start increasing. Then it becomes necessary to rectify the control valve or
use bypass to provide sufficient flow.
• If either kerosene, diesel flows come down drastically or fail totally, the liquid content
will get accumulated in the column bottom and raise the level.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
• If there is a sudden dip in 11F-01 COT due to FO or FG pressure fluctuation or some

other reasons, bottom level will go up.
17.10 COLUMN BOTTOM LEVEL LOW:
• The column bottom level can come down if there is excess vaporization in the column. This
can be seen and concluded from the column conditions. If the case is of excessive
vaporization, the COT needs to be reduced. Sometimes crude layers may get formed and the
instead of a blend of crudes coming to a unit, the case may happen that the lighter component
of the blend is coming to the column. This lighter crude mixture will have lower diesel yield.
Accordingly diesel flow has to be reduced and over flash to be normalized (which will reduce
in this case). The liquid has to be allowed to go down in the column to maintain the level.
• Also if the column pressure comes down suddenly, vaporization will be enhanced and the
contents rising up will be more. This will reduce diesel yield and thus the column level will
also come down if the diesel flow rate is not reduced.
17.11 RCO PUMPS PROBLEMS:
• Any seal leaks in RCO pumps will lead to a sudden fluctuation of flow and result in vacuum
heater tripping most of the times. Also due to RCO being at a very high temperature, the
chances of fire are high by auto ignition. So RCO pump seal leaks create very severe
situations in the unit. Immediately RCO pump has to be changed in case of any abnormality.
• Column level will start building up.
• Vacuum heater temperature will also start to shoot up if its feed reduces suddenly.
Immediately fires need to be removed because high temperature will lead to coking and even
chances of tube rupture may develop.
• Vacuum feed failure procedures have to be followed in case RCO pumps are not available for
a longer period.
17.12 DIESEL-CR PUMPS LOOSING SUCTION:
• The Diesel section level can come down if there is excess vaporization in the column. This
can be seen and concluded from the column conditions. If the case is of excessive
vaporization, the COT needs to be reduced. Sometimes crude layers may get formed and the
instead of a blend of crudes coming to a unit, the case may happen that the lighter component
of the blend is coming to the column. This lighter crude mixture will have lower diesel yield.
So, if the rundown of diesel is not reduced, the liquid level in the diesel section trays will
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
come down and Diesel CR pump will start loosing suction. Diesel CR pump discharge can be
pinched down to save pump from any damage. Accordingly diesel flow has to be reduced and
over flash to be normalized (which will reduce in this case). The liquid has to be allowed to
go down in the column to maintain the level.
17.13 COLUMN DP HIGH:
• Column DP high means either this will be due to excess vaporization in the column, or it is
because column flooding. Actually both these causes cannot be segregated but the primary
cause of high DP has to be known. In case of more vaporization, each section DP will
generally be high. For each plate, maximum DP has to be approximately 0.01 kg/cm2. If the
vaporization is more, the DP in each section will be more than its design DP (no. of trays in
section* 0.01 kg/cm2).
• But if there is flooding in a particular section, DP there will be very high but other sections
will not be high. Flooding in one section may lead to flooding in the ones below it, for
example, heavy flooding in KERO will result in fluctuations of Diesel yield and also increase
in diesel yield. In this case, Kero product flow and Diesel product flow have to be increased.
The reasons for column DP have to be carefully analyzed.
• If the column bottom level is abnormally high, the column DP will go up. In that case, the
level has to be reduced by pumping out the content. The level should be brought down to
approximately 50%.
• If either of the pressure transmitters of the column is not working properly, it will give wrong
indication and hence mislead the person operating the DCS.
• If the feed rate is more than what is prescribed by TSD, the column may not be able to take
that much load. It will result in increased DP of the column.
Whatever may be the cause of increase of DP, either increasing rundown or reducing COT
will reduce column DP. But the counter effects of each have to be considered before taking
any action. If problems like increased draw-off temperature or increased bottom level are
encountered, counter action has to be taken.
17.14 COLUMN TOP TEMPERATURE FLUCTUATIONS:
• The column top temperature will go up if sufficient reflux flow is not present. The reflux is
for controlling the temperature and if the temperature is not under control, it means either the
reflux is not present or effective reflux is not present (reflux at proper temperature). Here the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
pumps need to be checked for proper pumping and need to be changed if the pumping is not
sufficient or any fluctuations are there.
• The drum temperature also needs to be limited below the operating temperature of condenser
outlet. High drum temperature means the reflux temperature is high and thus the heat transfer
is less than the desired value. To reduce drum temperature over head condensers to be back
flushed.
• Top reflux and all CR control valves also need to be checked in case of sudden rise or fall of
column top temperature. In case of any control valve getting closed, the same has to be
bypassed and attended by maintenance.
17.15 PRODUCT DRAW-OFF TEMPERATURES HIGH:
• If the product draw-off temperatures are high the rundown rates need to be reduced. Drawing
more of a product increases the draw-off temperature. Draw-off has to be reduced for the
product to cut down its temperature. If the draw-off rate starts increasing the column DP, it
better to reduce COT because this is an indication of excess vaporization and carry over to
higher trays.
• Also the higher draw-off temperature may be due to insufficient flow of CR. Or the case may
be that CR return temperatures are high and thus they are not providing desired cooling
effects. Here the CR pump need to be checked as well as exchangers for checking that
bypasses are not open.
17.16 STABILIZER RE-BOILING FLUCTUATION:
• This can happen if the KERO-CR flow is fluctuating. KERO-CR is the heating medium in the
re-boiler and any fluctuation in KERO-CR flow will work as change in flow of heating
medium. The control valve will take care of that fluctuation but if it is too much then re-
boiling temperature will start to vary. In this case stabilize the CR flow and then the
temperature of re-boiling.
• If the response of KERO-CR control valve becomes erroneous or it gets stuck at a value, the
re-boiling will fluctuate. In this case, the flow has to be controlled by bypass valve and the
control valve has to be rectified on priority.
• If the level control valve of stabilizer opens suddenly and the level starts to fall down, the re-
boiling will shoot up very quickly. If the converse happens, the re-boiling will reduce very
fast.
• This can also happen if the feed to stabilizer valve gets wide opened or closed and thus
reducing or increasing the re-boiling respectively.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
• If the temperature indicator thermocouple is faulty then it will show a wrong value,
misleading the DCS operator.
17.17 STABILIZER TOP PRESSURE FLUCTUATIONS:
• This can happen if there is any problem with 11-PRC-501 A/B. If the FG control valve gets
wide opened or full closed, the pressure will start to collapse or build-up respectively. The
split control valves has to be immediately bypassed and system to be normalized.
Rectification of the control valve has to be done on priority.
• If the stabilizer top reflux flow varies suddenly due to a problem either in pump or the control
valve, the temperature of the stabilizer top section will vary and also the pressure. The root
cause of the flow variation has to be accessed and then rectified. If the problem is with pump,
change the pump to the standby. If the problem is with control valve, bypass it and establish
the flow through bypass.
• If the LPG drum level is low, the LPG pump will not get suction and that will let the
temperature and pressure of the system to shoot up. In this case, build-up the level by
reducing rundown. If required the rundown can be closed by informing MEROX.
• The pressure also shoots-up in case of salt water failure or salt water pressure reduction. In
this situation, inform to Manager/YSF and follow the instructions.
• The pressure also shots up if by some reason, 11-V-03 level becomes full. The gas flow will
experience back pressure and result in increasing the stabilizer pressure. Immediately the
level has to be brought down by increasing the rundown flow.
• If the top pressure transmitter is malfunctioning, it gives wrong indication misleading the
DCS supervisor.
• Drum boot level filled up, water carryover in reflux.
17.18 12-F-01 PASS FLOWS FLUCTUATIONS:
• This can be a result of RCO pump discharge flow fluctuations. If the RCO discharge is
fluctuating, then the feed to heater pass flows will vary, resulting in heavy variations in the
control valve opening to counter the effect. The variations will affect the flow through the
pass flows. In this case, the RCO discharge has to be stabilized first because that is the root
cause of the problem. After stabilizing the RCO discharge flow, if the control valves do not
get stabilized, then operate them manually and stabilize the feed flow.
• The feed flows can also fluctuate if a pass flow transmitter fails. For example, if Pass A FT
starts showing “0” value then the control valve will open further to normalize the value. But
the actual flow is not zero in the tube. But on the opening of control valve, flow will start to
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
increase and thus the total feed going to the vacuum heater will start increasing, thus
upsetting the heater conditions. The only solution here is to see the outlet temperature and
analyze if the flow has really reduced or is it transmitter problem. In case of transmitter
problem, the control valve has to be taken on manual immediately and control valve should
be given around the value before upset. Then monitor the pass outlet temperature and
accordingly operate the control valve. Transmitter has to be rectified on priority basis. Also
check for the steam tracings of the transmitter lead lines to be effective.
17.19 VACUUM SECTION DRAW-OFF TEMPERATURES SHOOTING –UP:
• If the draw-off temperature of any particular product shoots-up, check for the circulating
reflux of the product. The pump may not be giving sufficient pumping to maintain the draw-
off temperature in the limits. Check pumps and in any problem is with the pump then change
the pump.
• The CR flow may get interrupted incase the control valve gets affected like gets stuck or
closed. In this case, control valve has to be bypassed and rectified on priority basis.
• If all the product draw-off temperatures are high, it shows that the vaporization is more than
desired and heavier ends are getting carried to top. In this case it is better to reduce COT.
17.20 SUDDEN VACUUM DROP:
• The vacuum drop may be due to reduction of MP steam pressure or condensate carryover in
the steam. The ejector steam is responsible for holding the vacuum and if the steam fails then
the chances of maintaining vacuum are feeble. The steam supply has to be normalized
immediately or the feed rate has to be reduced after clearance from MP/ YSF. In case of
condensate carryover, proper draining has to be done to make steam free of condensate.
• If the salt water fails or the pressure drops, the holding of vacuum becomes very difficult.
Here also the water supply has to resume otherwise feed rate has to be reduced after clearance
from Manager/YSF.
• The vacuum may also get disturbed if the vacuum column bottom level is holding very high.
In this case, the column level has to be brought down by pumping it out.
• If these corrections also are not able to give any improvements, we have to suspect leaks in
the vacuum system and check for it. There are chances of blockage in dip legs also, which
can affect the system vacuum.
• If the COT is high, it increases cracking in the system and result in the loss of vacuum. In
such cases vacuum heater COT needs to be reduced quickly.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 17
PLANT NAME: CDU II
Chapter Rev No: 0
• If the hotwell water level is holding low, the vacuum will start breaking. In that case the
water level has to be restored to normal value and thus it will bring column to normal
conditions.
• In case the hotwell gas to 11-F-01 SDV gets closed and the hotwell vent does not open, the
vacuum will start getting upset. In that case, the SDV has to be reset immediately or the
hotwell vent to be opened temporarily.
• If the hotwell water level transmitter fails and the thermo-siphon leg gets clogged, the
vacuum will not hold and the column will get upset. Here gauge glass to be checked for level
confirmation and hotwell bottom drain to be opened and level to be brought down to 60%.
• If any of the CR flow fails, vacuum will get upset. Immediately the flow has to be restored
and if that is not possible, maximize other CRs and reduce feed if required after clearance
form Manager/YSF.
• If the top pressure transmitter fails then the faulty indication will misguide the DCS operator.
• Pumps vents opening
17.21 VACUUM BOTTOM LEVEL HOLDING HIGH:
• If the SR pump is not taking proper suction due to strainer plugging or pump problems, level
will start building up. In that case, the pump has to be changed and the problem has to be
found out.
• If the rundown line up is wrong.
• If the bottom level transmitter fails, it misleads the DCS operator.
• If there is a sudden raise in RCO flow, the level in vacuum column will go up due to rise in
column feed.
• Sudden increase in RCO flow or reduction in firing reduces the vacuum heater COT and thus
the level at bottom starts building up and yields are lost. Cot has to be normalized
immediately.
Drop in Vacuum will cause bottom, level to fill up.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 18
PLANT NAME: CDU II
Chapter Rev No: 0
AVOIDING DEVIATIONS AND PLANT UPSETS
In a process unit, there are some upsets that cannot be avoided. But some incidents and upsets
can be avoided by timely action and precautions. Proper checking in the field, following
DRJs, and ensuring that all the systems and procedures are followed is the only way to avoid
upsets. Some problems and upsets are discussed in the previous chapter and here we are
discussing the possible methods of avoiding those upsets.
18.1 FEED PUMP SUCTION LOSS:
• In the case where feed pump is losing suction because of insufficient flow from offsite, there
is nothing much that can be done to prevent it because the root cause of the upset is not from
the unit. But the suction loss due to suction strainer plugging can be avoided by timely
cleaning of suction strainer. The suction strainer cleaning of feed pump is a part of DRJ and it
should be followed every time it falls under the schedule. If it is cleaned as per the schedule,
then this situation can be avoided a number of times.
18.2 DESALTER PRESSURE FLUCTUATIONS:
• If the fluctuations are due to the feed pump discharge fluctuations, the same can be avoided
by proper monitoring of feed pump. In most cases, close monitoring of such critical
equipments will give us some indications before the problem becomes more critical. If any
problem is found with the pump before unit gets upset, same has to be referred to rotary and
advice to be taken for necessary actions.
• Water injection should not be given any sudden changes. If there is a need to increase or
reduce the water injection rate to desalter, same should be done very slowly so that the
interface level does not fluctuate.
• If the desalter effluent level control valve gets stuck or fails, there is nothing much that can be
done to avoid such situations. The failure of control valve does not give any indication before
the actual failure. So, the actions have to be taken after failure of valves and they need to be
taken very quickly.
18.3 BOOSTER PUMP SUCTION PRESSURE FLUCTUATION:
• If the booster pressure is fluctuating due to desalter pressure fluctuations, the precautions and
checks required for avoiding desalter pressure fluctuations have to be taken.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 18
PLANT NAME: CDU II
Chapter Rev No: 0
• The suction loss due to suction strainer plugging can be avoided by cleaning of suction
strainer. As the stand by pump being used for PFD the suction strainer cleaning of feed
booster pump should be carried out when the PFD was not in service. If it is cleaned then this
situation can be avoided.
18.4 FUEL OIL PRESSURE FLUCTUATIONS:
• Individual fuel oil lines to be flushed whenever any shutdown is there. And proper circulation
to be established for FO system.
• Lead lines of the pressure transmitter need to have proper steam tracing. In case the steam
tracing is not effective, the transmitter will show faulty reading and thus it will result in unit
upset. So, during rounds the effectiveness of tracing need to be checked.
• Any operation of supply or return block valves have to be done very slowly as their response
is very quick. It has to be done by a person with experience or under the supervision of a
person with experience.
18.5 FUEL GAS PRESSURE FLUCTUATIONS:
• Lead lines of the pressure transmitter need to have proper steam tracing. In case the steam
tracing is not effective, the transmitter will show faulty reading and thus it will result in unit
upset. So, during rounds the effectiveness of tracing need to be checked.
• While placing fire in heater utmost care to be taken and Fuel gas to be opened slowly and it is
ensured that pilots are on.
18.6 11F01 PASS FLOWS FLUCTUATIONS:
• For keeping the pass flows at a stable value, PFD turbine discharge or the booster discharge
pressure and flow has to be kept at a steady value. So, the measures discussed for keeping the
turbine or booster normal are required to keep the pass flows also steady. The healthiness of
the pump ensures that pass flows do not get upset due to its feed variation.
• The DCS operator has to ensure that there should not be any high variation in the heater
flows during feed switch. Care to be taken and step by step feed to heater to be increased or
decreased.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 18
PLANT NAME: CDU II
Chapter Rev No: 0
18.7 ATMOSPHERIC COLUMN PRESSURE SHOOTING UP:
• The column overhead drum 11V01 level should be closely monitored in case of any unit
upset and only LT value should not be trusted. Gauge glass level should be checked after
draining the gauge glass. Same should be done with the boot level also and ensure that both
the levels are within normal operating limits (not very low and not very high).
• During rounds in the field, all the condensers 11-E-17A/B, C/D, E/F, G/H should be checked
for any leaks, abnormality, valves drop seating should be observed in field so that the
problems are identified and resolved before becoming cause for major upset.
• The split control valves (gas make-up to column and gas to flare) should be checked regularly
so that any problem in them is identified quickly. Any problem in it will result in column
pressure variations.
• Water carryover can be minimized during feed tank switch by taking out water injection prior
to tank switch and settling of interface to be ensured.
18.8 12F01 PASS FLOWS FLUCTUATIONS:
• For keeping the pass flows at a stable value, the RCO pump discharge pressure and flow has
to be kept at a steady value. The healthiness of the pump ensures that pass flows do not get
upset due to its feed variation.
• The DCS operator has to ensure that there should not be drastic increase or decrease in Atmos
bottom level and heater pass flows.
18.9 SUDDEN DROP IN VACUUM:
• Steam has to be ensured to ejectors and the steam has to be condensate free. Proper draining
of condensate should be ensured for the MP steam line.
• Close monitoring of pumps will ensure that there is no vacuum drop due to failure of pumps.
Running pump healthiness and standby pump readiness has to be ensured.
• Both flame arrestors strainers have to be cleaned periodically and ensure one flame arrester
kept in service and timely drained so that there is no backpressure on vacuum column. The
water level has to be sufficient so that the dip legs are immersed in the water. Hot-well off
gas fires need to be checked to ensure that gas incineration continues uninterrupted.
• Vacuum column level should not be allowed to go very high. Parameters like flash zone
temperature of vacuum column have to be monitored as indicators of vacuum bottom level.
• Checks for leaks have to be done thoroughly if other parameters correction is not able to
improve the vacuum condition.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 18
PLANT NAME: CDU II
Chapter Rev No: 0
NOTE: The problems caused by failures of instruments like control valves, transmitters, etc
do not give any indication of their happening. So, there is no way we can avoid the upsets
caused by their failure. But the time taken to suspect or conclude the failure of an instrument
plays a very important role in the extent of upset it can cause. A robust approach in
identification of problem will result in quick and comfortable trouble shooting.
Regular field round need to be effective. Lots of emergencies can be avoided by close
observation in the field. Two most important things that need to be checked in the field are
the healthiness of running equipment and readiness of standby equipment. The DCS
supervisors can avoid many emergencies by timely assessment of unit condition changes and
by checking trends of varying parameters. If any upset is timely handled, it solves majority of
the problem compared to what happens if the action is not timely
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
RE-STARTUP AFTER EMERGENCY SHUTDOWNS
EMERGENCY PROCEDURES
When the safe routine operation is interrupted, emergency procedures are sometimes required
to overcome the potential hazards. If continuation of unit operations on limited basis is
impractical the unit must be shut down as safely as possible.
19.1 GENERAL
The emergency procedures attempt to overcome the hazard of a quick shut down.
Emergency can result from equipment failure and from interruption of utilities. Certain
features have been designed into the plant to minimize the likelihood of emergencies. These
include spare pumps, exchangers etc. Operators should be thoroughly familiar with
emergency procedures and understand the reasons for each work. Good judgment must be
exercised as no written procedure can completely cover all details or problems that can arise
in an emergency. Judgment is more likely to be exact if prior thought and planning have been
made. As during emergency there is no time, emergency procedure must be learnt before
hand.
The steps to be taken during various emergencies are given below.
It depends on common sense and prevailing condition of emergency. But normal
encountering emergency, we have to follow the sequence of operation for the safe unit
shutdown.
1. Inform YSF, MEROX, Power Plat, FCCU, DHDS and TPH.
2. Trip heater 11-F-01 and 12-F-01. Purge and isolate fuel oil and fuel gas with steam.
3. Take out feed by stopping feed pumps and PFD turbine and isolate West battery limit
feed Valve.
4. Monitor 11-C-01 pressure, accordingly open PCV Bypass valve (if pressure goes up)
and if pressure goes down open Fuel Gas make-up, close pressure control bypass.
5. Isolate stripping steam control valve and block valve and MP to LP steam.
6. Close BFW block valve to steam gens.
7. If power available use Top Reflux Pump for contain top temp and pump out level to
slop.
8. If power available pump out levels and close run-down valves. Close pump discharge
valves.
9. Close 12-C-01 ejectors steam and ensure slight positive pressure in Vac column (0.5
kg/cm2g) by operating Fuel Gas make-up and close Hot Well vent.
10. Close Hot Well Water and Atmos Water and Effluent water to SWSU and open the
Hot Well Water and Atmos water side block valves to OWS.
11. Check all the equipments for any leak.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
19.2 POWER FAILURE

The unit will be brought down as indicated below during power failure.
ATMOSPHERIC SECTION:
i.
Shut off individual burners and flush out oil form burners with steam.
ii.
Shut off stripping steam to the main column and side strippers.
iii.Close all pump discharge valves.
iv.Hold pressure in the crude column and Stabilizer by operating PRC-1409 and PRC-1501.
If required, open PRC1409 by pass valve to control the atmospheric column pressure.
v. Hold levels in columns, vessels by manually closing the respective control valves
/isolation valves. When power is restored, establish circulation by running crude pump,
booster pump and RCO pump as per normal practice.
VACUUM SECTION:
i. Shut off ejector steam.

ii. Close non-condensable return line to inlet of first stage ejectors.
iii. Open fuel gas to inlet of first stage ejectors to bring up the system pressure to 0.5
kg/cm2 g, if power is not resumed immediately or start-up of unit is delayed.
iv. Close all individual burner valves and flush out fuel oil burner guns one by one.
v. Close all pumps’ discharge valves.
As soon as power is available and unit start-up is delayed, flush the system with flushing
oil. Take fresh gas oil (cutter) and start the unit as per normal start-up procedure as
described earlier.
19.3 LOSS OF STEAM
Effects on Atmospheric Section

This will affect the following:
Stripping steam to crude column and strippers
Atomizing steam
Tracing Steam
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
In the event of loss of steam, the unit will be brought down as follows:
i. Cut off fire to the heater. FD/ID fans may be kept running
ii. Shut off all burners and flush out all oil burners, if possible.
iii. Keep fuel oil circulation on
iv. Resort to circulation in the bottom section using VR Circuit and crude tank. Vacuum
unit will be on short circulation through its furnace.
v. Start close circulation by diverting 11-P-10 A/B discharge to 11-F-01 inlet through VR
circuit and crude tank.
vi. Stop all the other pumps.
vii. Hold levels and pressures by taking all controls on manual.
viii. Switch over to normal start-up circulation, once emptying out of the Atmospheric
column is over.
If the duration of steam failure is long it is advisable to flush the lines and equipments
with flushing oil. The procedure outlined under normal shut down procedures in section -5
for flushing and emptying out shall be followed.
Effects on Vacuum Section

Atomizing steam to burners
Ejectors
Tracing Steam
The following steps have to be taken for safe shut down of the unit.
i) Close ejector steam valves.
ii) Close non-condensable return to inlet of first stage ejectors.
iii) Back in fuel gas and maintain pressure at about 0.5 kg/cm2 g.
iv) Shut down heater and isolate all burners. Purge out oil burners if steam permits. FD and
ID fans may be kept running.
v) Start circulation from 12-P-01 A/B to 12-F-01 inlet. Keep the coil flow at minimum level.
vi) Start emptying out heavy stocks to slop by diverting a part of 12-P-01 discharge through
VR circuit.
vii) Pump out products to slop.
viii) Cut in flushing oil to the bottom of vacuum column.
ix) Unit can be started back as per normal procedure on resumption of steam supply.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
19.4 LOSS OF COOLING WATER
ATMOSPHERIC SECTION
If cooling water failure is total, the unit will be brought down immediately.
All fires to the heater including pilot will be cut off.
Burner guns will be steam purged.
Other pumps can be run to empty out and cool the system as far as possible (if run
down temperature permits).
Stop stripping steam to crude column and strippers.
Crude column refluxing should continue at a flow rate to cool down the column.
Column pressure is to be watched. If necessary, open PR1409 control valve bypass
valve to control the pressure.
Crude column Circulating refluxing should continue to cool down the column. Stop
Top reflux pump.
Stop crude pump, crude booster, PFD booster if cooling water could not be
resumed.
Other pumps can be run to empty out and cool the system as far as possible (if run
down temperature permits
If cooling water supply is not restored soon and if flushing oil from off-sites is
available at sufficient pressure, RCO can be flushed out through VR circuit.
If cooling water failure is partial, it can be tackled by reducing throughput and

throttling water to cooler and condensers proportionately. In such cases careful watch should
be kept on column pressure and also on the pump where cooling water is used as coolant.
VACUUM SECTION
Loss of cooling water will result in failure of ejector condensers and other product
coolers. The following actions are to be taken in such emergency
Watch system pressure for any abrupt changes.
Cut off steam to ejectors. Normally with barometric seal provided, Atmospheric
air is not expected to enter the system. However, this is an added precaution.
Shut down the heater and close all burner valves. Flush oil burners and purge the
heater.
Cut off feed and resort to circulation.
Pump out heavy oils and take in flushing oil. Continue circulation.
Unit can be started as per normal procedure on resumption of cooling water.
Observe Tempered water system temperature .Open make up water if Temp is
crossing 90 Deg. Over flow tem water drum if required to avoid hammering.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
If SR R/d temp is limiting, Open Quench C/V to maintain minimum flow to SR

pump.
Pump out heavy oils and take in flushing oil.
Cut off feed and resort to circulation.
In case of partial failure of cooling water, Unit can be kept on running with reduced
throughput in conjunction with Atmospheric section by throttling cooling water to the
condensers. Close watch to be kept on the pumps, which are running with cooling water as
coolant.
19.5 LOSS OF INSTRUMENT AIR
Failure of instrument air will cause the control valves to go to fail-safe position. Pressure,
temperature, Flow and level indications of various equipment and headers will be available in
the control room. Emergency shutdown to be operated. Fuel Gas Make-up to Atmos column
control valve block valve should be shut and flare release control valve bypass valve should
be operated to control the pressure.
19.6 LOSS OF FEED
ATMOSPHERIC SECTION
When PFD online: Feed failure will be indicated audio-visually by low total flow alarm
provided at the feed pump discharge. Immediate attention may be paid for locating such
failure and restore the flow. PFD level may act as cushion to sustain minimum flow to heaters
for some time during feed failure due to offsite crude booster pump failure.
If pass flows low flow alarms activates (when PFD online) this may occur due to improper
functioning of 11-PT-02B, immediately turbine to be checked and PFD to be bypassed by
operating PFD ROV and stopping PFD turbine.
When PFD not in service: Feed failure will be indicated audio-visually by low flow alarms
provided in the crude heater pass flow controllers 11-FRC-1301 to 1304. Immediate attention
may be paid for locating such failure and restore the flow.
In case feed flow could not be restored immediately, further reduction of flow will cause
activation of low flow switches which will off fuel oil and fuel gas to the heater. Failure of
crude supply to unit may occur due to improper functioning of off-sites Crude Pump Unit,
Crude Charge Pump 11-PM-01 A/B and Booster Pump 11-PM-02A. If Crude Charge pump’s
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
discharge pressure tends to come down cut down unit throughput to restore normal pressure.
Look for the cause of the trouble. The operational factors responsible for pump
malfunctioning are low level in the tank, improper lining up, choking of strainers and
maintenance of improper temperature and pressure conditions in the Desalter. Any
operational mistake which is readily detected will be corrected at once. Standby pumps will
be pressed into service for any trouble with the running pump. If feed supply cannot be
restored immediately the unit will be brought to hot circulation by diverting 11-P-10 A/B
discharge to furnace inlet through VR line. Temperature will be maintained around 200 °C.
Products will be stopped. Water to coolers will be throttled. If the interruption is for a longer
period the unit will be shut down as per normal procedure.
VACUUM SECTION:
Feed failure to vacuum section can be due to interruption in the Atmospheric section.
Failure will be indicated by pass flow low alarm. Further reduction in flow will activate and
trip fuel oil and fuel gas to the furnace. If the failure is due to Atmospheric column bottom
pump, start the spare pump. If the flow cannot be restored immediately, the following steps
are to be taken.
i) Cut firing rate in the furnace in case FSL is not activated already.
ii) Put the unit of circulation by diverting 12-P-01 A/B discharge to furnace inlet through
start-up line.
iii) Bring down the unit as per normal procedure.
19.7 HEATER TUBE FAILURE
ATMOSPHERIC HEATER 11-F-01:
Vacuum section will be put under circulation and will be shut down as per normal procedure.
Atmospheric section will be brought down either by emergency procedure or by normal
procedure depending upon the extent of damage. A small crack in the tube may eventually
coke up and may not warrant and emergency shut down.
The following steps are to be taken in order to bring down the unit immediately in the event
of any major failure:
1. Feed to the heater will be stopped.
2. Fires to be minimized in the heater. Once HC in the furnace is burnt, take out all fires
including pilots.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
3. Snuffing steam will be opened in radiation and convection sections. Emergency coil
steam will be opened in all the passes of the heater.
4. Product / pump around pumps will be stopped when they loose suction.
5. Top refluxing will be continued as long as possible.
6. Column pressure will be closely watched for any rise of pressure due to additional
amount of steam put into the heater coil.
7. Stripping steam to crude column and stripper will be stopped.
8. RCO circuit will be flushed by taking flushing oil from offsite.
VACUUM HEATER 12-F-01:
Atmospheric section will be continued, diverting RCO through VR circuit and will be
shut down with normal shut-down procedure depending upon RCO handling facilities. If the
leak is small it does not warrant and emergency shut-down otherwise it has to be an
emergency shutdown. The plant supervisor has to assess the extent of damage and take
recourse to a normal shut-down or an emergency shut-down.
The following steps are indicated to bring down the unit on emergency in the event of a
failure of heater tube:
i. Fires to be minimized in the heater. Once HC in the furnace is burnt, take out all fires
including pilots Snuffing steam will be opened to heater box.
ii. Feed to the furnace will be cut off (RCO will be diverted through VR circuit).
iii. Emergency steam to coil will be opened and content of heater coils will be displaced to
column
iv. Cut off ejector steam and close cooling water to ejector condensers and drain water
from them. Vacuum should be broken with steam to avoid air entry through ruptured
tube.
v. Float the unit on fuel gas and allow gas to escape to furnace by sufficiently increasing
steam to heater coils.
vi. Empty out the tower by pumping from all trays and column bottom till pumps loose
suction.
vii. Take flushing oil into the column and dilute its content, pump out the oil from the
column.
viii. Drain out remaining oil from the column to CBD.
ix. Steam out the unit as per normal procedure and hand over to maintenance for installing
blinds as per master blind list.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
19.8 DCS FAILURE
We can view pages related to our unit on any of the YOKOGAWA control panels
installed in the MOI and also closely monitor APC system. If further control of the unit is
required from other unit control panel, then engineering keys for any control operation is
required. In case all the Yokogawa Control panels have failed, then no option is left but to go
for a unit shutdown. So at that time the trip bypass has to be kept in auto mode and press all
the five ESD switches. And then ask the field crew to switch off all the pumps.
Upon power failure to DCS, there will be no control from control room and all the
controllers and SDV's will go to their respective fail safe positions Depending on the
duration of failure, either operation can be resumed or unit shutdown resorted to.
19.9 FEED BOOSTER PUMP

Consequence:
1. Desalter pressure shoots up and Desalter RV may operate if the pressure of 12.5
kg/cm2g is breached.
Actions:
1. Take the Desalter pressure controller to manual and shut down the valve completely.
2. Stop the feed charge pump.
3. Take steam clearance from power plant and start Feed turbine pump.
If both the pumps are not running then, prepare for an emergency shutdown
In Atmos section
1. Trip the heater, keep the fuel oil in circulation
2. Purge out the oil from burners.
3. Stop stripping steam to the column and strippers.
4. Stop all other pumps one by one except the RCO pump and keep the Atmos
section in short circulation mode via SR circuit.
5. Maintain the pressure in the Atmos column by bypassing PR1409 to flare.
6. Close the discharge valve of all pumps and stop them.
In Vac section:
1. Put off steam supply to steam ejectors.
2. Isolate all the ejectors. Close non-condensable return line to the first stage
ejectors.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
3. Open fuel gas make-up line to the Vac column, and there-by maintain positive
pressure of 0.5 kg/cm2g.
4. Trip the heater and cut-off the fuel gas and fuel supply to it. Keep the fuel oil
circuit in circulation mode.
5. Isolate all individual burners and flush out the oil using steam.
6. For the entire furnace, use purging and snuffing steam.
7. Keep the Vac section in short circulation mode.
19.10 PFD TURBINE TRIPS:
If PFD turbine trips, then Atmos heater will also trip because of low pass flow
interlock. Try starting the turbine pump but if it is not starting then by-pass the PFD and
start the unit.
19.11 RCO PUMP

Consequences:
1. Atmos column bottom level will increase.
2. Feed to the Vac column will stop.
3. Vac section downstream units will suffer.
Actions:
Reduce over flash rates and the amount of over flash. Instruct the field crew to immediately
rush and start the stand-by pump or restart the pump after checking the condition. In the
meanwhile, reduce the feed rate to the Atmos heater and increase the heater COT. IF the
standby pump not available and the same pump is not starting then, trip the Vac heater. Put
the fuel oil to Vac heater in circulation mode. Close all block valve of fuel oil and fuel gas
.Put Vac section in short circulation mode and stop all pumps of the Vac side except the SR
pump.
19.12 ATMOS COLUMN TOP REFLUX PUMP
Consequences:
1. Atmos column top pressure shoots up.
2. Since reflux is immediately affected, the top temperature also starts rising.
3. Atmos column overhead drum level would start rising alarmingly.
4. Stabilizer would loose feed.
5. Atmos section product quality would degrade.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
Actions:
1. Bypass PR1409 to release excess pressure to flare.
2. Take clearance from power plant and start the turbine pump.
3. If the problem sustains for a bit longer time then bring down heater COT and if
required cut down feed rate.
4. Increase all CRs to maximum.
5. Reduce stripping steam flow rate to the main column bottom.
19.13 KERO CR PUMP
Consequences:
1. Temperature in the column will increase.
2. Product will go off spec.
Actions:
1. Start turbine pump (11-PT-08 B) by taking clearance from Power Plant.
2. Cut down the feed rate.
3. As temperature in the Atmos column is going to increase the Diesel, TPA CR to
maximum and also increase the reflux flow rate.
4. Decrease the heater COT.
5. Heavy Naphtha flow will increase, so start drawing off more Heavy Naphtha.
19.14 DIESEL CR
Consequences:
1. Stripper level will go.
2. Diesel draw-off temperature will increase.
3. Over-flash will decrease.
Actions:
1. Decrease COT
2. Reduce the feed rate.
3. Try to place standby pump.
19.15 DIESEL PUMP

Consequences:
1. Over flash will increase.
2. Diesel slips to RCO and will go to Vac column.
3. Vac column top temperature will increase and chances of loosing vacuum are there.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
Actions:
1. Cut the heater feed rate.
2. Increase the COT.
3. Increase KERO yield so as to allow maximum vaporization.
4. Try to place standby pump.
19.16 SR PUMP
Consequences:
1. Vac column level will start building up.
2. Vacuum will start going down.
3. Bottom temperature will start increasing as there will be no quench flow.
4. There will be no BBU feed if SR is routed to BBU from our unit.
Actions:
1. SR pump failure may have caused due to cavitation, so try opening the vent valve.
2. Start extra HVGO pump to pump out SR from the column.
3. If BBU is taking feed from our unit then, reduce air and put BBU in short circulation
mode.
4. Reduce feed rate.
19.17 HVGO PUMP

Consequences:
1. HVGO level in the Vac column will become high.
2. Wash zone pickings in the Vac column can get chocked.
3. Gradually Vacuum column bottom level will start increasing.
4. Degradation in SR quality.
5. LVGO level will drop and the LVGO pump may loose suction.
6. HVGO feed supply to FCCU will be interrupted
7. Drop in column vacuum.
8. MP steam generation in 12-E-10/10A steam gens. will be affected.
Actions:
1. Trip the heater and drop fires in the burners individually, and flush oil with steam.
2. Take HVGO to FCCU feed control valve in manual and then close it.
3. Empty LVGO from the column.
4. Cut off MP steam supply to the ejectors and isolate them.
5. Put the Vac section in short circulation in short circulation mode.
6. Empty slop level in Vac column and then stop the slop pump.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
7. Stop all the Vac section product pumps except SR pump.

8. Maintain a minimum feed rate in the Atmos section and adjust the operating
conditions accordingly.
9. If the BBU section is not receiving feed from CDU-2 then Bitumen section will not be
affected at all, but if BBU is receiving feed from our unit then CDU-1 or CDU-3 may
be asked to compensate for the loss in feed.
10. Maintain a minimum flow rate for the unit and adjust the operating conditions
accordingly.
19.18 LVGO PUMP

Consequences:
1. Vac column top temperature will shoot up.
2. Vacuum will loose in the column.
3. Hot feed to FCCU will stop.
4. LVGO will drop down to HVGO.
Actions:
1. Take out feed to FCCU.
2. Decrease COT.
3. Decrease feed to the heater.
19.19 TEMPERED WATER PUMP

Consequences:
1. Cooling for SR and Bitumen product will get affected.
2. Bitumen and SR lines run-down temperatures would be high.
3. SR pumps would have to be stopped because tempered water is used as bearing
coolant for 12-P-01/02.
Actions:
In case of tempered water failure the unit can be brought down as per the following plan:
1. Trip the heaters immediately, and keep the fuel oil system under circulation. Put off
all fires and flush out the oil.
2. Stop SR pump immediately.
3. Empty the Vac column HVGO, LVGO and Slop-Cut levels.
4. Stop MP steam supply to ejectors and then isolate it.
5. Introduce Fuel Gas to the Vac column, so as to maintain a positive pressure of 0.5
kg/cm2g.
6. Stop all the product pumps and let the CR pumps run.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
7. Maintain close circulation in the Atmos section.

8. Go for normal start-up when the Tempered water service has been resumed to normal
operation.
9. Empty the Vac column and Atmos column products to Slop.
10. Close the discharge for all the pumps.
11. Block stripping steam supply to the main column and the side strippers and close the
block valves at the shell flange.
For Bitumen section:

1. If the failure is for short duration then cut off feed, air and boiler feed water to the
Bitumen reactor, and then put BBU in circulation mode.
2. If the failure is for longer duration then dilute the system with cutter and then shut-
down the unit.
19.20 LOSS OF BOILER FEED WATER

Loss of BFW in CDU/VBU will affect the HVGO rundown temperature and CR.
Reduce the throughput and by pass the steam generator. After BFW sustains increase the feed
rate as accordingly.
Loss of BFW will affect the BBU unit steam generators and the Reactor temperature
control. If the failure is for longer duration, the unit is to be shutdown as per normal
procedure.
19.21 LOSS OF BEARING COOLING WATER
In CDU, all the pumps will be affected and all are to be stopped. Check for the
bearing house temperatures and if the temperatures are higher, then all the pumps are to be
stopped. If the failure is for longer duration, unit to be taken to shut down.
In BBU, Operation of air compressor and product pumps will be affected. These are
to be stopped accompanied by stoppage of feed, air and BFW to the Reactor. Establish
circulation. If the failure is for longer duration, the system should be diluted with flushing oil
and the unit should be shutdown. Circulation may be re-established when water is resumed.
Then, the unit is started again as per normal procedure.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
BRIEF SUMMARY OF EMERGENCY PROCEDURE:
Case Consequence Action required

Power failure to unit only All pumps, IN/FD fans of furnace Follow emergency procedure
will trip
Power failure to DCS only There will be no control from Follow emergency procedure
control and all the controllers &
SDV’s will go to fail safe
positions.
Power failure to unit and Same as above two Follow emergency procedure
DCS
BFW failure 1. BFW supply to PRDS will 1. Stop the steam let down system.
stop. 2. Reduce the throughput and by
2. BFW to steam generators will pass the steam generator.
stop which leads to high R/d
temp of VGO.
Failure of the crude charge 1. There will be no feed to CDU 1. Follow emergency procedure.
pump and crude booster furnace. (IF PFD not in service). 2. Take out fires in heater and stop
pump including stand by 2. Feed to furnace will be there of turbine, and go to emergency
pump PFD turbine is running. shut down procedure.
Failure of the RCO pump Crude column bottom level will Stop stripping steam to column &
including stand by pump increase & may cause vibration follow the emergency shut down
problem due to stripping steam procedure for VDU section only.
Failure of the SR/VR Vacuum column bottom level will Follow the emergency shut down
pumps including stand by increase & may cause will increase procedure for VDU section only.
pumps & may cause loss of vacuum
Failure of the CR pumps Column operating condition in that Route these products to slop header
including stand by pumps particular CR zone will disturb until the same CR pump will be
leading off spec products normalized.
Failure of the Product Product will overflow to just below Route this product to slop
pump including stand-by chimney tray leading to off spec header until the same product pump
pump product from this tray will be normalized
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0

The emergencies once normalized, the unit has to again go for start-up. In case of emergency
shutdown, many times it happens that the conditions are normalized very soon and the heater
COT, column pressure, etc don’t get upset very much. In such cases, unit has to go for hot
start-up due to constraints of meeting the throughput. The different emergencies will have
different time and in some cases, the normalcy can be very fast. For example, for emergency
like power failure, power supply can resume in 15 minutes only and we have go start the unit
again. But in case of problems like critical pumps failure, heater tube failure, clearance for
start-up may not come for hours or even days.
So, if the unit has to go for start-up after emergency situation, different procedures are
to be followed in different cases. The actions to be taken for start-up after any particular
emergency are discussed as below:
20.1 POWER FAILURE:
In case of the power failure, shut down the unit as mentioned in Chapter 19 under the
shutdown in case of power failure. Whenever the power supply is resumed and clearance is
available from MP/CMP/YSF for start-up, the system has to be flushed with flushing oil.
However if the power failure is long, the system should be steam purged. Then again fresh
cutter is taken and start-up is done as per normal start-up procedure.
20.2 STEAM FAILURE:
In case of failure of steam, the shut down procedure discussed in Chapter 19 has to be
followed. Atmospheric column has to be emptied out by pumping the level and after that
normal start-up circulation has to be started as discussed in the Chapter No. 12. But if the
steam failure is for a long duration, it is advisable to flush the lines and equipments with
flushing oil. The procedure outlined under normal shut down procedures in Chapter 21 for
flushing and emptying out has to be followed. Once the clearance is there, proceed with start-
up as per normal start-up procedure.
20.3 LOSS OF COOLING WATER:
In case of partial failure of cooling water, the unit can be sustained at a lower feed rate.
But in case of total cooling water failure, the unit has to be taken for a shutdown.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
During partial cooling water failure, the flow through coolers and condensers can be
throttled proportionately. In such cases careful watch has to be kept on column pressure and
also on the pumps which use cooling water as coolants. The feed rate can be increased to
normal value once the clearance has been given for desired usage of cooling water.
If the cooling water failure is total and not restored soon, and if flushing oil from off-
sites is available at sufficient pressure, RCO can be flushed out through VR circuit.
Alternatively, steam purging can be done to displace the heater stuff. After resumption of
cooling water, start-up has to be done as per normal start-up procedure.
20.4 LOSS OF INSTRUMENT AIR:
The failure of instrument air will place all the control valves in fail safe mode. Cross
check all the control valves to be in their fail safe positions. Flows, temperature, pressure and
other unit parameters can be controlled by operating the bypass of the control valves. To
facilitate better control of flows through the bypass line, the bypass valves provided are globe
valves. Try to sustain the unit if the loss of instrument air is for a short time but go for
emergency shutdown if the time is prolonged. After the instrument air supply is resumed,
again go for start-up as per normal start-up procedure.
20.5 LOSS OF FEED:
In case of loss of feed, if the supply cannot be restored immediately then the unit has to
be brought to hot circulation by diverting 11-PM-10 A/B discharge to atmospheric heater
through VR line. Temperature will be maintained around 200°C. Products routing will be
stopped and water to coolers will be throttled. If the interruption is for a longer period then
the unit has to be shut down as per normal procedure. Again after solving the problem, unit
has to be started as per normal start-up procedure.
Loss of feed to vacuum section can be due to interruption in atmospheric section. If the
failure is due to RCO pumps 11-P-10 A/B, immediately start the spare pump and normalize
the flow. If the flow cannot be restored immediately, the unit has to be taken on circulation
by diverting 12-PM-01A/B discharge to furnace inlet through start-up line. Then proceed to
shutdown as per normal procedure and after solving the problem go for start-up as per normal
start-up procedure.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 20
PLANT NAME: CDU II
Chapter Rev No: 0
20.6 HEATER TUBE FAILURE:
In case of heater tube failure in 11F01, the plant has to be taken for an emergency
shutdown. The decision whether the shutdown has to be emergency or normal, rests in the
hands of plant supervisor available at that time with consent of YSF/MP. The steps for
emergency shutdown are discussed in Chapter 19. After the shutdown and completion of
maintenance jobs, the unit has to be started again as per normal procedure.
If there is a tube leak in 12F01, there is no immediate need to shut down CDU. Atmospheric
section will be continued, diverting RCO through VR circuit and will be shutdown by normal
shut down procedure depending upon the RCO handling facilities. Whether the shut down
has to be as per normal or emergency depends upon the extent of damage. After the arrest of
leak, the start-up has to be done as per normal procedure.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
NORMAL SHUT DOWN PROCEDURE
21.1 PREPARATION
While shutting down the unit care should be taken, to avoid ingress of air into the system
until all hydrocarbon vapors have been removed. All related units including utilities should
be informed about the shutdown plan. It is to be ensured that a slop tank having sufficient
ullage is lined up to the unit to receive the slops / off-spec material. Closed Blow down
(CBD) should be emptied out and should be kept in a position to receive draining / flushing
from the equipment. Flushing oil should be made available.
21.2 SUMMARY
The summary of shutdown procedure is as follows:

The throughput will be gradually reduced to about 50% of normal capacity by
decommissioning PFD. Necessary adjustment will be done in reflux rates / withdrawal rates
in both the sections to keep the product on specification. Number of burners will be reduced
in the furnaces 11-F-01 and 12-F-01, if necessary. Chemical injection will be discontinued.
Adjustment will be done in Stabilizer column operation to stop production of LPG, which
will be released to the fuel gas system. Naphtha caustic wash will be bypassed. Desalter will
be taken out of service. Transfer temperature of vacuum section will be gradually reduced to
350 °C. Products will be diverted to slop. Vacuum section will be put to close circulation and
RCO from Atmospheric section will be diverted to fuel oil tanks / slop tanks through SR
circuit. Vacuum section circulation will be continued and allowed to cool off on its own.
Atmospheric section will be running at 50% throughput with all products except light
Naphtha on specification. 12-F-01 fire will be cut-off as there is no heat load. Cut-off steam
to ejectors one by one. Bring the system to positive pressure by backing up fuel gas. Pump
out the materials to slop when temperature reaches below 200 °C. Take flushing oil and flush
out all heavy materials to slop. Bring down the temperature of Atmospheric section slowly to
300 °C. Divert product to slop when they become off-spec. Cut off stripping steam. Re-
circulate RCO along with other product through slop header. Back up fuel gas when pressure
tends to become low. Bring down the temperature to 200 °C.
Cut off fire in 11-F-01. Allow to cool down while on circulation. When system is sufficiently
cooled empty out all equipment to slop. Flush out the heavy oil system with gas oil. Flush out
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
fuel oil system. Steam out columns, exchangers etc., to remove hydrocarbon vapors so that
maintenance work can be started.
The important steps in the shutdown procedure can be summarized as below:
1. Decommission PFD.
2. Reduce feed rate to 50%
3. Discontinue Chemical Injection facilities
4. Decommission Desalter
5. Shut down vacuum section
6. Discontinue LPG Production
7. Shutdown Stabilizer
8. Shutdown Atmospheric section
21.3 DETAILED PROCEDURE
The procedure indicated below will ensure a safe and smooth shutdown of the unit but is not
mandatory. It is important that operators understand the purpose and effect of each activity.
In particular, operators should make sure that their actions will not result in the creation of
hazardous conditions either because actions taken were wrong or these were taken at wrong
time.
Atmos section shut-down procedure:
A) Bypassing PFD & Reduction of Feed Rate
i) Reduce the feed rate slowly to 450 m3/h and bypass / shutdown PFD by operating the
ROV. Simultaneously, change the heater pass flow made to F1104R from F1902R by
operating the software switch FR1804S1.
ii) Inform FCCU-II regarding CDU-II shutdown and ask them to slowly withdraw
circulating oil to 11-E-40 A/B.
iii) Reduce throughput gradually to 50% of normal rate step by step. Cut down coil flow
about 10% in each step. Operate Atmospheric furnace flow controllers (FRC-1301 to
1304) for this purpose.
iv) Make adjustment on all operating variables in each step so that normal pressure and
temperature conditions are maintained and the products are also on-spec, which
allows them to be routed to the respective tanks.
v) Shut down the vacuum section (refer section E).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
B) Discontinuing Chemical Injection Facilities
i) Stop caustic injection pumps 11-P-13 A/B/C. Isolate the following:

ii) Caustic injection to suction of Crude charge pump
iii) Caustic injection to suction of Crude booster pump
iv) Stop Demulsifier pumps 11-P-16 A/B and isolate the valves near crude charge pump.
v) Stop liquid ammonia solution injection and isolate the following injection lines:
i) Ammonia injections to crude column overhead vapor line and reflux line.
ii) Ammonia injection to vacuum column overhead vapor line and down stream of
ejector.
iii) Stop corrosion inhibitor injection after stopping the ammonia injection.
vi) Isolate the vessels including cylinder and drums, which contain chemicals.
Depressurize and drain pumps and lines including the calibration pots.
C) De-Commission the Desalter

(Refer Vendors instruction manual)
i) Stop water to Desalter and then switch off power.

ii) Shut off Desalter effluent water (brine) line after ensuring the water level is lowered
to minimum.
iii) Wide open the emulsifying valve (mix valve). The pressure control system of the
Desalter should continue to work so that booster pump suction pressure is ensured.
D) Cut off LPG Production and Shut down Stabilizer
Control system of Stabilizer column shall be changed from total condensation to partial
condensation operation. LPG downstream treatment unit will be informed about
discontinuing LPG production.
i) Increase reflux to Stabilizer and cut off LPG production. Operate FRC-1501 (Reflux
controller) and FRC-1502 (LPG product) for this.
ii) Reduce the column top pressure very gradually by operating PRC- 1501. Care must be
taken to reduce the pressure very slowly to avoid lifting of heavy ends to the top and
sudden release of heavy gas to the fuel gas system.
iii) Bring the column to total reflux operation, by maintaining pressure such that only
sufficient vapor condenses to maintain the reflux flow.
iv) Reduce feed to Stabilizer.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
v) By utilizing the available pressure, keep emptying out the Stabilizer bottom to storage
tank and maintain Stabilizer bottom level. Pressure control valve PV-1501 may be closed
to aid the emptying out.
vi) Reduce heating medium flow to reboiler 11-E-25
vii) Take TIC-1501 on manual and bypass KCR to exchanger 11-E-25 through TV-1501.
viii) Pump out reflux drum (11-V-03) liquid to Stabilizer till pump looses suction.
ix) Keep receiving feed to Stabilizer till Atmospheric column runs on total reflux and then
cut off feed to the Stabilizer. Close the isolation valve in the Stabilizer feed line and
empty out the Stabilizer bottom as explained below.
x) Open LV-1501 and empty out Stabilizer to storage tank by its own pressure bypassing
the caustic wash system. Heat up bottom if necessary for this purpose. Care must be
exercised to prevent gas blow by while emptying out the column.
xi) Stabilizer column pressure, Naphtha flow and Stabilizer bottom level will give indication
about emptying out of the column. After emptying out isolate the column by shutting off
valve on the inlet and outlet streams and then depressurize slowly by releasing to flare
through depressurizing valve.
xii) After depressurizing, residual liquid in column, piping and exchangers will be drained to
CBD or OWS.
xiii) Open the LP steam connection provided at the Stabilizer column bottom and start
steaming. Open vent at top and reflux drum. This step can be taken up only after
shutdown of the rest of the unit so that cooling water can be isolated for effective
steaming. Steam out for a period of about four hours, after which it will be discontinued.
xiv) Allow the system to cool down by putting water and with vent valves full open.
E) Bringing Down Vacuum Section
This should be done first after throughput reduction:

i) Start reducing 12-F-01 outlet temperature by operating TRC-2133 at 30 °C per hour to
350 °C.
ii) Divert products to slop when they go off-spec.
iii) Start column to furnace circulation by diverting 12-P-01 A/B discharge to 12-F-01
through start-up line. Simultaneously divert Atmospheric column Bottom (11-P-10 A/B
discharge) to SR circuit, which will be lined up to Fuel oil tanks / slop tanks.
iv) Stop side stream withdrawal and increase internal refluxes to make the bottom lighter.
v) Cut off fire to furnace 12-F-01 as there is no major heat removal from the system.
Purge out the furnace as defined in furnace shut-down procedures.

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
vi) When circulating RCO temperature is around 250 °C, stop ejectors one by one closing
12-J-01 A/B/C first and then the other stages. Close hot well liquid seal valve, vent valve
and non-condensable return valve along with the last stage ejector. Care should be taken
to prevent air entry into the system.
vii) Bring the system pressure to around 0.5 kg/cm2 by backing up with fuel gas.
viii) Maintain bottom level by opening 12-PM-01 A/B discharge to SR circuit whenever
necessary.
ix) Allow the system to cool down to 200 °C, when the temperature reaches below 200 °C,
empty out the column to slop / fuel oil tanks through SR circuit along with RCO.
x) Line up flushing oil to 12-C-01 LVGO section and flush out all circuits by running
circulating pumps.
xi) When sufficient level is built up at the column bottom, start 12-P-01 A/B and circulate it
through furnace coil.
xii) When the system is thoroughly flushed, divert 12-P-01 A/B to slop. Pump out liquid
from all trays to the slops by connecting the respective product lines with the slop
header. Stop the pump when it loses suction.
xiii) Blind the fuel gas line. Isolate all inlet and outlet lines at the battery limit.
xiv) Reverse blinds on CBD lines from various equipments.
xv) Isolate cooling water to condensers.
xvi) Drain all the oil in the CBD. Ensure adequate ullage in CBD drum by pumping out
CBD drum contents to slop.
xvii) Open steam to column and open furnace coil emergency steam. Steam out all
piping/exchangers etc. Continue steaming vigorously for about 8 hours to make the
system hydrocarbon free.
xviii) Once steaming is over, isolate steam and keep all vents and drains open for handing
over to maintenance.
F) Reducing Heater Outlet Temperature (Atmospheric Section)
Atmospheric section is running with 50% of normal capacity with:

• RCO routed through SR circuit to Fuel oil tanks.
• Rest of the products are going to respective tanks.
i) Start reducing heater outlet temperature by TRC-1301 @ 30 °C/h. All controls will be
taken on manual.
ii) As temperature of crude oil drops, there will be less of distillate products and column
pressure will tend to fall. Admit fuel gas into the reflux drum by pressure controller PV-
1409B if fuel gas is available from elsewhere.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
iii) As product temperature starts dropping, products will go off-spec. Divert all off-spec
distillate products to slop at the battery limit.
iv) The overhead product yield will gradually come down. Stop withdrawing Naphtha
product and resort to total refluxing. Liquid in reflux drum will be emptied out into crude
column slowly
v) Gradually reduce product withdrawal rates and pump around rates.
vi) Stop pump around pumps one by one starting from TPA pump.
vii) Stop product pumps when they lose suction.
viii) With lowering of the heater outlet temperature, RCO yield will increase and viscosity
will come down. Line up the slops receiving tanks to crude charge pump suction and
establish close circulation of RCO through SR circuit. Isolate the crude feed tank.
ix) When heater temperature drops to about 200 oC, cut off all fires. Purge out burners and
fire box as per details under furnace shut down procedure described in General
Operating Manual.
x) Continue circulation till system gets cooled down sufficiently to about 100 oC at the
column base. After this, stop crude charge pump 11-P-01 A/B. Route RCO to slop tank.
Stop booster pump 11-P-02 A/B and RCO pump 11-P-10 A/B when they lose suction.
xi) Inform MEROX to charge flushing oil header. Take flushing oil to the distillation column
through RCO pump 11-P-10 A/B suction. Build up about 30% level at the base of the
column.
xii) Start circulation through SR circuit to crude charge pump and complete the circuit up to
the column. Take flushing oil to feed pump suction and use pumps 11-P-01 A/B, 11-P-02
A/B and 11-P-10 A/B for this purpose.
xiii) Flush out heavy oil from exchangers/control valve bypasses by operating them one by
one.
xiv) Continue circulation till entire circuit is flushed out.
xv) Check the consistency of the circulating material. When it is sufficiently light, stop
circulation and pump out the material to slop tank. The flushing operation may have to be
repeated more than once.
xvi) Slowly open steam to the discharge of crude charge pumps 11-P-01 A/B and flush the
lines and equipments. Isolate Desalter and drain the content to the CBD system. Admit
LP steam and thoroughly steam by opening vent and try-cocks. Stop steaming when oil is
fully emptied in Desalter, care should be taken steam should not enter CBD system. Keep
the Desalter pressure around 0.3 kg/cm2 during steaming.
xvii) Steam the crude exchangers from the discharge of the crude booster pump 11-P-02 A/B
and displace the material into the column. Open emergency steam to the four passes of
the furnace 11-F-01 to expedite the displacement.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
xviii) Pump out the material collected in crude column to slop tank. Run RCO pump as and
when necessary.
xix) Steam out the discharge of RCO pumps and route the material into slop tank. Care
should be taken to avoid steaming beyond battery limit.
xx) After maximum quantity of material has been removed from the unit, drain all
equipment and lines to CBD one by one. CBD drum level and temperature should be
watched during this draining.
xxi) Isolate fuel gas header from the reflux drum (11-V-01). Reverse the blind to close
position) of the fuel gas header in the plant battery limit.
xxii) Depressurize the crude column to flare. After depressurization, close all valves
releasing to flare. Close cooling water at plant the battery limit and drain out water from
condensers and product coolers.
xxiii) Start steaming of crude column, preheat exchangers, furnace coils and coolers and
condensers as detailed under the section of start-up procedures. Continue steaming till all
hydrocarbon vapors are removed from the system. Vents at column top and reflux drum
will be opened after ensuring clear condensate appears in the reflux drum.
xxiv) Flush out fuel oil header by taking flushing oil at unit battery limit. Drain out oil to
OWS. Steam out the header till hydrocarbon is eliminated.
xxv) Shut off tracing steam to the lines.
xxvi) Carry out insertion of blinds as per the master blind list for isolating the unit for
maintenance.
21.4 SPECIAL SHUTDOWN PROCEDURES
21.4.1 ATMOS SECTION CUTTER FLUSHING PROCEDURE
1) Ensure Desalter is in bypassed condition and keep Desalter R/V bypass valve in open
position and empty out crude from Desalter to CBD. Keep close watch on Desalter top
pressure to avoid creation of vacuum in Desalter.
2) Cutters flush and displace crude from exchangers (11-E-01 to 11-E-07) to CBD
(inclusive of all tie-ins) using individual flushing oil tie-ins.
3) Bypass and isolate the crude side of exchangers of 11-E-08 to 11-E-16 (both BH and PG
mode tie-ins) and cutter flush to CBD using individual flushing oil tie-ins.
4) Bypass and isolate both sides of the exchangers of 12-E-01 to 12-E-06 and cutter flush
both sides to CBD using individual flushing oil tie-ins.
5) Take cutter to 12-PM-01 A/B discharge manifolds and flush SR circuit (11-E-16, 12-E-
06 A/B, 12-E03, 12-E-01 A/B/C, 12-E-09 A/B/C/D [SR side]) to slop tank.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
6) Cutter flush both preheat trains (crude side) and 11-F-01 coils to 11-C-01 as shown in
the circuit below:-
12-PM-01 A/B discharge

Cutter stock header
manifold
11-E-01 to 11-E-
07 (bypass all SR circuit (bypass
exchangers) all exchangers)
11-PT-01 B
11-E-08 TO 11-E-16
PFD manifold
11-PM-02
12-E-01 to 12-E-06
11-C-01 11-F-01 coils 11-E-40 A/B
7) Pump out 11-C-01 bottom stock to slop tank again via SR circuit. Since, SR circuit is
involved in both Atmos. and Vac. Side flushing operation, it is to be carried out
alternatively. Continue the flushing cycles till we observe clear cutter stock at SR sample
point.
8) After thorough flushing, depressurize individual equipment to CBD and prepare for
steaming.
9) Remove blind on 11-C-01 vent & 11-V-03 vent boiler makers. Isolate 11-C-01 overhead
condensers and stabilizer overhead condensers salt water side and remove boiler makers
on salt water lines to drain salt water.
10) Close 11-PV-409B (fuel gas to 11-C-01) control valve’s block valve and bypass valve.
Maintain column pressure by using column bottom stripping steam and place 11-PV-
409A in service (auto mode). Maintain column pressure in the range of 1-1.5 kg/cm2.
11) Depressurize flushing oil header, install blind at battery limit and back up MP steam to
header.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
Note:-
a) While carrying out above operation, coordinate with YSF/TPH for usage of cutter
stock & slop system.
b) Keep CBD pump in Auto mode and pump out the stock to slop system.
c) While carrying out flushing ensure that control loop bypass valves are in open
position.
d) Ensure all the FTs & PTs impulse lines are flushed thoroughly.
21.4.2 DESALTER STEAM OUT PROCEDURE
1) Bypass the Desalter and get the transformers isolated electrically.

2) Keep Desalter R/V bypass valve in open position and empty out crude from Desalter
to CBD. Keep close watch on Desalter top pressure to avoid creation of vacuum in
Desalter.
3) Steam out Desalter by introducing LP steam (MP steam would damage Teflon
bushings of transformers), and steam the R/V line to 11-C-01 through R/V bypass
valve.
4) Steam Desalter brine line up to MEROX OWS and blind at unit limit.
5) Steam the stripped water to Desalter line from SWSU up to Desalter via 11-E-18 by
opening check valve discharge flange (coordinate with MEROX unit).
6) Carry out steaming till the sweet steam comes out.
21.4.3 STEAM OUT PROCEDURE PREHEAT TRAIN AND FRACTIONATOR
1) Introduce MP steam at 11-PM-01A/B discharge and displace 11-E-01 to 11-E-07

cutter stock to CBD and carry out initial steaming. (Ensure 11-PM-10A/B discharge
and warm up valves are in closed position)
2) After backing up steam into cutter into cutter stock header, steam out the 11-E-08 to
11-E-16 and 12-E-01 to 12-E-06 and 11-E-40 A/B using individual cutter lines and
carry out thorough steaming (both initial and final steaming). Co-ordinate with
FCCU-2 for steaming circulating oil side.
3) Open purge steam to 11-F-01 passes and steam common inlet line up to PFD
manifold.
4) Steam out each pass for a minimum of 1½ hour and keep all the passes under steam
purge for thorough steaming.
5) Pump out 11-C-01 bottom to slop tank.
6) After completion of 11-F-01 steaming, isolate passes purge steam and depressurize
11-F-01 coils and 11-C-01 vents/drains respectively.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
7) Steam out 11-C-01 thoroughly by opening stripping steam to column bottom and
strippers (monitor column pressure and maintain a pressure in the range 1-1.5
kg/cm2).
8) Steam out all connected pump suction through OWS funnels using steam from 11-C-
01. Isolate pumps and depressurize by opening vents and drains.
9) Open over-flash loop bottom drain valve boiler maker and steam the loop thoroughly.
Also steam the connected gauge glasses and level trolls and other instrument leads of
11-C-01 thoroughly.
21.4.4 STEAMING OUT OF PRE-FLASH DRUM
1) Take cutter stock into PFD via cutter tie-in.

2) Displace this cutter stock at 11-PM-10A CBD/OWS and 11-PT-02B suction
CBD/OWS by taking MP steam to PFD.
3) Steam the PFD and its manifold with existing MP SOP thoroughly. While steaming,
ensure that PR1902 control valve bypass and PFD relief valve bypass are in open
position.
21.4.5 STEAMING OUT OF CIRCULATING REFLUXES
1) Top Reflux:
a) Isolate pump suction and discharge valves

b) Steam out the 11-PM-06 A/B suction line to OWS by backing steam from 11-C-01.
c) Steam the Top reflux line by backing steam from 11-C-01 up to 11-PM-06A/B
discharge including FR1403 control valve and its bypass as shown in the following
circuit:-
11-C-01 FR1403 11-PM-06A/B discharge
d) Back up steam to pump casing and displace the hydrocarbon from pump casing by
opening casing drain (Minimize steaming through pump to protect mechanical seals).
2) TPA
a) Isolate pump suction and discharge valves

b) Steam out the 11-PM-09A/B to TPA return line and steam upto pump discharge as
shown in the circuit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
11-C-01 FR1406 11-E-04A/B 11-PM-
c) Open warm up valve of the pump and steam the pump casing at slow rate and until
hydrocarbon is displaced (Minimize steaming through pump to protect mechanical
seals).
3) KERO CR
a) Isolate the KERO CR pump suction and discharge valves

b) Steam out the 11-PM-08A/B suction line to OWS by backing steam from 11-C-01.
c) Steam out the KERO CR circuit (Both BH and PG circuit) SOP as shown in the
circuit below.
i)
11-E-25
11-PM-08A/B
11-E-11
Discharge
11-E-09
11-PM-08C/D
OWS 12-E-
ii)
11-C-01 12-E-01A/B/C
4) DSL CR
a) Isolate the Diesel CR pumps suction and discharge valves

b) Steam out the 11-PM-07 C/D suction lines to OWS by backing up steam from 11-C-
01.
c) Steam out the Diesel CR circuit (both BH and PG tie-ins) from 11-PM-07 C/D
discharge with newly provided SOP as shown below.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
FR1404 c/v
11-PM-07 C/D 11-E-15 11-E-13
u/s
d) Back up the steam from 11-C-01 to Diesel CR return upto FR1404.

e) FR1404 bypass also to be steamed either from 11-C-01 or from circuit.
5) Overhead system
a) Open boiler makers on salt water outlet of overhead condensers.

b) Back up steam to 11-V-01 from 11-C-01.
c) Displace 11-V-01 hydrocarbon to flare via PR1409 control valve bypass and newly
provided 3” line at ground level.
d) Open vents and drains of gauge glasses, LTs of 11-V-01.
e) Steam the overhead condensers, 11-V-01 and its boot sour water to MEROX line
thoroughly. Provide additional steam hose to 11-V-01 for effective steaming.
21.4.6 STEAMING OUT OF RUNDOWN CIRCUITS
1) HN Product
a) Isolate the HN pumps suction and discharge valves.

b) Steam out the 11-PM-05 A/B suction line to OWS by backing up steam from 11-C-01.
c) Open the warm up valve of the pump and steam the pump casing at slow rate and till
hydrocarbon is displaced.
d) Steam out HN rundown lines both HN to SRN and HN to diesel using cutter tie-ins to
11-E-01 and 11-E-26 as shown in the circuit (cutter stock header is with steam).
11-PM-05 A/B
Discharge 11-E-01 11-E-26
HN to DSL up to HN to SRN
unit limit
Note:- 11-E-26 salt water side boiler makers to be opened after isolation on cooling water
side.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
2) KERO Product
a) Steam out the 11-PM-04 A/B suction lines to OWS by backing up steam from 11-C-
01.
b) Steam out the KERO rundown lines i.e. KERO to Diesel, KERO to KERO, KERO to
fuel oil, and KERO to LDO by using the newly provided MP SOP to 11-PM-04 A/B
discharge as shown in the circuit.
11-PM-04 A/B 11-E-10

Discharge 11-E-05 11-E-02
11-E-24/24A
R/D FR1204 FR1203 R/D
Slop KERO to KERO to

LDO fuel oil
Note: - Isolate salt water to 11-E-24,24A and remove boiler makers.
3) DSL Product
a) Steam out the 11-PM-03A/B/C suction lines to OWS by backing up steam from 11-C-
01.
b) Steam out the Diesel rundown lines i.e. Diesel to Diesel, Diesel to LDO and diesel to
slop as shown in the circuit below.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
11-PM-03 A/B/C 11-E-14 A/B 11-E-12
11-E-03 11-E-06 11-E-08
DSL to 11-PM-07 C/D,

13-PM-02 A/B seal
flushing lines
11-E-23/23A
Hot DSL to cutter header
Hot DSL to FCCU

FR1202 FR1207Q
R/D R/D Slop
Note: - Isolate salt water to 11-E-23A and remove boiler makers.
4) RCO Circuit
a) Displace the cutter stock of 11-PM-10 A/B suction lines to OWS and steam out those
lines by backing up steam from 11-C-01.
b) Displace the cutter stock of SR circuit to respective exchangers to OWS/CBD and
steam the above circuit by newly provided MP SOP to 11-PM-10 A/B discharge.
c) Displace the cutter stock and steam the quench line. After dropping TR2201 control
valve steam quench line from both 12-C-01 and 12-E-03 thoroughly.
21.4.7 STEAMING OUT OF AUXILLIARY SYSTEMS
1) FUEL OIL SYSTEMS
a) Close fuel oil supply and return lines unit limit block valves.
b) Open the Cutter stock to fuel oil supply line at unit limit and flush it thoroughly to slop
header.
c) After flushing with cutter stock, disconnect individual fuel oil hoses of 11-F-01 & 12-
F-01 and drain the line stock into empty drums and also drain the line stock of SDVs.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
d) Steam out the whole fuel oil supply and return lines by backing up steam from 11-F-01
& 12-F-01 atomizing lines.
e) After initial steaming, install spread blinds on fuel oil supply and return lines.
f) Carry out final steaming till sweet steam comes out and then make up the blind.
2) FUEL GAS SYSTEM:
a) Close fuel gas header block valve at unit limit.

b) Depressurize header stock to flare via 11-V-01 (Ensure that before starting the
steaming of 11-V-01, fuel gas depressurizing is to be completed).
c) Open the SOP to fuel gas at the unit limit, steam out the 11-F-01, 12-F-01 fuel gas
lines, 11-V-01 fuel gas make up line and 12-C-01 vacuum break up fuel gas line.
d) After initial steaming install spread blinds at unit limit and other dead ends.
e) Carry out final steaming and make up the blinds.
3) FLARE HEADER
a) Steam the flare header by backing steam from PR1409 bypass and 3” line at ground
level.
b) Block unit limit block valves.
c) After initial steaming install spread blinds at upstream of block valves.
d) Carry out the final steaming and make up the blind at unit limit.
4) CHEMICAL INJECTION SYSTEM
a) Close chemical injection block valves on the 11-C-01 side and break open the flanges.
b) Hook up the steam hoses to ammonia, Kontol, DMF and caustic lines and steam out
the drums and connected lines.
c) Steam out fresh caustic and spent caustic lines which are coming from MEROX by
hooking steam hoses at unit limit.
Note: - Carry out thorough water washing of all the chemical pots connected piping before
introducing steam
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
21.4.8 VACUUM SECTION CUTETR FLUSHING PROCEDURE
1) LVGO Circuit:
Take cutter stock to 12-C-01 top section via cutter stock tie-in to cold LVGO reflux
line. Build up level in the LVGO section and start circulating in the following manner
for stream No. 1:
12-C-01 Top
(LVGO 12-PM-04 A/B 11-E-07
Vac. Column 11-E-22/22A 12-E-12A

via 12-FV-205 (parallel) (Top cooler)
Stream No. 2 of LVGO to HVGO is to be flushed via 12-E-11 under LI2205. The
third stream of LVGO from pump (12-PM-04 A/B). Discharge to be flushed into HVGO
section of 12-C-01 via 12-FV-201 to build up HVGO level.
2) HVGO CIRCUIT:
Take cutter stock into HVGO section via. 12-FV-201 (through hot LVGO reflux to cold
HVGO reflux line using 12-PM-04 A/B). After building up level, start circulating in the
following manner: -
12-PM-03 A/B 12-E-05 A/B 12-E-02
12-E-04
12-E-10 12-E-
Slop 12-E-12 A/B

12-C-01
Hot feed line to TK3 OR TK4

(whichever is not being used by
FCCU-2)
Another stream of hot HVGO reflux is to be flushed to 12-C-01 via FR2202.

Continue routing cutter stock via FR2202 to build up slop cut level.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
3) SLOP CUT CIRCUIT:
After building up slop cut level, start flushing as described in the following manner:
i) Circuit 1 : -
12-PM-02 12-F-01 passes via FR2109
ii) Circuit 2 : -
12-PM-02 12-E-01 A/B/C via LI2203
4) SR CIRCUIT:
Take cutter into 12-C-01 bottom via 12-PM-01 A/B suction and start building up
level. After up the desired level, start flushing as shown in the circuit given below.
12-PM-01 A/B 11-E-16 A/B 12-E-06 A/B
12-E-01 A/B/C 12-C-01 (Via TR2201)
12-E-09 A/B/C/D BBU
Slop Tank
Continue cutter stock flushing of all the above given circuits till we start observing clear
cutter stock at SR sample point.
21.4.2.2 VACUUM SECTION STEAM OUT PROCEDURE
• Steam the 12-F-01 coils with passes purge steam for a minimum of two hours each
pass keeping 12-C-01 under vacuum.
• After 12-F-01 coils are steamed, reduce coil steam to bare minimum and break
vacuum by isolating the ejectors of 1st stage, 2nd stage and finally 3rd stage. Get the
column vent blind removed. Stop surface condensers cooling water and drain salt
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
water by opening boiler makers. Make sure that the column pressure is maintained at
0.5-1.0 kg/cm2 maximum (Install one PG 0-5 kg/cm2 range at 12-C-01 flash zone).
• After breaking vacuum, steam displace cutter from LVGO, HVGO, slop & SR pump
suction lines and SR to HVGO pump suction to respective CBD/OWS.
• Isolate LVGO, HVGO, Slop & SR pumps and depressurize by opening vents and
drains. Before backing up MP steam ensure that vent line block valve at 12-C-01 shell
is closed. Now back up steam into vacuum section pumps venting line and displace
the line content to respective pumps.
1) LVGO CIRCUIT
a) Open SOP (pump vent line) to 12-PM-04 A/B discharge line. Displace the cutter
stock and steam the LVGO circuit thoroughly as shown below.
12-PM-04 A/B 11-E-07 12-E-12A 11-E-22/22A
LVGO CR strainer A
HVGO
rundown (unit
12-E-11
LDO/DSL (up
to unit limit)
Note:- a) 12-E-11, 12-E-12A & 11-E-22/22A coolers salt water side to be isolated and
remove boiler makers.
b) If required open strainer drain valve.
2) HVGO CIRCUIT:
a) Open SOP (pump vent line) to 12-PM-03 A/B discharge line. Displace the cutter
stock and steam the HVGO circuit thoroughly in the following manner.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
12-PM-03 12-E-05 A/B 12-E-02
12-E-04
Hot Reflux Strainer
HVGO Strainer 12-E-10/10A
R/D up to unit 12-E-12B

limit
Hot Feed to
FCCU-2 up to
unit limit
Note : - a) Isolate S/W to 12-E-12B and remove boiler makers.

b) Isolate BFW to 12-E-10/10A & open vents on steam side.
c) If required open strainers drain valve.
3) SLOP CUT CIRCUIT :
a) Open SOP (pump vent line) to 12-PM-02 A/B discharge. Displace the cutter stock
and steam the slop cut circuit as shown below.
12-F-01 passes via FR2109
12-PM-02 A/B
12-E-01 A/B/C via LI2203
b) Slop cut to CDU-1 cooler box line cutter stock displacement and steaming also to be
done.
Note: - Carry out steaming of 12-PM-02 A/B discharge to 12-F-01 passes via FR2109 after
completion of 12-F-01 individual passes.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 21
PLANT NAME: CDU II
Chapter Rev No: 0
4) SR CIRCUIT :
a) Open the SOP (pump vent line) to 12-PM-01 A/B discharge and displace cutter stock
at SR manifold.
b) Steam the SR circuit thoroughly.
c) Steam the tempered water drum before handing it over to Maintenance.
Note: - Isolate tempered water to 12-E-09 A/B/C/D and open boiler makers.
5) OVERHEAD SYSTEM:
a) Remove the blind on LP steam to 12-C-01.

b) Open Surface condensers salt water outlet line boiler makers.
c) Steam 12-C-01 and connected systems with LP steam for initial steaming.
d) Open block valves bypass valve of top pressure control valve and steam fuel gas make
up line.
e) Maintain column pressure at 0.5-1.0 kg/cm2 maximum.
f) Steam hot well oil/water lines up to unit limit by connecting steam hose at pump
discharge line.
g) Open the 12-C-01 vent boiler maker and then carryout final steaming.
After completion of final steaming, take water to 12-C-01 via 12-PM-04 A/B suction for
water washing the column and then drain water at 12-C-01 bottom and continue till it gets
clear water.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 22
PLANT NAME: CDU II
Chapter Rev No: 0
TEMPORARY OPERATIONS
TEMPORARY OPERATIONS
Temporary operations are those which we use to overcome the operation problems by
adapting a method so that till the completion of job there will be no disturbance to plant
operating conditions. The job can be either online or shut down or T&I nature. Till the
completion of job the temporary operation will be in place. Generally in the following cases
temporary operations are required:
1. If any control valve is having problem then as a temporary operation we will bypass
the control valve and operate the plant till the rectification of the same.
2. If any line plugged then if at all any bypass line is available then as a temporary
operation we will use the bypass line till the rectification of the same.
3. If any exchanger or cooler or APH is having tube leak then as a temporary operation
we will bypass the same and operate the plant till the rectification of the same.
22.1 CDU-II UNIT TEMPORARY OPERATIONS STATUS:
Temporary Reason for Date from Temporary operation Remarks

S.NO operation temp which temp job completion ( online/
details Operation operation is in Opportunity S/D / T&
place I)
1
10
11
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 23
PLANT NAME: CDU II
Chapter Rev No: 0
PROCESS SAFETY INFORMATION
PROCESS SAFETY INFORMATION
The following Process Safety Information is to be included in the manual.

• Information on deviation from the design limits of major equipment and minimum
Consequence- PSM/FR/2.6
• Information of plant relief system- PSM/FR/2.7
• List of Process System and Interlocks- PSM/FR/2.10
• List of Enclosed facilities- PSM/FR/2.8
• Information on Plant Holdups- PSM/FR/2.5
• Design Codes and Standards Employed.
As per TSD-PAD, preparation of documents is under consideration.

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
SAMPLING REQUIREMENT AND SAMPLING PROCEDURES
SAMPLING REQUIRMENT AND SAMPLING PROCEDURES

Product timely representative sampling, immediate lab analysis, feed back to plant
personnel and necessary corrections in plant parameters, wherever required is an
important loop, which should be continuously completed. Correct representative
collection is an important aspect in the entire chain of sample collection. The results
given by lab are utilized by unit supervisors for proper monitoring and improving the
operation of the units. These results are being used by planning and technical personnel
to fine tune and optimize the operation of the unit.
24.1 SAMPLE COLLECTION:
All regular samples should be collected as per LAB sampling schedule in cleaned
bottles/grabbers/tin with the required quantities as mentioned by lab. These samples
should be tagged correctly writing the origin of the sample, name of the stream, tests to
be performed and date/time. The tagged bottles should be kept at the designated place
15 minutes ahead of sampling schedule. In case, sample is not collected in time due to
any problem, the technician concerned should highlight to supervisor. The plant
technician, during routine rounds, should observe that the samples are taken by
laboratory and inform shift supervisor and laboratory if the samples are not collected in
time. If sample collection is further delayed then shift supervisor should remind
laboratory once again and inform Shift Foreman. The overall responsibility of ensuring
availability of the sample at the collection point rests with the unit shift supervisor.
Shift supervisor should ensure that sufficient number of cleaned bottles/grabbers and
sample tags are available in the unit for sample collection. The quantity of samples
should vary as per the volume requirement list given by laboratory.
24.2 SAMPLING PROCEDURES:
Samples are to be collected in clean and dry bottles. Sometimes samples are taken to find out
the affect of certain changes brought about in plant conditions. The samples are to be taken
with great care so that they represent the actual plant conditions of the collection time. The
line content is to be properly drained to ensure representative sample is collected and the
bottles are to be thoroughly rinsed with the product before collection of sample. The
products, specifically those which are prone to oxidation in contact with air, are to be filled to
top of the bottle. The sample points are suitably located to provide the representative samples.
There are various precautions that need to be taken during sample collection and also
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
different samples have different precautions. Draining excessively for sample collection
results in wastage of finished products and reduces overall through-put.
24.2.1 Liquid sampling procedure (non-flashing type):
• The person taking sample should wear proper safety clothing like face-shield, aprons,
rubber-gloves etc, to protect face, hands etc.
• Whenever hot samples are taken check for proper cooling water flow in sample
cooler.
• Sample points usually have two valves in series, one gate valve for isolation and
second globe valve for regulating the flow. Open gate valve first and then globe valve
slowly, after placing sample container. After the sample collection, close globe valve
first and then gate valve. Then re-open globe valve to drain the content for congealing
liquids. In case of bitumen sampling two gate valves are used. The purpose of two
gate valves is to facilitate poking in case the line gets choked.
• Sample valve should be slowly opened, first slightly to check for plugging. If the
plugging gets released suddenly the liquid comes-out at a dangerously uncontrolled
rate. Never tap the line to clear plugging, instead ask maintenance for assistance. For
avoiding plugging of the line in case of congealing type samples, sample points are to
be equipped with proper copper coil type steam tracer. It should be ensured that steam
tracing is functioning properly.
• The operator taking the sample should be careful to stand in a position such that the
liquid does not spill on him and he has unobstructed way out from the sample point in
case of an accident. While collecting dangerous toxic material’s samples, proper gas
mask is to be used. It is advisable to stand opposite to wind direction in case of
volatile toxic liquid sampling.
• Sample should be collected in clean, dry and capped bottle. In case of congealing
samples use clean and dry grabber/tin.
• Rinsing of bottles is to be done thoroughly before collecting the sample.
• Before collecting ensure that the content has been drained and fresh sample is
collected.
• Gradually warm-up the sample bottle/metallic tin by repeatedly rinsing it before
collecting the sample
• Cap the bottle immediately after collecting the sample
• Attach a tag to the bottle indicating the concerned details.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
• A few products suffer deterioration with time. For example, the color of the heavier
distillates slowly deteriorates with time. So these samples should be sent to laboratory
at the earliest after collection.
• The samples after collection should be kept away from any source of ignition to
minimize fire hazard.
• Volatile samples (naphtha) should be collected in bottles and kept in ice particularly
for some critical tests like RVP. Moreover sample should not be collected fully to
maintain vapor phase.
24.2.2 High pressure hydrocarbon liquid samples (flashing type):
• The person taking sample should wear personal protection equipments like apron, gas
mask and hand gloves to protect him.
• Ensure that sample bomb is empty, clean & dry.
• Connect the sample bomb inlet valve to the sample point with a flexible hose.
• Open the inlet valve of the sample bomb. Hold the sample bomb. Hold the sample
bomb outlet away from person. Keep face away from hydrocarbon vapor and stand in
such a way that prevalent wind should blow hydrocarbon vapor away. Open the gate
valve of sample point slowly till it is fully open. Then slowly crack open the
regulating valve. One should be careful at the time of draining because chances of
icing are there. As a result the formation of solid hydrates is a continuing process
which leads to the plugging of valves.
• When all the air in the hose and bomb are displaced as seen by the hydrocarbon vapor
rising from the outlet of sample bomb, close the sample outlet valve. Allow a little
quantity of liquid to spill to make sure that the bomb is receiving liquid. Frosting will
be an indication of liquid spillage.
• Allow liquid hydrocarbon to fill the bomb. When the bomb is full, close the valves on
sample point. Close inlet on the sample point. Carefully disconnect the hose from the
sample bomb. To allow for some vapor space in the bomb for thermal expansion in
case of overfilling, crack open the outlet valve of bomb and displace a small part of
liquid and then close outlet valve.
• Closed sampling facilities are provided at some locations where it is not desirable to
waste the costly product or if the material is toxic. For filling the sample bomb,
pressure drop across a control is usually utilized or across pump suction and discharge
air is expelled from the bomb after it is connected to the upstream of control valve.
The bomb is then connected to the downstream of control valve or pump discharge
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
side. The sample is then collected and bomb is detached after closing valves on the
both sides. Send sample bomb to Laboratory for analysis.
24.2.3 Gas sample:
• For collection of gas sample which are not under high pressure and temperature,
rubber bladders are used. For the operation under vacuum or low pressure, aspirator is
used. For representative sample, purge the bladder 3 to 4 times with the gas and then
take the final sample. Use of three-way valve with bladder/aspirator will facilitate
purging & sampling.
• Sample bombs are to be used for taking gas samples from high pressure and high
temperature.
Note: DM water Samples should be collected in clean dry plastic bottles to avoid silica
leaching in glass bottles
24.3 RESULT ASSESSMENT AND CORRECTIVE ACTION:
When the testing is completed, laboratory will enter the results in LIMS. If the results are not
entered in time, the shift supervisor should enquire the status of testing from the laboratory.
In case of any problem, YSF should be kept informed. After checking the results in LIMS,
the shift supervisor should compare them with planner’s requirements in the unit regulation
sheet and take appropriate corrective actions. This includes adjusting the unit parameters if
required, informing the persons concerned, i.e., YSF, unit Manager, operations planner and
TPH personnel (if any stream is to be re-routed). If any parameter becomes off even though
unit conditions are same, the technician on the advice of unit supervisor should collect a
check sample indicating on the tag the required parameter to be tested.
24.3.1 Significance of Individual Parameters in Product Testing:
Each individual test is designed to represent one particular property of the product. Every
parameter is critical in itself. If the sample collected is not representative, the results will be
erroneous and misleading. If the product with off spec parameters is routed to product tank,
the product in the tank becomes of spec. Correction of the same subsequently becomes
difficult and time consuming. Sometimes this leads to down gradating of the product or
sloping it back to the crude for reprocessing, which has a negative impact on operation
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
expenditure. Also each test on each product consumes precious time of lab personnel. Hence
proper knowledge of sampling procedure is essential.
Petroleum Products Determination of Color:
(ASTM SCALE)
Applicable to products: HSD, LDO, JBO

Significance: This method is used to determine color of black oils. Color is an indication of
overall purity of the sample. When the color is deteriorated it indicates:
Thermal decomposition, may be due to high temperatures
Entrainment or trace contamination due to presence of heavier products
This scale ranges from 1 to 7, in increments of 0.5, 7 being the darkest and 1 being lightest.
(SAYBOLT CHROMOMETER)
Applicable to products: MTO, SKO, ATF, NAPTHA

SAYBOLT Color: It is the number related to the depth of a column of material, the
Color of which is compared with specified glass standards. The range of numbers is +
30 (lightest color) to -16 (darkest color)
Significance: White oils are used in the manufacturing of paints, fertilizers, cosmetics,
pharmaceuticals, agriculture, food and industrial usage. Color is an important factor to show
that the product is not contaminated by the heavier streams while refining. When the color of
the sample is > +25 then it is considered to be better than the color of the pure water whose
saybolt color is +24.
Determination of Flash Point by:
(ABEL CLOSED CUP METHOD)
Applicable to products: MS, MTO, ATF, SKO, HSD
Significance: This method is for determination of flash point of petroleum products and other
liquids ranging between -30°C and 70°C inclusive. Lowest temperature corrected to a
barometric pressure of 101.3 kPa at which application of a test flame causes the vapor to
ignite is the flash point. This method is suitable for products whose flash ranges between -
30°C to 70°C. Flash point is used in shipping, storage and handling and safety regulations as
a classification property to define ‘flammable’ and combustible materials. It also indicates
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
possible contamination of a sample by highly volatile material in a relatively non-volatile or

non-flammable material.
(PENSKY–MARTENS CLOSED CUP METHOD)
Applicable to products: FO, LDO, LSHS, Heavy Diesel, Bitumen

Measuring Range: This test method is applicable to petroleum products and other liquids,
which are having flash points ranging between 400C and 3600C.
Significance: It is one of the properties which must be considered to assess the overall
flammability hazard of the material. Flash point is a response to heat and an ignition source
under specified conditions in the laboratory but should not be used to appraise the fire hazard
or fire risk of a material. It may be used as an element pertinent to an assessment of the fire
hazard of a particular end use.
Determination of Kinematic and Calculation of Dynamic viscosity:
Applicable to products: ATF, JBO, LDO, HSD, FO, LSHS

Kinematic viscosity (γ) is the resistance to flow of a fluid under gravity.
Dynamic viscosity (ή) is the ratio between the applied shear stress & rate of shear of a liquid.
It is also called coefficient of dynamic viscosity or simply viscosity. Thus dynamic viscosity
is a measure of the resistance to flow or deformation of a liquid.
Significance and use: Viscosity is one of the most important heating oil characteristics. It is
indicative of the rate at which the oil flows in fuel systems and the ease with which it can be
atomized in a given type of burner. With improper viscosity at the burner tip, carbon
deposition on the walls of the fire box or other conditions, leading to poor combustion will
occur. Difficulties in moving the oil in fuel oil systems will be encountered below the
temperature at which the viscosity is reached.
Determination of Salt Content in Crude Petroleum:
Applicable to products: Crude

Significance: Excessive salt in the crude oil will result in higher corrosion in the process of
refining. Knowledge of it is useful to decide desalting requirements.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
Determination of Pour Point:
Applicable to products: JBO, LDO, HSD, FO, LSHS

Pour point: It is the lowest temperature at which a sample of petroleum product will
continue to flow when it is cooled under specified conditions. Pour point of a product
indicates its ease of handling at low temperatures.
Determination of Carbon Residue by RAMSBOTTOM METHOD:
Applicable to products: LDO, HSD, FO, LSHS

Carbon residue: The residue formed by evaporation and thermal degradation of a carbon
containing material.
Significance: The carbon residue value of a fuel oil is a rough approximation of its tendency
to form deposits on the burners. In case of motor oils the value was once regarded as direct
indication of its tendency to form carbon deposits in the combustion chamber of the engine.
Additives may increase the value of carbon residue but they will decrease the tendency to
form the carbon deposits. In case of gas oils it is a guide in the manufacturing of gas.
Distillation Characteristics:
Applicable to products: Naphtha, MS, MTO, ATF, SKO, HSD, JBO

The distillation (volatility) characteristics of hydrocarbons have an important effect on their
safety in handling and performance, especially in case of fuels and solvents. The boiling
range gives important information on composition and behavior during storage and use.
Limiting values are applied in the end –use performance and to regulate the formation of
vapors which may form explosive mixtures with air or otherwise escape into the atmosphere
as emissions.
Definitions:
I.B.P: It is the temperature (corrected) observed at the instant that the first drop of condensate
falls from the lower end of condenser tube.
E.P/F.B.P.: It is the maximum thermometer reading (corrected) obtained during the test. This
usually occurs after the evaporation of all liquid from the bottom of the flask.
Corrosiveness of Copper Strip:
Applicable to products: LPG, MS, SKO, ATF, MTO, HSD

Significance: Hydrogen sulfide is one of the sulfur compounds present, in the refined
products, having highly corrosive nature. Copper corrosion is an indication of the nature of
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
the product to corrode the storage containers and other metal tubes during various operations
and handling of petroleum products.
It is reported as 1A, 1B, 2A, 2B. Up to 4D
Conradson Carbon Residue:
Applicable to products: Heavy petroleum products

Significance: R.C.R. as discussed is preferred method for the samples that are mobile below
90°C and for other samples like heavy residue fuels, Coker feed stocks etc., C.C.R. is
preferred.
Determination of Needle Penetration:
Applicable to products: Bitumen

Penetration of a bituminous material is its consistency expressed as the distance in tenths of a
millimeter that a standard needle penetrates vertically into a specimen of the material under
specified conditions of temperature, load and duration of loading.
The usual temperature is 25 0C, applied load is 100gm and the time traversed by the needle is
5 seconds. It is used as a measure of consistency. Higher values of penetration indicate softer
material.
Determination of Softening Point:
Applicable to products: Bitumen

Softening point is the temperature at which the substance attains a particular degree of
softening under specified conditions.
Significance: Softening is a measure of consistency or the hardness of the bitumen sample.
Bitumenous materials do not change from the solid state to the liquid state at any definite
temperature but gradually become softer and less viscous as the temperature rises. For this
reason determination of the softening point must be made by a fixed arbitrary and closely
defined method.
WATER:
Determination of pH:
It is the logarithm of reciprocal of hydrogen ion concentration.

Significance: Values below 7 and approaching 0 are increasingly acidic. Similarly values
higher than 7 and approaching 14 are increasingly basic. pH is a measure of relative acidity
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
or alkalinity of a sample. pH indicates corrosive tendency of a sample. Low pH causes

corrosion of equipment and pH higher than 8 causes sludge formation. pH values are to be
maintained as per design values.
Determination of Alkalinity:
Alkalinity is due to presence of bicarbonates, carbonate and hydroxide ion. In lab, P & M
alkalinity are measured.
Determination of Conductivity:
This helps in detection of ionized impurities dissolved in condensed steam, BFW etc. This is
a simple blow down control parameter.
Determination of Chlorides:
The chlorides of Ca, Na and Mg are very soluble in water. Hence during usage in boilers etc
their precipitation will not take place.
Determination of Iron:
Iron will get precipitated out of solution. Scale formation may be due to deposition from
water or washing away of metal surface.
Determination of Silica:
Presence of silica is objectionable as it forms hard dense scales which have high resistance to
heat transfer. In addition to scale formation, it also gets deposited on turbine blades, resulting
in lowered turbine efficiency. As silica is relatively inert, it can not be precipitated like other
inorganic materials. This can be removed by basic anion exchange.
Total Hardness:
Hardness of water is the amount of Ca & Mg salts present. Hardness of water is undesirable
due to its scale forming nature. Also in evaporation surfaces, harness leads to sludge
formation.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
Total Dissolved Solids (TDS):
This indicates the concentration of dissolved impurities in water sample. This parameter
helps in controlling the blow down.
Oil & Grease:
Oil contamination can occur in treated water due to pump seal leaks etc. As oil floats it can
not be removed by blow down. This impurity if gets deposited on heating surface leads to
reduction of heat transfer efficiency. This may lead to localized heating and tube rupture.
Floating oil on the surface causes entrainment.
NOTE: For the tests required for every product and their significance, refer to the HOD
guidelines Vol. 1.
LAB SAMPLING
Testing Details:
SRN
RVP -------------------------------------- < 7 psi
H2S -------------------------------------- Absent
Color -------------------- --------------- + 30 min
KERO
Saybolt Color -------------------------- +20 min
Flash ------------------------------------ 37 0C min
End Point ------------------------------- 290 0C
MTO/
Saybolt Color -------------------------- +25 min
Flash ------------------------------------- +32 min 0C
IBP --------------------------------------- 130 min 0C
FBP -------------------------------------- 230 max 0C
ATF
Saybolt Color --------------------------- +15 min
Flash ------------------------------------- 38 min 0C
EP --------------------------------------- 250 max 0C
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
DSL
ASTM COL ----------------------------- < 2
Flash ------------------------------------- > 100 0C
POUR ------------------------------------ < +15
Recovery 85/95 % -------------------- 350/370 0C (BS-II HSD regulation)
95 % ------------------------------------ 360 0C (EURO – III HSD regulation)
Density ----------------------------------- 0.82 – 0.86 (BS-II HSD regulation)
----------------------------------- 0.82 – 0.845 (EURO – III HSD regulation)
BITUMEN
PEN (mm) ------------------------------ 80-100
------------------------------ 60 -70
SR
Flash ------------------------------------ 180 min 0C
FRESH CRUDE (MON/WED/FRI/SUN)

SALT ----------------------------------- 140 ppm max
S&W ------------------------------------- % vol 0.15 max
Desalted crude
SALT ------------------------------------ 5 ppm max
S&W ------------------------------------ % vol 0.05
ATMOS WATER
pH ---------------------------------------- 5.5-6.5
Cl ----------------------------------------- <20 ppm
Fe ------------------------------------------ 0.3 wt% max
HOTWELL WATER
pH ----------------------------------------- 5.5-6.5
Cl ------------------------------------------ <20 ppm
Fe ------------------------------------------ 0.3 max wt%
WASH WATER
pH ------------------------------------------ 5.0-8.0
Cl ------------------------------------------ 100 ppm max
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 24
PLANT NAME: CDU II
Chapter Rev No: 0
EFFLUENT WATER
pH ----------------------------------------- > 7.0
OIL (ppm) ------------------------------- 100 max
Si ------------------------------------------ <0.5 ppm
TDS -------------------------------------- <1500 ppm
Note:
Time Period:
Regular samples: 07:00 hrs /19:00 hrs
Special Samples: 07:00 hrs / 11:00 hrs / 15:00 hrs / 19:00 hrs / 23:00 hrs / 03:00 hrs.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
LIST OF PLANT EQUIPMENTS
25.1 HEAT EXCHANGERS: SHELL SIDE DATA:
EQPT NO. DUTY FLUID QTY SP.GR DG.PR OP.PR OP. D.P AREA
MMKCal Kg/hr @15 C Kg/cm 2 Kg/cm2 TEMP c Kg/c m2/shl
*1000 g g IN/OUT m2g
/hr
11-E-01 1.10 CRUDE 367.6 0.848 30.7 23.8 30/35 0.7 119
11-E-02 2.12 CRUDE 367.6 0.848 30.7 23.1 35/44 0.7 119
11-E-03 3.39 CRUDE 367.6 0.848 30.7 22.4 044/060 0.7 200
11-E-04A/B 7.40 CRUDE 367.6 0.848 30.7 21.7 060/095 1.4 298
11-E-05 3.43 CRUDE 367.6 0.848 30.7 20.7 095/112 0.7 200
11-E-06 1.46 CRUDE 367.6 0.848 30.7 20.0 112/118 0.7 200
11-E-07 1.44 CRUDE 367.6 0.848 30.7 19.3 118/125 0.7 119
11-E-08 0.58 CRUDE 183.3 0.848 40.0 35.0 120/126 0.7 48
11-E-09 3.89 KERO CR 333.4 0.810 13.4 09.7 208/191 0.7 200
11-E-10 0.88 CRUDE 183.8 0.848 40.0 33.6 161/168 0.7 48
11-E-11 3.89 KERO CR 190.2 0.810 13.4 10.7 241/210 0.7 335
11-E-12 1.52 DIESEL 066.1 0.853 15.0 10.6 250/218 0.7 331
11-E-13 1.13 DIESEL CR 135.1 0.853 11.2 08.6 277/257 0.7 156
11-E-14A/B 1.78 DIESEL 066.1 0.853 15.0 11.3 288/250 1.4 156
11-E-15A/B 3.00 DIESEL CR 135.1 0.853 11.2 09.6 307/277 1.4 156
11-E-16 1.44 CRUDE 183.8 0.848 40.0 28.8 278/290 0.7 156
11-E-17A-H 25.3 NAPTHA 114.6 0.670 04.8 02.3 128/45 0.4 230
11-E-18 1.37 DES. WATER 125.0 1.00 21.6 16.1 070/125 0.7 36
11-E-19A/B 2.36 STAB.FEED 057.8 0.667 24.9 18.6 045/110 0.7 82
11-E-20A-D 2.89 LPG 033.7 0.555 14.0 07.6 060/040 0.3 186
11-E-21 1.13 NAPTHA 049.2 0.684 14.2 08.2 082/043 0.7 167
11-E-22 1.19 LVGO CR 029.2 0.891 12.0 09.2 184/070 0.7 85
11-E-22A 1.19 LVGO CR 029.2 0.891 12.0 09.2 184/070 0.7 223
11-E-23 1.67 DIESEL 066.1 0.853 15.0 09.2 080/043 0.7 335
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
11-E-23A 1.67 DIESEL 066.1 0.853 15.0 09.2 080/043 0.7 335
11-E-24 1.01 KEROSENE 067.5 0.810 15.0 07.8 070/043 0.7 167
11-E-24A 2.05 KEROSENE 060.0 0.810 15.0 09.2 085/043 0.24 283
11-E-25 3.21 STAB.BOT 140.89 0.684 14.0 07.9 155/160 0.1 243
11-E-26 0.72 HN 018.7 0.772 10.7 07.0 060/043 0.7 36
11-E-40A/B 4.90 CIRC. OIL 065.0 0.930 15.2 11.5 395/285 0.54 242
12-E-02 2.20 CRUDE 183.3 0.848 40.0 33.5 164/184 0.7 178
12-E-03 3.60 SR 112.0 1.020 28.7 300/250 0.7 311
12-E-04 3.19 CRUDE 183.8 0.848 40.0 32.1 213/241 0.7 311
12-E-05A/B 3.48 HVGO CR 126.4 0.921 16.0 315/276 0.7 114
12-E-06A/B 2.24 CRUDE 183.8 0.848 40.0 30.7 271/290 1.0 242
12-E-07A 3.90 HC+STEAM 8.39 - 1.5 71mm 250/65/3 3.2m 963
5 m
12-E-07B 3.00 HC+STEAM 5.975 - 1.5 240mm 218/60/4 2.0m 120
5 m
12-E-07C 2.78 HC+STEAM 5.409 - 1.5 812mm 247/60/4 2.0m 120
5 m
12-E-08A 2.14 TEMP.WATE 179.4 1 06.2 072/060 - 122
R
12-E-08B 8.24 TEMP.WATE 154.8 1 06.2 090/050 - 330
R
12-E-09A-D 2.63 SR 083.5 1.020 28.7 154/40 1.0 242
12-E-10 4.42 STEAM 007.0 19.0 11.5 160/189 120
12-E-10A 4.42 STEAM 007.0 19.0 11.5 160/189 120
12-E-11 0.96 LVGO 11.5 0.891 12.5 213/070 43
12-E-12A/B 6.46 HVGO 63.0 0.920 16.0 242/070 167
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
TUBE SIDE DATA:
EQPT NO. FLUID QTY SP.G DG.P OP.PR OP. PASS D.P TUBES
Kg/hr Kg/hr R R Kg/cm2g TEMP C Kg/c
*1000 @15 Kg/cm IN/OUT m2g
2
C g
11-E-01 HY NAPTHA 18.7 0.772 10.7 08.6 141/43 08 0.7 320
11-E-02 KEROSENE 67.3 0.810 13.5 09.9 121/70 04 0.7 320
11-E-03 DIESEL 66.1 0.853 15.0 08.5 167/80 06 0.7 540
11-E-04A/B TPA 333.6 0.694 10.2 08.3 131/91 02 1.4 800
11-E-05 KEROSENE 0.7 0.810 13.5 10.6 201/121 06 0.7 540
11-E-06 DIESEL 66.1 0.853 15.0 09.2 204/167 06 0.7 540
11-E-07 LVGO CR 29.2 0.891 12.6 08.9 213/136 06 0.7 320
11-E-08 DIESEL 66.1 0.853 15.0 09.9 218/204 02 0.7 128
11-E-09 CRUDE 183.8 0.848 40.0 34.3 126/161 04 0.7 540
11-E-10 KERO 67.4 0.810 13.5 11.3 219/201 02 0.7 128
11-E-11 CRUDE 183.8 0.848 40.0 32.9 168/205 04 0.7 898
11-E-12 CRUDE 183.8 0.848 40.0 32.2 205/218 04 0.7 850
11-E-13 CRUDE 183.8 0.848 40.0 31.5 218/235 02 0.7 420
11-E-14A/B CRUDE 183.8 0.848 40.0 30.5 235/252 02 1.4 420
11-E-15A/B CRUDE 183.8 0.848 40.0 29.5 252/278 02 1.4 420
11-E-16 SR 111.9 1.020 28.7 16.4 350/331 04 0.7 420
11-E-17A-H SEA WATER 146. 0.677 05.0 02.0 032/045 02 0.7 619
11-E-18 LP STEAM 2.7 - 07.0 03.5 147/147 02 0.7 052
11-E-19A/B SEA WATER 49.2 0.683 14.0 07.9 155/82 02 0.7 220
11-E-20A-D SEA WATER 361.7 1.00 05.0 02.0 32/40 02 0.7 500
11-E-21 SEA WATER 102.9 1.00 05.0 03.0 32/40 04 0.7 450
11-E-22 SEA WATER 91.2 1.00 05.0 03.0 32/45 02 0.7 228
11-E-22A SEA WATER 91.2 1.00 05.0 03.0 32/45 02 0.7 600
11-E-23 SEA WATER 108.0 1.00 05.0 03.0 32/45 06 0.7 900
11-E-23A SEA WATER 108.0 1.00 05.0 03.0 32/45 06 0.7 900
11-E-24 SEA WATER 91.9 1.00 05.0 03.0 32/45 04 0.7 450
11-E-24A SEA WATER 115.0 1.00 05.0 02.0 32/45 04 0.4 750
11-E-25 KERO CR 143.2 0.810 14.0 11.4 241/207 02 0.7 450
11-E-26 SEA WATER 16.1 1.00 05.0 03.0 32/43 06 0.5 382
11-E-40A/B CRUDE 397.0 0.828 40.0 19.0 260/271 02 0.9 650
12-E-01A-C CRUDE 183.8 0.848 40.0 34.0 120/164 02 1.5 850
12-E-02 HVGO CR 126.4 0.921 16.0 - 276/253 04 0.7 210
12-E-03 CRUDE 183.8 0.848 40.0 32.8 181/213 04 0.7 850
12-E-04 HVGO 63.1 0.921 16.0 - 315/242 06 0.7 850
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
12-E-05A/B CRUDE 183.8 0.848 40.0 31.4 241/271 02 0.7 470

12-E-06A/B SR 112.0 1.020 28.7 - 331/300 04 1.0 650
12-E-07A SEA WATER 1000. 1000. 05.0 02.0 32.1/36.1 03 0.3 2600
0 0
12-E-07B SEA WATER 750.0 750.0 05.0 01.5 36.1/40.1 02 0.3 1050
12-E-07C SEA WATER 250.0 250.0 05.0 01.5 36.1/47.2 02 0.3 390
12-E-08A SEA WATER 356.6 - 05.0 03.0 032/045 02 0.7
12-E-08B SEA WATER 329.0 - 05.0 03.0 032/045 02 0.7
12-E-09A-D TEM. WATER 65.0 1.00 05.0 - 060/085 04 1.0 650
12-E-10 HVGO CR 126.3 0.92 16.0 - 253/230 04 0.7 260
12-E-10A HVGO CR 126.3 0.92 16.0 - 253/230 04 0.7 260
12-E-11 SEA WATER 73.4 - 05.0 03.0 032/045 02 0.7 116
12-E-12A/B SEA WATER 99.5 - 05.0 03.0 032/045 02 0.7 450
25.2 PUMPS: (motors/turbines)
Service FLOW (m3/hr) Discharge Avail Operating FLC KW

Pump Max Min Normal Pressure NPSH Temp (amp)/
Number (kg.f/cm2) (mts.) (oC) (RPM)
10-PM-01A/B CAUSTIC CR 30.0 12.0 25.0 7.30 5.0 40 14.0 7.5
10-PM-03A/B WATER 30.0 12.5 25.0 7.30 5 40 25.2 7.5
11-F-01 FD - - - - 160 90
11-FM-01 - Ambient
FAN
11-F-02 ID - - - - 34 150
11-FM-02 -
FAN
11-PM-01A CRUDE 114 550
482.0 219.0 438.0 23.45 6.0 30
CHARGE
11-PT-01B Feed turbine 482.0 219.0 438.0 23.45 6.0 30 5522
CRUDE 114 500
11-PM-02A 515.0 234.0 468.0 33.60 6.0 120
BOOSTER
11-PT-02B PFD TURBINE 515.0 234.0 468.0 33.60 6.0 120 3120
DIESEL 97 55
11-PM-03A/B 137.0 51.0 102.0 11.30 3.8 228
PROD.
11-PM-04A/B KERO. PROD. 128.0 52.0 105.0 10.40 6.0 219 97 55
11-PM-05A/B HN 36.0 14.0 28.0 8.60 6.0 141 27 15
11-PM-06A TOP REFLUX 250.0 89.0 178.0 18.5 3.5 45 43 200
Top reflux 2970
11-PT-06B 250 89 178 18.5 3.5 45
turbine
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
11-PM-07C/D DIESEL CR 280.0 425.0 10.10 7.1 307 218 132

11-PM-08A KERO. CR 643.0 268.0 536.0 11.40 10.5 241 43.5 200
KERO CR 2950
11-PT-08B 643.0 268.0 536.0 11.40 10.5 241
turbine
KERO. CR 236 145
11-PM-08C/D ---- ---- 625.0 12.5 AMPLE 190
BOOSTER
11-PM-09A/B TPA 699.0 291.0 583.0 9.00 7.6 131 224 125
11-PM-10A/B RCO 232.0 83.0 200.0 11.00 3.4 343 152 90
11-PM-11A/B LPG/ REFLUX 80.0 21.0 66.0 14.60 3.2 40 63 55
11-PM-12A/B DES. WATER 25.0 6.0 15.0 17.10 6.0 30 63 37
11-PM- CAUSTIC 1.1 0.28
75* ---- - 15.00 3.0 30
13A/B/C INJECT.
11-PM- AMMON. 1.1 0.38
20* ---- - 15.00 3.0 30
14A/B/C INJECT.
CORR. 1.1 0.38
11-PM-15A/B 10* ---- - 14.00 3.0 30
INHIB.
11-PM-16A/B DMF 12* ---- - 10.00 ---- 45 1.3 0.18
11-PM-18A CBD ---- ---- 40.0 6.00 FLOOD 80 62 37
12-F-01 FD 53 45
12-FM-01 - - - - - ambient
FAN
12-F-01ID 80 45
12-FM-02 - - - - - -
FAN
12-PM-01A/B SR 174.0 30.0 133.0 22.30 4.1 350 49.7 200
12-PM-02A/B SLOP CUT 32.0 12.0 24.0 17.00 >6.0 385 97 55
12-PM-03A/B HVGO 400.0 211.0 333.0 11.22 9.0 315.0 43.5 200
12-PM-04A/B LVGO 109.0 42.0 85.0 8.90 10.0 213 137 55
HOTWELL 18 9.3
12-PM-05A/B 3.0 ---- 3.0 7.0 4.0 45
OIL
HOTWELL 78 15
12-PM-06A/B 15.0 ---- 6.0 7.0 4.0 45
WATER
TEMP. 62 17
12-PM-07A/B 200.0 87.5 175.0 4.80 5.5 60
WATER
12-PM-08A/B Vac Neutralizer 25.0 0 ---- ---- ---- ----
Note: * =Chemical Injection Pumps flow rate is in litres/hr.

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
Details of Lube oils used in the pumps:
Pump Number Service Pump side Turbine side Remarks

lube oil lube oil
10-PM-01A/B CAUSTIC CR T-68 -
10-PM-03A/B WATER T-68 -
11-FM-01 11-F-01 FD FAN T-68 -
11-FM-02 11-F-02 ID FAN T-68 -
11-PM-01A CRUDE T-68 -
CHARGE
11-PT-01B Feed turbine T-68 T-77
CRUDE T-68 -
11-PM-02A
BOOSTER
11-PT-02B PFD TURBINE T-68 T-77
11-PM-03A/B DIESEL PROD. T-68 -
11-PM-04A/B KERO. PROD. T-68 -
11-PM-05A/B HN T-68 -
11-PM-06A TOP REFLUX T-68 -
Top reflux T-68 T-77
11-PT-06B
turbine
11-PM-07C/D DIESEL CR T-68 -
11-PM-08A KERO. CR T-68 -
KERO CR T-68 T-77
11-PT-08B
turbine
KERO. CR T-68 -
11-PM-08C/D
BOOSTER
11-PM-09A/B TPA T-68 -
11-PM-10A/B RCO T-68 -
11-PM-11A/B LPG/ REFLUX T-68 -
11-PM-12A/B DES. WATER T-68 -
CAUSTIC T-68 -
11-PM-13A/B/C
INJECT.
AMMON. T-68 -
11-PM-14A/B/C
INJECT.
CORR. T-68 -
11-PM-15A/B
INHIB.
11-PM-16A/B DMF T-68 -
11-PM-18 CBD T-68 -
12-FM-01 12-F-01 FD FAN T-68 -
12-FM-02 12-F-01ID FAN T-68 -
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
12-PM-01A/B SR T-68 -
12-PM-02A/B SLOP CUT T-68 -
12-PM-03A/B HVGO T-68 -
12-PM-04A/B LVGO T-68 -
12-PM-05A/B HOTWELL OIL T-68 -
HOTWELL T-68 -
12-PM-06A/B
WATER
12-PM-07A/B TEMP. WATER T-68 -
12-PM-08A/B Vac Neutralizer T-68 -
25.3 COLUMNS:
11-C-01 Atmospheric Column

11-C-02 Heavy Naphtha Stripper
11-C-03 Kerosene Stripper
11-C-04 Diesel Stripper
11-C-05 Naphtha Stabiliser
12-C-01 Vacuum Column
25.4 VESSELS:
Tag No Description Operating Temp (C) Operating Pressure (Kg/cm2g)

PG BH PG BH
10-V-01 Naphtha Caustic Wash 40 40 6.5 6.5
10-V-02 Naphtha Water Wash 40 40 5.5 5.5
11-V-01 Overhead Naphtha 44 44 2.0 2.0
Accumulator
11-V-02 Crude Desalter 129 136.5 14.0 14.0
11-V-03 Stabilizer Reflux 40 40 8.0 8.0
Drum
11-V-04 Desalting Water 50-70 50-70 Atmospheric Atmospheric
Vessel
11-V-05 Decoking Drum 100 100 Atmospheric Atmospheric
11-V-06A/B Ammonia Vessels Ambient Ambient Atmospheric Atmospheric
11-V-07A/B Caustic Drums Ambient Ambient Atmospheric Atmospheric
11-V-08 CBD Drum 40-150 40-150 Atmospheric Atmospheric
11-V-10 PFD 250-275 250-280 8-15 3.5-9
12-V-01 Hot Well Drum 44 44 Atmospheric Atmospheric
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0
12-V-02 Tempered water drum 60-80 60-80 Atmospheric Atmospheric

12-V-03 Steam Blow Down 100 100 Atmospheric Atmospheric
Drum
Demulsifier drum Ambient Ambient Atmospheric Atmospheric
Corrosion Inhibitor Ambient Ambient Atmospheric Atmospheric
CDU-II PSV LIST
S NO Tag Number Description Set Pressure

(Kg/cm2 g)
1. 10-PSV-101 10-V-01 SRN CAUSTIC WASH 14.00
2. 10-PSV-102 10-V-02 SRN CAUSTIC WASH 14.00
3. 11-PSV-101 11-V-02 DESALTER 12.50
4. 11-PSV-301 11-F-01 SUPERHEATED STEAM OUTLET 14.00
5. 11-PSV-302 11-F-01 SUPERHEATED STEAM OUTLET 14.00
6. 11-PSV-401A 11-C-01 ATMOS DISTILLATION COLUMN 4.80
7. 11-PSV-401B 11-C-01 ATMOS DISTILLATION COLUMN 4.80
8. 11-PSV-401C 11-C-01 ATMOS DISTILLATION COLUMN 4.80
9. 11-PSV-403 11-V-01 ATMOS. ACCUMULATOR 5.30
10. 11-PSV-501 11-C-05 NAPHTHA STABILIZER 14.00
11. 11-PSV-502 11-V-03 STABILIZER REFLUX DRUM 14.00
12. 11-PSV-601 11-V-06 AMMONIA TANK 2.50
13. 11-PSV-603 11-P-13A CAUSTIC SOLUTION PUMP 19.00
14. 11-PSV-604 11-P-13B CAUSTIC SOLUTION PUMP 19.00
15. 11-PSV-606 11-P-14 AMMONIA SOLUTION PUMP 19.00
16. 11-PSV-608 11-P-15 CORROSION INHIBITOR PUMP 19.00
17. 11-PSV-609 11-P-16 DE EMULSIFIER PUMP 11.30
18. 11-PSV-701 11-P-17A SEA WATER BOOSTER 12.47
19. 11-PSV-702 11-P-17B SEA WATER BOOSTER 12.47
20. 120-PSV-1201A PFD RV 25.5
21. 120-PSV-1201B PFD RV 25.5
22. 12-PSV-202 12-C-01 VACUUM DISTILLATION COLUMN 3.50
23. 12-PSV-202B 12-C-01 VACUUM DISTILLATION COLUMN 3.50
24. 12-PSV-203 12-E-07A EJECTOR CONDENSER 1.50
27. 12-PSV-206 12-E-07B EJECTOR CONDENSER 1.50
30. 12-PSV-209 12-E-07C EJECTOR CONDENSER 1.50
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 25
PLANT NAME: CDU II
Chapter Rev No: 0

33. 12-PSV-301 12-E-10 HVGO CR STEAM GENERATOR 13.50
34. 12-PSV-301A 12-E-10A STEAM GENERATOR 13.50
35. 12-PSV-301B 12-E-10A STEAM GENERATOR 13.50
36. 12-PSV-302 12-E-10 HVGO CR STEAM GENERATOR 13.50
25.5 CDU-II TSV LIST
S NO Tag Number Description Set Pressure

(Kg/cm2 g)
37. 11-PSV-703 LP STEAM TO PUMP SEAL 1.48
38. 11-STV-001 11-PT-01 CRUDE CHARGE PUMP 4.87
39. 11-STV-002 11-PT-02 CRUDE BOOSTER PUMP 4.87
40. 11-STV-003 11-PT-06 ATMOS. COLUMN REFLUX PUMP 4.87
41. 11-STV-004 11-PT-08 KERO CR PUMP 4.87
42. 11-TSV-101 11-E-22 COOLER SW OUTLET 4.40
43. 11-TSV-102 11-E-26 HN COOLER SW OUTLET 4.40
44. 11-TSV-103 11-E-07 SHELL OUTLET 12.10
45. 11-TSV-201 11-E-21 SRN COOLER SW OUTLET 4.40
46. 11-TSV-202 11-E-23 DIESEL COOLER SW OUTLET 4.40
47. 11-TSV-203 11-E-24 KERO COOLER SW OUTLET 4.40
48. 11-TSV-204 11-E-16 CRUDE/SR SHELL OUTLET 35.10
49. 11-TSV-303 12-E-01 CRUDE/SR CRUDE OUTLET 35.20
50. 11-TSV-401 ATMOS. O/H CONDENSER SW OUTLET 4.40
53. 11-TSV-501 11-E-20A SW OUTLET 4.40
54. 11-TSV-502 11-E-20C SW OUTLET 4.40
55. 12-TSV-201 Vac. o/h condensers SW outlet 12-E-07B 4.4
56. 12-TSV-202 Vac. o/h condensers SW outlet 12-E-07A 4.4
57. 12-TSV-304 12-E-02 CRUDE/HVGO CRUDE OUTLET 35.20
58. 12-TSV-305 12-E-03 CRUDE/SR CRUDE OUTLET 35.20
59. 12-TSV-306 12-E-04 CRUDE/HVGO SHELL OUTLET 35.20
60. 12-TSV-308 12-E-05 CRUDE/HVGO SHELL OUTLET 35.20
61. 12-TSV-403 12-E-08A TEMP. WATER COOLER 4.40
62. 12-TSV-404 12-E-08B TEMP. WATER COOLER 4.40
63. 12-TSV-404 12-E-11 LVGO COOLER SW OUTLET 4.40
64. 12-TSV-405 12-E-12A HVGO COOLER SW OUTLET 4.40
65. 12-TSV-407 12-E-12B HVGO COOLER SW OUTLET 4.40
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
PLANT CHEMICALS
26.1 CHEMICALS WITHDRAWAL MANAGEMENT (FROM WARE HOUSE)

AND MINIMUM QUANTITY:
The monthly requirement for CDU-II for various chemicals is shown below (no chemical is
used in BBU). An inventory corresponding to 30 days chemical consumption (buffer stock) is
to be always maintained in the field at any point of time. The details are as follows:
SL. Generic Name Approved Considered quantity for 30 days inventory

No. Chemical Name withdrawal from Stores needs to be
every month maintained at
field (Kg) approx.
Kg/ Month No. of drums
(approx.)
D 9004 2177 11 2200
1. Demulsifier EC2040A 1512 8 1600
DM 101 2722 14 2800
Embreak 2W157
- HS Case 1240 6 1200
- LS Case 696 3 600
2. Filmer Nalco EC1021A 411 2 360
(Atmos ) ESK50 1512 8 1440
Philmplus 5K7 423 2 360
Thermosol V 472 3 540
3. Neutralizer Ammonia 605 12 600
4. Caustic Caustic 1512* - 1800*
o
* Caustic is obtained from MEROX Plant as 15 % (20 Be) solution which is directly used
for naphtha-caustic wash and for dosing in crude after dilution with water to 3 % (5 oBe)
solution.
Note:
1. Information to be given by Operations to PAD in case any chemical consumption
increases above or below the recommended quantities.
2. Information to be given by Materials to PAD in case of change in any proprietary
chemical for usage in CDUs.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
26.2 MAXIMUM ALLOWABLE STORAGE OF CHEMICALS IN THE

REFINERY:
CHEMICAL STORAGE ALLOWABLE (MT)

Anhydrous Ammonia 9.099
Caustic 100% 327
Corrosion Inhibitor (EC1020A) 0.39
Corrosion Inhibitor (Eloguard) 5.4
Corrosion Inhibitor (NALCO 5186) 7.344
Demulsifier (EC2040A) 10.656
26.3 STORAGE PRECAUTIONS:
26.3.1 Storage in Tanks:
• The tanks should be located so as not to pose safety problems due to leakage and
reaction with other chemicals stored nearby. The environment at the location must be
compatible with the chemical stored.
• The tanks should be fitted with vents/relief systems of adequate capacity discharging
to a safe height. Capacity requirement in case of high vapor evolution resulting from
heating due to fire of adjacent tank also should be considered. Wherever atmospheric
release of the vapor is not advisable, the relief should be routed to a neutralizing
system.
• The vents of atmospheric storage tanks should contain flame arrestors for Class A
chemicals (flash point less than 23°C). The location of flame arrestor must be easily
accessible for a periodic inspection to ensure that flame arrestor is free of any
choking.
26.3.2 Storage of Chemicals in drums/Other Containers:
The chemical drum storage of hazardous chemicals (liquids) pose potential hazard
compared to tank/bulk storage due to the following:
• The drums normally being less resistance to fire would collapse faster escalating and
spreading of fire to other drums of the stack.
• Each drum of a cluster of drums can become a source of leakage.
Basis the above, ensure the following while handling chemical drum/other containers:
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
• Periodic site inspection should be carried out to ensure that there is no leakage from
any of the drums.
• Where combustible solid materials are stored, the dust content of the air must be kept
below the lower explosive limit. Efficient dust collection system and good house
keeping should be followed.
26.3.3 Storage of Compressed Gas Cylinders:
The nature of chemical gas apart, the high pressure of storage amplifies the hazard of
the storage gas cylinders. The following guidelines shall be ensured for storage of
cylinders.
• Cylinders containing flammable gases and toxic gases shall be kept separated from
each other and from cylinders containing other types of gases be an adequate distance
or by a suitable partition wall.
• For inflammable gases, the cylinder storage area should be made of non-combustible
materials and flameproof fittings should be used.
• Cylinder nozzle should be suitably protected against damage. Oil or similar lubricant
should not be used on valves or other fittings of cylinder containing gas.
• In case of liquefied gas like liquid nitrogen, the cylinders should be stacked vertical so
that in case of defective regulator only gas would escape.
• The floor level at storage area should be sufficiently above ground level to prevent
water logging and corrosion. Flooring of the storage areas should not be wet or
muddy.
• Periodic inspection of cylinders for ascertaining leakage should be made. Automatic
gas detectors where applicable should be provided at suitable points so that in case of
leakage, alarm is hooted at control room.
• Emergency kit, safety protective equipment and clothing should be available in the
close vicinity to storage area. Adequate and suitable fire extinguishers must be
available at site.
• Some of the other storage precautions for agents/chemicals used in refinery as

follows:
a) Oxidizing Agents: Oxidizing substances must be stored away from all flammable
materials even if they are only slightly flammable. Oxidizing material must be
kept away from substances which are reducing agents.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
b) Water Sensitive Substances: These substances react with water or steam to

produce flammable or explosive gases and evolve heat. For example, conc. acids
like sulfuric acid and conc. Alkali like sodium hydroxide react with water later to
evolve heat. Such materials must not be stored in areas where water flooding from
pipe leakages or leaky roofs can happen.
c) Toxic Materials: These substances must be stored in well ventilated areas,
preferably cool and certainly away from direct sun rays. Periodic checks should be
organized for all parts of storage areas.
d) Incompatible Chemicals: Incompatible chemicals should not be stored near each
other.
e) Corrosive Chemicals: The flooring of the area where corrosive chemicals are
stored shall be impervious and made of corrosion resistant materials.
• The inventory of all hazardous chemicals shall be stored as minimum as possible.

Attempt should be made to find suitable less hazardous alternate chemicals, to replace
hazardous chemical.
26.4 LOADING AND UNLOADING PROCEDURES:
• The tank truck should be in good condition with proper seal for contents.
• Driver should have all the relevant papers.
• CISF should have given the clearance for the vehicle.
• Permit is issued to driver and he is wearing proper PPE.
• MSDS and chemical handling procedures are available in field room.
• Area is barricaded and caution boards are displayed.
• Condition of hoses and other hardware is good.
• Receipt sample is collected and lad report is verified with vendor specification.
• Valves to be opened slowly and in case any leak is observed, abort the operation
immediately.
• Safety shower in the surrounding area has to be in working condition.
• In case of flammable chemicals, the prime mover (engine) should be kept off. The
tanker should be properly blocked from movement before connections are made for
unloading hazardous chemicals. The unloading point should be located at a safe
distance outside the storage dyke.
• Pressurizing with air/inert gas for unloading should be avoided. It is recommended to
use pumps/vacuum systems for unloading. Pumps should preferably be of seal less
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
type and valves should be of glandless type. Solid chemicals in bulk should be
handled with lifting machines and conveyors.
• Coupling used for connecting hose to tanker must be leak proof. Flange connections
are preferred. Where threaded connections are used, the threaded portion should be
properly preserved against corrosion/wearing of threads and thoroughly inspected
before connecting are made.
• The unloading hose should be devoid of cracks & blisters and should be capable of
withstanding whatever pressure developed during unloading operation. The hose
should be hydro-tested at a frequency guided by experience. Proper records of hydro-
test should be maintained.
• Provision of sample quantity of water/ neutralizing medium to take care of
leakage/spillage must be made. Also steam and inert gas hose stations must be
available at unloading point.
• The unloading systems should have facility to vent/drain the remaining chemical in
the hose to a suitable safe point. The hose should be kept blinded when hot in use.
The thermal safety valve discharging to safe disposal or handling facility should be
provided.
• Suitable protective clothing should be used while handling drums/containers and the
operator should position himself such that he is I the upwind direction so that even in
case of accidental release of chemical, he is safe.
• Manual handling of drums/containers/cylinders should be minimized. It is preferable
fork-lifters and suitable cradles are used to handle drums.
• Carboys/cylinders containing hazardous chemicals should not be subjected to impact.
26.5 EMPTY CONTAINER DISPOSAL:
• There should be a designated place for all empty drums and cylinders with proper
name plates indicating name and how many drums to be stored there. It has to be
ensured that all the empty drums/cylinders are reaching to designated place (scrap
yard).
• The empty drums are to be timely removed and they are made free of their contents
before being kept in safe place.
• The consumed cylinder valve should be fully closed first and then the process valve
has to be closed. Then the connection to be removed and put an “empty” label on the
cylinder and then stored in designated area.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
26.6 HANDLING PRECAUTIONS:
• The proper precautions are to be taken while loading and unloading, as discussed in
this chapter separately.
• Before handling any chemical, its MSDS should be thoroughly read and understood.
Also the emergency system to be followed in case of any leaks should be known.
• Proper PPE should be used before handling any chemical and everyone should be
forced to follow the same.
• Every chemical injection pump must have a “drawdown cylinder” to facilitate
periodic dosing rate measurement and pump stroke adjustment accordingly.
• Every chemical storage tank must have necessary instruments to monitor its level,
pressure and temperature.
• Every tank should have a dyke of a suitable material (compatible with the chemical)
of volume equal to the volume of the larger storage tank. The dyke should have
facility to:
a) Drain off rain water into storm water channel.
b) Route high volume spillage/leakage to suitable neutralizing pit nearby.
c) Discharge safe effluent to oily water system, as applicable. The isolation valves on
dyke drains should be located outside the dyke.
d) Connections and openings to tank should be as less as possible so that the possibility
of leakage and maintenance hazards is minimized.
• Suitable breathing canisters and first aid box should be available at site for use in case
of emergency.
• The fire access roads provided to storage are should not be blocked and storage
tanks/area should have adequate fire protection and fire fighting facility.
• Adequate communication facility like PA system is available for interaction with
control room, fire station, medical unit and communication system is in working
condition.
• No loose cables or temporary electrical fittings should be used to prevent risk of open
spark.
• All the drums in use should be kept in a proper rack.
• Before charging any drum, it has to be ensured that sufficient ullage is there before
the filling is started.
• Drums should never be filled full with the liquid chemical and sufficient ullage to take
care of thermal expansion and provision to collect accidental spills for safe disposal
should be available.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
• As soon as the chemical is received from the stores, it should be ensured that it is the
right chemical and check for proper labeling, authenticity, etc.
• Due date should be checked for cylinder testing and if the date is over, the cylinder
should not be accepted.
• Periodic check should be done to ensure that there is no leakage from cylinder top or
body. The cylinder should not be dropped /bumped against any other cylinder or hard
object.
26.7 DESCRIPTION OF CHEMICAL DOSING SYSTEM:
Four process Chemicals are used in CDU-II. The name of the chemicals and their functions
are as below:
SL. Chemical Use of Chemical
No.
1 Demulsifier To facilitate proper separation of water and crude in
desalter by breaking emulsion formed between crude and
desalter wash water
2 Atmos and Vacuum O/H To maintain pH of column overhead liquid and minimize
Neutralizer corrosion.
3 Atmos and Vacuum O/H To prevent overhead corrosion by forming a protective
Filmer (Corrosion Inhibitor) film on the overhead pipe internal surface and prevent
direct contact of corrosive materials with the pipeline
metal.
4 Caustic 1. To neutralize Calcium and Magnesium chlorides
carried over in desalted crude.
2. For SRN Caustic wash to remove H2S from SRN.
26.7.1 Approved Chemicals for usage:

Following are the presently approved Process Chemicals/ brands for usage in CDU-II:
SL No Generic Name Brand Name

SM DYECHEM, D 9004
NALCO, EC 2040A
1. Demulsifier
ATSUAN, DM 101
EMBREAK 2W157
2. Atmos Overhead Neutralizer Ammonia
ESK 50
3. Atmos Overhead Filmer
NALCO, EC1021A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
SL No Generic Name Brand Name

PHILM PLUS 5K7
THERMOSOL V
4. Vacuum overhead Neutralizer Ammonia
5. Caustic Conventional Chemical
26.7.2 Location of Injection for Process Chemicals:
Following are the chemical injection locations.
SL No Process Chemical Injection Point

1. To crude line upstream of desalter (after 11-E-07)
a Demulsifier1
2. To crude line at crude feed pump (11-PM-01 A/B) suction
Atmos and Vacuum 1. To Column Top vapor line
b
O/H Neutralizer2 2. To Column Atmos Column Top Reflux return line
Atmos and Vacuum 1. To Column Top vapor line
c
O/H Filmer3 2. To Column Atmos Column Top Reflux return line
1. To desalted crude line downstream of desalter (at the suction of
d Caustic4 11-PM-02 A/B)
2. To crude line at crude feed pump (11-PM-01 A/B) suction
1
Provision for DMF (and wash water) injection in crude line at feed pump suction is to be
used only if salt content of fresh crude in > 50 ppm. Normal dosing shall be in crude line
upstream of desalter (after 11-E-07).
2
Provision for injection neutralizer or filmer in atmos column top reflux line (for 11-C-01) to
be used only if overhead corrosion is consistently high in spite of maintaining overhead
filmer as per norm. Normal dosing shall be in column overhead line.
3
Provision for caustic injection at crude feed pump suction to be used only if desalter effluent
pH is < 8.0. Normal caustic dosing in crude shall be at crude line downstream of desalter.
4 Caustic in subsequent sections refers only to caustic injection in crude.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
26.7.3 Chemical Diluents and their Ratios:
Usage details required for the chemicals are as follows:
SL Approved Chemical Diluent Dilution Ratio

Generic Name
No Name Medium (chem:diluent)
SM DYECHEM, D 9004 Water 1:3
NALCO, EC 2040A Water 1:3
1. Demulsifier
ATSUAN, DM 101 Water 1:3
Embreak 2W157 KERO 1:4
Atmos Overhead
2. Ammonia Water 4%
Neutralizer
ESK 50 1:3
Atmos Overhead NALCO, EC1021A 1:3
3. KERO
Filmer PHILM PLUS 5K7 1:3
THERMOSOL V 1:3
Vacc overhead
4. Ammonia Water 4%
Neutralizer
5. Caustic Conventional Chemical Water 3 % (5 oBe)
i. Norm for Chemical Injection:
Consumption norm for the above mentioned process chemicals are as follows:
Base Norm
Quantity of Quantity of Quantity of
of injection
SL Generic Approved neat chemical neat chemical neat chemical
w.r.t crude
No Name Chemical Name to be injected to be injected to be injected
feed rate
(Kg/Hr) (Kg/Day) (Kg/Month)
(wt-ppm)
D 9004 7.2 3.0 73 2177
EC2040A 5 2.1 50 1512
1. Demulsifier DM 101 9 3.8 91 2722

Embreak 2W157
4.1 1.7 41 1240
- HS Case
2.3 1.0 23 696
- LS Case
Atmos +
Vacuum
2. Ammonia 2 0.8 20 605
Overhead
Neutralizer
3. Atmos Nalco EC1021A 1.36 0.6 14 411
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
Base Norm
Quantity of Quantity of Quantity of
of injection
SL Generic Approved neat chemical neat chemical neat chemical
w.r.t crude
No Name Chemical Name to be injected to be injected to be injected
feed rate
(Kg/Hr) (Kg/Day) (Kg/Month)
(wt-ppm)
Overhead ESK50 5.0 2.1 50 1512
Filmer Philmplus 5K7 1.4 0.6 14 423
Thermosol V 1.56 0.7 16 472
4. Caustic Caustic 5* 2.1 50 1512
* Caustic in crude to be dosed as per requirement only. Caustic Dosage Rates for caustic
dosing guidelines is based on overhead chloride. 5 ppm is the max limit for caustic injection
irrespective of overhead chlorides content.
Note:
• Unit is considered to be in service for all the days in the month.
• Actual dosage to be recorded and monitored daily based on the daily consumption
of the chemical.
• Consumption figures are arrived at considering 420 TPH (500 m3/hr) of Crude
throughput. The same will vary based on actual crude throughput of the unit.
ii. Dosage Rates:

Dosing rates (along with diluents) for the above mentioned chemicals are as follows:
SL No Chemical Dosage Pump Number & Pump stroke
Rate Capacity (Lt/Hr) %
(Lt/Hr)
1. Demulsifier
D 9004 12.1 100
EC2040A 8.4 70
DM 101 15.1 11 PM 16 A/B 100, 25
Embreak 2W157 (12 Lt/Hr)
- HS Case 8.6 70
- LS Case 4.8 40
2. Atmos Overhead Filmer
EC1021A 2.3 20
ESK50 8.4 11 PM 15A/B 80
Philmplus 5K7 2.4 (10 Lt/Hr) 20
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
Thermosol V 2.6 25
3. 21 11PM14A/B/C 50
&
Ammonia
12PM 08A/B 50
(20 Lt/Hr)
Caustic Dosage Rates (3 % caustic solution) in Crude
Overhead Sweet Crude Case Sour Crude Case

Chlorides Neat Diluted Pump Neat Diluted Pump
(ppm) Caustic Caustic Stroke Caustic Caustic Stroke
(ppm) (LPH) (%) (ppm) (LPH) (%)
25 0 0 0 0 0 0
50 1 14 20 2 28 40
75 1.5 21 30 3.5 49 65
100 1.7 24 35 4.5 63 85
Note:
• Chemical dosing rates to be measured every shift using draw down cylinders and
pump stroke to be adjusted to meet the required dosing rate.
• It is assumed that the pump stroke of the pump follows a linear relationship with
flow
• Unit is considered to be in service for all the days in the month.
• Actual dosage to be monitored and consumption of the chemicals to be recorded
on daily basis.
• Dosages rates are arrived at considering 420 TPH (500 m3/hr) of Crude
throughput. The same is required to be varied based on actual crude throughput of
the unit and monitoring parameters (as mentioned in section 26.7.3.iii)
• After every batch of 3 % caustic solution preparation (for dosing in crude), caustic
strength is to be confirmed by sending sample to lab for checking strength.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
iii. Monitoring Requirements:

Target monitoring parameters are as follows:
SL Monitoring Allowable
Chemical Testing Schedule
No. Parameter Parameter Limit
Oil content in Desalter Daily Thrice
1 Demulsifier < 100 ppm
effluent Water (once in a shift)
Atmos Sour Water < 0.3 ppm
2 Atmos Filmer Once in 2 days
Iron
Atmos Daily Thrice
3 Atmos sour water pH 5.5-6.5
Neutralizer (once in a shift)
4 Vacuum Filmer Hot well Water Iron < 0.3 ppm Once in 2 days
Vacuum Daily Thrice
5 Hot well water pH 5.5-6.5
Neutralizer (once in a shift)
Caustic Atmos Overhead
6 <30 ppm Once in 2 days
(to crude) Chlorides
Caustic
7 H2S content in SRN 0 Twice Daily
(for SRN wash)
Note:
• Filmer dosing to be increased if iron content in overhead water is higher than
allowable limit. If iron content in overhead water is within limit, filmer injection
rate to be maintained as per recommended dosage rate.
• Demulsifier dosing rate to be increased if oil content in desalter effluent water is
higher than the allowable limit. If oil in desalter effluent water is consistently within
limit then demulsifier dosing can be reduced and may even be stopped, if necessary.
• Neutralizer injection to be varied in order to maintain overhead water pH content
within 5.5–6.5. In case of pH consistently higher than 6.5, neutralizer injection can
be stopped.
• In case of any monitoring parameter persists to be beyond the limit consistently, the
same is to be referred to PAD for any further analysis and recommendations.
• Caustic in crude to be injected as per guidelines provided under section 3.5.2
• Caustic to SRN caustic wash drum to be checked for strength (% availability) every
15 days. However, if SRN is reported to contain H2S, caustic strength to be checked
immediately and fresh batch to be loaded, if % availability of caustic in circulation
is < 25 % (strength <3.5 % or 5 oBe). Irrespective of H2S levels in SRN, caustic to
be dumped and fresh batch to be loaded once caustic strength falls below 3.5 % (5
o
Be).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
iv. Preparation for Chemical Dosing:
• The concerned plant technician should be familiar with procedure, physical and
chemical properties and respective MSDS of the chemical to be prepared for dosing
into the system, before starting the preparation of chemical.
• Proper PPE should be used and required safety precautions pertaining to that
chemical as mentioned in PPE safety manual and MSDS register should be
followed.
• The chemical should be prepared as per the standard procedure given in manager
instructions. After preparation of the chemical, proper data should be maintained in
the chemical inventory book and also the TOB. Any problems faced should also be
recorded in TOB.
• The records should always be maintained as soon as the preparation is done so that
any confusion is avoided.
• It has to be ensured that there is no wastage or spillage of chemical like pump leak,
flange leak, hose leak, etc., in the plant area. If any leak is observed then
immediately standby pump has to be placed in service.
• The dosing rates have to be measured /checked by draw down cylinder.
• Periodical cleaning of pumps strainer has to be done. Also for viscous chemicals,
suction lines may get plugged often and need to be unplugged.
Standing Instructions for Empty oil & chemical drums collection for washing(SI 23):
The following activity to be carried out on continuous basis as per the procedure given below
S.No Activity Record Responsibility

1. Maintain a record of full lube Enter in Chemical Field Technicians
oil/chemical drums received inventory register
2. Maintain a record of empty drums 1.Enter in unit waste log Field supervisor
after loading. Ensure that drums arebook
capped. 2.Raise job card for
cleaning of drums
3. Empty drums are to be labeled as Label the Empty drums Field Technicians
given below with respective stickers.
Empty oil based drums- Label type 1
Empty water based drums- Label
type 2
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 26
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT CHEMICALS
4. Mobilize and store the empty drums Segregate (Oil or water Field Technicians
at the designated area in field based) the drums at the
storage area
5. Arrange for lifting and transporting Issue work permit to Field supervisor
the empty drums to washing Maintenance
area(WWTP) as per routine schedule
6. Maintain a record of empty drums Enter in dispatched empty Field supervisor
dispatched for washing drums register.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
OCCUPATIONAL SAFETY AND HEALTH
27.1 CHEMICAL HAZARDS (MSDS):
HPCL-VR is determined to ensure that all the chemicals used are handled in a safe manner
and information on their toxicity and hazards are made available to the personnel involved in
handling the chemical. It will enable adequate safety planning and prevent accidents. This
manual termed as “MSDS Manual” contains the Material Safety Datasheets (MSDS) of all
the chemicals used by the refinery & the products manufactured by the Refinery.
For detailed MSDS of all the chemicals, refer to the MSDS manual available in the field
room or the same can be viewed or downloaded from VISAKH REFINERY portal. VR
Portal > Department > Technical > Process Safety Management Portal > MSDS Manual >
Chapter 2.
27.2 FIRST AID PROCEDURES:
27.2.1 Animal Bites:
In case of animal bites, the following action has to be taken:

• Calm the affected person
• Wash hands before attending to wound
• Wash wound with soap & running water
• Apply antibiotic ointment
• Dress using sterile bandage
• After first aid, medical treatment must be sought quickly
• Suturing may be required
• Tetanus booster / antibiotics required
• Treatment depends on type / location of wound
27.2.2 Back Pain:
In case of back pain, the following first aid has to be provided:

• Rest in a comfortable position.
• Apply ice pack to affected area
• Painkillers or relaxants may be used
• Avoid strenuous exercise
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• Avoid pillows
• Avoid sleeping on soft mattress
27.2.3 Burns:
Burns can be of first, second and third degree. Categorization depends on severity of tissue
damage.
First Degree Burns:
Injuries are superficial / mild, swelling & redness of the injured area is observed.
Pain develops but no blisters are seen. Burned area becomes white on touching. Follow the
first aid mentioned below in this case:
• Remove patient from heat source
• Remove the burnt clothing
• Run cool water over burnt area
• Gently clean the injured area
• Gently dry
• Apply anti biotic such as silver sulpha-diazine
• Use a sterile bandage to cover burns
• Take tetanus vaccination, if required
Second-degree burns:
Burns extends to middle skin layer, dermis and swelling, redness and pain is
observed. Burnt area may turn white on touching, blisters develop, that ooze a clear fluid.
There are chances of scars development. Follow the first aid mentioned below in this case:
• Clean the affected area thoroughly
• Gently dry
• Apply antibiotic cream over affected area
• Make the patient lie down
• Keep burnt body part at a raised level
• Skin graft may be required
• Physical therapy may be essential to aid mobility
• Splints may be used to rest affected joints
• Hospitalization is essential
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
Third-degree burns:
Damage occurs to all three skin layers and destroys adjacent hair follicles, sweat
glands, nerve endings. There is lack of pain due to destroyed nerves and injured area does not
turn white on touching. No blisters are observed and swelling occurs. The skin develops
leathery texture and discoloration of skin observed. Follow the first aid mentioned below in
this case:
• Requires immediate hospital care
• Dehydration treated through intravenous fluid supply
• Oxygen is administered
• Eschars are surgically opened
• Periodically run clean cool water over burns
• Nutritious diet helps to heal quickly
• Regular monitoring essential
• Mental Depression treated by anti-depressants
27.2.4 Cardio-pulmonary Resuscitation (CPR):
CPR is an emergency life-saving measure and is a combination of rescue breathing & chest
compressions. It is done on unconscious/ non-breathing patient. It is done on people suffering
from cardiac arrest and also for near-drowning/ asphyxiation/ trauma. CPR conducts
defibrillation and supports heart pumping for short duration. It allows oxygen to reach brain,
thus buying time till help arrives. It is more effective when done as early as possible
The Vital Steps:
• Clear the airway

• Assess if the person is conscious / breathing
• Lay the person on his back on a hard surface
• Using a head tilt -chin lift open his airway
• Check for breathing sound
• If not breathing, start mouth-to-mouth breathing
Mouth- to-mouth breathing:
• Pinch the person's nostril shut

• Seal his mouth with your own
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• Give the first breath, lasting one second

• Watch if chest rises
• If it rises, give second rescue breath
• If it does not rise, give a head tilt- chin lift
• Now give second rescue breath
Restore circulation through compression:
• Place heel of your palm on patient's chest

• Place your other hand above first
Keep elbows straight
• Push down using upper body weight (compress)
• Push hard and fast
• After 30 compressions, clear airway
• Give two rescue breaths
• This is one cycle
• Give 100 compressions /minute
• Continue CPR till medical help arrives
27.2.5 Chemical Burns:
In case of burns, the following first aid has to be provided:

• Remove patient from accident site
• Wash injury with tepid water liberally
• Identify chemical for effective therapy
• Seek medical treatment
• IV fluids need to be administered
• Pain medications and antibiotics needed
• Wounds cleaned and bandaged
• Follow -up care compulsory
• Consultation with specialist is a must
27.2.6 Chemical Splash in the Eye:
In case of Chemical splash in the eye, the following first aid has to be provided:
• Lay the person on the floor
• Keep eye lids open forcibly
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• Use clean cold water to wash eyes gently

• Keep washing steadily for at least 20 minutes
• Rinse/wash hands thoroughly to remove chemical
• If wearing contact lens remove them
• Do not rub eyes
• Do not use eye drops until told
• Wear sunglasses to minimize irritation
• After these basic steps seek medical help
• Remember the name of chemical to tell doctor
27.2.7 Dislocation:
In case of dislocation, the following first aid has to be provided:

• Call medical help as soon as possible
• Do not move the joint or try to place it back
• Place ice to control swelling
• If skin is cut, clean gently and bandage with sterile gauze
• Sling or splint the injury in its original position
• If injury is serious, check for breathing
• If not breathing, provide Cardio pulmonary resuscitation (CPR). Elevate the feet up to 12
inches
• Cover the patient with a blanket
27.2.8 Electric Shock:

In case of Electric shock, the following first aid has to be provided:
• Do not attempt to move the victim from current source
• First step is to switch off the current source
• Otherwise, move the source using a wooden stick
• Attend to the victim
• Check for breathing
• No breathing, do Cardio pulmonary resuscitation (CPR)
• Call emergency medical aid
• If breathing, do a physical examination
• Treat for minor burns
• Re-establish vital functions
• Excessive burns may require hospitalization/ surgery
• Supportive care must be provided
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.2.9 Foreign Object in the Ear:
In case a foreign object falls in the ear, the following first aid has to be provided:
• If object is protruding, use tweezers to remove
• If object is small, shake head with ear facing downward
• If it is insect, turn head to place affected ear upward
• Place few drops of mineral oil/baby oil inside ear
• Flush the insect out using clean water
• Use oil only in case of insect otherwise it may lead to swelling
Steps to Avoid:
• Do not push your finger into the ear

• Do not strike the head to dislodge object
• Do not shake a child to remove object
• Do not try to remove object on your own
• Do not block any discharge from ear
• Do not try to clean the ears
27.2.10 Foreign Object in the Eye:
In case a foreign object falls in the eye, the following first aid has to be provided:
• Wash hands before helping the victim
• Seat the person in a lighted area
• Gently examine the eye
• Pull lower eyelid downward
• Ask the person to look upward
• Then hold upper eyelid while person looks down
• If object is floating try flushing it out
• Otherwise, touch the object with wet cotton bud
• Object should cling to the cotton bud
• If object is removed, flush eyes with saline/warm water
• If object cannot be removed, see a doctor
• If object is embedded, do not touch
• Cover the eyes with paper cups and tape it
• Consult doctor immediately
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
Steps to Avoid:
• Avoid rubbing eyes

• Do not remove an embedded object
• Do not try to remove a large object
27.2.11 Foreign Object in the Nose:
In case a foreign object falls in the nose, the following first aid has to be provided:
• The person must be urged to breathe through mouth
• The person should avoid breathing with force
• Close the unaffected nostril
• Blow out gently through the affected nostril
• Get medical aid if this method fails
Steps to Avoid:
• Do not probe an object which is not seen

• Do not probe an object that is not easy to grasp
• Do not blow nose too hard
• Do not use sharp instruments to remove the object
27.2.12 Foreign Object in the Skin:
In case a foreign object falls in the skin, the following first aid has to be provided:
• Wash hands well
• Clean the affected area using soap, water
• If object is visible above skin, squeeze the area around
• When object pops out, remove using sterile tweezer
• If embedded under skin, use a sterile needle
• Sterilize needle by flaming/wiping with alcohol
• Use needle to break skin over affected area
• Lift tip of the object
• Use a small tweezer to pull it out
• Gently squeeze the area and let bleed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• Clean the area with soap, water. Pat dry

• Apply an antibiotic
Steps to Avoid:
• Do not wet if the object is of wood

• Wet wooden objects swell- becomes difficult to remove
27.2.13 Fracture:
There are two types of fractures.

• Open fracture: Skin breaks causing open wound
• Closed fracture: Skin not broken
In case of both the fractures, the first aid differs and is followed as discussed below:
For open fractures:
• Control bleeding before treatment

• Rinse and dress the wound
For open / closed fractures:
• Check the breathing

• Calm the person
• Examine for other injuries
• Immobilize the broken wound
• Apply ice to reduce pain / swelling
• Consult a doctor
Do not:
• Massage the affected area
• Straighten the broken bone
• Move without support to broken bone
• Move joints above / below the fracture
• Give oral liquids / food
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.2.14 Heart Attack:
In case of a heart attack, the following first aid has to be provided:

• Try to relax
• Loosen tight clothes
• Take medicines if any
• Pain subsides within 3 min of medicine intake
• If not, see a doctor.
• Give artificial respiration if required
• Give Cardiopulmonary Resuscitation (CPR):
a) If no pulse is detected
b) By placing palm on chest to pump
• 15 pumps are followed by 2 artificial respiration
• Continue till ambulance / doctor arrives
27.2.15 Heat Stroke:
In case of a heat stroke, the following first aid has to be provided:

• Remove the person to a shady place
• Cool the person by sponging with wet towel
• Apply ice packs in armpits and groin
• Water with electrolyte, fruit / vegetable juice should be given
• Victim must be rested
27.2.16 Severe Bleeding:
In case of severe bleeding, the following first aid has to be provided:

• Wash hands well before administering to patient
• Wear synthetic gloves
• Make the victim lie down
• Slightly elevate the legs
• If possible keep the affected area elevated
• Remove any obvious debris/particle
• Apply direct pressure using clean cloth/bandage
• Use hand if cloth is not available
• Apply pressure continuously for at least 20 minutes
• Do not remove the cloth to check the bleeding
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• Hold the bandage in place using an adhesive tape

• If bleeding seeps through bandage, do not remove it
• Add extra bandage on top of the first one
• Apply direct pressure on the artery if necessary
• The pressure points for arm--below arm- pit/above elbow
• For leg--behind knee/near groin
• Squeeze the artery keeping finger flat
• Continue applying pressure on the wound
• Once bleeding stops immobilize the affected part
• See a doctor
27.2.17 Spinal Cord Injury:
In case of spinal cord injury, seek medical help or call for an ambulance as soon as
possible. Meanwhile the following first aid has to be provided -
• Move the person, if surrounding is not safe
• Immobilize the head, neck and body on both sides
• Movements may dislocate vertebra and cause further injury
• If there is no sign of breathing, perform CPR
• Do not tilt head backward during CPR
27.2.18 Sprain:
In case of sprain, the following first aid has to be provided:

• Apply a cold compress to injured area for 20 min
• This may be done 4-8 times a day
• Use a plastic bag with crushed ice, wrapped in a towel
• Use compression bandages to reduce swelling
• Keep the injured leg elevated on a pillow
• Take anti inflammatory pills if necessary
• Take rest for the recommended period
• When pain/swelling is diminished, do recommended exercises
Steps To Avoid:
• Do not return to normal activities if not completely cured

• This could lead to the problem turning chronic
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
The contents of the First Aid box in the refinery are as follows:
S. No. First Aid Box Content Required No.
1 Small Sterile Dressings 4
2 Medium Sterile Dressings 4
3 Large Sterile Dressing 4
4 Burn Dressings 4
5 Absorbent Cotton (25gm) 1 Roll
6 Dettol Bottle 1
7 Burnol 1 tube
8 Disprin Tablets 6
9 Tincture Iodine Bottle 1
27.3 PERSONAL PROTECTIVE EQUIPMENT (PPE):
PPE are the equipments used to protect the person from hazards associated with the
work being performed. PPE acts as a barrier between the hazard and the person exposed.
Each unit and section is provided with certain PPEs depending on the layout, potential
hazards and access for fire fighting. Fire & Safety carries out monthly check of all the
equipments and releases inspection report.
PPE are characterized into two categories:

a) Respiratory devices
b) Non-respiratory devices
• All the personnel should always ensure that everyone in field is wearing required PPE. For
regular jobs like collecting H2S rich gas, heater checking, chemical handling, etc. specific
and recommended PPE is a must in an addition to safety helmet and work gloves.
• Breathing apparatus should be wore before attending/attempting to arrest leaks like H2S, CO,
LPG, hydrocarbon vapor leaks.
• Breathing apparatus should be checked and ensured that accessories are maintained in good
and ready to use condition like oxygen cylinder is filled with pressure specified and face
mask is free of dust etc. Organic and ammonia canisters should not be kept after their expiry
date.
• PPE boxes in the control rooms should be painted with a display of all the required items in
the unit. All the PPE items should be cleaned by the plant personnel twice in week and
maintain in good condition.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
• The usage of any PPE in case of any incident in the unit is to be recorded in the TOB by the
shift in charge with details of the persons.
• All the safety showers in the unit have to be checked and ensure that both eye washers and
the shower are in working condition.
• In every shift, it has to be recorded in every shift that “the contents of the First Aid Box are
intact”. If any item has been used in the shift, it should be recorded in shift TOB with proper
reasons.
27.3.1 Commonly Used PPE and its functions:
Safety Helmet:
Helmet is one of the most important items of personal protective
equipment used by the industrial workers for protection against head injuries. The injuries
can be caused either by falling objects or by hitting inadvertently against the pipe lines.
Safety Shoes:
Safety shoes are also one of the most important items of PPE used in the
industrial workers for protection against foot injuries. These injuries can be caused either by
falling objects or hitting anywhere inadvertently.
Safety Belt:
It is used to protect persons from free falling while working at higher
elevation. It is a must for working above a height of two meters.
Chemical Cartridges:
It will provide against low concentration of relatively non-toxic gases and
vapors as given in the table.
Type of Chemical Cartridge Suggested maximum use concentration in ppm

AMINES 100
AMINE DERIVATIVES 30
AMMONIA 300
CHLORINE 10
SULFUR DIOXIDE 50
Canisters:
It can provide protection against high levels of toxic air contaminants as
high as 20,000 ppm. Canisters/respirators are classified according to the type of gas and their
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
concentration. The most commonly used canisters are acid gas, ammonia, and hydrocarbon
vapor canisters.
Safety Gloves:
Safety gloves are used to protect hands against common industrial hazard.
Asbestos gloves are used in hot work environment. It will provide protection up to 120°C.
PVC gloves/apron/shoes/suit:
It provides protection against chemicals such as caustic /acid /amine, etc. It
should not be used as a protection against hydrocarbon and hot work environment. The
maximum temperature allowed is 50°C.
Ear Muffs and Ear Plugs:

They are used to protect ears from high decibel noises. They are to be used
while moving in the field.
Face Shield:
Face shield is used to protect face from any thing falling while looking up.
Generally for checking the heaters, it has to be used to protect from any oil dripping.
PPE available in CDU-III field room:
S. No. PPE Name Quantity Available

1 Acid Gas Canister 2
2 Ammonia Canisters 4
3 Asbestos Gloves 2
4 Ear Muff 4
5 Face Mask Canister 2
6 Face Shield 2
7 Organic Vapor Canisters 4
8 Pan View Goggles 4
9 PVC gloves 4
10 PVC hood 2
11 PVC pant and Coat 2
12 Water Gel Blanket 1
13 Safety Belt 1
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.4 FIRE FIGHTING SYSTEM & EQUIPMENT:
Water is the most important medium available for fire protection. Water is
used for fire extinguishing, fire control, cooling of equipments and protection of equipment
and personnel from heat radiation. For these purposes water is used in various forms such as
straight jet, water jog, water curtain, water spray, deluge, sprinkler for foam making etc. The
system is designed in such a way that it can fight two fires requiring largest water demand at
the same time.
Fire water system is designed for a minimum residual pressure of 7.0 kg/cm2
at the hydraulically remotest point of application at the designed flow rate at that point. The
fire network shall be kept pressurized at minimum 7.0 kg/cm2 all the time.
27.4.1 Hydrants:
Hydrants are located keeping in view the fire hazards at different sections of
the premises to be protected and to give most effective service. At least one hydrant post shall
be provided for every 30 meters of the perimeter of unit battery limit. The hydrants should be
located at a minimum distance of 15 meters from the periphery of hazardous equipment.
Double headed hydrants with two separate landing valves on 4”stand post should be used. All
hydrant outlets shall be situated at a workable height of about 1.20 meters above the ground
level.
27.4.2 Monitors:
Monitors are located at strategic locations for protection of cluster of columns,

heaters, etc. and where it may not be possible to approach the higher levels. Monitors shall be
located to direct water on the object as well as to provide water shield to firemen approaching
the fire. The monitors should not be installed less than 15 meters from the hazardous
equipment and shall not exceed 45 meters from the hazard to be protected. The butterfly
valves of the monitors should be periodically checked for free operation and if isolation
valves are gate valves, it should be greased regularly and medium sized wheel spanner should
be welded near it. Monitor rotation levers should be periodically checked for its function.
27.4.3 Fixed Water Spray System:
Fixed water spray system is a fixed pipe system connected to a reliable source
of water supply and equipped with water spray nozzles for specific water discharge and
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
distribution over the surface of area to be protected. This system should be provided in high
hazard areas where immediate application of water is required.
27.4.4 Fixed Water Sprinkler System:
Fixed water sprinkler system is a fixed pipe tailor made system to which
sprinklers with fusible bulbs are attached. Each sprinkler system includes a controlling valve
and a device for actuating an alarm for the operation of the system. The system is usually
activated by heat from a fire and discharges water over the fire area automatically.
27.4.5 Carbon Dioxide System:
Carbon dioxide is an odorless and colorless inert gas and it extinguishes fire
by cutting off the oxygen and creating an inert atmosphere around the hazard. If the inert
atmosphere is maintained for a reasonable time the possibility of flash back is also reduced.
Carbon dioxide is best applied to fire hazards through the fixed system consisting of CO2
storage, distribution and discharge nozzles.
27.4.6 Dry Chemical Powder (DCP)-10 kg capacity:
This is the most common fire extinguishing medium in the refinery. The
number should be determined based on the maximum traveling distance of 15 meters in
hazardous areas. At least one fire extinguisher should be provided for every 250 sq.mt. of
hazardous operating area.
It is provided in critical operating areas. At least one fire extinguisher should

be provided for every 750sq.mt.of hazardous operating area.
It is provided at elevated locations for easy handling.
Note: Any of these cylinders if used, should be immediately informed to Fire and Safety and
get a replacement cylinder. Also the same has to be mentioned in the TOB and informed to
unit manager/YSF.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.4.9 1” Rubber Hose Reel:
They are provided for immediate usage of fire water during fire emergency or
push the spilled oil into OWS. They are of 30 meters length as per OISD guidelines and
contain a nozzle at the open end. It should not be used for floor washing but can be used for
pushing spilled oil into nearest storm sewer/OWS. In this condition, immediately car seal
should be put back.
27.5 SPILL HANDLING:
27.5.1 Ammonia:
If a spill or release to the environment has occurred, fire department,

emergency response, and/or hazardous materials spill personnel should be notified
immediately. Cleanup should be attempted only by those trained in proper containment
procedures. Contaminated soils should be removed for incineration and replaced with clean
soil. If ammonia should contact the water table, aquifer, or navigable waterway, time is of the
essence. It is readily miscible in water and total containing and remediation may not be
entirely possible. When such spills occur, the local and/or state emergency response
authorities must be notified. A comprehensive emergency response or disaster preparedness
recovery plan should be in place prior to any operations involving the use, transportation,
storage, or disposal of ammonia. If ammonia is spilled or leaked, the following specific steps
are recommended:
• Restrict persons not wearing protective clothing from area of spill or leak until cleanup is
complete and area can be opened for normal work.
• Remove all ignition sources.
• Ventilate area of spill or leak.
• If applicable, stop flow of leaking liquid or gas. If leak source is a cylinder and the leak
cannot be stopped in place, remove leaking cylinder to a safe place in the open air, and repair
or allow cylinder to empty.
• Keep ammonia out of a confined space, such as a sewer, because of the possibility of
explosion (unless the sewer is designed to prevent the buildup of explosive concentrations).
• It may be necessary to dispose of ammonia as a hazardous waste. The responsible state
agency or the regional office of the federal Environmental Protection Agency (EPA) should
be contacted for specific recommendations.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.5.2 Caustic 100%:
If a spill or leak to the environment has occurred, fire department, emergency

response and/or hazardous materials spill personnel should be notified immediately. Cleanup
should be attempted only by those trained in proper spill containment procedures. If sodium
hydroxide should contact the water table, aquifer, or navigable waterway, the local and/or
state emergency response authorities must be notified. A comprehensive emergency response
or disaster preparedness/recovery plan should be in place prior to any operations involving
the use, transportation, storage, or disposal of sodium hydroxide. If sodium hydroxide is
spilled or leaked, the following specific steps are recommended:
• Restrict persons not wearing protective clothing from area of spill or leak until cleanup is
complete and area can be opened for normal work.
• Do not allow exposure to incompatible materials.
• Close or remove all ignition sources and ventilate area of spill.
• Collect powdered materials in the safest and most efficient manner possible. Place materials
in a sealed drum. Do NOT dry sweep (generates dusts). Use a vacuum equipped with a high
efficiency particulate air (HEPA) filter instead.
Do NOT use water or damp mop residues.
• It may be necessary to dispose of sodium hydroxide as a hazardous waste. Consult state,
local, or federal environmental regulations.
27.5.3 EC 1020A:
• Small spills: Contain with absorbent material such as clay, soil or any commercially available
absorbent into recovery or salvage drums for disposal.
• Large Liquid Spills: Dyke to prevent further movement and reclaim into recovery or salvage
drums or tank truck for disposal.
• For large indoor spills, evacuate employees and ventilate the area. Those responsible for
control and recovery should wear breathing apparatus, impermeable (PVC) gloves, boots
apron and a face shield with chemical splash goggles.
27.5.4 ELOGUARD 86:
In case of any spillage or leak, the spill has to be flushed with plenty of
water. Those responsible for flushing should wear breathing apparatus, impermeable (PVC)
gloves, boots apron and a face shield with chemical splash goggles because of alkaline nature
of the chemical.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 27
PLANT NAME: CDU II
Chapter Rev No: 0
27.5.5 NALCO 5186:
Restrict the access to area till the clean up operations are complete and
ventilate the area properly. Do not touch the spilled material by bare hands. Stop or reduce
the source of leak if possible and remove source of ignition if any. Those responsible for
• For cleaning small spills, soak the spill with absorbent material and the residue should be
kept in properly labeled and covered containers. The affected areas should be washed.
• For large spills soak the spill with absorbent material or by digging trenches or by making
dykes. Reclaim it into salvage drums or tank trucks for proper disposal. Wash the spillage site
thoroughly with water. Contact an approved water hauler for disposal of contaminated
recovered material.
27.5.6 EC 2040A (DMF):
Restrict the access to area till the clean up operations are complete and
ventilate the area properly. Do not touch the spilled material by bare hands. Stop or reduce
the source of leak if possible and remove source of ignition if any. Those responsible for
• For cleaning small spills, soak the spill with absorbent material and the residue should be
kept in properly labeled and covered containers. The affected areas should be washed.
• For large spills soak the spill with absorbent material or by digging trenches or by making
dykes. Reclaim it into salvage drums or tank trucks for proper disposal. Wash the spillage site
thoroughly with water. Contact an approved water hauler for disposal of contaminated
recovered material.
Note: For any new chemical, the spillage handling procedure can be obtained form MSDS.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 28
PLANT NAME: CDU II
Chapter Rev No: 0
PLANT DRAINAGE SYSTEM

All hydrocarbon stream contaminated with water, water contaminated with hydrocarbons or
chemicals and such liquid streams that cannot be disposed off directly are collected and
treated either for recovery of hydrocarbons or to render themselves harmless to receiving
stream or for both the purposes. For these purposes CBD system and OWS system are
provided. These systems are described sequentially in the following paragraphs.
28.1 CLOSED BLOW DOWN SYSTEM:

(Refer P&ID No. 10-1100-E-204 Rev.7 and 10-1100-E-205 Rev.7)
Those hydrocarbon streams that are either free of water or only slightly contaminated with
water are received in closed blow down (CBD) vessel (11-V-08). Such hydrocarbon streams
are generated especially during shutdown periods when equipment and systems are drained
under gravity to clear oil hold up. The hydrocarbon in the CBD vessel should be received at a
temperature well below flash point of lightest component present inside.
CBD network helps in reducing the amount of hydrocarbon loss. It helps in the avoiding
hazardous conditions that may result in from draining of hot liquid from the equipment, by
providing a collection point for such liquids. It also helps in reducing the oil going to the
effluent treatment facility. Uncontaminated hydrocarbon from equipment draining is
collected and routed to CBD vessel via CBD headers, covering the entire unit.
An 8" underground CBD header has been provided with ballast points at different locations
on the CBD header for flushing the line after draining heavy or viscous oil into it. The header
is finally routed to the CBD drum (11-V-08). It is an under ground vessel placed horizontally.
The drum is provided with a coil through which cooling (salt water) water or LP steam can be
passed. The drum caters to hydrocarbon blow down from CDU/VDU-II, BBU.
LI-1701 and TH-1702 on 11-V-08 indicate the level and temperature of the CBD drum. It is
also provided with low and high level alarms for LI-1701 respectively. There is also an
indication of the CBD inlet temperature TH-1701. It is provided with low and high
temperature alarm for (TI-2601). CBD pump (11-P-18) is interlocked with high / low level
alarms for auto start and auto stop. Hydrocarbon is pumped out by CBD pumps to slop
header in the unit.
Under normal conditions it is expected to remain at atmospheric pressure. A small purge of

steam is provided at the event of the drum to guard against fire at the vent top due to
lightening and static electricity hazard. Service water connection is given to the drum for
cleaning purpose
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 28
PLANT NAME: CDU II
Chapter Rev No: 0
28.2 OILY WATER SEWER:
This system also called OWS is mainly to collect water contaminated with hydrocarbon oil.
Such streams are generated during equipment draining and flushing during routine operation.
Streams suitable for OWS also generated as a result of floor washing and cleaning or spilled
oil etc. Drained streams received through OWS funnels etc. are routed to ETP-II through a
combined header. Contaminate d rain water from the unit paved area is also routed to OWS
System. All equipments having CBD connections are normally provided with OWS
connection also. No OWS points are provided near the heater for safety reasons. The OWS
manholes are sealed and a vent pipe provided releases any hydrocarbon trapped at a higher
elevation. The final outlet of the OWS is located at the south east corner of the unit. The
OWS system is common for both CDU and BBU units. The effluent generated in the unit
reaches ETP-II for treatment and oil recovery.
Care should be taken that at no time any spark reaches vapor space of OWS funnels. This
may result in explosion immediately there or elsewhere in network wherever explosive
mixture of air and hydrocarbon vapors is present in appropriate concentration for explosion.
28.3 SURFACE DRAIN SYSTEM:
The peripheral surface Drain with double valve arrangement to route it either to OWS or to
Storm Sewer System depending upon its oil content. Normally, surface drain outlets are kept
floating on OWS system. During rains, the outlet is changed over to Storm water sewer after
one hour to reduce the load on ETP-II.
28.4 SLOP SYSTEM
Off-spec hydrocarbon streams are routed to an 8" slop header at unit battery limit which is
then routed to slop tanks. The slop generated within CDU-II is primarily dry slop and is
hooked up to slop headers from flare area. This header is routed to the dry slop tanks located
in off-sites.
Dry slop can be recycled back to CDU for reprocessing either by direct injection of slop oil to
crude feed line during Refinery crude tank (120-T-01 C/D/E/F) processing or via crude tanks
as slop is sent to crude oil tanks. All product rundown lines have access to slop header to
route them to slop tanks when their quality goes off-spec. (Mainly during start-up / shut
down).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 28
PLANT NAME: CDU II
Chapter Rev No: 0
Standing Instructions for Effluent monitoring: (ADM/OPRN/PRODN/SI/011):
The following guidelines needs to be followed for monitoring of the draining’s of Oil/Water
in to OWS,
• The normal operation liquid draining’s in to OWS each shift wise to be recorded,
starting with shift I personnel of the day.
• Each shift to ensure record the approximate quantity in the column with signature.
• A team has been formed, consisting of Operations and Technical members for
surprise check of the system weekly.
• Objective of this implementation in operations is to achieve “MINAS” standards of
ETPs outlets.
Standing Instruction on OWS system (SI:12):
Presently during wet weather, the collection of Rain water was exceptionally high and is
more than what ETP’s are actually to hold. This is resulting in over flowing of the surge
ponds and oil breakthrough in to Refinery Effluent.
In View of the above, it is required to ensure that, the entire OWS system is properly
maintained and operated in order, not to get excess/un wanted influent entry in to oily water
sewer system.. The following actions need to be compiled in Process Units.
a. Ensure that all the OWS catch basin covers are in position.
b. During wet weather conditions, switch surroundings OWS to open drain after first
hour of the rain.
c. Ensure that no Fire water usage for Housekeeping/Floor washing.
d. Ensure no draining of spent caustic and chemicals in to OWS.
e. Ensure sour water routing to SWSU.
f. If any oil carry over in Desalter Effluent water reported by ETP-II operator, CDU
block shift in charge to respond immediately, if required suspend wash water injection
to Desalter till it is corrected in consultation with YSF.
Ensure that spent caustic is routed to Merox unit for dumping in Chemical sewer.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
ENVIRONMENTAL MANAGEMENT
The Refinery got ISO 14001 certified for its EMS in May 2002 by SGS Yardley Certification
Services of UK and since then it has been sustained till now with recertification in May 2006
complying with the revised ISO 14001:2004 standards. Refinery also submits environmental
compliance reports to APPCB regularly. In the unit, the air emissions are generated mainly
from the heater as combustion gases (flue gases). They contain a mixture of SO2, CO, NOx,
SPM, etc. If proper care is not taken for these emissions, they can be fatal to living beings.
29.1 ENVIRONMENTAL POLLUTION CONTROL MANAGEMENT &

FACILITIES:
Environmental pollution through air émissions, liquid effluents discharge and hazardous
wastes is managed by :
(i) Control
(ii) Monitoring mechanisms as described below:
29.1.1 Air Emissions Control:
Emissions into ambient air from Refinery operations which significantly affect the
environment are (i) Sulfur Dioxide (SO2), (ii) Carbon Monoxide (CO), (iii) Oxides of
Nitrogen (NOx), (iv) Suspended Particulate Matter (SPM), (v) Hydrocarbon (HC), and (vi)
Noise.
Sulfur Recovery Units (SRUs):
Refinery has installed two identical units of 16 LTPD capacity Liquid Oxidation based
Catalytic units (LOCAT) licensed by erstwhile ARI Technologies, USA for desulfurization of
the sour fuel gas (0.5 wt%-14wt% H2S) to sweet fuel gas (less than 100 ppm H2S) for use in
heaters/ boilers in Sept. 1994 and Dec. 2000. Another unit (DHDS-SRU) with a capacity of
130 MTPD was installed along with DHDS block in the year 2000 to desulphurize Amine
Acid Gas (AAG) and Sour Water Stripper Gas (SWSG). The SRUs will help in reduction of
SO2 emissions to atmosphere when the gases are burnt. Under VRCFP, an additional SRU of
65TPD was commissioned.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
Low sulfur content in the internal Fuel:
Sulfur in the internal fuel ,that is, Low Sulfur Heavy Stock (LSHS) used in Boilers, Furnaces
& Gas Turbines is maintained in the range of 0.5 to 0.6wt% by in-house blending so as to
meet present SO2 emission norm of 11.5 TPD stipulated by APPCB
CO Boiler in FCCUs:
CO boilers are installed at downstream of Fluid Catalytic Cracking Units (FCCUs) for
converting highly harmful CO to CO2, and in turn generating HP steam as it is an exothermic
reaction.
Low NOx burners in Furnaces:
Low NOx burners have been provided in furnaces and boilers installed after the year 1999 to
reduce NOx emissions.
High efficiency cyclones in FCCU:
FCCUs utilize zeolite based catalyst in regenerator and reactor for catalytic cracking of heavy
molecular weight complex hydrocarbons to low molecular weight simple hydrocarbons. In
this process, part of the catalyst gets deformed and forms fines which tend to escape to the
atmosphere along with the flue gas from the regenerator. The installation of cyclones within
regenerator and reactor enables retention of the fines within the process system.
Smoke less Flare:
The refinery flare gases are safely burnt in a tall vertical flare stack with proper water seal
and steam dispersion to avoid black smoke. The flare piping network is closed system
interconnecting all the process units.
Floating roof tanks & mechanical seals:
To facilitate control of fugitive emissions from tanks and pumps, refinery has installed
floating roof tanks for Crude oil tanks and light product storage tanks. All pumps in use are
equipped with mechanical seals and for of LPG and lighter product pumps double mechanical
seals are used.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
Low noise machines/ motors:
At the time of equipment purchase itself it will be specified that noise level to be below the
statutory limit with required acoustic enclosures.
Tall Stacks:
Process furnaces, boilers and gas turbines are provided with tall stacks (about 60m) for better
dispersion of flue gases and to get ground level concentration within allowable ambient air
quality limits.
After installation of the pollution control facilities, it is to be ensured

that the facilities are functioning properly so as to meet the emission norms consistently.
Monitoring of air emissions is carried out as follows:
On-line stack monitors:
Refinery has all the stacks equipped with on-line stack analyzers to monitor SO2, NOx, SPM,
HC and CO.
Continuous Ambient Air Monitoring Stations (CAAMS):
Based on predominant wind direction and neighboring population, three CAAMS have been
installed to monitor ambient air quality with respect to SO2, NOx, HC, SPM, RSPM, CO and
Noise. One of the CAAMS is also equipped with Weather Monitoring Station (WMS) to
measure wind speed, direction, relative humidity, rainfall, temp, etc.
CCTV for flare:
A Closed Circuit color TV (CCTV) is installed at the centralized process unit control room
for monitoring the flare flame and its quality. The unit personnel keep a watch on the CCTV
and diagnose the problems within their units and check the condition of the relief valves for
their passing based on the quality of the flare.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
Noise Monitoring:
Exposure to noise at high levels and for long duration can have adverse physiological and
psychological effects. Periodic measurement of the noise pollution is carried out by Fire &
Safety Department.
29.1.2 Liquid Effluent Management:
Liquid effluents which significantly affect the environment are (i) Sour Water (ii) Equipment/
Floor washings, contaminated with oil & chemicals, (iii) Spent Caustic and Chemicals from
process & product treatment units, and (iv) Hydrocarbon draining from columns, vessels,
heat exchangers etc. These pollutants are controlled with use of the following facilities:
Sour Water Stripping Units:
During the distillation process of the hydrocarbons in the column sour water, containing
hydrogen sulfide, ammonia, phenols etc, gets collected in the overhead accumulator drum.
The sour water is stripped off the pollutants in strippers with a steam reboiler. The off gases
viz. hydrogen sulfide and ammonia are routed to SRUs while the stripped water is reused
partly as desalter wash water and the balance stripped water is routed to Effluent Treatment
Plant (ETPs) prior to discharge as refinery effluent to the sea.
OWS & Chemical Sewers:
Segregated sewer systems of Oily Water Sewer (OWS) and Chemical sewers are provided for
better separation of oil from water and other spent chemicals. All the process units, product
treatment units and tank farm areas are provided with underground OWS network. Spent
chemicals like spent caustic (rich in sulphides) from Mercaptans Oxidation (Merox) units and
Diesel Hydro-desulfurization (DHDS) unit have dedicated underground sewer system for
routing the effluents separately to the ETP.
Closed Blow Down System:
All process and treatment units have Closed Blow down (CBD) system installed to facilitate
draining of hydrocarbons from equipment/ heat exchangers prior to giving for maintenance &
repairs. This drain facility ensures that the hydrocarbon is recycled back to the process
system as slop oil and not let out to ETPs.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
Effluent Treatment Plants:
ETPs are equipped with physico-chemical, biological treatment and effluent polishing
facilities to remove free oil, emulsified oil and reduction of Biological Oxygen Demand
(BOD). There Tilted Plate Interceptors (TPIs), Dissolved Air Floatation (DAF) cells,
ammonia stripping tower, trickling filter, activated sludge process reactor, Dual Media Filters
(DMFs), Granulated Activated Carbon (GAC) filters etc. for effective stage-wise pollutant
removal from the liquid effluents. The effluent quality is measured at the outlet through a
composite auto-sampler.
The Refinery liquid effluent is tested daily to check its quality and take
corrective actions. APPCB also monitors the liquid effluent discharge from the refinery
premises by collecting regular legal samples for checking compliance with Minimal National
Standards (MINAS). Following studies have been taken up for further improving the liquid
effluent:
Zero effluent discharge:
To achieve zero liquid discharge from the Refinery by internally reusing and recycling the
waste water, the study was taken up with assistance of EIL.
Dedicated sour water collection and reprocessing:
The study was taken up with assistance of EIL to provide dedicated sour water collection
system in the refinery to safeguard ETP from shock loads during emergency or abnormal
plant status.
Correction of excess oil ingress at ETP-I/II:
The study was taken up with assistance of EIL to reduce oil ingress into the ETP’s. The
study was completed and project is under implementation.
Performance evaluation of Bio-system at ETP-II:
The study was taken up with assistance of NEERI and the recommendations on improvement
of plant performance are under implementation.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
29.1.3 Hazardous Waste Management:
Hazardous wastes are managed through minimization at source, recycle or reprocess, sale and
explore usage or alternate disposal options and store it for safe disposal in future. In Refinery,
oily sludge generation from storage tanks forms major portion of the hazardous wastes, other
wastes being spent catalysts, charcoal, lead acid batteries, slop oil, etc. The following
facilities are provided to effectively control the hazardous wastes:
Side entry mixers in tanks:
The sludge generation in crude tanks varies with type of crude oil stored and duration of
usage of the tank. With usage of side entry mixers, settlement of the tank sludge to the
bottom is avoided. All crude oil and heavy oil tanks are provided with side entry mixers and
the service factors of the mixers are maintained high.
Proper Housekeeping in Process units:
Wastes generated in the units are segregated into ferrous and non-ferrous and kept stored at
the earmarked unit peripheral limits for subsequent removal and proper disposal of the
wastes.
Empty Drum Washing:
The empty chemical and oil drums (plastic and metallic) are labeled into oil based and water
based and kept stored at the earmarked unit peripheral limits for subsequent removal to the
empty drum washing area near WWTP. These empty drums are washed with suitable solvent
depending on whether the drum was oil based or water based and using jet sprayer and tilted
drum shaking equipment.
Centrifuges at ETPs:
ETPs are equipped with centrifuges for effective solid–liquid separation and the ETP sludge
is then treated in bioremediation farm, through the process of which the quantum of sludge
reduces considerably.
Monitoring and disposal involves an elaborate mechanism. The hazardous waste generation
is monitored through Disposal Requisition Notice (DRN) system since the year 2000. The
waste generating section/ unit raises DRN indicating the waste details (type of waste, source
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
of generation, quantity etc.) and based on this management or disposal method for the waste
shall be advised. Following actions have been taken for reprocessing or recovery and disposal
of the hazardous wastes:
29.1.4 Ex-situ processing of high oily sludge:
The Refinery pioneered in processing high oily sludge generated from tank farms. About
34,000 m3 of the sludge was treated by M/s.Singaport Cleanseas Pte Limited, Singapore
during Apr. 2001 thru Aug. 2003. Presently, M/s Balmer Lawrie & Co. Ltd, Kolkata, carried
out the sludge processing till Nov 2008. Presently, sale of sludge is being taken up.
29.1.5 In-situ processing of high oily sludge:
• Chemical method:
Crude tank bottom high oily sludge from four Crude tanks was
processed successfully to recover oil using a chemical (EC9007A) supplied by M/s Nalco
Chemicals since the year 1998.
• Mechanical method:
Crude tank bottom sludge was also processed in 2005-06 using

mechanical method of Blabo technology.
29.2 EFFLUENT, EMISSIONS AND SOLID WASTES:
The liquid effluent of CDU-II is the sour water which is removed from the column overhead
drum, Desalter and hot well drum. This is sour water and needs to be treated in Sour water
stripping unit. While routing this water to SWSU, it has to be ensured that the water contains
very minute traces of oil (limit up to 100 ppm). If the water contains more oil, then it
becomes difficult to dispose off or treat this water. The water should be oil free and the
stripped water is used for desalting in the desalter.
The effluent sometimes is required to drain to OWS or local drains in case of

some problem in Merox or due to any process or line constraints. This time of this operation
has to be minimized as this is not an environment friendly practice. This can only be done as
a temporary measure and cannot be continued for a longer period of time.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 29
PLANT NAME: CDU II
Chapter Rev No: 0
The flue gas of heaters is the emissions from the unit. There are various methods of
controlling these emissions. The environmental regulations are very stringent for emissions
and already the actions taken in the refinery to control emissions have been discussed. All the
stacks have online analyzers for SOx, NOx, CO, HC and SPM. They will give us an idea of
the amount of these gases generated and which gives an idea of the quality of fuel that is
getting incinerated in the heater. The fuel being used is generally sweet fuel (sweet fuel gas
and LSHS) and thus it helps to keep the emissions inside the permissible limits. The technical
department keeps a constant check on the values of these meters and the emissions from the
unit so that there is no harm caused to environment from the refinery.
Solid wastes generated in the unit are either ferrous or non- ferrous. The wastes include
insulation material, cotton wastes, insulation cladding material, replaced line portions, etc.
They are kept in the designated scrap yard of the unit. The scrap yard is situated in south-west
corner of the unit and separate yards are available to keep ferrous and non-ferrous materials.
The scrap generated from the unit has to be kept in these yards. Once the quantity of scrap is
more in the yard, job-card is given to remove scrap from the unit and the same is carried out
by the maintenance department. It is to be ensured that the scrap yard is always emptied once
it becomes full and thus there is always sufficient dumping space for the scraps. Any waste
generated has to be shifted to the scrap yard. If during maintenance, scrap is generated then it
should be ensured that proper housekeeping has been carried and the scrap generated has to
be put in the scrap yard. Always the ferrous and non-ferrous scraps have to be kept in their
separate yards
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
SPECIAL OR UNIQUE HAZARDS
“THE BEST PROTECTION AGAINST ALL HAZARDS IS PREVENTION”
Hazard is defined as a chemical or physical condition that has the potential for causing
damage to people, property or the environment. People working in the field must be well
known to the actions that need to be taken in case of such situations. The unexpected hazards
are discussed in the chapter but there are some hazards which may not be covered in the
chapter. Accidental release of flammable or toxic vapor can result in severe consequences
like BLEVE, vapor Cloud Explosion or Toxic Vapor Cloud. A BLEVE occurs when there is
a sudden loss of containment of a pressure vessel containing a superheated liquid or liquefied
gas. Delayed ignition of flammable vapors can result in blast overpressures covering large
area. Toxic clouds may cover yet larger distances due to the lower concentration threshold
value for potentially lethal situations in relation to those in case of explosive clouds.
In contrast, fires have localized consequences. The extent of damage to people depends on
the heat flux and duration of exposure. Fires can be put out or contained in most cases, but
there are few mitigating actions one can take once a vapor cloud gets released. Major
accident hazards arise, therefore, consequent upon the release of flammable or toxic vapors.
Safety of personnel and equipment is very important. Ignorance of the details of the unit or
the techniques of safe and efficient operation reduces the margin of safety of personnel and
subjects the equipment to more hazardous conditions. All the operating and maintenance
crew therefore must be fully familiar with the equipment and materials being handled in the
unit and recognize the hazards involved in handling them and the measures taken to ensure
safe operations.
Since the unit handles with one of the most potential source of fire and explosion, LPG and
chemicals like caustic, adherence of safety rules should be given uphill importance.
30.1 SAFETY OF PERSONNEL:
General safety rules, which shall be practiced and enforced for all personnel who enter the
unit, are summarized below:
• Safety helmets and boots shall be worn by all personnel at all times in the plant. They
may be removed when inside rooms or buildings which do not have overhead or other
hazards.
• Smoking is not permitted in side the refinery.
• Each employees assigned to work in the unit shall know where the safety and fire
suppression equipment is located and how to operate equipment.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
• Safety glasses, goggles or face shields shall be worn while performing work, which
could result in eye or face injury.
• Operations personnel golden rule
• Do not open or close any valve without first determining the effect.
• Maintenance personnel golden rule:
• Treat each piece of equipment or piping as if it is under pressure.
30.2 PRESENCE OF FLAMMABLE HYDROCARBONS AND SAFETY

PRECAUTIONS:
30.2.1 Hazards Related to Handling of Liquefied Petroleum Gases Systems:
In the design of the LPG handling area (absorber section) major consideration has to be given
to the Hazards of LPG which are listed in this subsection.
Liquefied Petroleum Gas is a mixture of commercial Butane and commercial propane both
saturated and unsaturated hydrocarbon. LPG is inherently dangerous on account of fire,
explosion and other hazards. This calls for special attention on the manner in which it is
stored, transported or used. These hazards can have an impact on both the public. As a
consequence of this special emphasis has been given on the safety regulations while
designing this system.
• LPG at atmospheric pressure and temperature is a gas which is 1.5 to 2.0 times
heavier than air. It is readily liquefied under moderate pressure. The density of liquid is
approximately half that of water and ranges from 0.525 to 0.58 at 15 0 C. Since LPG
vapor is heavier than air, it would normally settle down at ground level / low lying places
and accumulate in depressions. Under still conditions the dissipation of accumulated
vapor is slow. This accumulation of LPG vapors gives rise to potential fire and explosion
hazard.
• LPG has an explosive limit range of 1.8% to 9.5% volume of gas in air. This is
considerably narrower and gives an indication of hazard of LPG vapors accumulated
involving areas in the eventuality of leakage or spillage.
• The combustion reactions of LPG increase the volume of product in addition to the
generation of heat. LPG requires 24 to 30 times its own volume of air for complete
combustion and at the same time yield 3 or 4 times its own volume of carbon dioxide
yielding approximately 10,900 k cal of heat per kg. Leaking liquid phase LPG will
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
rapidly expand around 250 times its won volume therefore creating a greater risk than
would occur with a similar size vapor leakage. When the pressure is reduced, LPG
vaporizes rapidly reducing the surrounding temperature. This may lead to burns in contact
of LPG with the skin.
• LPG liquid released forms a vapor which travels long distance. This explains the
hazardous aspects of faster spreading of LPG fire. The vapors of LPG can give more
violent conclusion in explosion as in case of Hydrogen due to higher flame propagation
• Liquid phase LPG expands considerably when it s temperature increases, exceeding

most of petroleum products. The coefficient of expansion is around 0.000237 per degree
centigrade at 15 C. This high rate of expansion has been taken into account when
specifying the maximum quantity of LPG permitted to be filled into any pressure vessel.
• LPG is colorless in both liquid and vapor phase.
• The vaporization of liquid cools the atmosphere and condenses the water vapor
contained in them to form a whitish fog which makes it possible to see an escape of LPG.
• LPG has only faint smell and consequently it is necessary to add some odorant so that
any escaping gas can easily be detected.
• LPG has low viscosity and can leak when other petroleum products normally cannot
thus demand a very high integrity in the pressurized system to avoid leakage. It is also
poor lubricant and leaks are therefore likely to occur at pump seals and glands. In view of
this, special attention has been given e.g. to the selection of mechanical seals etc.
• The hazards associated with release of a boiling flammable liquid to atmosphere

show themselves disproportionately when large quantities are involve - they can give rise
to two phenomena which are highly hazardous the unconfined vapor cloud explosion and
the boiling liquid expanding vapor explosion.
Vapor cloud can ignite and burn as fireballs causing lot of damage by radiation starting
secondary fires at some distance. Vapor cloud ignites and explodes causing high
overpressures and very heavy damage. The latter is termed as Percussive unconfined Vapor
Cloud Explosion' i.e. PVUCE in short. Even though large quantities of LPG emission are
necessary only a fraction of this contributes to percussive effect.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
The boiling liquid expanding vapor explosion (BLEVE) is due to holding pressurized
flammable liquid above its boiling point. This may result from inadequate vapor space for
temperature expansion of the content or high temperature due to radiation heat from the
adjacent vessel under fire or due to a mechanical damage. BLEVE even though not as serious
as PUVCE, the potential for spreading fire over a wide area makes them significant in terms
of both life and property posing hazard to fire-fighters.
Ejection of boiling liquid produces reaction rupturing the vessel causing the rocket projecting
of dish ends. The released liquid flashed and atomizes immediately often resulting in large
fire ball. Although the fire ball lasts only a few seconds, its effects can be devastating due to
flame contact and thermal radiation.
30.3 SAFETY PRECAUTIONS WHILE HANDLING FLAMMABLE

HYDROCARBONS:
i) LEL Detectors: LEL detectors are provided at various locations in the unit at critical
locations. This will help in early identification of any hydrocarbon leaks so that immediate
responsive action can be taken. Activation of LEL detector raises alarm in DCS.
ii) The unit handles hydrocarbon liquids and gases which can cause fire and explosion if
conditions for the same are favorable. Direct contact of hydrocarbons with any source of
ignition of fire such as spark or open flame should be avoided. Sparks or open fire should not
be allowed in the operating area while the unit is operating or has potential of hydrocarbon
leakage. Even during shutdown. When an open flame work is absolutely essential, this should
be allowed with the permission of the authorized person after suitable precautions have been
taken. Approved safety & work permit systems should be strictly followed.
iii) Propane gas is highly explosive in air mixtures containing 2.4 to 9.5 % by volume of
Propane vapors. Its concentration in air should normally be not allowed to exceed 0.4%. It
must be stored in a cool, isolated and ventilated area free of acute fire hazard. A
concentration in air above 1% of Propane may have mild narcotic effect. Inhalation of
excessive amounts causes progressive aesthesia. Liquid Propane in contact with skin will
cause frostbite through rapid evaporation.
iv) Improper earthing of equipment may produce static charges. All equipment must be
provided earthing connections as per standards.
v) The drain / vent valves and sample points on hot and heavy products and steam lines
are likely to get plugged, if the lines are not in constant use. Such valves should be crack
opened for a few minutes under personal supervision and only after the liquid flow has
started the opening of the valves should be adjusted as required.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
vi) Leakage of hydrocarbons from equipment and pipe joints are undesirable and must be
reported to the immediate supervisor without delay.
vii) The set pressure of relief valves should never be altered without prior permission of the
authorized persons in writing.
Wherever block valves are provided for isolation of relief valves, these valves should be kept
opened all the times as per stipulations in P&ID’s.
viii) The closure of block or control valves which isolate exchangers or piping from relief
protection devices can subject the equipment to possible overpressure due to thermal
expansion of the blocked fluid. The expansion may be caused by heat from the atmosphere or
adjacent hot equipment. In order to prevent such over pressurizing some suitable drains/vents
or other valves connected with some closed system in the network should be left opened, to
take care of such expansion.
ix) Poor house-keeping in the operating area is a potential cause of accidents. Spillage of
oil etc. is very dangerous. Maintain a high standard of house-keeping in the work area.
x) Releasing equipment for maintenance without properly preparing it e.g. blinding /
isolating & making it hydrocarbon free and electrical isolation etc. should be avoided as this
can also result in major accidents.
30.4 CAUSTIC SODA:
Permissible Exposure Limits in Air:
The recommended limit on airborne work place sodium hydroxide concentration is 2.0 mg
sodium hydroxide / m3. This is to protect against the irritation of the respiratory tract.
Harmful Effects and Symptoms:
This compound is extremely alkaline in nature and very corrosive to body tissues. Dermatitis
may result from repeated exposure to dilute solutions in the form of liquids, dusts or mists.
Local contact of sodium hydroxide with eyes, skin etc. can result in extensive damage of
tissues, with resultant blindness and burns.
First Aid:
If this chemical gets into eyes, irrigate immediately. Washing should start within 10 seconds
and continue for at least 15 minutes to prevent permanent injury. If this chemical contacts the
skin, flush with water immediately to prevent slow healing chemical burns. If a person
breathes in large amount of this chemical, move the exposed person to fresh air at once and
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
perform artificial respiration. When this chemical has been swallowed, get medical attention.
Give large quantities of water and do not induce vomiting.
Personal Protective Methods:
Wear appropriate clothing to prevent any possibility of skin contact. Wear eye protection to
prevent any possibility of eye contact. Wash immediately when skin is wet or contaminated.
Work clothing should be changed daily if it is possible that clothing is contaminated. Provide
emergency showers and eyewash.
Recommended Respirator Selection:
100 mg/m3 HiEPF/SAF/SCBAF

200 mg/m3 PAP HiEF/SAF/PD.PP,CF
Escape DMXSF/SCBAF
Disposal Method Suggested:
Discharge into tank containing water. Neutralize then flush to sewer with water.
30.5 HYDROGEN SULPHIDE
Hydrogen sulfide is a deadly poison, having a very quick action. Its hazard is compounded by
the fact that the sense of smell is paralyzed once the concentration of H2S is becomes
dangerous. Therefore, under no circumstances should appropriate safety measures be omitted
whenever H2S is present. When sampling or purging operations are being carried out on
streams carrying H2S, appropriate precautions must be taken.
Prevention of hydrogen sulfide poisoning:
The best method of preventing H2S poisoning is to stay out of the plant areas known or
suspected to contain it. Sense of smell is not an infalliable guide to its presence; though the
compound has the distinct and unpleasant odor of rotten eggs, it will in higher concentrations
paralyze the olfactory nerves so the victim cannot smell it.
A good method of prevention is to check systematically the atmosphere of the suspected areas
for the presence of H2S by testing with portable H2S detectors, moist lead acetate paper, or by
Tutweiler H2S determination.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
Gas masks suitable for use with hydrogen sulfide must be worn during work when exposure to
it is likely to occur; masks must be frequently checked to ensure they are functional.
When working under conditions of likely exposure, the presence of a second operator is
compulsory.
Acute hydrogen sulfide poisoning:
Breathing air or gas containing as little as 600-1000 ppm of H2S for one minute can cause acute
poisoning. One full breath of highly concentrated hydrogen sulfide gas will cause
unconsciousness, and death may occur if the victim falls and remains in the presence of the gas.
Operations using processing gases containing H2S are safe, provided precautions are taken. No
work should be undertaken where there is danger of breathing H2S, and no one should enter or
remain in an area without wearing a suitable mask.
The symptoms of acute hydrogen sulfide poisoning are muscular spasms, irregular breathing,
feeble pulse, odour of the breath, nausea. Loss of consciousness and suspended respiration
quickly follow.
When acute poisoning has occurred, immediately remove the victim to fresh air. If breathing
has not stopped, keep the victim in fresh air and keep him calm and warm. Call a physician
and keep the patient quiet and under close observation for about 48 hours for possible edema
of air passages on lungs.
If the victim is unconscious, breathing has stopped and there is no heartbeat (check on the
main artery), then artificial respiration must be started at once. Quick action in starting
respiration is essential. For correct procedure on artificial respiration, consult the first aid
manual.
In all cases of acute H2S poisoning, the use of oxygen containing 5% carbon dioxide is
recommended as an inhalant, whether or not breathing has stopped. This mixture is a
respiratory stimulant which must be administered by someone familiar with the use of
respiratory apparatus.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
Sub-acute hydrogen sulfide poisoning:
Breathing air or gas containing 100-600 ppm of H2S for an hour or more may cause sub-acute
hydrogen sulfide poisoning. Symptoms of sub-acute poisoning are headache, inflammation of
eyes and throat, dizziness, indigestion, excessive saliva and weariness.
Edema of the air passages on lungs may also occur. When sub-acute poisoning has occurred,
keep the patient in the dark to reduce eye strain and have a physician treat inflamed eyes and
throat. Check for possible edema.
H2S leak handling procedure:
Actions to be taken up for the following cases :

a. H2S hooter alarm is activated
b. H2S smell is detected
c. Portable detector indicates presence of H2S
d. DCS supervisor informs high H2S indication in any of the detector
ACTIONS:
1. The DCS supervisor will announce in PA 'H2S leak' and 'vacate the unit' atleast six times
in English and Telugu, once an alarm is activated, so that all persons present in the unit can
go out to a safe place.
2. Concerned Operator to wear BA set and carry spare BA set/cylinder. Spare BA
set/cylinder will be left in the field in a safe location, where field supervisor is stationed.
3. With portable detector, the Operator (with BA set 'on') moves to the location of leak and
tries to ascertain the leak.
4. All other operating personnel (technicians and supervisor) in the field will also wear BA
sets and go to location along with all the spare BA sets & cylinders available in the field
room, but will stand in a place where there is no H2S is present (they also carry portable
detectors).
5. Field supervisor will station himself in a safe location where communication with DCS is
available and H2S is not present. All spare BA sets/cylinders will also be kept at the location.
He shall co-ordinate all activities from this location.
6. Stand by Operators will go around the unit to evacuate any person affected by H2S leak
and send out all other contract/maintenance persons of the unit towards upwind direction.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
7. The first Operator will immediately give preliminary condition of leak to Supervisor
after coming to the safe location. The supervisor shall send additional operators with BA set
‘ON’ for follow-up actions to the location of leak, if required.
8. BA set shall not be removed for any reason (like communication), while the person is
in the area of H2S leak.
9. Field supervisor shall assess the situation and inform YSF/F&S for additional help (if
required) through DCS supervisor.
10. If the search takes more than 30 min or low pressure alarm is given by BA set, the
operator shall come to the field supervisor and gives feed back regarding the areas checked.
11. Once leak is ascertained, field supervisor will decide on the course of action.
i. isolation if possible
ii. attending the leak if minor
iii. Shutdown of the plant
30.6 FURNACE EXPLOSIONS:
Statistics have shown that 90% of the furnace explosions occur during start-up or low load
operation. More than 50% of the furnace explosions happen during a start-up some years after
the initial start-up. These observations pinpoint the need for additional care, instructions and
training in start-up operations. Most explosions happen in gas-fired furnaces.
30.6.1 Explosion theory
Three conditions must be met to get an explosion:

− A combustible gas (vapor) must be present
− The combustible gas (vapor) is mixed with oxygen (air) in the proportions required to
produce an explosive mixture.
− A source of ignition must be available to start the explosion (unless the temperature of the
mixture is above the auto-ignition temperature).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
30.6.2 Fundamental operating procedures:
Heater flame-out
The questions of what action should be taken after a flame-out of a furnace is subject to
controversial opinions resulting from different interpretations of the explosion theory. Take
care of following operation:
− Shut off fuel and feed supply (this is automatically done in the case of shut-down)
− Close main hand valves
− Close individuals burner valves
30.6.3 Heater light-off:
Heater light-off after flame-out
When the cause of the flame-out (shut-down) is such that the furnace can be re-ignited again
before it has been cooled off entirely, the recommended procedures are as follows:
− Check firebox with an explosion meter for hydrocarbons and hydrogen to make sure that
there are no explosive mixtures in any part of the firebox.
− When negative hydrocarbon tests are obtained, start re-ignition in the normal way.
Heater light-off during normal start-up

− Make sure individual burner fuel valves and registers are closed
− Open air registers
− Check furnace firebox for hydrocarbons
− Follow start-up instructions
Note: During the light-off of the burner, check very carefully through the end-wall peepholes
and/or burner peep sights to ascertain that the pertaining burners are really ignited and are not
impinging on the heater tubes.
30.6.4 Fire in the firebox of the heater:
In case of an unintended fire in the firebox, for instance caused by the tube rupture, the
following procedure is recommended :
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
− Shut off fuel and feed

− Close all openings (air registers) and keep the peepholes closed to prevent air
introduction
− Stop forced draft fan
− Open snuffing steam to firebox
30.7 EMERGENCY HANDLING OF TOXIC / CORROSIVE CHEMICALS:
DO’S:
• In case of leak move in upwind direction away from the contaminated area.
• If respiratory equipment’s are not available then use wet handkerchief to cover your nose.
• In case of skin contact, wash the affected area with large quantity of water. In case of eye
contact, flush the eye with large quantity of water atleast for 15 minutes, keeping eyelids
open.
• In case of inhalation, go to open fresh air area and take plenty of water.
• Keep the victim warm.
• In case a feeling suffocated, then give artificial respiration.
• Consult doctor and act as per his advice.
DONT’S:
• Become panicky.
• Go close to the leaky cylinders without right PPE and respiratory equipment.
• Apply little water on to the leaky cylinder.
• Spread rumors.
• Apply ointment to the injured due to the chemicals.
• Take any medicine without consulting Doctor
• Induce vomiting, keep warm and quiet.
• Attempt to neutralize acid in contact with skin.
DO’s:
• Assess the wind direction and approach from upwind side.

• Keep all persons out of vapor cloud area. Evacuate the area in the path of vapor cloud.
• Isolate the source of vapor if possible.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
• Eliminate any source of ignition in the surrounding areas (Spark arising out of operation of
electrical switches or electrical equipment, operation of i/c engines and vehicles, or any hot
job including welding and grinding).
• Stop the traffic on the road if the vapor cloud is moving towards the road.
• If the vapor cloud is moving out of the refinery, stop the traffic on the main road and alert the
nearby residents to eliminate all source of ignition. Activate mutual aid if required and
contact district authority for activating Offsite Emergency Preparedness plan. Operate water
spray system for dispersing vapor cloud and operate water monitors for dispersing the cloud.
• Continue the water operation till the entire vapor cloud is safely dispersed into the
atmosphere.
• In case of the escaping gas/ vapor in fire, immediately apply large quantity of water as
quickly as possible to all surface exposed to heat.
DONT’S:
• Don’t do any hot jobs in the close vicinity.

• Don’t operate electrical switches or electrical equipment in nearby vicinity.
• Don’t approach from downwind direction.
• In case of fire, do not extinguish unless leak is stopped, if the source can not be isolated after
extinguishing the gas will continue to flow and spread over a wide area and re-ignition can
result in more hazardous situation.
30.8 INCASE ANY ACCIDENT HAPPENS:
The probable areas where a person can get trapped during an emergency are:
• Switch Gear room

• Within a lift and elevator
• High rise structures
• Confined space like tanks / vessels under maintenance
• Buildings
• Near to the source of release of toxic/ flammable gas leak In the process unit / pipe tracks
Search and rescue operation to be carried out with the help of following equipments:
• Self contained Breathing Apparatus sets with life line.

• Rescue tools such as hydraulic spreader/ cutter, pneumatic lifting bags, fire man hook.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
• High voltage resistant safety shoes and PVC / rubber gloves

• Extension ladder
• Torch lights
• Stretchers
During the search and rescue following precautions to be taken:

• Carry out the rescue operation in a pair not as an individual.
• Proceed cautiously anticipating tripping hazard.
• Keep yourself as low as possible.
• Follow the instructions of the Rescue controller.
• Cut-off the water, electricity and gas supplies of rescue operation area.
• Collect and check all equipments before returning from site.
• In case of usage of Breathing Apparatus sets follow the BA set usage instructions and in no
case the user to remain in the danger area after the sounding of warning whistle.
• Keep constant communication with rescue coordinator.
Important considerations for fighting petroleum liquid fires and Gas fires:
• Approach should be made from the upwind side.

• The vehicles should be parked in such a way that in case of danger to the vehicles or fire
fighters, the vehicle can be removed immediately without any delay.
• Role clarity of all the personnel available at the emergency site is very important. The
personnel whose presence is not warranted at the fire / emergency site should be evacuated
from the site.
• Brief details of the fuel involved in fire to be collected from the Incident Controller /
operation controller/ concerned Plant In-charge.
• Cutting off the fuel supply is the best method for putting off any petroleum fire. Before
making any attempt for fire fighting it is preferable to cut off the fuel supply.
• Selection of extinguishing media plays a very important role in putting off the fire.
Depending on the equipment and fuel involved in fire the extinguishing media is to be
selected.
Selection of extinguishing media:
The following points are to be kept in mind during selection and use of different fire
extinguishing media:
• Quantity of different extinguishing media required to be used in different type of fires to be
pre-estimated so that sufficient quantity of extinguishing media can be made available
without any delay.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 30
PLANT NAME: CDU II
Chapter Rev No: 0
• In case water attack is to be initiated, minimum two parallel lines to be put into action.
• In case Fire is to be attacked with DCP or CO2 in an enclosed chamber, proper ventilation,
evacuation of the area and means of exit to be ensured before attack.
• If foam is to be applied in low lying areas or on ground, the stream has to be applied to the
nearest smooth elevated surface, where from the foam generated will flow down and spread
over the burning liquid uniformly.
• Before applying DCP through DCP tender the downwind area is to be evacuated after
consulting the Incident Controller. DCP should be applied from the upwind direction and
preferably from hose reel hose.
• Back up of fire fighting equipment and manpower is very important for fire fighting
operations. While fighting with foam ensure that sufficient quantity of foam is reaching the
site to prevent the chances of re-ignition. Further there should not be any shortage of water.
After extinguishing the fire ensure the use of water/ Foam application for some time for
preventing re-ignition. The frontline fire fighters should be given adequate protection.
• The mutual aid scheme help can be mobilized in case of requirement.
30.9 FIRE IN PROCESS UNITS:
Fire in process unit can be due to leak from flanges, mechanical seal leaks and leak from
pipelines etc. It may be at ground level or at elevation. It can be a minor fire due to leak or a
major fire due to rupture and formation of pool of oil. Before attacking the fire details of the
source of fuel, isolation of the source and adjoining equipment to be essentially obtained.
• If the fire is minor, it can be attacked with DCP extinguisher or fine spray of water using
spray nozzles. However DCP attack should be back-up with water spray to prevent re-
ignition.
• If the fire is major, it is to be attacked with the help of DCP from DCP tender and with back
up of foam for ground fires and back up of water for ground fire.
• Simultaneously isolation of the source of fuel to be carried out followed by isolation of
adjacent equipment, stoppage of rotary equipment, (from substation), shutdown of fired
equipment, shutdown of entire unit, isolation of power to unit etc. as per requirement.
• Water spray if provided to be operated and cooling of nearby vessels and vessels exposed to
the fire to be carried out.
Water spray protection may be provided to the operation staff to approach and close the valve
for isolation of fuel if isolation valve is on fire. The fire at a height can be fought with water
spray monitor and DCP tender.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
SAFE WORK PRACTICES
Set of best industrial practices, standards and statutory requirements grouped together and
compiled to act as a guide to the employees in for executing the assigned job in a safe way.
They act as guidelines helping the executors for the safe execution of the jobs in the refinery.
Safe work practices list out the essential requirements that are to be ensured for carrying out
jobs safely in the refinery.
So far total of 9 safe work practices were developed, and released for implementation.
SWP – 01 : Specification of Personal Protective Equipment.
SWP – 02 : Minimum Personal Protective Equipment for various activities.
SWP – 03 : Examination of Eyesight of certain personnel.
SWP – 04 : Requirement of PPE availability in plants and other locations.
SWP – 05 : Control of loose materials, unfixed tools and equipment in plant areas.
SWP – 06 : Contractor job equipment safety assurance.
SWP – 07 : Operations safety huddle.
SWP – 08 : Control & monitoring of slippery areas in plants.
SWP – 10: Lock out and tag out procedure.
For updated SWP details refer safe work practices manual or in website link
http://teaming.hpcl.co.in/WebApplications/VR/IS_VR/fs/Safe%20Work%20Practices/Forms/
AllItems.aspx
31.1 WORK PERMIT PROCEDURES:
Work permit system in the refinery is for carrying out various types of works after ensuring
the safety of people, equipment and material when performing any work within the refinery
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
premises. The issuer and the receiver of the permit have their responsibilities and roles before
issuing the permit. The details have been discussed it this chapter.
Based on the nature of hazards involved in the work to be carried out, the “Work Permits” are
of following types:
Type No. Type of Work Permit Color of Permit
I Cold Work Permit Yellow

II Hot Work Permit Dark Pink
III Electrical Isolation /Energisation permit Dark Blue
IV Excavation Permit Light Green
V Confined Space Entry Permit. Brown
VI Loading / Unloading of Hazardous Chemicals permit Light Blue
Note: Only the employees undergone Training on “Revised Work Permit System” and with
“Authorization Card for Work Permit” are eligible for permit issuing or Receiving based on
their nature of job.
ASSET CUSTODIANS FOR ISSUE OF WORK PERMITS:
Sr. ASSET TYPE ASSET NAME CUSTODIAN PERMIT ISSUING

No. DEPARTMENT AUTHORITIES
1 BUILDING Block-A
Concerned Nominated officer of Respective
Department Dept for the respective premises.
Block-B Concerned Nominated officer of Respective

Department Dept for the respective premises.
Block-C HR Nominated officer of the Dept.
Dispensary HR Medical Officer
Security Gates & HR HR security officer

Check Posts
Refinery Materials Nominated warehouse officer.
Warehouse
Project Project Nominated warehouse officer.
Warehouse Materials
F&S Building Fire & Safety F&S shift in charge
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
Sub-stations Maintenance Shift in-charge
Rack Rooms, Maintenance Instrumentation shift in-charge or

Instrumentation nominated Instrumentation officer.
panel rooms etc.
2 PLANTS All process units, Operations Respective Plant shift in-charge
P&U & OM&S
facilities and
CPP
3 UTILITIES Steam lines, Operations TPH shift in charge and counter
water lines , Air signed by Manager of P&U and
lines, in offsite Merox respectively.
area,
N2 lines
4 ROADS Between plant Operations Respective plant supervisor and
areas counter signed by other plant
Manager
Offsite areas Operations TPH shift Officer and counter

around tank signed by adjacent plant Manager
farms, along pipe
tracks.
North-west Respective Nominated officer.
FABRICATION boundary & east Projects / Minor
5 of O/H foam Project
YARDS
tanks etc.
Fire ground and Fire & Safety F&S shift in charge
FIRE GROUND, fire water lines
6 FIRE WATER
LINES
- Operations Area in charge on approval of GM-

FLASH / VIDEO Operations (Designated Factory
7 Manager)
PHOTOGRAPHY
- Materials Designated Materials Officer

STORAGE /
9
SCRAP YARDS
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
TYPES OF WORK PERMITS WITH DETAILS:
TYPE OF DEFINITION EXAMPLE SCOPE APPLICAB

WORK ILITY
PERMIT
Cold Work Permit for an activity Opening process Blinding & All areas
Permit which does not produce machinery. Deblinding. under
sufficient heat or spark Tightening of Hot bolting Refinery
to ignite a flammable flanges. control.
air-hydrocarbon mixture Inspection. Painting.
or a flammable Scaffolding. Grass Cutting.
substance.
Hot Work Permit for an activity Welding. Grinding. All areas
Permit that can produce a spark Gas Cutting. Shot Blasting. under
or flame or other source Burning. Soldering. Refinery
of ignition having Chipping. Hammering (metal) control.
sufficient energy to Open Fire. Use of certain non-
cause ignition, where the explosion proof
potential for flammable equipment.
vapors, gases, or dust Use of Stress relieving,
exists. Diesel preheating and
Generator. induction heating.
Electric flash Concrete chipping
unit/ flash bulb
for taking
videography /
photography.
Fire Water Radiography.
usage,
Isolation of
Fire Water
network
Hot tapping. Road Closure.
Stopping of Use of ultrasonic
steam leaks on instruments for
line using thickness
pneumatic drill. measurements.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
Electrical Permit to enable an Energizing & isolation of all electrical All areas
Isolation & equipment / facility Equipment connections at sub-stations. under
Energi electrically safe and that Refinery
sation the electrical power is control.
Permit isolated to the extent
necessary for the safe
conduct of the
authorized work.
Excavation Permit for an activity i. Road Cutting. All areas
Permit which involves under
breaking of any ground ii. Tank Dyke wall breaking. Refinery
surface by person or control.
machinery for any
purpose, including iii. Digging for cable & pipeline
penetrating the ground laying
surface to drive steel or
wooden pickets. Core
drilling, drilling for
fixings, vertical boring
into decking, floor slabs
etc. (Taking out layers
of soil using any tool)
Confined Permit for an activity Process Vessels Boilers. All areas
Space within an enclosure with (above ground & under
Entry known or potential under ground) Refinery
permit hazards and restricted Furnaces Storage tanks. control.
means of entrance and Large Diameter OWS
exit which is not pipes. manholes.
normally occupied by Effluent Switch Chemical storage
people and is usually not pits. room / shed.
well ventilated. Chemical / Entering
Process Pump Excavation more
Houses than 1.2 meter
deep
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
Loading Permit for an activity of Unloading of HCL, H2SO4 , NaOH, NH3, All areas
/Unloading loading / unloading of H2O2 and such other chemicals from a under
of chemicals having tank or other containers Refinery
hazardous potential of causing control
chemicals spillage / leak resulting
Permit into environmental /
health / property
damage.
Validity of Work Permit:
i) Permit shall be issued for single shift. Where the work has to be continued, the same permit may
be revalidated / extended shift wise for a period not exceeding Seven Calendar Days in the
succeeding shifts by authorized person after satisfying the
permit conditions.
ii) In instances like plant turn around, project jobs, Storage Tank T&I jobs work permit of extended
duration may be issued with the approval of Division Head for a period not exceeding Thirty
Calendar Days. In such cases Manager of Executing Department
should receive the permit An additional Extension of Work Permit sheet shall be used for this
purpose.(attached as in Format PSM-FR-9.17)
DSI on Generation of Work requests for Plant Maintenance (DSI-0-6):
Work request is fundamentally an instrument for requesting repairs and in kind replacement
of plant equipment through maintenance department.
Work request is also used for facilitating various plant shutdown and start-up operations like
steaming, blinding, other isolation and sanitizing methods, inert methods like hose
connection, drain & vent connection etc.
Types of jobs requiring work request: Job types for which Work Request is required to be
placed are as below:
No Job type
J-1 Requirement of Repair or in kind replacement of existing plant equipment and
facilities
J-2 Requirements of isolation, blinding, de-blinding, de-pressuring, testing, inerting,
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
system cleaning, steam-water-air hose connections for start-up shut down

operations.
J-3 Housekeeping, Cleaning, Dressing
J-4 Preventive, Predictive maintenance of existing plant equipment
J-5 Provision (part or full, modification) of external features like supports, access
structures, protective guards or covers, instrument steam tracing, external fire
fighting systems, Civil works like kerb walls, routing channels, paving, fire
proofing, Insulation, painting, stencilling, new lighting, safety boards, external
safety features, Field room facilities, personnel communication systems.
Approvals for different types of jobs are authorized as below:
Job Type Approval by

J-1 Plant Shift In charge
J-4 Area Maintenance Manager
J-5 Plant Manager
In all the case Except J-4 , The work requests are generated by the respective plant shift in
charge and they are routed to respective officials based on the job type and priority.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
Job Type approval:
Priority No Approval By
0 Division Head or above
1 Division Head or above
2 Plant Manager
3 Shift In charge
4 Plant Manager
5 Shift In charge
Quantitative limits for raising work requests:
Maximum work requests per shift
C-1 C-2 C-3 C-4 C-5

J-1 5 n.u.l n.u.l n.u.l n.u.l
J-2 n.u.l n.u.l n.u.l n.u.l n.u.l
J-4 n.u.l n.u.l n.u.l n.u.l n.u.l
n.u.l : No upper limit
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• The quantitative limits for raising work requests is to avoid bunching of work
requests, not intended that in every shift work request rising is necessary.
• In case of requirement crossing the quantitative limit, then work request should be
routed through division head.
• At the time of placing work request an assessment of the existing area of the work
environment to be carried out.
• Information on plant process conditions for non-routine work PSM-FR-9.7 is to be
attached to every work request.
• It is ensured that for all the recommendations of the OSI, IWL, work request is
compulsorily raised within 2 working days of its receipt.
GUIDELINE FOR EXPLANATORY NOTES TO WORK PERMIT FORMS
Sr. Checklist Explanatory notes

No points
1 Exact Location Exact location of the area or the unit in which the work is to be carried
(Area / Unit / out shall be written against it. For example: CDU-I, 2-F-01 Tank farm of
Equip no) 20-D-4, Tank 501 etc.
2 Description of Precise description of the work to be performed shall be written.
work Sketches should be attached wherever possible to avoid
miscommunication.
3 Equipment / Equipment or area where work is to be conducted should be inspected to
Area inspected ensure that it is safe to carry out the work and assess other safety
requirements / stipulations. In case of equipment / vessel box-up permit,
it should be ensured that the work is complete, all personnel are out, no
maintenance gear is left behind and debris removed.
4 Surrounding Unsafe conditions for performance of work may arise from surrounding
area checked / area. It should be cleaned up
cleaned to remove flammable material such as oil, rags, grass etc.
5 Sewers, Flammable gases may be released from nearby sewers. Hot un-insulated
Manholes, surfaces (equipment / pipelines) may provide a source of ignition and
Closed Blow therefore, these are to be properly covered to prevent fires.
Down (CBD)
etc. and Hot
Surfaces
covered.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
6 Hazard from Other activities (routine / non-routine) being carried out near-by, which
other routine / can create conditions unsafe for performance of the permit work, should
non-routine be taken into consideration and the concerned persons should be alerted
operations accordingly.
considered and
persons alerted:
7 Equipment Before issuing a permit, it shall be ensured that electrical isolation has
electrically been done, switches are locked-out and cautionary tags duly signed with
isolated and date and time are attached.
tagged
8 Running water Running water hose and portable fire extinguisher are required to flush /
hose / Portable dilute in case of release of any hazardous chemical or to quench sparks
extinguisher and to put out small fires immediately.
provided / Fire In order to meet any contingency, it should be ensured that the fire water
water system system including firewater pumps, storage, network etc. is checked and
available kept ready for immediate use.
9 Equipment Equipment, for which the work permit is being issued, should be isolated
blinded / from the rest of the plant in order to ensure that there is no change in the
disconnected / work environment with respect to presence of toxic / flammable gases,
closed / isolatedliquids, hazardous chemicals etc. in the course of the work. Blinding is
/ wedge opened one of the most effective ways of isolation. Blinds should be installed as
close to the equipment as possible. If lines cannot be blinded, these
should be disconnected and the open ends should be made safe by
installing pipe caps / plugs, blind flanges etc.
10 Equipment Equipment under pressure should be depressurized after isolation. This
properly drained should be followed by draining / purging / water flushing etc. as the case
/ may be.
depressurized Equipment containing liquid hydrocarbons should be drained
completely. There may be a possibility of overlooking of liquid collected
in pockets or inaccessible areas such as level gauges, small nozzles /
bleeders on vessels, laterals in pipe work etc. All low point drains should
be in unplugged condition.
11 Equipment Purging of equipment (tanks, vessels, pipelines etc.) is done to make
properly them free of flammable hydrocarbon and toxic gases. Steam / Inert Gas
steamed / is used for gas freeing of vessels and pipes in refineries and other
purged locations. Other means of purging is by displacement with water and
final traces of gas removed by properly earthed air eductor. All high
point vents should be unplugged while purging. It should be done in a
systematic manner to cover the entire equipment / plant and continued
till the concentration of toxic / flammable gas is lowered to allowable
level.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
12 Equipment Water flushing is an effective means of cooling, cleaning and even gas
water flushed freeing of equipment. It is also employed to remove traces of acids /
chemicals. Equipment metallurgy must be considered before using sea /
saline water. Sometimes, flushing with demineralized water would be
necessary depending upon the metallurgy of the equipment.
13 Gas / Oxygen Gas test includes measurement of:
deficiency test (i) Hydrocarbons, (ii) Oxygen Deficiency by Oxygen Meter, (iii) Toxic
done gases like Hydrogen Sulphide, Carbon Monoxide, Nickel Carbonyl, and
Chlorine etc. by techniques like Indicator Tube method, Lead Acetate
Paper etc.
Measurement of lead in air is required for entering tanks (which stored
leaded gasoline earlier) and personal protective equipment shall be worn
before entering the tank
14 Shield against Hot works like welding, grinding etc generates sparks which can provide
sparks provided source of ignition to the surroundings. In order to protect operating area
from the hazards of sparks generated, shields are to be provided to
contain the sparks generated. The shield material should be non-
flammable and should be kept wet with water.
15 Proper Where natural ventilation is not available, fans / air eductors are
ventilation and provided. These are also required for
lighting Speedy dispersal of fumes generated by welding job. Only approved
provided reduced voltage extension lights (not exceeding 24 volts) are to be
allowed for work inside vessels from consideration of personal safety.
16 Proper means of Proper means of exit is required in case of emergencies developed on
exit provided account of the work or otherwise. Availability of an alternate route of
escape should be considered.
17 Area cordoned To prevent any unwarranted entry in the work area and also to caution
off and caution other personnel taking actions which may endanger people working on
boards provided the permit job, precautionary tags / boards are to be provided to display
like "No Entry" sign on roads or "Caution - Men at Work Inside" on the
manhole of a vessel, Danger - Radiography in progress" etc.
18 Portable As a precaution against static electricity generation, portable equipment /
equipment / hose nozzles e.g. nozzle of a shot blasting gun, are to be grounded. Use
Hose nozzles of hydrocarbon lines for earthing should be avoided. 30
properly Milli-amp circuit breaker shall be installed on electrical circuits / cables
grounded feeding power supply to portable equipment.
19 Standby person Whenever a person is entering in a confined space, minimum two
provided for designated persons shall be kept at the manhole or entry point. The
entry to designated person shall be in constant communication with the persons
confined space inside the confined space.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
20 Standby Depending on the criticality of the job, work permit issuer shall decide
personnel the type of standby to be provided i.e. from which department, of which
provided for fire level, how many and also additional firefighting support facilities etc.
watch from
Process /
Maintenance /
Contractor / Fire
Department
21 Iron Sulphide Pyrophoric substances may be present in operating area / equipment
removed / kept handling hydrocarbon. Iron Sulphide scale is the most common
wet pyrophoric substance encountered. These should be either removed to
safe locations or kept wet all the time to prevent their auto-ignition.
22 Clearance For any excavation work which may affect underground sewers /
obtained for telephone lines / cables / pipelines
excavation / etc., clearance shall be obtained from all the concerned sections.
Road cutting / Markers should be put around the area where excavation is to be done
dyke cutting etc and the depth to be indicated in the work permit.
Road cutting can hamper the movement of the fire vehicles; initial
clearance should be obtained from Fire Department and final approval
from the higher designated authorities.
When the dyke is cut, any mishap in the tank farm can lead to a free
flow of oil to outside the bund. A higher level authority should be
designated for authorizing dyke cutting. Further, it should be ensured
that dyke would be reconstructed in the shortest possible time.
23 Checked spark No vehicle / engine without spark arrestor shall be permitted in
arrestor on operating areas.
mobile
equipment
24 Checked for oil / Before undertaking hot jobs, a check should be done for oil / gas trapped
gas trapped behind lining in the equipment.
behind lining in
equipment
1. BASIC RULES OF WORK PERMIT SYSTEM:
1.1 It is the policy of the company to ensure the safety of people, equipment and materials
when performing any work within the Refinery premises.
1.2 Jobs shall be performed only after obtaining the stipulated permit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
1.3 Permit shall be issued / renewed and received only by personnel designated for the same
and are to be signed by the issuing / renewing and receiving personnel.
1.4 All necessary checks and tests shall be conducted to ensure safety of the jobs prior to
issue of permits. All precautionary measures required to be taken shall be clearly
indicated on the permit and their compliance ensured before handing over the permit to
receiver
1.5 Permits shall be worded so as to limit the work to the designated areas / equipment /
facilities, agencies and time.
1.6 If any of the conditions vary during the work which may affect safety of human beings
and equipment, the job is to be stopped, the permit to be withdrawn and given back to
the issuer. Reason for withdrawing the permit to be mentioned on the permit
1.7 If a permit is withdrawn, the work should be restarted only after safe conditions are
established back and clearance obtained from the issuing / renewing authority and Fire &
Safety.
1.8 Work permits shall be made readily available at the work site for verification by
concerned personnel. The permit shall be put in a plastic folder and same will be
displayed at work site. Failure to present the permit on demand for verification shall
result in stoppage of work.
1.9 Work permits are valid only for the time period specified in the permit. Normally the
permits will be issued for the General Shift timings i.e. 08:00 Hrs to 16:30 Hrs.
1.10 If the job is to be continued beyond the time limit specified in the permit, it has to be
renewed at the beginning of the next shift.
1.11 Permits up to maximum of 30 days can be issued for major shutdown / project jobs.
However, this permit must be presented every day prior to starting of the work in each
shift by the concerned Executing person to issuing authority for renewal.
1.12 While renewing a work permit that has already been issued by another Issuing authority
of the concerned department, the renewing authority is no way relieved of the duties and
responsibilities specified by the original issuing authority.
1.13 At the time of renewal of a permit or when the job is in progress, if the issuing or
renewing authority as the case may be feel that some additional conditions or precautions
are to be stipulated or any of the conditions or precautions already stipulated are not
necessary based on the prevailing conditions, a new permit is to be issued incorporating
the changes and the previous permit should be withdrawn.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
1.14 All work permits must be closed on completion of the job by the Supervisor of the
executing department / section and the permit duly signed for closure is to be returned to
the issuer. Work permits once closed cannot be renewed.
1.15 The work permit should be issued for one job one location only. Separate permits to be
issued for performing separate work on same equipment.
1.16 No hot work shall be allowed to be included in the hot work permit already Issued for
other jobs.
1.17 Whenever there is a job in pipe track which is in close vicinity (5 meters) of process unit
then prior to issuing of the permit the clearance from the concerned unit in - charge
should also be taken.
1.18 Each hot work permit shall have only a single job with scope written on it and the
person who is taking the gas test must sign on the permit.
1.19 Always "Receiver" has to sign the permit last, after taking all the necessary approvals
and understanding the necessary safety measures.
1.20 The job demarcation of each contractor shall be clearly defined on the permit
beforehand, incase more than one contractor working in the same area.
2. SPECIFIC RULES FOR WORK PERMIT ISSUING / RENEWING PERSONNEL:

The issuing/renewing authority is primarily responsible for the safe execution of the job
covered under the work permit and as such is to perform the following duties:
2.1 Analyze and determine the condition of the facility and the area involved and Stipulate
necessary measures to be taken to ensure safe execution of the work.
2.2 Stipulate precautionary measures such as area preparation, blinding / isolation / tagging,
provision of safety and fire protection equipment, standby personnel etc. in the permits
and ensure the compliance.
2.3 Stipulate preparatory, preventive and precautionary measures to be carried out and
ensure their compliance.
2.4 Coordinate with other departments / sections wherever precautions are necessary to be
taken from their end also and counter signature to be obtained prior to issuing of the
permit
2.5 Verify and certify installation and removal of blinds / isolation and their tagging.
2.6 Perform necessary gas and other tests and the person performing the gas test to sign on
the permit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
2.7 Ensure that the facilities and the area at and around the place where permit is issued /
renewed are made safe prior to commencement and also during the progress of the job.
2.8 Check periodically the progress of the job permitted and stop the job if conditions
become unsafe.
2.9 Ensure that while hot work is in progress, no other work conducive to hazards is
permitted in the vicinity eg. repairs to Oil or Gas lines, bleeding or sampling of
flammable materials etc.
2.10 Ensure that all personal protective equipment / clothing stipulated in the work permit are
available at site before commencement of work and the same used by the personnel
while performing the work.
2.11 If a hot work permit is issued or if Hot Work Permit continues beyond the normal office
working hours (after 4.30 p.m.) then the permit is to be renewed as per permit renewal
procedure.
2.12 If the job is being done through contractor and in case more than one contractor is
working in the same area then the issuer shall clearly define beforehand the demarcation
of each job per contractor to avoid over lapping of different jobs.
2.13 The issuer shall give clearance to the Job Engineer for carrying out the hot jobs and not
directly to the contractor personnel.
2.14 In case of Hot Work Permit for cutting, welding, grinding etc. the issuer or his
representative and the receiver must be present for the first cut / first weld / first
grinding.
2.15 For unit housekeeping, mopping (regular contract) Operations Supervisor will give cold
work permit to contractor Supervisor directly.
2.16 Ensure that "Receiver" returns back permit duly signed on completion of job and
"Housekeeping" is maintained. Scrap is shifted to designated area. Returned closed
permit are preserved for 30 days.
3. SPECIFIC RULES FOR WORK PERMIT RECEIVING / EXECUTING

PERSONNEL:
Although a work permit has been issued for performing a certain job, no way it relieves
the supervisor of the executing department or the person executing the work of their
responsibility for safe execution and completion of the job. The receiving authority /
executing personnel is / are responsible for the compliance of the precautions /
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
conditions prescribed in the permit. Their duties and responsibilities include the
following:
3.1 Carry out Job Hazard Analysis and ensure precautions as per that.
3.2 Secure necessary work permit from the concerned department before commencement of
the job.
3.3 Provide for and comply with all necessary precautionary measures stipulated in the
permit.
3.4 Ensure basic safety precautions like usage of Safety belts, provision of ELCB (of
30mA), Flash back arrestor to cutting torch, DCP extinguisher / charged fire hose are
provided as per the need of the job. Ensure that DCP and fire hoses are in good operable
condition and available at site prior to start of the permit
3.5 Take extra care when commencing the work, especially while breaking flange joints,
cutting through lines, striking an arc for the first time etc. Permit receiver to be present at
job site for first cut or first weld.
3.6 Ensure safe working practices throughout by continuous supervision (Either by

executing personnel or contractor personnel)
3.7 Ensure the availability of all the Personal Protective Equipment / Firefighting equipment
at site before commencement of work and also ensure that the same are used during the
work.
3.8 Stop the job if conditions become unsafe and report to the issuing / renewing authority.
3.9 Ensure that the work permit is duly put in a plastic folder and displayed at the work site
for verification.
3.10 Ensure that no blinds or other isolations specified for the work are removed or disturbed
during the work.
3.11 Ensure usage of grit blasting hood while Grit Blasting with air supply line connected
with vortex cooling system and job area is fully covered to contain dust particles.
3.12 Grit blasting hopper to be tested at 1.5 times of maximum working pressure. Contractor
should maintain test certificate.
3.13 Ensure that 24 V (Ac) hand lamps are used in the confined space.
3.14 Ensure that grade area is barricaded with red & white colour tape to cover excavated area
or in case of material handling at overhead.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
3.15 On completion of the job, measures and maintain normal conditions at the area of work.
Clear all scrap material and maintain good housekeeping.
3.16 On completion of job the receiver will sign for closure of the permit at space provided at
the back of the permit and return the permit to the issuer.
3.17 Receiver to ensure that registration number is entered in the permit before commencing
the job
3.18 Ensure that the Contractor has received a booklet on "Safety Regulations for
Contractors".
31.1.1 Procedure for Cold Work Permit:
Issuing Authority:
Cold work permits can be issued/renewed by authorized personnel of the department to

which the equipment or area belongs.
31.1.2 Procedure for Hot work Permit:
Responsibilities of Renewing/Issuing Authority:
• Hot will permits will be issued/ renewed by duly authorized supervisor of the owner
department of the equipment or the area.
• Identify the hazards and note on the permit. Suggest additional safety measures to carry out
the job.
• Permit is valid for one shift and may be extended for one subsequent shift if condition
permits. Issuer to note the extension of permit on his copy and in TOB.
• Issuer and receiver of the permit should be company employees, will arrange to deposit Fire
House copy of the permit at box provided at MOI control room by 10:00 hrs, 18:00 hrs and
02:00 hrs.
• After office hours the hot work to be carried out with a fire watch from Operations
department/ executing department/ F&S, as decided by the permit issuing authority.
• If the permit is renewed, the issuer will inform fire house on telephone.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
31.1.3 Procedure for Electrical Work Permit:
Duties of Permit Issuer:
The operations department personnel/owner of the equipment will raise the perm in the
prescribed format and fill the permit as required. On receipt of permit from electrical section
duly filled and signed then only issuer can take further action.
Explanatory Notes for Hot Work Permit Form:
Excavation/ road cutting/ fire water usage/crane operation/ radiography/ vehicle entry into
restricted areas:
• Clearance obtained for excavation from Electrical departments and telephone in charge: For
any excavation which may affect underground electrical cables, electrical maintenance
should give clearance. Markers would be put around the area where excavation can be done
and depth should be indicated in the work permit. Clearance from telephone in charge to be
taken to ensure that no telephone cables get damaged while excavation.
• Shoring Provided: If the depth of excavation is mote than 2 meters, shoring is to be provided
to avoid the caving in of the earth.
• Equipment/ Area Inspected: To be checked to ensure it is safe to carry out work and access
other safety requirements.
• NRV provided on fire inlet line: In case of fire water usage for filling water in the tank or
flushing the pipelines, NRV is to be provided on fire water line to avoid the back up of tank
content/ line content into fire water network.
• Overhead HT cables Isolated: In case of crane entry and movement, the issuer of the permit
will inform the electrical department to isolate the overhead electrical cables if there is a
chance of crane touching the cables.
• Flame arrestor on exhaust checked: Every vehicle must have a flame arrestor on the exhaust.
• Area Cordoned off: In order to prevent unauthorized entry of personnel and to avoid
accidents due to excavated pits, work areas must be cordoned off by red and white tape.
• Danger Sign Displayed: To prevent unwanted entry into the work area and to caution the
people, danger sign boards must be displayed.
• Hydrocarbon Gas testing Reading: Hydrocarbon presence to be tested by explosive meter to
ensure that the area is free of hydrocarbon. The person carrying out the gas test has to write to
value and put his signature at the designated place.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Clearance from F&S: In case of crane movement and road closure, the issuer of the permit
will inform F&S department and take shift F&S officer’s signature at the prescribed place in
the permit.
Vessel Entry/ Vessel Box-up/ Hot work/ hot tapping:
• Equipment/ Area Inspected: To be checked to ensure it is safe to carry out work and access
other safety requirements. In case of box-up permit, it should be ensured that the work is
complete, all personnel are out, no maintenance gear is left behind and debris removed.
• Surrounding area checked/ cleaned: Areas should be clean and free of any oil, rags, grass, etc.
• Sewers, manholes, CBD etc and hot surfaces covered: The hydrocarbon vapors may be
present in these areas, which may be ignited during hot jobs. Therefore such areas should be
covered. Hot un-insulated lines/ surfaces may provide a source of ignition. Therefore these
are to be covered properly to prevent fires.
• Consider hazard from routine/non-routine operations and concerned personnel alerted: Other
activities being carried out nearby areas, which can create conditions unsafe for performance
of the intended job. Therefore these activities should be taken into consideration and the
concerned personnel should be alerted accordingly.
• Equipment electrically isolated and tagged: Before issuing the permit for starting
mechanical/electrical job, it has to be ensured that the equipment is electrically isolated and
switches are locked out, cautionary tags duly signed with date and time area attached.
• Running water hose, portable extinguishers provided and fire water system checked for
readiness: They are used to flush/ dilute in case of release of any hazardous chemical or to
quench sparks and to put out small fires.
• Equipment blinded/ isolated/ disconnected/ closed/ wedged open: Equipment on which work
permit is being issued should be completely isolated from the rest of the plant with which it is
connected during the normal operation, in order to ensure that there in no change in the work
environment with respect to toxic/ flammable gases, liquids, hazardous chemicals, etc.
• Equipment properly drained and de-pressured: Equipment under pressure should be de-
pressured after isolation. This will be followed by draining/purging, water flushing as the
case may be.
• Equipment properly steam purged/ water flushed: It is done to make equipments free of
flammable hydrocarbons and toxic gases.
• Gas/ oxygen deficiency test done and found ok: Area should be free of hydrocarbon and same
has to be tested by explosive meter. In case of confined space entry, in addition to
hydrocarbon, presence of oxygen and toxic gases to be checked. The results have to be as
follows, only then conditions are considered to be safe for working.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
a) Hydrocarbon = 0.
b) Oxygen Content > 19.5%.
c) Hydrogen sulfide < 2 ppm.
d) CO < 10 ppm.
• Shield against spark provided: It is provided to protect the operating areas from the source of
ignition generated during welding.
• Proper ventilation and lighting provided: Where natural ventilation is not available fan/ air
educators are provided. Wherever sufficient light is not available, lighting has to be arranged.
• Proper means of exit provided: proper means of exit is required in case of emergencies
developed on account work or otherwise. Availability of an alternate route should be
considered.
• Precautionary tags/boards provided: To prevent any unwarranted entry and also to caution
other personnel taking actions which may endanger people working on the permit job.
• Portable equipments/ hose nozzles properly grounded: As a precaution against static
electricity generation, portable equipment/ hose nozzle is to be grounded.
• Check flame/spark arrestor on mobile equipment: No vehicle to be allowed without them.
• Welding machine checked for safe location: It should be in non-hazardous and ventilated
areas. It should have proper supervision while welding job is in progress. It should be
switched off immediately after completion of job.
• Checked for earthing/ return connection to the equipment being welded: All earthing
connections should be given as per welding codes.
• Oxygen and acetylene cylinder kept outside the vessel/tank: While cutting/welding in
confined spaces, oxygen and acetylene cylinders should be outside and their hoses should be
in healthy condition.
• Standby person provided for vessel entry: Standby person has to be present at the man way or
entry point holding the rope connected to safety belt of person working inside. In case of
emergency inside or outside the vessel, the standby person can pull the person out.
• Standby person provided for fire watch from Process/ Maintenance/contractor/ F&S:
Depending on the criticality of the job, the work permit issuer will decide the type of standby
to be provided that is from which department and of what level, how many and also
additional fire fighting support facilities.
• Iron sulphide removed and kept wet: Pyrophoric substances may be present in the operating
area/ equipment handling hydrocarbon. Iron sulfide scale is the most common pyrophoric
substance encountered. This should be either removed to safe location or kept wet all the time
to prevent auto ignition.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Checked for oil/ gas trapped behind lining in the equipment: Many times oil/ gas trapped
behind linings depicts itself in the form of swelling and can be confirmed by way of drilling
holes.
• Area cordoned off: In order to prevent un-authorized entry of people and to avoid accidents
during excavations work areas are to be cordoned off.
• Clearance obtained for dyke cutting: Applicable to offsite tank dyke cutting.
• Inspection Approval: While it is presumed that modification job will be undertaken always
with the approval of designated authority, it is further to be noted that hot tapping should be
undertaken after an approval from Inspection personnel. Continuous flow in the line is to be
ensured. Gas and airlines are not permitted for hot tapping work.
Exempted Areas:
The following areas do not require a work permit to carry out a job.
• Project Building
• Machine Shop
• Fire House
• Garage
• Contractor Yard
• Dispensary
• Administration and Technical Service Building
• South and main gate
31.2 CONFINED SPACE ENTRY PROCEDURE:

Any place is termed as confined space if it meets the following criteria:
a) It is large enough and configured such that an employee can bodily enter and perform the
assigned task.
b) And has limited or restricted means for entry or exit.
c) And is not designed for continuous employee occupancy.
d) And it may contain or produce dangerous contaminants.
The examples of confined space in refinery are vessels, tanks, furnaces, boilers, pits,
manholes, sewers, heat exchanger shells (open from one end), excavation deeper than 1.2
meters, entry on floating roof tanks when roof is more than 3 meters below from the top of
tank shell, AC ducting systems, etc.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
31.2.1 Hazards Involved:

• Oxygen Deficiency (less than 19.5% volume): This leads to asphyxiation.
• Presence of toxic, corrosive, hazardous materials: Maximum allowable are H2S= 2ppm,
HC=20% LEL, CO= 10 ppm, NH3=25ppm.
• Presence of flammable, combustible, explosive or pyrophoric materials: They lead to
incidents like fire, etc.
• Restricted Access- Limited number of entry, exit points: This can lead to problem of
evacuating the entrants immediately in case of an emergency.
• Restriction of freedom of movement inside confined space: This can cause unwanted
emergencies due to space constraint problem.
• Falling/tripping hazard: Falling hazards can cause injuries, accidents, etc when any object
falls from higher elevations. Uneven flooring/obstructions in the walk way etc. Can cause
tripping hazard.
• Inadequate Illumination/visibility/communication: this can cause unwanted incidents and
confusion in case of emergencies.
• High temperature and humidity: Surfaces of high temperature can cause injuries
humidity/vapour can cause suffocation problems and breathing problems.
• Electrical, static or radioactive hazards: This can cause electric shocks to human life and may
create sparks/fire, etc.
• Mechanical Hazards: Mechanical hazards can cause accidents, incidents, injuries to human
life.
31.2.2 Preparatory work Before Issuing Confined Space entry Permit:
• All personnel involved with confined space entry should be aware of hazards and no person
should enter the confined space unless entry permit has been obtained by the concerned
supervisor.
• All the connected lines to the confined space have to blinded or disconnected by blind
flanges. No entry can be given without positive isolation.
• Power driven internal equipments such as mixers shall be disconnected electrically by an
authorized person.
• Mechanical ventilation equipment shall be properly grounded (earthed) to dissipate any static
charges. Pneumatic air movers (educators) and exhaust fans are recommended for this
purpose. Electrical powered fans if any shall be explosion proof types. Air intake of forced
ventilation equipment shall be from an uncontaminated location.
• Utility or instrument air cannot be used as means of ventilation or as air supply to breathing
apparatus. All entrants shall wear personal monitors as required (H2S, CO, O2).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Adequate illumination shall be provided using 24V or below explosion proof lamps. Use of
any electrical equipment above 24V shall have ‘earth leakage circuit breaker’ and also F&S
department approval.
• Wherever possible, the confined space shall be adequately ventilated to enable entry without
requirement of respiratory protection equipment. At least two manways should be open in
every chamber of vessel for proper ventilation.
• Care should be taken when ventilating vessels containing ‘pyrophoric iron scales to avoid
spontaneous ignition. In such situation entry with required safety precautions or handling
pyrophoric iron in wet condition should be adopted.
• The confined area shall be made safe for entry by such methods as depressurizing, venting,
draining, steaming, washing and ventilating. Radiation sources if any shall be removed.
• Shift in charge should be aware of possible behavioural effects of hazard exposure in
confined space area before issuing the work permit at confined space area.
31.2.3 Gas Testing Procedure:
• Shift in charge has to ensure all the meters/instruments to be used for gas test are ready to
use.
• Technicians have to ensure that the meter is in good condition and it has to be checked and
logged in TOB at the starting of the shift. If any problem is found with the instruments, it has
to be brought immediately to shift in charge’s notice.
• The gas tests have to be carried out and the testing result values have to be recorded in the
permit. F&S personnel can be called for entry into critical areas for witnessing gas test and
providing guidance as required.
• First, the meter should be checked in fresh air (preferably in safe zone/field room). Batteries
should not be changed or charged in hazardous area. Testing immediately after stopping the
purge may give misleading results. Purge medium or air mover should be stopped
temporarily for 15 minute or more depending on the size of space prior to measurement.
• Initially the test has to be done from outside the confined space, using a long probe. If the
initial gas tests indicate a concentration above the permissible limits, further was freeing
should be done until the gas concentration is within permissible limits.
• Test result should be representative of the entire confined space. Hence the need may arise to
enter for gas testing at different locations inside large tanks or towers and complex vessels
based upon number of man ways, toxic material handled, size of vessel, etc to get a
representative result. Operation shift supervisor should decide at initial stage, the need for
entering the confined space for gas testing.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• The job executing supervisor should witness or satisfy himself, that actual gas test has been
done before issuing and accepting the permit. Receiver can refuse the permit if proper gas test
was not done. For critical entries, the receiver should accompany the gas tester up to the man
way.
• At least 13% oxygen is required to obtain an accurate LEL reading from a combustible gas
meter. Hence, these cannot give a proper reading in atmospheres such as vessel purged with
steam/nitrogen. Hence LEL and O2 shall be measured simultaneously.
• Gas meters should be calibrated once in a month and certified by HPCL instrumentation
section. Record for each gas tester is maintained by instrumentation section. Next calibration
due date should be marked on the tester.
31.2.4 Confined Space Entry Permit:
• The permit receiver should give “safety pep-talk” to entrants about the hazards and
precautions prior to entry.
• The receiver has to provide means for easy exit and entry of personnel into and out of the
confined space. Safety rope should be provided where required.
• Hot work permit has to be issued in case of confined space entry and should be completely
filled. Non-relevant items should be struck off.
• The issuer has to make the receiver aware of the hazards involved in confined space entry and
precautions to be taken.
• Where atmosphere within confined space is initially safe, but there is a reason to believe that
it may become unsafe during the period for which entry is authorized (from emission of
fumes from sludge or deposits contained in the space or welding fumes), continuous gas
monitoring is required. The same has to be mentioned on the permit at the time of issuing.
31.2.5 Communication at Confined Area:
• Shift in charge should make effective communication visually or by voice with the entrants,
effective means of communication should be available. Intrinsically safe hands-free
communication sets should be preferred.
• In IDLH (immediately dangerous to life or health) atmosphere, a common communication
link system should be provided and used by personnel who are entering, standby, and
maintaining the life support system. IDLH values for toxic gases are H2S =300 ppm and
CO= 1500 ppm.
• Shift in charge should ensure that all the entrants should be evacuated if the communication
is interrupted.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Shift in charge may enter a confined space to attempt a rescue with the help of F&S
personnel and co-ordinate for rescue operations.
• Shift in charge should monitor all the activities inside a confined space to determine if it is
safe for entrants to remain in the space and can order all the entrants to evacuate in case he
feels the presence of any prohibited condition.
• F & S personnel have to be communicated as soon as the shift in charge determines that
authorized entrants may need assistance to escape from confined space hazards.
31.2.6 Requirements for Entry with Respiratory Protection:
• Entrants should wear air supplied respirators in oxygen deficient atmospheres, when toxics
are beyond TLV and where atmosphere within confined space is initially made safe, but there
is a reason to believe that it may become unsafe during the period for which entry has been
authorized.
• Under no circumstances chemical cartridge/canister type gas masks should be used for
confined space entry. Particular respirators have to be used if required.
• Receivers have to ensure that air supplied respirators are in good condition, well maintained
and inspected according to manufacturer’s specifications.
• Breathing apparatus users should be medically certified and properly trained to use breathing
apparatus.
• Entrants should wear harness attached to lifelines and be attended by an attendant who should
have breathing apparatus and clothing ready for use outside the confined space.
• In IDLH atmospheres, entrants shall wear breathing apparatus or airline mask attached with
standby escape set. Rescue arrangements should be made ready with the help of F&S.
31.2.7 Additional Requirements for Inert Entry:
Creating inert atmosphere is required where it is impossible to gas free below 20% LEL
and/or presence of pyrophoric material. Inert atmosphere are IDLH due to oxygen deficiency.
• Oxygen concentration in the inert confined space should not exceed 5%. Hydrocarbon should
be below 100% LEL at the manway. LEL reading inside is not required.
• Issuer has to ensure continuous oxygen monitoring and alerting the attendant to evacuate
entrants if oxygen level is exceeded. Audio-visual alarm is recommended.
• The people not entering the confined area have to wear respiratory protection if the effluent
from the confined space contaminates the air.
• Independent source of air for different people with low pressure alarm and escape cylinder
attached to waist shall be provided.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
31.3 PROCEDURE FOR OPENING PROCESS EQUIPMENT AND PIPING:
In the refinery any maintenance job needs a preparatory work prior to conducting the job.
When any jobs (cold or hot) has to be done in areas where flammable/hazardous mixtures are
likely to be present, the isolation of equipment involved in the job, has to be done in a proper
and scientific way for the safety of the equipment and personnel.
31.3.1 Purging/ Isolation of the Equipment:
Before any maintenance job is done in the plant, it is necessary to remove all flammable or
toxic gases from the system. Inert gas, nitrogen or steam may be used for purging. Water is
used for flushing after ensuring that the equipment can carry weight of water involved. The
part of the plant or the system to be purged is to be isolated either by closing appropriate
valves or by proper blinding. No valves should be considered leak proof and in any the cases
of maintenance jobs. Isolation of equipment is to be done by blinding. A blind list should be
prepared for isolation of equipment and check shall be done to comply with it.
If the line to be welded has contained flammable material it must be drained and section
should be disconnected at both ends. The whole section or the isolated portion should be then
gas freed and tested before welding commences. Where isolation and gas freeing are
impracticable, the line after draining should be washed thoroughly with water and
welding/hot job while charged with low-pressure steam or filled with water.
31.3.2 While opening any flange joint for installation of blind, the following procedure must
be followed:
• Wear protective clothing and appropriate eye/face protection.

• Ensure adequate working platform is provided.
• Initially flange bolts to be slackened slowly by standing upwind direction and cross check for
presence of flammable or toxic gas, blots opening can be performed at a faster rate.
• Removing flange bolts leaving a minimum of two bolts, then loose last two bolts without
completely removing the nuts. Spread the flanges to install blinds. Always open flange on the
side away from the person so that any sudden release will be directed away from the
personnel.
• The presence of concerned operation technician is a must for any emergency help, like
further isolation etc.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Hot cutting for flange nut bolts will be permitted only when presence of flammable of toxic
gases is ensured zero.
31.3.3 Mud Packing:
Most common method used for plugging the end of pipeline for hot work is “MUD
PACKING”. The main objective of mud packing is to block the hydrocarbon vapour, which
might be present in the pipeline.
Procedure for Mud Packing:
• Cold cut the line on which the flange is to be welded.

• Insert the plug into the pipe as shown in the sketch.
• The plug must have a hollow 1” pipe connected at the centre and pipe will be extended to a
distance 5 feet away from the hot work area. The purpose of hollow pipe at the centre is to
prevent any pressure build-up on the upstream. At frequent intervals the presence of
toxic/flammable gases is to be checked and recorded so as to ensure that there is no abnormal
situation at the site. The gap between the pipe and plug shall be nicely packed with clay mud
as shown in the sketch.
• The gas coming out from the vent point to be continuously monitored.
• Once the welding is completed, the plug has to be taken out along with the mud by pulling.
Typical sketch of mud packing:

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
31.3.4 Removal of Scaling:
• After draining and isolation of the vessel is completed, the material left, such as sludge has to
be removed. A powerful jet of water applied through an open manhole can remove sludge. If
this is not possible, use reagent to dissolve the sludge/scale. The liquid may be removed
through the drain and the whole system may then be flushed with water.
• Where the scaling cannot be removed by liquid, it should be chipped away. Care in this case
has to be taken that non-sparking tools are used for chipping purposes and the area is kept
wet with water if there is even a possibility of generation of inflammable vapour.
• When process equipment is removed from a unit and must be sent elsewhere for repair, it is
operations supervisor’s responsibility to see that it is thoroughly cleaned and/or properly
tagged if it has contained flammable, corrosive or toxic chemicals or iron sulfide.
• Equipment having contained ‘sour’ stock must be inspected by operation personnel for iron
sulphide deposits. Arrangements must be made to remove them after wetting till such time
such deposits should be kept wet to prevent spontaneous combustion.
• Personnel entering tank which are not declared ‘free’ of hydrocarbon vapour should wear
breathing apparatus set. Personnel should enter with “Entry Permit” and keeping a person as
standby.
31.3.5 Preparation for Hot work after cleaning the equipment:
• All cold work cleaning rules must be observed in preparing equipment for hot work.
• When normal cold work preparation has not satisfactorily removed rust, oil or lead sludge
from internal surfaces of vessels they must be hand scrapped or if practicable, they must be
sand blasted with the nozzle bonded to the equipment being sand blasted.
• Sewers openings in the area of hot work are to be sealed to ensure prevention of flammable
atmosphere. The seal must be removed upon job completion. Sand should not be used for
sewer sealing because vapors may escape through the porous material. Pit covers can be
sealed by mud packing.
• Lines, vessels, etc which have contained flammable, toxic or otherwise injurious materials
must be carefully checked and appropriate measures taken to ensure that liquids or gases are
not entrapped between lines and vessel shell.
31.3.6 Preparation of Equipment for return to service:
• It should be ensured that all foreign materials/scales/rust etc are removed and equipment is
properly cleaned prior to giving box-up permit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• It has to be ensured that water or test liquid has been drained properly.
• Carefully inspect all the equipment that has been repaired before returning it to service in
order to be sure that all the guards and safety devices are placed back and they are in safe
condition to operate.
31.4 PROCEDURES FOR CRITICAL EQUIPMENT HANDING OVER:
31.4.1 Pumps / Turbines seal repairs:
For Handing over to maintenance:
1. Isolate suction, discharge and warm up valves.

2. Allow the system to cool down and then flush it with cutter to CBD through casing after
removing blinds on cutter and CBD of the concerned.
3. After ensuring the stock becomes light depressurize it to CBD. Open pump vent point value
for proper depressurizing.
4. Blinding is to be done for proper isolation on suction, discharge, warm-up, flushing oil, seal
oil, seal steam and CBD lines and update blinds register.
5. Isolate power to the pump & tag.
6. Isolate steam to the turbine &depressurize and blind it on steam side.
7. Issue permit, decouple turbine /pump after ensuring the above.
8. Keep equipment under maintenance display board.
Note: disconnect instrument thermocouples as per rotary.
After the seal replacement on pump/ Turbine:
1. Check BCW, seal system, seal oil systems and remove any foreign materials in and around
pump/turbine basements
2. Remove blinds on suction, discharge and warm up, CBD, seal systems, seal oil and flushing
oil. Ensure proper gaskets are installed.
3. Close pump vent, open casing drain to CBD. Throttle pump discharge PG drain valve to
remove air.
4. Open flushing oil slightly to fill casing and to remove air from downstream PG point.
5. Once oil is coming through downstream PG point, close it. Also close casing drain to CBD
and check pump blind flanges with FLO pressure (9 Kg\Cm2) for leaks.
6. De-pressure the cutter to CBD and open pump warm up valve slightly for warm up condition
(only for hot service pumps).
7. Allow rotary to do hot alignment.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
8. Allow maintenance to do hot bolting on blind flanges.

9. After hot alignment and coupling fixing, check for free movement of shaft.
10. Check no load and direction of motor rotation before coupling as per rotary/Electrical and
isolate power.
11. After ensuring all the jobs are over power to motor is to be released. Steam blind to turbine is
to be removed.
12. When all the above factors are ok place the pump /Turbine and see the performance.
13. Keep casing drain to CBD\OWS blind.
14. Ensure updating of gaskets and blind registers.
15. Remove equipment under maintenance display board.
31.4.2 Pump \ Turbine suction strainers cleaning:
For Handing over to maintenance:
1. Isolate suction, discharge and warm up valves.

2. Allow the system to cool down and then flush it with cutter to CBD through casing after
removing blinds on cutter and CBD of the concerned.
3. After ensuring the stock becomes light depressurize it to CBD. Open pump vent point value
for proper depressurizing.
4. Blinding is to be done for proper isolation on suction, discharge, warm-up, flushing oil, seal
oil, seal steam and CBD lines and update blinds register.
5. Isolate power to the pump & tag.
6. Isolate steam to the turbine &depressurize and blind it on steam side.
7. Issue permit, decouple turbine /pump after ensuring the above.
1. Check BCW, seal system, seal oil systems and remove any foreign materials in and around
pump/turbine basements
2. Close pump vent, open casing drain to CBD. Throttle pump discharge PG drain valve to
remove air.
3. Open flushing oil slightly to fill casing and to remove air from downstream PG point.
4. Once oil is coming through downstream PG point, close it. Also close casing drain to CBD
and check pump blind flanges with FLO pressure (9 Kg\Cm2) for leaks.
5. De-pressure the cutter to CBD and open pump warm up valve slightly for warm up condition
(only for hot service pumps).
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
6. After ensuring all the jobs are over power to motor is to be released. Steam blind to turbine is
to be removed.
7. When all the above factors are ok place the pump/Turbine and see the performance.
8. Keep casing drain to CBD\OWS blind.
9. Ensure updating of gaskets and blind registers.
31.4.3 LPG/ Naphtha pumps seal repairs:
1. Isolate suction, discharge and warm up valves

2. Isolate self coolant lines.
3. Depressurize the content to flare through casing vent to flare.
4. Provide steam hose connection pump D\S PG point.
5. After ensuring gas is depressurized close casing vent to flare, Open casing drain to OWS and
check if any gas is coming.
6. Observe passing of valves during depress ring to flare through of lines.
7. Ensuring system is depressurized blind S\C,D\S ,and self coolant, casing CBD\OWS and
flare systems, update blind register.
8. Isolate power to the pump and disconnect steam hose.
9. Issue permit to rotary to carry out the seal replacement job.
Note: Inform instrument people to check and repair seal pot pressure and low level switches
if any.
1. Provide steam hose at pump downstream PG point.

2. Check self coolant systems.
3. Check and remove all foreign materials in and around pump basement area.
4. Remove blinds on suction, downstream and self coolant systems.
5. Open steam and pressure test the pump for blinding flange leaks.
6. Close vents and bleeders.
7. During slight steam purge open suction valve and casing vent to flare for some time, and
close steam completely.
8. Close casing vent to flare after some time.
9. Open casing drain to displace condensate if any.
10. Blind pump casing drain to OWS\CBD.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
11. Check for no load test before fixing coupling as per rotary \ electrical.
12. When all jobs are over release power to motor and check direction of pump.
13. Place the pump online slowly and check the performance.
14. Ensure updation of blind and gasket registers.
31.4.4 Releasing and commissioning of coolers, condensers and exchangers for tube leaks:
Coolers/condensers:
1. Isolate inlet and outlet valves on shell and tube.

2. Depressurize the hydro carbon content to CBD after removing blind.
3. Cooling water is to be de-pressured to intermediate sewer.
4. Provide steam connection on shell side vent and start initial steaming.
5. After ensuring sweat steam and non passing of isolation valves stop steaming and blind both
sides shell and tube inlet and outlet lines and update blind register.
6. Again carry out final steaming for 2 to 3 hrs then stop steam.
7. Again put blinds to CBD lines.
8. Allow maintenance to carry tube leak jobs.
9. Care should be taken while bundle is pulled out and when fixing and dropping of
components.
Air fin coolers:
1. Isolate inlet and outlet valves on shell and tube. .

2. Depressurize the hydro carbon content to CBD after removing blind.
3. For attending the tube leak of one AFC, both the common inlet and outlet are to be isolated.
Power to AFC fans is also to be isolated.
4. Provide steam connection on tube side and start initial steaming.
5. After ensuring sweat steam and non passing of isolation valves stop steaming and blind both
sides shell and tube inlet and outlet lines and update blind register.
6. Carry out final steaming for 2 to 3 hrs then stop steam.
7. Put blinds to CBD lines.
8. Allow maintenance to carry tube leak jobs.
9. Care should be taken while bundle is pulled out and when fixing and dropping of
components.
10. Other standby AFC can be placed on line as per procedure after properly isolating & blinding
the AFC handed over to maintenance.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
For exchangers:
1. Isolate inlet, outlet, warm up valves, TSV’s on shell and tube sides and open bypass.
2. Steam connections are to be given to vents and depressurize to CBD\OWS on both sides.
3. Ensuring sweat steam and non passing of isolation valves blind both shell and tube side inlet
and outlet. Also carry out hot bolting of component bolts for dropping during steaming
condition.
4. Release exchanger for dropping components after closing steam valve. Disconnect it only
after final steaming for 2 to 3 hours.
5. Blind CBD lines and update blind register.
Commissioning of cooler/condenser:
1. After the maintenance jobs are over connect steam hoses on shell side vents.
2. Deblind the shell and tube sides.
3. Carry out steam test for blinding flanges at 5 to 6 Kg\Cm2.
4. When there is no leak, deblind FLO and CBD blinds.
5. Cutter flush to CBD.
6. Remove all steam hoses and cap off vents.
7. Ensuring water/cutter is displaced open inlet and outlet valves slightly keeping bypass in
wide open condition. Slowly open inlet and outlet valves and slowly close bypass valve.
8. Establish cooling water flow through cooler/condenser and close intermediate sewer valve
before establishing flow on shell side.
9. Observe pressure and temperature and slowly open valves on shell & tube.
10. Check for flange leaks if any.
11. Blind CBD\OWS and FLO lines.
12. Ensure blind and gasket registers are updated.
Commissioning of Air fin cooler:
1. After the maintenance jobs are over, connect steam hoses on tube side after isolating the
common inlet and outlet valves and power to fans.
2. Deblind the tube side.
3. Carry out steam test for blinding flanges at 5 to 6 Kg\cm2.
4. When there is no leak, deblind CBD blinds.
5. Flush to CBD.
6. Isolate all steam hoses and cap off vents.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
7. After filling with product on tube during slight steam purge by opening slightly inlet and
outlet so as to displace water to CBD/OWS, remove all steam hoses.
8. After ensuring water is displaced, open inlet and outlet valves wide.
9. Restore power to the fans for starting.
10. Observe pressure and temperature and slowly open valves on tube.
11. Check for leaks for flanges if any.
12. Blind CBD\OWS lines.
13. Update gasket and blind register.
Commissioning of exchanger:
1. After the maintenance jobs are over connect steam hoses on shell and tube side vents.
4. When there is no leak deblind FLO and CBD blinds.
5. Cutter flush to CBD\OWS.
7. After filling with cutter to displace water/condensate to CBD\OWS through top of the bundle
on shell & tube, displace cutter. Open inlet and outlet valves slightly. Keep open wide seeing
the unit conditions then close bypass valve.
8. Ensuring water is displaced open warm-up valve on crude from top to displace cutter. Slowly
open inlet or outlet valves and slowly displace cutter to CBD on shell side. Ensuring cutter is
displaced to CBD on crude side open the inlet and outlet valves, warm-up valves slightly to
prevent vapour lock. This may lead to feed failure to furnace, hence slowly open them wide
after checking unit conditions. Afterwards open inlet and outlet valves slightly. Ensuring the
conditions keep valves wide open and close bypass valve.
9. Observe pressure and temperature on both sides.
10. Slowly keep the exchanger fully in service. Check for leaks on flanges and update blind
register.
For steam generator:
1. Isolate inlet and outlet valves, TSV’s on shell and tube sides and open bypass.
2. Isolate BFW. Depressurize 42V21 level at 42E19A/B drains and blow down valves. By
opening 2”vent depressurize the system after closing PSV and warm-up valves on MP steam.
3. Steam connections are to be given to vents and depressurize to CBD\OWS on both sides.
4. Ensuring sweat steam and non passing of isolation valves blind both shell and tube side inlet
and outlet.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
5. Release exchanger for dropping components after closing steam valve. Disconnect it only
after final steaming for 2 to 3 hours.
6. Blind CBD lines and update blind register.
Commissioning of steam generators:
1. After the maintenance jobs are over connect steam hoses on shell and tube side vents.
4. When there is no leak deblind FLO and CBD blinds.
5. Cutter flush to CBD.
7. Build up levels in steam generators and 42V21 up to 30 %.
8. Keep steam generator vents open.
9. After filling with cutter displace cutter to CBD with SR through top of the bundle.
10. Ensuring cutter is displaced open inlet and outlet valves slightly keeping bypass in wide open
condition. Slowly open inlet and outlet valves and slowly close bypass of one steam
generator.
11. Keep 42V21 warm up open.
12. Observe steam generator pressure and temperature and slowly open steam outlet valves.
13. Slowly close SR side bypass and keep steam generators one by one online.
14. Close local vent and keep the steam pressure control on system finally. Blind CBD\OWS and
FLO lines. Update gasket and blind register.
31.4.5 Process Equipment: Towers, Vessels etc.:
Before opening any equipment, it should be purged to render the internal atmosphere non-
explosive and breathable. Operations to be carried out are:-
• Isolation with valves and blinds.

• Draining and depressurization.
• Replacement of vapors or gas by steam, water or inert gas.
• Take care about instrument tapping.
• Washing of towers and vessels with water.
• Ventilation of equipment.
• Opening of top manhole.
• Testing of inside atmosphere with explosive meter.
• Complete opening if inside atmosphere is satisfactory.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Analyze the atmosphere inside for O2 content and any poisonous gas.
Note: Open a vent on the upper part of the vessel to allow gases to escape during filling and
to allow air inside the vessel during draining. Ensure proper ventilation inside the vessel by
opening all manholes. For hydrocarbon or other gases, pressurize the vessel with N2 or gas
and fill in the liquid and drain under pressure. This is to avoid hydrocarbon going to
atmosphere.
Precautions before Handing Over Equipment:
Following items should be checked by a responsible operating supervisor before equipment is

handed over for maintenance after it has been purged.
a) Ascertain that equipment is isolated by proper valves and blinds.

b) Ascertain that there is no pressure of hydrocarbons in the lines, vessels and equipment.
c) Purge the system with N2 first and later by air and check for 02 content at vent and drain to
ensure that the vessel is full of air.
d) Check that steam injection lines and any inert line connections are disconnected or isolated
from the equipment.
e) Provide tags on the various blinds to avoid mistakes. Maintain a register for blinds.
f) Check for pyrophoric iron and if existing. Keep this wet with water.
g) Keep the surrounding area cleaned up.
h) Get explosive meter test done in vessels, lines, equipment and surrounding areas.
If welding or hot work is to be done also:
a) Keep fire fighting devices nearby, ready for usage.

b) Close the neighboring surface drains with wet gunny bags,
c) Keep water flowing in the neighboring area to cool down any spark bits etc.
d) Keep steam lancers ready for use.
After the above operations have been made, a safety permit should be issued for carrying out
the work. A responsible operating supervisor should be personally present at the place of hot
work till the first torch is lighted. Hot work should be immediately suspended if instructed by
the supervisor or on detecting any unsafe condition.
When people have to enter a vessel for inspection or other work, one person should stand
outside near the manhole of the vessel of for any help needed by the persons working inside.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
The person entering the vessel should have tied on his waist a rope to enable pulling him out
in case of urgency.
31.4.6 Procedure for dropping Hot well off gas burners:
• Inform to DCS supervisor before dropping burner

• During dropping and placing Hot well off gas fire, make sure stack damper is in wide
position with DCS to prevent excessive pressure developing in the furnace.
• Open hot well vent.
• Remove Hot well off gas fires from the all the hot well burners for this isolate flame arrester
inlet valve. Wait for some time till hot well gas in the line is completely burnt. After that
remove gas fires and pilot fires.
• Start steaming hot well off gas header from the downstream of flame arrester. M.P. steam
provision is available.
• Make sure that all the hot well burners are properly steamed out and then isolate flame
arrester outlet valve.
• Blind the hot well off gas line, fuel gas line and pilot line (one which is required to drop).
• Close air registers.
• Use face shield and asbestos gloves during checking and dropping of Hot well off gas burner
tips
• After dropping Hot well off gas burners with face shield and asbestos gloves check for tip
condition and line plugging condition.
• Replace the tip if required and unplug the line by soaking in oil and then with steam
• Fix Hot well off gas burner with new gaskets.
• De-blind Fuel-gas/Hot well off gas lines & pilot gas lines.
• Keep open hot well off gas individual valves and flame arrester outlet valve and start
steaming
• Ensure no leaks then stop steaming.
• Inform to DCS supervisor before placing any fire in heater.
• Ignite pilot first and put gas fire. Adjust air registers.
• Keep open flame arrester inlet valve.
• Keep one person at hot well vent valve, one person at “PA” for communication and one
person at heater to observe hot well gas fire.
• Hot well vent to be closed slowly and hot well gas fire to be to be monitored.
• Advise maintenance to carry out house keeping.
• Finally, up-date burner spares register. Blind registers.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
31.4.7 Procedure for dropping Fuel gas burners:
• Inform to DCS supervisor before fuel gas raisers cleaning.

• During dropping and placing Fuel-gas make sure stack damper is in wide position to prevent
excessive pressure developing in the furnace.
• Remove Fuel-gas fire& oil and pilot fires. Also isolate air registers.
• Purge oil gun with steam for some time to congealing fuel-oil flexible hose.
• Atomizing steam and purge steam valves are to be closed.
• Blind fuel gas line. One person to be stationed there till completion of blinding. While
slackening the blinding flange make sure fuel gas line plug cock valve is not passing for
which gas tester may be used while slackening blinding flange. If valve is not passing, fuel
gas line to be blinded. If valve is passing suspend the job.
• Check burner in-side for oil accumulation through burner view ports
• Use face shield and asbestos gloves during checking and dropping of Fuel-gas burner tips
• Keep burner drain at assembly open to drain oil inside, if any. After removing all fires&
closing air registers allow the burner to cool for 2to3hrs.
• After dropping Fuel-gas raisers with face shield and asbestos gloves soak it in the soaking pit
after cooling
• Remove and replace damaged tips of the burners with new parts after checking condition if
any, before assembling after cleaning.
• Fix Fuel-gas raisers.
• De-blind Fuel-gas line.
• Inform to DCS supervisor about completion of job and placing of fires.
• Ignite pilot.
• Adjust air registers.
• Place gas fire and then oil fire slowly.
• Check for any leaks with gas detector.
• Advise maintenance to carry to house keeping.
• Finally, up-date burner spares register, blind registers.
31.4.8 Procedure for burner’s assembly dropping:
• Inform to DCS regarding the job and ensure stack damper is in wide open condition to
prevent excessive pressure developing in the furnace
• Remove oil fire, gas fire and pilot fires and hot well off gas fire (if it is a hot well burner).
• Purge oil gun with steam for some time to prevent plugging with fuel-oil
• purge steam valves are to be closed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
• Close atomizing steam valves.

• Disconnect oil& steam flexible hoses.
• Drop oil gun, after cooling keep it sample trough for soaking and subsequently gun to be
cleaned as per procedure.
• After removing all fires& closing air registers allow the burner to cool for 2 to 3hrs.
• Disconnect pilot burner electrical power.
• Check burner in-side for oil accumulation through burner view ports
• Use face shield and asbestos gloves during checking and dropping of burner assembly
• Keep burner drain at assembly open to drain oil inside, if any.
• Drop Fuel-gas/pilot gas burners/tips as per the procedure mentioned in fuel gas burner
dropping; with face shield and asbestos gloves soak it in the soaking pit after cooling.
• Drop the burner assembly for repairs and fix a dummy plate at the bottom.
• Fix burner assembly after repairs and after removing plate at the bottom after taking
clearances from INSPECTION/TSD.
• Fix Fuel-gas/Hot well off gas/pilot burners .connect oil burner flexible hoses and oil gun.
Restore power to pilot burner.
• De-blind Fuel-gas/Hot well off gas lines and pilot gas lines.
• Lit up pilot burner and then keep Fuel-gas/Hot well off gas fires (if it is a hot well burner) as
per procedure.
• Check for any leaks at pilot gas line, fuel gas line and hot well gas line flanges with gas
detector.
• Place oil fire as per procedure and check for leaks if any after placing oil fire
Finally, up-date burner spares register, blind registers.
31.5 ELECTRICAL LOCKOUT/ TAGOUT PROCEDURES:
Multi-lock system is used to prevent injury by accidental energizing of any equipment while
it is attended by different sections/agencies:
• The executing authority and the issuing authority will jointly decide the requirement.
• The issuing authority issues the work permit to competent electrical person to isolate the
electrical equipment from sub-station.
• The competent electrical person and the executing authorities install their locks in the multi-
lock pad as per colour coding.
• Electrical and other parties sign the isolation work permit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 31
PLANT NAME: CDU II
Chapter Rev No: 0
SAFE WORK PRACTICES
Colour coding of pad locks:

a) Electrical maintenance- Brass Yellow
b) Mechanical Maintenance- Black
c) Others- Blue
• Each lock should be numbered and the key should be same number.
• After locking, the person who installs the lock is the responsible custodian of the key. The
locks should be removed by individual craft after completion of their jobs.
• If the custodian of the key has to leave the site, responsibility has to be transferred to the next
shift person.
• Electrical maintenance division shall be the last party to remove the lock only after receiving
the necessary permit.
Use of “DANGER-DO NOT OPERATE” tag with isolation by local switch shall be limited
to minor electrical jobs carried out by Electrical Maintenance division, such as re-lamping.
Electrical Isolation Procedure:
• Electrical isolation may be required before starting work on or near electrical equipment to
avoid electric shock and other hazards. The extent of isolation required will depend on the
nature of work.
• Requirement of isolation and extent of isolation shall be jointly decided by the issuing
authority and executing authority by using electrical isolation permit.
• When multiple sections/ agencies are involved, the multi-lock system shall be followed. If
only electrical maintenance is involved they may use single lock.
• Wherever the possibility of electric shock or injury is expected due to inadvertent staring,
lock of power circuit at substation is mandatory. Locking the control circuit at local switch
shall not be considered as adequate.
When an electrical circuit/equipment is fed from two different sources of power supply, both
the source of power to be switched off to avoid back feeding.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
STANDARD OPERATING PROCEDURES OF PROCESS EQUIPMENTS
EQUIPMENT OPERATING PROCEDURES
32.1 CENTRIFUGAL
PUMPS
32.1.1 INTRODUCTION
A centrifugal pump is a rotodynamic pump that uses a rotating impeller to increase
the pressure of a fluid. Centrifugal pumps are commonly used to move liquids
through a piping system. The fluid enters the pump impeller along or near to the
rotating axis and is accelerated by the impeller, flowing radially outward into a
diffuser or volute chamber (casing), from where it exits into the downstream piping
system. Centrifugal pumps are used for large discharge through smaller heads.
General procedures for start-up/shutdown and trouble shooting of centrifugal pump
are discussed in this section. For detail operating procedure refer the vendor
operating procedure.
32.1.2 START UP
i) Inspect and ensure all the mechanical jobs are completed before going for
start-up of pump.
ii) Carryout no load run of the motor without coupling the pump. Then, de-
energize the electrical supply and couple the motor with pump.
iii) Check bearing cooling water, Jacket cooling water for proper flow Open
external seal flushing liquid to mech. seal in pumps having such facility.
iv) Check oil level in the bearing housing; flushing may be necessary if oil is dirty
or contains some foreign material.
v) Rotate the shaft by hand to ensure that it is free and coupling is secured.
Coupling guard should be in position and secured properly.
vi) Testing of New pump with water: Ensure that pump motor is suitable for
operation of increased load due to pumping of water. Also such operation may
need approval of pump vendor/specialist rotary group engineer in certain
cases. However, normally all pump's minimum continuous flow and motor
ratings are checked with water as pumping medium.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
vii) Open suction valve. Ensure that the casing is full of liquid. Bleed, if necessary,
from the bleeder valve. Keep discharge valve closed.
viii) Energize the motor. Start the pump and check the direction of rotation. Rectify
the direction of rotation if not correct.
ix) Check the discharge pressure.
x) Open the discharge valve slowly. Keep watch on the current drawn by the
motor, if ammeter is provided. In other cases check at motor control
centre/MCC.
xi) Check temperature of the bearings and if necessary adjust the cooling water
flow (if provided).
xii) Check the gland/seal and if necessary adjust gland tightness/flow of the
coolant for the seal.
xiii) In case of hot stand by pump: Ensure that casing attain pumping temperature
by draining to suitable closed blow down system. This is to avoid vapour
locking.
32.1.3 SHUT DOWN

i) Close discharge valve fully if pump is single stage. If pump is multi-stage,
having high tension electric motor, follow pump vendors instructions
particularly regarding minimum continuous flow requirements.
ii) Stop the pump.
iii) If pump is going to remain as stand by and has provision for keeping the pump
hot-cold proceed as follows:
Open the valve in the bypass line across the discharge valve and check valve.
The circulation rate should not be so high as to cause reverse rotation of idle
pump or overloading of the running pump. Reverse rotation of pump may
have adverse effect on thrust bearings as they are not designed for the same.
iv) If pump is to be prepared for maintenance, proceed as follows:
Close suction and discharge valves.
Close valve on check valve by-pass line, if provided.
Close cooling water to bearing, if provided.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
Close external flushing liquid to mechanical seals, if provided.

Slowly open pump bleeder and drain liquid from pump. If the liquid is very
hot or cold, allow sufficient time before draining is started. Ensure that there is
no pressure in the pump. Also drain pump casing.
Blind suction and discharge and check valve by-pass line.
Cut off electrical supply to pump motor prior to handing over for maintenance.
32.1.4 TROUBLE SHOOTING

i) Pump not developing pressure
Bleed/ vent pump casing.
Check the lining up of the suction side.
Check the suction strainer for plugging.
Check the liquid level from where the pump is taking suction (physical
verification).
Check pump coupling and rotation
Check the foot valve (in case of vertical lift pumps).
Check the temperature of liquid. If it is higher than for what the pump has
been designed, available NPSH may come down.
Check for any air leakage in the pump suction line or pump casing. This may
occur at various joints and packing boxes as the packing ages.
ii) Unusual Noise
Check if coupling guard is touching coupling.
Check for proper fixing of fan and fan cover of the motor.
Check for pump cavitation.
Get the pump checked by a Rotary EED group.
iii) Rise of bearing temperature
Generally the bearing oil temperature up to 80oC or 50oC above ambient
whichever is lower can be tolerated. Refer vendors’ instruction manual for
maximum tolerable pump bearing temperature.
Arrange lubrication if bearing is running dry or oil level is low.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
Adjust cooling water to the bearing housing if there is such provision.

Stop the pump, if temperature is too high, call the Rotary EED group.
iv) Gland Overheating
Adjust cooling water if facility exists.
Slightly loosen the gland nut, if possible.
Stop the pump and hand over to maintenance.
Arrange external cooling if pump has to be run for some time.
v) Unusual Vibrations
Check the foundation bolts.
Check the fan cover for looseness.
Stop the pump and hand over to maintenance for checking alignment.
vi) Leaky Gland
Check the pump discharge pressure.
Tighten the gland nut slowly, if possible.
Prepare the pump for gland packing adjustment or replacement of mechanical
seal as the case may be.
vii) Mechanical Seal Leak
Stop and isolate the pump and hand over to maintenance.
Refer to vendor's instruction for more details on trouble shooting of pumps.
32.2 POSITIVE DISPLACEMENT PUMPS

32.2.0 INTRODUCTION
A positive displacement pump causes a fluid to move by trapping a fixed amount of
it then forcing (displacing) that trapped volume into the discharge pipe.A positive
displacement pump has an expanding cavity on the suction side and a decreasing
cavity on the discharge side. Liquid flows into the pump as the cavity on the suction
side expands and the liquid flows out of the discharge as the cavity collapses. The
volume is constant given each cycle of operation.
General procedure for start-up/shutdown and trouble shooting of the positive
displacement pumps are discussed. Vendor's operating manual should be studied for
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
further details, specific to pump under reference:
32.2.1 START UP
i) Check for mechanical jobs are completed.
ii) No load runs of the motor to be carried out before coupling with the pump.De-
energize electrical supply. Couple the motor with the pump.
iii) Flush and renew oil in pump gear box.
iv) Check whether suction/discharge blinds are removed.
v) Check whether suction strainer is installed and is clean.
vi) Check for proper lining up including the pulsation dampener and pressure
safety valve in the discharge. Open suction valve fully.
vii) Check that the motor shaft is reasonably free and coupling secured. Coupling
guard should be in position.
viii) Energize motor. Open discharge valve. Start the motor and check direction of
rotation. If wrong correct it. Never start the pump with discharge valve closed.
ix) Adjust the pump stroke in case of reciprocating pumps and run the pump at
desired settings.
x) Watch discharge pressure and check the rate of pumping using the flow meter
or by taking suction from the calibration pot. The valve on the recirculation
line (provided in case of gear pump, screw pump etc.) shall be adjusted to
obtain the required discharge pressure.
xi) Care should be taken to avoid dry running of pump and back flow of liquid.
Bleed if necessary to expel vapour/air.
xii) Check for unusual noise, vibrations, rise of temperature of both motor and
pump.
32.2.2 SHUT DOWN :

i) Stop the pump.
ii) Check the discharge pressure for gradual reduction.
iii) Close the suction and discharge valves and flush the pump if required.
iv) Drain the liquid if maintenance jobs are to be carried out on the pump.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0

i) Insufficient discharge pressure
Check the line up in suction side.
Checkup suction pressure.
Check the functioning of the safety valve and pressure control valve on
discharge to suction.
Check the strainer on the suction side.
Check for insufficient liquid level in the vessel from which pump is taking
suction.
Check pump’s coupling and rotation.
Get the pump checked by pump technician.
ii) High Discharge Pressure
Check the line up on the discharge side.
Check pressure control valve opening.
iii) Leaky Gland
Check for normal pump discharge pressure.
Tighten the gland nut slowly if possible.
Handover the pump for replacing gland packing.
iv) Unusual Vibration
Check the foundation bolts.
Check motor fan cover for looseness.
Stop the pump and hand over to maintenance.
32.3 CENTRIFUGAL COMPRESSORS

32.3.0 INTRODUCTION
Centrifugal compressors, sometimes referred to as radial compressors, are a sub-class
of dynamic axisymmetric work-absorbing turbo machinery. In an idealized sense, the
compressive dynamic turbo machine achieves a pressure rise by adding kinetic-
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
energy/velocity to a continuous flow of fluid through the rotor or impeller. This

kinetic energy is then converted to an increase in static pressure by slowing the flow
through a diffuser. This may seem trivial, but it is actually quite complex to
understand and precisely predict. This general class of turbo machinery includes
pumps, fans, blowers, and compressors in axial, mixed-flow and radial/centrifugal
configurations
General procedure for start-up, shut-down and troubleshooting are discussed in this
section. For detail operating procedure refer the vendor operating procedure.
32.3.1 START UP
i) Ensure all mechanical jobs have been completed on the compressor that is to
be started including suction line passivation.
ii) No load run of the motor to be completed before the compressor is coupled.
After no load run, de-energize the electrical supply. Couple the motor and
compressor.
iii) Check oil level in lube oil tank and refill as required to bring the oil level to
the high mark on the sight glass. Do not overfill.
iv) Start the standby motor operated lube/seal oil pump keeping pressure regulator
at a value given by the Vendor. Establish the pressure of lubricating oil in
bearings and seal oil to seal.
v) Bar the unit over once to be sure all moving parts are clear.
vi) Open cooling water and ensure it is operative. Commission cooling water to
all water coolers viz.oil cooler, gas coolers etc. as applicable.
vii) Ensure that compressor casing has also been purged with inert gas, if
applicable.
viii) Line up the antisurge valves of the compressor.
ix) Open suction valve/discharge valve and line up to the system. Remove any
accumulated liquid from the casing by opening casing drain.
x) Start the drive as per the vendors’ recommendations and run the compressor.
Adjust the minimum circulation valve, so that the drive does not consume
excess power.
xi) Allow the oil to warm up to 40o C. Watch compressor motor amperage. Listen
for unusual noise during the warm up period. Auxiliary motor driven lube oil
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
pump will be stopped when shaft driven pump develops normal oil pressure
and kept ready for auto start.
xii) When the unit is warmed up and determined to be operating satisfactorily,
gradually start throttling the valve beyond surge requirements of the
compressor.
xiii) Load the compressor to the required capacity in the above mentioned manner.
NOTE : The compressor before trial run on the actual medium may be tried on air with
suction and discharge open to atmosphere. While attempting to run the Compressor on air,
Vendor's instructions and recommendations are to be followed. It is to be noted that scaling
arrangement may be required to be changed to suit the machine running on air.
32.3.2 SHUT DOWN

i) Stop the drive and close the antisurge valves.
ii) Start the oil pump to lubricate the bearing till required. iii) Close the discharge
valve.
iii) Close the suction valve.
iv) Turn off cooling water to oil cooler as applicable.
v) If the compressor is to be given for maintenance, isolate, depressurise and
purge with inert gas to make the compressor free of hydrocarbons.
32.3.3 NORMAL OPERATION
i) Check oil level in lube oil tank and add oil as required to maintain the proper
level as indicated on sight glass.
ii) Log all temperatures, pressures, levels, flows and amperage.
iii) Adjust cooling water flows to compensate for changes in inlet water
temperature or ambient temperature.
iv) Listen for any unusual noise while the machine is operating. These should be
investigated immediately.
v) Periodically drain from suction KOD/inter cooler etc.
vi) Watch differential pressure across oil filter to check cleanliness; change over
filter, if necessary and arrange cleaning of choked filter.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
vii) Keep the exterior of the compressor and the compressor room floor clean.

Follow vendor's recommendations. However, some general guide lines are given:
i) Surging
Restricted flow due to plant operating at partial load or throttling at discharge.
Blocked suction due to strainer choking or line choking if a permanent strainer
is not provided.
Liquid carry over from suction K.O. drum.
ii) Heavy vibrations in machine
Misalignment
Bent rotor
Damaged rotor
Imbalance
Weak foundation
Mechanical Loosening etc.
Increase in gas temperature at suction along with drop in compression ratio
Increased circulation of gas due to internal leakage as a result of 'O' ring of end
cover/diaphragm damage.
iii) Oil carry over in the compressor unit in the product side
Faulty operation of seal oil level control system.
Damaged oil seals.
H.P. seal oil drain collector levels not being maintained properly.
At stand still condition, check the seal oil level controls, and check the drain
oil quantities from HP seals near the compressor and compare with previous
data.
Check seal oil traps and drain collectors.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
Check for any damage to the membranes in differential pressure indicators,

and differential pressure control valves to avoid leakage of pressure oil into the
reference gas chamber.
Check that the balance gas pressure at the compressor is at least 200 mm WC
higher than the respective reference gas pressure.
Check oil seals.
Avoid flooding of oil through reference gas lines from seal oil overhead tanks.
32.4 RECIPROCATING COMPRESSORS

32.4.0 INTRODUCTION
General procedures for start-up, shutdown and troubleshooting are discussed in this
section. Vendor's operating manual should be studied for further details.
32.4.1 START UP
i) Ensure all mechanical jobs have been completed on the compressor machine and
auxiliary systems. Check if fine mesh strainer is installed as per vendor’s
recommendations.
ii) No load run of the motor to be carried out before the compressor is coupled to the
motor. De-energize electrical supply and couple the compressor with the motor.
iii) Check oil level in frame sump and refill as required bringing the oil level to the
high mark on the sight glass. Do not over fill.
iv) Start the stand by motor operated frame oil pump keeping pressure regulator at a
value given by vendor. Establish the required pressure of lubrication oil in
bearings & crossheads.
v) Bar the unit over once to be sure all moving parts are clear.
vi) Open cooling water and ensure it is operative. Commission cooling water to
frame oil cooler, cylinder jacket cooling and packing cooling as applicable.
Remove the suction and discharge valve of the compressor if recommended by
compressor vendor. Valve flanges should be covered to prevent entry of foreign
material into casing. The machine has to be tried with the valves in removed
condition.
vii) Before running on no load, give a bump start. Time for which an unloaded
machine continues to roll after driving power has been cut-off gives a fair
indication of no load friction.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
viii) Start the motor and run the compressor with the suction and discharge valves in
removed condition for about say 1 hour. After ensuring that the machine
performance is okay, stop the compressor, Isolate power, and Reinstall the
valves.
ix) Commission inert gas (IG) purge pressure controller to the packing and vent to
safe height in atmosphere, as applicable (distance piece purging). It is assumed
that compressor has been purged with IG while desiring of the system using IG.
Compressor cylinder is to be purged with IG by temporary hose connection if for
some reason compressors was under maintenance and cylinders are full of air.
Steam purging of compressor should be avoided as it may lead to excessive
rusting of parts afterwards.
N.B. The above is applicable when the gas handled is of explosive nature.
x) Unload the compressor manually.
xi) Open suction valve/discharge valve and line up to the system. Open bypass
valves/purge valve as applicable.
xii) Before running on no load, give again a bump start. Time for which an unloaded
machine continues to roll after driving power has been cut off gives a fair
indication of no load friction.
xiii) Start the motor and run the compressor on no load for 10 minutes until the frame
oil warms to about 35oC. Watch compressor motor amperage. Listen for unusual
noise during the warm up period. Periodically check any heating of bearing and
other moving parts. Operating satisfactorily gradually start loading the
compressor by manually operating the suction unloader/clearance pocket.
xiv) Load the compressor to the required capacity in ascending sequence of steps.
xv) Observe the discharge pressure, temperature and bearing temperatures when the
machine is loaded step by step.
32.4.2 SHUT DOWN
i) Unload the compressor in descending sequence of steps and bring it to o% capacity.
ii) Stop the motor.
iii) Close the discharge valve.
iv) Close IG purge to piston rod packing, if provided. v) Close suction valve.
v) Turn off cooling water to cylinders, packing and frame oil cooler.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
vi) If the compressor is to be given for maintenance, isolate, depressurise and purge with
inert gas to make the compressor free of hydrocarbon gas, if handled.

i) Check oil level in frame sump and add oil as required to maintain the proper level
as indicated on sight glass.
ii) Log all temperatures, pressures, levels and amperage.
iii) Adjust cooling water flows to compensate for changes in inlet water temperature or
ambient temperature and for change in compressor loading.
iv) Listen for any unusual noise while the machine is operating. These should be
investigated immediately and periodically.
v) Periodically drain from volume bottles, distance piece etc.
vi) Watch differential pressure across oil filter to check cleanliness. Change over filter
if necessary and arrange cleaning of choked filter.
vii) Keep the exterior of the compressor and the compressor room floor clean.

Follow vendor's recommendation. Some guide lines are given below:
i) Low Lube Oil Pressure
a) Low oil level-Plugged oil pump strainer
b) Leaks in suction and discharge lines of the oil pump.
c) Worn out bearings of the oil pumps.
d) Defective oil pump.
e) Dirt in oil filter check valve.
f) Broken oil filter check valve spring
g) PSV/ by pass of PSV passing.
h) Defective pressure gauge.
ii) High Oil Pressure
a) Plugged oil pressure lines.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
b) Defective oil filters mechanism.

c) Excessive spring tension in oil pressure adjusting mechanism.
d) Defective pressure gauge.
iii) Overheated Cylinders
a) Insufficient cooling water, scoured piston or cylinder.
b) Broken valve and valve springs.
c) Insufficient lubrication
d) Packing too tight.
e) Choked cooling water passage.
iv) High Intercooler Pressure
a) Broken or leaking valves.
b) Defective gauge.
v) Low Inter Cooler Pressure
a) Broken or leaking valves.
b) Leak in inter cooler.
c) Piston rod packing leaking.
d) Defective pressure gauge.
vi) Knocking Sound
a) Scoured piston or cylinder.
b) Defective lubrication.
c) Foreign material in cylinder.
d) Piston hitting cylinder head.
e) Loose piston or piston pin.
f) Loose main bearing.
g) Scoured cross heads or crosshead guides.
vii) High Suction Temperature
a) Broken or leaking suction valves.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
32.5 HEAT EXCHANGERS
32.5.0 INTRODUCTION
A heat exchanger is a piece of equipment built for efficient heat transfer from one
medium to another. The media may be separated by a solid wall, so that they never
mix, or they may be in direct contact.
Shell and Tube type heat exchangers can be broadly classified into following types:
− Water Coolers/condensers
− Steam heaters
− Chillers
− Exchangers
Start-up/shut down procedures for each unit shall vary slightly from case to case.
However, general start-up/shut-down procedures are discussed in the following
paragraphs.
32.5.1 START UP
After the heater exchanger has been pressure tested and all blinds removed, proceed
as follows:
i) Open cooling medium vent valve to displace non-condensable (air, fuel gas,
inert gas etc.) from the system. Ensure the drain valves are capped. For high
pressure system, drain valves should be flanged. This activity is not required if
gas is the medium.
ii) Open cooling medium inlet valve. Close vent valve when liquid starts coming
out through it, then open cold medium outlet valve and fully open the inlet
valve also. Where cold medium is also hot, warming up of cold medium side
gradually is also essential.
iii) Open hot medium side vent valve to displace non condensable (air, fuel inert
gas etc.). Check that the drain is closed and capped. This activity is not
required if gas is the medium.
iv) Crack open hot medium inlet valve. When liquid starts coming out from the
vent valve, close it. Open hot medium inlet valve and then open the outlet
valve fully. In case of steam heaters, initially the condensate shall be drained
to sewer till pressure in the system builds up to a level where it can be lined up
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
to the return condensate header.

v) In case by passes are provided across shells and tube side, gradually close the
bypass on the cold medium side and then the bypass across the hot medium
side.
vi) Check for normal inlet and outlet temperatures and pressures. Check that
TSVs are not passing.
vii) The opening of inlet and outlet valves should be done slowly ensuring that the
exchangers are not subjected to thermal shock.
viii) In case of coolers/condensers, adjust the water flow to maintain the required
temperatures at the outlet. The return water temperature should not exceed
45OC.
ix) For avoiding fouling, velocity of water should be at least 1 m/sec in a
cooler/condenser.
32.5.2 SHUT DOWN

i) Isolate the hot medium first. In case both hot and cold medium are from process
streams, exchanger shall remain in service till the hot stream has cooled down
enough.
ii) Isolate the cold medium next.
iii) Drain out the shell and tube sides to OWS/Sewer/Closed blow down system as
applicable.
iv) Depressurize the system to atmosphere/flare/blow down system as applicable.
v) Purge/flush if required. This is particularly important in congealing services.
vi) Blind inlet and outlet lines before handing over the equipment for
maintenance.
AIR COOLERS
The air coolers/condensers comprise of a fin tube assembly running parallel between the inlet
and outlet headers. These are of the forced draft type. The forced draft fans provided have
auto variable pitch rotors in which the fan blades are adjustable in pitch during rotation. This
allows variation in air flow as per the cooling requirements. These coolers are also provided
with manually and/or automatically operating louvers for the control of the cooler outlet
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
temperature.
Refer to vendors instructions for the detailed procedure of start-up, shut down and
normal operation.
32.6 AGITATORS
32.6.0 INTRODUCTION
General procedures for start-up, shut down and troubleshooting are discussed.
Vendor's operating manual should be studied for further details.
32.6.1 START UP
i) Ensure that all mechanical & electrical jobs have been completed on the
agitation assembly that is to be started. ii) Check lubrication of bearing housing,
gear box etc. It is preferable to change to fresh lubrication material before
starting.
ii) Energize the motor. Start the motor & check the direction of rotation. Rectify
the direction of rotation if necessary. Check the no load current.
iii) Check cleanliness of the vessel.
iv) Rotate the shaft by hand to ensure that it is free & coupling is secured.
Coupling guard should be in position & secured properly.
v) Before filling liquid check whether the vessel outlet valve is closed or not. If
not, close the valve.
vi) Fill liquid in the tank up to normal operating height. Generally water could be
used for initial test. Commission level instrument if any.
vii) Start the motor & check for any vibration/heating of gear box, any excessive
vibration of the shaft etc. Measure load current drawn by the motor.
viii) If any solid to be mixed, slowly open the solid charge. Hold & start mixing
slowly. xi) Check for unusual noise, vibration, rise of temperature of both
motor & gear.
ix) If any heating arrangement is there slowly commission the system & ensure it is
operative.
32.6.2 SHUT DOWN
i) Stop the motor.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
ii) If any heating arrangement is there, stop it. If any hot oil heating is there, slowly
change over to cold oil from hot oil. But keep the circulation on.
iii) If the liquid is sticky type, drain it as early as possible (in hot condition) & flush the
system.
iv)Motor to be de-energized

i) Check lubrication system of bearing housing & gear box.
ii) Log all temperatures, level & amperage.
iii) Listen for any unusual sounds while the m/c is operating. If any, it should be
investigated immediately.

Follow vendors' instructions. General guidelines are given below:
i) Unusual vibration: Check for misalignment and improper facing of bracket.
ii) Seal getting heated: Adjust cooling water flow, if provided.
32.7 EJECTORS
32.7.0 INTRODUCTION
An ejector is a pump-like device that uses the Venturi effect of a converging-
diverging nozzle to convert the pressure energy of a motive fluid to velocity energy
which creates a low pressure zone that draws in and entrains a suction fluid. After
passing through the throat of the injector, the mixed fluid expands and the velocity is
reduced which results in recompressing the mixed fluids by converting velocity
energy back into pressure energy. The motive fluid may be a liquid, steam or any
other gas. The entrained suction fluid may be a gas, a liquid, a slurry, or a dust-laden
gas stream.[
General procedure for startup, Shut down & trouble shooting are discussed here in
this section. Vendor's operating manual should be studied for specific details.
32.7.1 START UP
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
• Ensure all mechanical jobs have been completed on the ejectors with all
accessories.
• Check all the blinds have been removed or not.
• Check hot well is properly filled with water or not. If not, fill it up.
• Charge the steam header to the ejector. Drain condensate from low point drains.
Ensure steam is dry before it is charged to the ejector.
• If there are pre-condensers, inter condensers & after condensers, open condensate
drain valve provided on the pre condenser, inter condenser & after condenser.
• If there is an after condenser, be sure that the air vent on the hot well is open &
free to discharge to the atmosphere.
• If there is no after condenser, be sure that the ejector discharge is open & free to
discharge to the atmosphere or against a back pressure only equal to that for
which it was designed.
• If there are pre-condensers, inter condensers & after condensers, start circulation
of cooling water through' the tubes of inter, pre and after condensers. In case of
barometric condensers, open water to the spray nozzles.
• Open all isolating valves on the first & subsequent stages of the ejectors.
• Open upstream & downstream isolating valves of the pressure controller for controlling
vacuum.
• Before opening steam to the ejector, open the strainer bleeder and purge the strainer.
• Open steam valve slowly to the last stage (which discharges to the atmosphere or after
condensers). Next open steam valve on preceding stage & so on until all stages are in
operation. The vacuum on the vessel to be evacuated should then start to rise steadily.
Observe maximum vacuum pulled. Adjust vacuum to operating level.
• When hot well level starts increasing, try to control level of the hot well. After level
becomes steady put it on auto level control, if provided.
• In case of H/C service, once sufficient level is there on the H/C side, start H/C recovery
pump, and control the level. When steady, put it on auto, if provided.
32.7.2 SHUT DOWN

i) Close steam valve to first stage.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
ii) Close steam valve to second & subsequent stages (if any) in their respective
order.
iii) Close isolating valves on all stages.
iv) Close circulating water valve.
v) Open water make up for hot well.

If vacuum starts falling, the reason may be:
i) Insufficient inlet steam pressure.
ii) Inlet water temperature to the condensers higher than normal temperature.
iii) Air leaks in the tail pipe of inter condensers.
iv) Flooding of the inter condensers by excessive water flow (direct C.W.
condensers).
v) Starving of any inter-condenser by insufficient cooling water flow.
vi) Plugging of water distribution system in the condenser.
vii) Plugging of the tail pipe.
viii) Plugging of the steam nozzle ejector and jets due to pipe scale.
ix) Steam leak at nozzles throat. The defects mentioned above are to be ascertained &
rectified for proper operation.
32.8 PRECOMMISSIONING
As the new projects nears mechanical completion of new equipment / units, operating
personnel have to carry out preparatory works for ensuring safe and smooth start-up of the
facility. These activities are termed as Pre-commissioning activities
− Some of the pre-commissioning works can be carried out simultaneously along with
construction. But, care in carryout work is necessary so that it will not interfere with
construction work. It is most important to plan schedule and record with checklists
and test schedules all the preliminary operation and to co-ordinate the construction
program.
Once mechanical contractor completes work, sections of the unit should be checked out by
PMC, refinery and vendor personnel in those areas. Immediately punch lists that indicate the
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
deviations from the design specifications, should be written following inspection of those
areas, and distributed to the contractor. In this manner mistakes in construction can be found
and corrected early.
Inspection of the plant can be basically divided into the following areas:
− Vessels
− Piping
− Heater
− Exchanger
− Pumps
− Compressors
− Instrumentation
− Catalyst/Chemicals Inventory
While detailed Format for checking is provided in Annexure-I, a discussion and lists of the
major points that must be examined in the inspection of these areas follows:
32.9 VESSELS INSPECTION

The actual installations must be compared against the drawings to assure that the
vessels will function as intended. The reactor internals must conform exactly to the
design specifications if good distribution is to be attained and catalyst migration is to
be avoided. Particular attention must be paid to the following details:
32.9.1 Specification Check

i) Review design specifications with the vendor drawings to verify agreement on:
− Pressure, temperature, and vacuum ratings.
− Shell metallurgy, thickness, and corrosion allowance.
− Nozzle size and orientation; flange rating, type and finish.
− Type of lining, thickness and material.
− Stress relieving and/or heat treatment.
− Foundation design for full water weight.
ii) Confirm that the vessel has been hydrostatically tested.
iii) Verify that all code plate information on the vessel is correct.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
32.9.2 Internal Inspection

i) Reactors
− Inlet distributors, quench distributors: metallurgy, type, size, opening sizes,
freedom to expand.
− Vapor/liquid collection and distribution trays: tightness, vertical positioning, liquid
tightness of bubble caps and risers, metallurgy, dimensions, packing, supports,
welding, levelness, cleanliness.
− Catalyst support grids: metallurgy, grid type and dimensions, screen type and size,
supports, welding.
− Catalyst unloading nozzles: metallurgy, orientation, length.
− Thermowells: orientation, length, and metallurgy.
− It must be verified that sufficient quantities of bolts, washers and hold downs of the
proper size and metallurgy are available to reassemble any disassembled portions
of the reactor internals.
ii) Other Vessels

− Vessel trays: spacing; levelness, orientation and dimensions of weirs, downcomers,
accumulators, draw off and trap trays, seal pans, distributors, baffles, nozzles, tray
contact devices; metallurgy of trays, contact devices, clips, bolts, nuts and gaskets;
freedom of movement of valve caps or other contact devices; number, size, and
distribution of tray contact devices or perforated plate holes; proper fit of all
internals and proper welding of support rings or other support devices; liquid
tightness of draw off trays, seal pans and accumulators, all bolting and clips
tightened.
− Mesh blankets and outlet screens: size, location, and levelness, suitability of fit (no
bypassing allowed), metallurgy of blanket, support, tie wires, and grids.
− Vortex breakers: type, size, and orientation.
− Baffles: type, orientation, levelness.
− Instrument nozzles: location, orientation, cleanliness, thermowell length and
metallurgy, baffle size and type.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
− Inlet distributors: type, size, orientation, levelness, freedom to expand.

− Non-fired reboilers: location, orientation, proper supports.
− Packing: type, size, support, installation.
− Internal ladders and other devices: location, size, orientation, properly secured.
− Lining and refractory:-
• Hex-steel for concrete lining: clean and properly secured. Lumnite or other
specified cement applied according to the specifications, with no holes or gaps
in the applications.
• Metal linings in good condition. Weld overlays have no gaps or holes in the
application.
• Lining is of the proper thickness and covers the required portion of the vessel.
• Other refractory installed correctly with no gaps or holes in the application.
iii) General
The vessel should be clean (free from trash) and should not have excessive mill scale.
32.9.3 External Inspection

i) Manways and nozzles: location, size, flange rating and finish, metallurgy, with proper
gaskets, nuts and bolts.
ii) Ladders and platforms: correctly positioned, secure and free to expand.
iii) Insulation and steam tracing: provided as specified and has expansion joints as
required.
iv) Vessel grounded correctly.
v) Correct vessel elevation.
vi) Valves and instrumentation: easily accessible from grade or platform.
vii) Piping:
− Adequate supports and guides for all connecting lines.
− Level and pressure instrument connections drain to a safe location.
− Vents to atmosphere or blowdown provided as specified.
− Relief valves have been bench tested.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
− Check valves exist on utility line connections where hydrocarbon backup could
occur.
− Connections available for steaming/purging of the vessel.
viii) Fireproofing of structure and supports is complete.
ix) Instrumentation:
− Level glass floats center positioned correctly with respect to vessel tangent line,
and are readable from grade or platform.
− Through-view level glasses have rear light for illumination.
− Flange ratings, metallurgy, size, etc. are all correct.
− Reactor skin thermocouples are located properly and installed so that they have
good contact with the wall.
32.10 PIPING
The unit must be constructed in accordance with Piping and Instrumentation
Diagrams (P&ID's), including all details, elevations, dimensions, arrangements, and
other notes on the P&ID's.
Check the piping adequacy for carrying out normal operations of the unit as
envisioned in the licensor design. Also, check whether piping is adequate for special
procedures such as dry-out, special materials preparation, regeneration and/or
alternative flow schemes incorporation in the unit design.
Check piping adequacy for receiving feed and sending products without
contamination of these streams. Check all tankage interconnections to minimize the
possibility of stream contamination outside of the battery limits.
Check that adequate means of measuring flows, pressures, and temperatures, and
sampling of all process streams has been provided.
The following items must be checked to ensure conformity to the design
specifications:
32.10.1 Flanges: rating, facing, and metallurgy; type (typically, 2" and smaller
are socket weld, 2½" and larger are weld neck flanges).
32.10.2 Gaskets: type; metallurgy (materials of retainer, jackets, winding, filler,
etc.); thickness, ring size, etc.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
32.10.3 Fittings, connections and couplings: rating and metallurgy.

32.10.4 Valves: rating and metallurgy (body, trim, seats, etc.); packing; seat
inserts; bonnet gaskets; grease seals; socket-weld or flange type, rating and
facing; installed in correct direction of flow; lubricant provisions; gear
operators; extended bonnets; stops; ease of operation.
32.10.5 Bolting: stud or machine bolts; bolt and nut metallurgy; bolt size.
32.10.6 Pipe: metallurgy, thickness; seamed or seamless; lining.
32.10.7 Tubing: size and thickness; metallurgy; seamed or seamless.
32.10.8 Gauge glasses:
− Through-view types should have rear-mounted lights.
− Design pressure and temperature.
− Special materials of construction.
− Drains to safe location.
− Visible from grade (or platform, if required).
32.10.9 Pressure relief valves:
− Size and style.
− Lever requirement.
− Inlet/outlet flange material, facing and rating.
− Set pressure - must be bench tested.
− Metallurgy of nozzle, disc, spring, etc.
− Type (pilot operated, balanced, etc.).
− Inlet/outlet block valves car-sealed open; valve stems installed in horizontal
or below.
32.10.10 General:
i) Utility systems within the battery limit should follow all relevant pipe class
specifications in the same detail required for process lines.
ii) Package systems (modular units, etc.) shown on the P&ID should follow all
relevant pipe class specifications in the same detail required for other process
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
lines.
iii) Expansion: review the physical installation to ensure that no expansion problems
will occur when the unit gets hot and that:
− Column overhead, reflux, feed and other lines are free to expand.
− Rotating equipment will not be pulled out of alignment.
− Sufficient expansion loops have been provided on long hot lines.
− Pipe shoes are free to move in one direction, and are resting on supports of
sufficient size that the shoe will not fall off the support.
iv) High point vents and low point drains should be installed where necessary.
v) Spectacle blinds should be provided where required.
vi) Car-sealed valves should be locked in proper position.
vii) Spring hangers should have locking pins removed (after hydrotesting) and necessary
adjustments should be made for hot/cold position after startup.
32.11 HEATER
The heaters must be inspected to ensure that they can be operated in a safe and
efficient manner and that the required heat duty needed for the process can be
provided. After all, it is important that the possibility of a tube rupture or other heater
mishap be minimized. In particular the following items must be checked:
32.11.1 Specification Check
All design specifications should be reviewed with vendor drawings to verify agreement on:
i) Conformity to process requirements.
ii) Heater type.
iii) Tube arrangement, metallurgy, size, and thickness (note that tube metallurgy may be
different for radiant, convection, and convection shield tubes).
iv) Instrumentation connections.
v) Tube supports and support metallurgy.
vi) Refractory.
vii) Access doors, observations ports, steam smothering connections, and explosion
doors.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
viii) Stack arrangement.
32.11.2 Internal Inspection

i) Radiant Section
a) Arrangement and symmetry of tube-coil with respect to heater wall, burner rings,
and tube spacing.
b) Vertical length of tube coil with respect to supports and guides.
c) Fuel gas, fuel oil and pilot burner tips are clean and oriented properly. Burners are
properly mounted with clearance for firing and removal. Castable refractory has
not been used for burner blocks. Fuel oil tip sizing is adequate with respect to
actual fuel oil viscosity.
d) Tube skin thermocouples, if required, are located properly and installed so that
they have good contact with the tube skin.
e) Refractory is in good condition before and after refractory dry-out. No refractory
is resting on tubes.
f) Heater shell expansion joints are packed with designed insulation material and
clean.
g) Adequate space for tube expansion.
h) Heater shell is sealed to prevent escape of hot gases and entrance of atmospheric
moisture during shutdown.
i) Smothering steam and instrumentation connections are not covered by refractory.
j) Heater is clean and free from debris.
k) Heater instrument connections are open - not filled or covered with refractory.
ii) Convection Section and Stack
a) If extended surface elements are allowed, the bottom three or more rows of
convection tubes must be bare.
b) No refractory is on the tubes.
c) Expansion provisions are adequate.
d) Damper is free to move fully open and closed; its position indicator is correct both
at the stack and at the damper control; damper is weighted to fail open; the
damper, support pipe and bolting are all of the correct metallurgy.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
e) Soot blowers, if specified, are provided with provision for inspecting the soot
blowing operation.
f) Other checks should be conducted as in the Radiant Section inspection.
32.11.3 External Inspection
i) Location with respect to process equipment.
ii) Platforms for access to all observation ports, instrumentation, sample
connections, soot blowers, and damper connections.
iii) Adequate number and arrangement of observation ports to permit visual
inspection of the entire length of all wall, hip and shock/shield tubes, and the
burner blocks.
iv) Hand firing equipment located adjacent to an observation port from which that
burner can be viewed.
v) Explosion doors located such that heater gases will not flow towards process
equipment and platforms.
vi) Explosion doors located such that doors can open completely.
vii) Symmetry of external piping and crossovers.
viii) Instrumentation and sampling connections.
ix) Damper position indicator visible from damper control; damper control
functioning properly.
x) Pocketed crossover connections have flanged drains.
xi) Decoking connections as specified.
xii) Sufficient smothering steam connections into heater firebox. Box valves on
smothering steam are located remote from the heater, with drain valves and/or
steam traps upstream of final block valve for condensate removal. Weep holes
provided in smothering steam lines at low points.
32.11.4 Fuel Systems
i) Fuel lines have battery limit block valves that are remote from the heater and
easily accessible. Fuel oil piping and its steam tracing are arranged such that
no dead legs or pockets are formed. Fuel lines to burners can be easily
disconnected from burners for burner removal. All fuel lines have been leak
tested.
ii) Fuel oil lines at burner valves are correctly piped with steam crossovers. All
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
steam lines have adequate traps and condensate drains.

iii) Shutdown solenoids for fuel shutoff valves have been set properly.
iv) Fuel oil circulating lines are provided.
32.11.5 Heater Instrumentation

i) All draft gauge, pyrometer and analyzer connections are as specified.
ii) All heater TRC's fail upscale during power failure or open circuit.
32.11.6 PROCEDURE FOR REFRACTORY DRYING
Purpose
Furnace dry-out procedure is utilized as a means of curing of furnace refractory before initial
process operation and also whenever refractory is repaired / replaced. At the same time the
dry-out period is also used as means of checking the operation of heater components such as
burners and such control device as may be used during the dry-out period.
Duration
The drying time of the furnace refractory varies with the porosity of the refractory and the
Atmosphere humidity. A 3-5 day dry-out period is generally required during which furnace
temperature is gradually increased to the point at which refractory is completely dry. If
linings are excessively wet, then only the pilot burners should be left alight for a day or two
to dry off this excess moisture. During the dry-out cycle, moisture in heater close to the
burners is evaporated within a very short time. However, the incipient moisture of the
refractory needs gradual heating and evaporation. Generally over a three day cycle, moisture
inside refractory is removed completely.
Tube Protection
During the dry out period it is necessary to pass steam through all the process tubes to
prevent overheating of the tubes. Steam is introduced after warm-up to prevent undue
condensation and water hammering. Steam will be vented out through the vents provided on
preheat coil outlet, steam super heater outlet and the decoking stack. The tube metal
temperature should be monitored and the same should not exceed the tube metal design
temperature.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
Dry out
For the initial phase of dry-out, only fuel gas should be used to facilitate control and easy
change over of burners. Carry out following steps for dry-out.
i) Open the stack damper wide. Purge furnace firebox thoroughly with steam.
ii) Open all burner air register and peep holes. Allow refractory to dry under natural draft for
24 hours.
iii) Bypass cut off circuits on fuel gas lines and open fuel gas shutdown valves.
iv) Remove blinds on fuel gas circuit.
v) Light up the pilot burners as uniformly as possible as per Burner / Vendor's
instruction.
vi) Raise the temperature with lighting sufficient main burners to bring arch temperature up
to 120 oC at a rate of 25 oC/h.
vii) Hold the temperature at 120 oC for 12 hours by rotating the burners for heat uniformity
and then increase to 200 oC at a rate of 25 oC/h. Introduce steam through tubes at 200 oC
after making sure that all condensate has been drained off. Check all burners, observe the
condition inside the firebox and the inspect areas of expansion.
viii) Hold the temperature at 200 oC for 12 hours. Increase the arch temperature to 400 oC
again at 25 oC/h. Hold at this temperature for 24 hours and repeat checks as above. Increase
the flow of steam if tube metal temperature is found exceeding design temperature.
ix) The heat duty requirement during dry-out may not warrant firing of all burners. Sufficient
number of burners, with good flame, may be fired and the operation of burners may be
rotated every 2 hours to maintain uniformity.
x) Before proceeding to the final stage of drying out, ensure that sample supply of steam is
available to prevent over-heating of the tubes.
xi) Increase the arch temperature at a rate of 25 oC/h to 500 oC and hold for 24 hours .Make
a thorough check so the heater during this period and in particular, expansion should be
noted.
xii) During dry-out period it is advisable to try all instruments on automatic control and see
that all alarms etc. are functioning properly.
xiii) Check tube wall temperature frequently during process, to avoid possible overheating.
xiv) At the end of 500 oC drying out period, reduce the arch temperature at a rate of 50 oC/h
and accordingly start reducing the steam flow through the tubes.
xv) When the arch temperature is around 200 oC, firing can be cut off together with steam
flow through tubes. Allow the heater for natural cooling.
xvi) When firebox is cool enough and the inside entry permits available, inspect refractory
thoroughly for any damage and if required repair it.
32.11.7 OPERATING PROCEDURE

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
The CDU/VDU furnace can be fired both on fuel oil and fuel gas. Each main burner is
provided with a pilot gas burner. The furnace should be fired so that at no time flames
impinge on the tube. The burners should be operated to provide fires, which are as uniform in
length as can be obtained. It is normally desirable to fire all burners even at reduced operating
capacities for a uniform heat flux distribution. Excess air for satisfactory combustion is 30%
for fuel oil and 20% for fuel gas. The amount of excess air should be measured at the inlet to
convection and at the base of the stack. The excess air in the furnace should be reduced till
the flue gas analysis indicates traces of carbon monoxide. It must then be increased till no
carbon monoxide exists. The pass outlet temperatures should be maintained equal. Inequality
of flow among the passes should not go beyond 10% (maximum). Skin, box and intermediate
pass temperature indicators have been provided. Refer to vendors instructions on operation
of the burners.
32.11.8 START-UP IN NATURAL DRAFT MODE
a) Preliminary Checks:
i) Ensure cleanliness inside the heater. Check and confirm that there are no flammable
materials such as oil accumulation in the fire box.
ii) Zero check all draft systems (gauges / meters). Stroke check the control valves of FO, FG
and atomizing steam. Also check the action of FO and FG SDV’s.
iii) Ensure that the burner air registers are moving freely.
iv) Check the free operation of the stack damper and all the DOD’s.
v) All safety valves including the superheating coil RV should be commissioned.
vi) Commission the tempered water system and cooling water system.
vii) Commission the atomizing steam. Disconnect steam flexible hoses and purge them till
dry steam appears and then connect them back. This is to ensure that no condensate enters the
fire box.
b) Commissioning the FO & FG system:

i) Ensure that steam tracing to the FO lines is commissioned before circulation is established
ii)After opening the SDV’s, the return header has to be commissioned first. Establish fuel oil
circulation in all the headers of the furnace. The rate of circulation should be such that the
fuel oil returned should be equal to the fuel oil consumption in the furnace. Keep instruments
on manual control and ensure that the burner valves and gaskets are not leaking.
iii) Commission the fuel gas system after ensuring that the FG is free from any liquid by
draining the liquid thoroughly at the FG KOD in gas plant.
iv) After commissioning the FO and FG lines, check and rectify any leaks in the system.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
v) It is also to be ensured that the fire box is free from any flammable mixtures. For this, keep
the stack damper and the DOD’s of the furnace open and steam purge the furnace chamber at
least for 30 minutes using LP steam. Atomising steam or FO purge steam can also be used
for this purpose.
c) Before lighting the furnace,

i) Keep the primary air register and secondary air register open.
ii) Keep stack damper and all the DOD’s wide open. Close all peepholes explosion doors.
iii) Sufficient amount of feed flow is to be established in all the passes and each pass inlet
pressure is to be maintained at least 14 kg/cm2 g.
iv) Cut the snuffing steam and light the pilot burner with the portable ignitor. If the pilot
burner does not light up, shut off fuel gas and steam the furnace again and light the pilot. All
the pilot burners are to be ignited in a similar way. While lighting the burner, it is advisable
not to stand under the burner.
d) Lighting the furnace:

i) Keep all burners valves closed. Bypass shut-down circuit.
ii) For lighting oil burner, flush the fuel oil line by opening the cross over valve. Set the
steam differential pressure controller so that steam pressure is about 1.8 – 2.0 kg/cm2 higher
than fuel oil pressure.
iii) Crack open the atomising steam to the burner that is to be lighted. Insert a lighted torch
and open oil valve for a small flame. Steam valve is to be adjusted for a clean bright flame.
iv) When required number of burners have been lighted, open the FO and atomising steam
valve full and control the flames by adjusting the fuel oil pressure.
v) Maintain furnace draft about minus 1 to 2 mm water gauge at the inlet to convection zone.
vi) Check excess air in the furnace and adjust the damper, primary secondary air registers to
give the required excess air.
vii) For lighting the fuel gas burners, operate the FG plug-cock valves and maintain 1.5
kg/cm2 g. on fuel gas header pressure and follow the same lighting procedure as in the case
of FO burner.
viii) It is preferable to operate a burner either on fuel gas or fuel oil only at a time.
ix) When the unit stabilizes, take all controls and commission the TRC control cascading
either on FG or FO depending on the number of burners on FO or FG service. x) Commission
the shutdown circuit of the furnace.
32.11.9 NATURAL DRAFT TO BALANCED DRAFT CHANGEOVER

The following steps have to be taken to change the furnace operation from natural draft to
balanced draft mode
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
i) Ensure that the display of the annunciator lamps is normal. Check whether they are lit up
during the lamp test. The trip switches of FD fan and ID fan are to be kept in manual bypass
mode.
ii) Start the FD fan with the outlet damper and the suction vanes in fully closed position.
iii) Close the air bypass damper and open all the damper blinds in the air and flue gas lines.
iv) Open the suction vanes to half open position. Open the outlet damper to allow about 20%
of the maximum flow. Start closing the drop out doors (DOD’s). There are 5 DOD’s for 11-
F-01 and 2 for 12-F-01.
v) Close one DOD from the panel.
vi) Open FD fan outlet damper to 40% and close the second DOD
vii) Similarly, close the other DOD’s one-after-the-other by opening the discharge damper in
increments of 20%
viii) While doing so, care should be taken so that the furnace pressure doesn’t go to the
positive side. If it does, the discharge damper should be closed till such extent where the
furnace pressure becomes negative again.
ix) After checking the firebox conditions for sufficient combustion air, the FD fan trip can be
put in auto-interlock mode.
x) Take the ID fan suction vanes in manual control and close them fully.
xi) Start the ID fan (after obtaining clearance from CPP in case of 11-FM-02)
xii) Increase the suction vanes opening slowly watching the furnace arch pressure.
xiii) After the ID fan is fully stabilised, close the stack damper and put the ID fan suction
vanes in auto control.
xiv) The ID fan trip can be put in auto-interlock mode after ensuring normal operating
conditions.
32.11.10 BALANCED DRAFT TO NATURAL DRAFT CHANGEOVER

i) Place the ID fan trip in manual-bypass mode
ii) Open the stack damper and check the lamp position. Then trip the ID fan
iii) Allow the system to run on forced draft so that the APH system cools down.
iv) Place the FD fan trip in manual-bypass mode.
v) Open one DOD and decrease the FD fan discharge correspondingly so that the furnace
pressure never to the positive side.
vi) Open the other DOD’s in the same procedure as mentioned above. The number of DOD’s
to be kept open is decided by checking the fire box conditions and the O2 analyser.
vii) Trip the FD fan
viii) Now the furnace is under natural draft.
32.11.11 SHUT DOWN THE HEATER

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 32
PLANT NAME: CDU II
Chapter Rev No: 0
Fuel to the heater should not be cut off abruptly unless an emergency shut down is called for.
The product pass outlet temperatures should be slowly reduced. As burnerstend to become
unstable when fired at low rate, reduce the number of burners as required.Follow the
procedure outlined below for shutting off individual burners.
i) First change the heater to natural draft operation from the balanced draft mode.
ii) Close fuel oil valve and open steam purge valve on the fuel oil line to the burner.
iii) Purge all the oil into the firebox and continue steaming for about 5 minutes.
iv) Close atomising steam to the burner.
v) Pull out oil gun in case the gun is not withdrawn; leave a little stem blowing through the
tip to cool it. This may be done when a burner is to be taken out of service during normal
operation.
vi) For shutting down the furnace, cut the burners one by till all oil fires and gas fires
are cut off. Bypass the shut down circuit of the furnace, so that fuel oil and fuel gas supply
are not interrupted when the feed flow to the furnace is reduced.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
CHEMICAL AND HYDROCARBON SPILLAGE HANDLING

“Spill” means an event of coming out of a liquid of its container especially
accidentally. In a refinery, this will mean oil coming out of any of the equipments whether it
is storage, transport, pump, processing equipment, etc. Every time a spill occurs, it has a
potential to lead to secondary events like fire, environmental damage, personnel injuries or
injury/effects on public outside the refinery. The occurrence and extent of these events will
depend on the size and type of oil spills. Best strategy is to prevent an oil spill. In order to
achieve this, the design of the facilities needs to be in a manner that prevents oil spillage from
entering any surface drain or a water body and the mechanical integrity of the equipment will
have to be ensured all this time. This will also require proper management practices and day
to day administration in a manner that the activities are under close control. However,
residual risk always exists and in-spite of all precautions and an emergency response plan is
meant to tackle and manage the residual risk.
33.1 GENESIS OF AN OIL SPILL:
An oil spill can occur during any of the routine or non-routine operations associated
with the operating facilities of the refinery. There are four broad reasons for the generation of
an oil spill. It is possible that in a certain instances, inadequacy in one of them can get
covered by the adequacy of the other. These reasons are:
33.1.1 Mechanical Integrity Failure:
The failure of structural/construction integrity of any civil or mechanical part of facility can
be termed as mechanical integrity failure. Successful management of Mechanical integrity
has many elements. The mechanical integrity of the facility can get violated due to
inadequate/improper design, job execution inadequacies, gaps in preventive and turnaround
inspection programs, operation outside safe operating envelope and many such gaps in
management. A safe operating envelope again can get violated due to many reasons which
may not be in control every time like instruments failure, etc. every time a mechanical
integrity failure occurs in a hydrocarbon oil bearing system, the oil spill (small or large) will
occur. The oil spill may be a surface oil spill or ingress of oil into soil if it is an underground
system. The consequence of the oil spill will depend upon layout, surrounding etc of the area.
Examples can be line rupture, gasket failures, equipment failures, etc.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.1.2 Operational Control Inadequacies:
These are related to the day to day administration and operation of an operational facility.
Well laid out procedures, controls on activity, proper authorization, clarity in instructions,
proper communication, training, etc. are some of the important elements in managing
operational activities. Gaps in these areas can lead to abnormal situations and depending on
the system involved and type of operation, oil spill can occur. Management practice should
ensure proper execution of every workflow element associated with the operation of the
facility. Examples can be delay in reporting of a flange leak, de-pressuring of a line in pipe
track without ensuring complete flushing, overflow of a tank due to gaps in monitoring
system-both management and hardware.
Operational co-ordination in the management of loading and unloading operations associated

with ships and tankers has very high importance. Impact of lapses in operational activities
associated with loading and unloading can be very high as there is a high possibility of the oil
getting into the sea.
33.1.3 Collection System Design Philosophy Inadequacies:
A design philosophy of oil containment and secured handling, considering the type of
operations occurring in the facility, is absolutely essential to make sure that the oil gets
properly contained and is lead to the collection system without causing any oil spill beyond
the boundary of that facility. If proper philosophy of segregation of oil handling area and
non-oil handling area is not followed, oil spills can become a routine affair. Examples can be
non-provision of OWS facilities at an area which involves routine operations of valve
operation, blinding, etc.
33.1.4 Capsizing or Damage to Ships/Tankers:
These are one of the most serious type of oil spill scenarios since they may involve huge
volumes and the spill area directly takes place over a turbulent water body. The impact area
can be very vast and serious environmental damage can result. Many living species get
affected and liabilities can be very heavy and long term. In order to protect the interests of the
company, it is required to ensure that the chartered ships are having appropriate mechanisms
to prevent oil spills. Suitable agreements for mutual inspections and adherence to prescribed
standards are some of the tools which can be adopted.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.2 OIL SPILL MITIGATING FEATURES:
There are certain features incorporated in the refinery facilities which help wither in
preventing an oil spill into a surface drain or a non oil handling area. These features can be
preventive type or mitigating type. The mitigating type may mean that it provides some
elapsed time before a response can actually be implemented. These are described below:
33.2.1 Design Philosophy of Collection System:
The oily water system collection system has certain features which are provided for the
purpose of segregating an oil handling area from a non-oil handling area. The basic
philosophy features of the system are described here. These are the key features which
contribute to keeping oil contained in oil handling area or contain the oil to a restricted area
and prevent it from going to surface drain:
• An area where a large number of routine operations are held and a number of oil handling
equipments are located is a paved area. Paving is generally impervious and is done by RCC.
This paved area is provided with OWS facility. Depending on the complexity and size, the
area is also provided with a surround OWS channel. This surround OWS channel acts as a
barrier between the outside unpaved area and the plant paved area and is thus a facility
provided to contain an oil run-off.
• All storage tanks are provided with Dyke walls around it to contain the leakage from the tank
in case of a failure of tank. The OWS system provided in the tank passes underground out of
the Dyke wall with a valve at just outside the Dyke wall. Facility is provided to route the
accidental oil collected in the Dyke area to OWS. Operating philosophy requires all the three
valves at the Dyke wall outlet to be kept closed and open only when required for the specific
purpose. This philosophy and Dyke wall provision ensures that no oil can pass to the external
surface drain.
The above basic philosophy features play a key role in maintaining the surface drains free
from oil in the Refinery. If the philosophy is followed and the other issues mentioned in this
chapter are satisfied in a sustained manner, the risk of an oil spill can be minimized.
33.2.2 Certain Other Mitigating Features:
There can be many such provisions and features existing in the Refinery which help in
increasing the response time available for handling an oil spill and some of them may
contribute decisively in containing the oil spills to a restricted area or within the Refinery
premises.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
Oil Catchers:
Existence of oil catchers at the outlet of all the Refinery surface drains before the drain leaves
the Refinery premises can provide time to mobilize an oil evacuation device like gully
sucker. Also in case· of smaller oil spills, the oil catcher can fully prevent it from going out of
the Refinery premises depending on the volume of the oil catcher and the spill volume.
Non-running Open drains:
If there is an open drain which is being used to cater to water flow requirement in normal
operation of a facility in the Refinery, it can be big liability in case of an oil spill. As the drain
is under water flow in normal times, it will take very .less time for the oil to go out of the
Refinery in case it enters such a drain. In wet weather, such a scenario will be valid for all the
surface drains. Thus wet weather oil spills are to be considered more serious than dry weather
oil spills in case of the Refinery. If there is no running drain in dry weather, it will enable
total blocking of the drain by weirs/baffles to contain the oil spills and recover them. If there
is water flow, total blockage is not possible and oil catcher type mechanism can only be
provided which invariably leads to some oil breakthrough.
Kerb Wall Provisions:
Kerb wall provisions around the oil equipment facility in offsite areas help to contain the oil
spill within the area of the facility. In oil wharf area a spill containment barrier is provided all
around the loading/unloading manifold. This barrier provides protection against smaller spills
and in most cases if the response .during a hose rupture is rapid, these barriers can play a
decisive role in preventing the oil from entering the sea.
Similarly in many offsite areas, pump bays, valve manifolds are provided with Kerb walls
around them with OWS facility.
Provision of Floating Booms on water bodies:
Usage of barrier floating booms around the probable area of oil spill is a preventive measure
against the spread of oil spill beyond a limit. If the oil spill occurs it can be recovered from
the contained area and spread of oil spill can be avoided. Such provisions can be made while
loading/unloading a ship, at the mouth of the intake canal, at the effluent canal etc. Nature of
booms is different for still waters, turbulent waters and flowing waters.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.3 EFFECTS OF AN OIL SPILL
There can be many after effects of an oil spill. These can be listed as:
a. Monetary loss.
b. Loss of oil.
c. Damage to environment- flora, fauna.
d. Resultant fire and associated losses.
e. Loss in organizations credibility.
f. Public or statutory liability.
g. Expenditure on cleanups.
Many effects may be secondary or tertiary nature also. In extreme cases where the damage to
environment is severe, the liabilities may be huge. Marine environment comprising of Man
groves, coral reefs, fish, birds and other marine population are sensitive ecosystems and are
the main sufferers during an oil spill in the sea. Sea waves make the oil to spread far and wide
and increase the impacted area. The coastline can get awash with oil and result in loss of
many areas of tourism for the populace. Such occurrences give wide publicity to the event
and are detrimental to the existence and reputation of the industrial establishments like oil
refineries.
Another complexity arises when there is an oil spill' from a tanker which is chartered by the
refinery and it spills oil in the far high seas. Since quick response is needed, logistics may be
extremely cumbersome. And if the impacted area is a sensitive eco-system, the problems
increase many fold. The refinery may have to depend on the services of very specialized
agencies with huge costs. Also such events get wide media coverage and create almost a
permanent negative image about the organization in the minds of public. Images of affected
areas, marine species and birds provide motivation for penal action against organization.
33.4 CERTAIN MAJOR OIL SPILL POSSIBILITIES FROM REFINERY

FACILITIES
• Rupture of any Crude Tank.

• Rupture of any product tank.
• Rupture of pipelines in any pipe-tracks.
• Rupture or leaks at loading/ unloading hoses from Ships.
• Leaks of the loading arm.
• Overflow of a HC storage Tank.
• Rupture of pipes between ATP and Refinery North wall.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
• Partial or full capsizing of the Ships chartered by the refinery.

• Overflow from the Tanker.
• Crude unloading line leak.
The associated risk in each case will depend upon the quantitative extent of the abnormality.
Also the impact of the event will depend upon the environment around the event location. If
the event is occurring at wharf, OSTT the impact is high due the escape of oil into the sea.
The response time also can be low due to the rapidity of the event. Rupture of hoses, loading
arms, joints leak, rupture of subsea pipeline, overflow of ship tanks are high impact scenarios.
Oil can escape from the facilities in the refinery premises also due to any of the earlier
mentioned reasons and reach the sea through the effluent canal and other drains.
Apart from the spill itself, the occurrence of secondary events like fire will depend upon the
quality of the oil and situation can get complicated. Response strategies should be planned to
suit the requirements of the event.
33.5 MOVEMENT OF OIL SPILL
It is important to predict the probable direction of movement of the oil spill. This helps in
taking mitigating measures to control the impact of the oil spill. The movement and drift of
spilled oil spill on a water body will depend upon spread of oil will invariably impact the
shore as it will travel with the wave fronts.
In case of oil wharf area, since there is a continuous flow towards the LLPH intake canal, the
oil spill is likely to move towards the intake area, though' there is a parallel impact of the
wind direction. Areas towards Shipyard and ENC are likely to get washed with oil spill in
case there is a larger oil spill. This again will depend upon the size of the spill and wind
direction.
In case of OSTT, the movement of the spill will depend mainly upon the wind direction. The
turbulence of the waves will result in movement of certain patches of spill in different
directions also. In case of flowing streams, however, like refinery effluent canal, there is little
impact of the wind direction. The flowing canals act as a contained transport medium for the
oil to flow and reach the destination. At the final delivery point the oil spill will spread over
water body and there the wind direction will affect the spill. It is important to know the wind
direction at the time of oil spill. This helps in planning the response.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.6 FACILITIES & RESOURCES AT RISK
Different types of shorelines are affected in different ways. Thus cleanup is strategies should
be suitable to the needs. The type of the affected area will dictate the cleanup strategy. The
resources at risk will need to be protected with measures in order to minimize the impact.
Environmentally and commercially sensitive areas which will get affected under different
spill scenarios are presented below:
SPILL SCENARIO SPILL AFFECTED AREAS MECHANISM OF

MOVEMENT CLEANING
CHANNELS
Spill from the main Refinery Main Western Harbor Arm Boat Mounted Skimmer
refinery area Effluent Canal
Mangrove area of Boat Mounted Skimmer
Western arm
Navy Jetty in the western Boat mounted skimmer
arm
VPT Drain Municipal drain on the Gully sucker/ Vacuum truck

south of refinery
VPT Drain Gully sucker/ Vacuum truck
ENC/ Shipyard Area Bay/ Boat mounted skimmer
Wharf
LLPH pipe track ENC/ Shipyard Area Bay/ Boat mounted skimmer/
Wharf Manual
Spill from Oil Directly into the ENC/ Shipyard Area Bay/ Boat mounted skimmer
Wharf Sea Wharf
LLPH intake area/ Bay Boat mounted skimmer/
Manual
Spill form OSTT Directly into the Fishing Harbor Boat mounted skimmer
area/ crude Sea
offloading line
Beaches and Coastline Boat mounted skimmer and
Manual. Drum Skimmers
Main Harbor Boat mounted skimmer and

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0

Ship Capsizing/ Directly into the Beaches and Coastline Boat mounted skimmer and
Grounding Sea Manual. Drum Skimmers
Fishing Harbor Boat mounted skimmer and
Rushikonda Aqua farms Boat mounted skimmer and
Main Harbors Boat mounted skimmer and
33.7 CHARACTERISTICS AND BEHAVIOUR OF OIL
The behavior of oil spill on a water body depends mainly on the characteristics of the Oil and
the environment of the spill. Following characteristics of the oil are important for
consideration and provide information about the possible behavior of the oil:
• Specific gravity of the oil provides a broad clue about the class of the oil as to whether it is
heavy, middle or light etc. It will indicate whether oil will float or sink.
• Pour point will indicate congealing characteristic of the spilled oil. Oils like LSHS, VGO
with high pour points will congeal on water bodies.
• Viscosity will determine the spread and flow of the spilled oil. The spilled oil film thickness
will also depend on its viscosity. Low viscous 'oil spillage will spread more rapidly than a
high viscous oil.
• Asphaltene content may determine the emulsion forming tendency of the spilled oil. Oil with
Asphaltene content higher than 0.5% exhibit tendency to form oil-water emulsions.
Turbulence in the water body increases the formation in emulsions. This then makes
recovery, storage and handling of the oil difficult.
• Flash point of the spilled oil is an indicator of the fire hazard associated with the oil spill.
• Color of the spilled oil will provide a first hand visible conclusion of the area affected by the
oil. Transparent clean oils spillage poses problems in judging the spread unless a detailed
survey is made.
33.8 CATEGORISATION OF VARIOUS OIL SPILL SCENARIOS IN THE

REFINERY
The.oil spills occurring in a refinery may be of varied nature. The quantity-of the oil spilled
will depend upon the type of failure, type of operation, operating condition of the system etc.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
The impact of the oil spill will depend upon the topography and the features of the area at
which the oil spill has taken place. It will also depend upon the prevailing weather conditions.
An oil spill scenario can become a fire scenario if appropriate timely precautions are not
taken. If there has been a breakthrough of oil from the refinery and there is a coupled fire
scenario, the impact on the surrounding population and facilities of other establishments can
occur. There can also be secondary fire scenarios due the fire originating from an oil spill of
the refinery. In such cases the liability increases manifold. In some cases quantity of the
spilled oil may be less but the danger of fire may be very high and thus requiring a more
rapid response.
In case of an oil spill in oil handling process plant area, the issue may be more concerned
with the immediate danger of fire rather than environmental damage. The process plant area
is a paved area and has a barrier surround OWS system which will be instrumental in
preventing oil escaping to the surface drains and unpaved area, though this is dependent on
the quantity. In wet weather, however, the dynamics may be slightly different. The
requirements of handling an oil spill event in off shore area are vastly different. The spread of
oil in offshore can be very rapid and it immediately starts impacting the marine species. The
wind direction, oil quality and turbulence/flow of the water body are the parameters which
determine the spread of the spill.
While planning response to an oil spill scenario, all these factors need to be considered.
While planning the infrastructure associated with the response elements, there always needs
to be a lead over the severity of actual scenario so that adequacy is always ensured. It is also
required that mechanism is in place for handling smallest to the largest spill.
Thus, based on the severity, effects and logistics involved, the OIL SPILLS are categorized
as below in TABLE - 1 : (In the order of lower to higher environment impact):
CATEGORY TYPE OF OIL SPILL

ZERO An oil spill occurring in a paved area of a process plant or an operating facility
which is provided with ZERO OWS facility provided the spill is of such magnitude
that it is not entering any surface drain.
ONE An oil spill excluding Naphtha, MS, Crude (or similar lighter oils with fire hazard),
occurring in any area and the oil is entering surface drain. But there is no immediate
danger of oil going out of the refinery.
TWO An oil spill of Naphtha, MS or Crude (or similar light oils with fire hazard)
occurring in any area and the oil is entering surface drain. But there is no immediate
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
danger of oil going out of the refinery.

THREE An oil spill excluding Naphtha, MS or Crude (or similar lighter oils with fire
hazard), occurring in any area and the oil is entering surface drain. But there is an
imminent danger of oil going out of the refinery.
FOUR • An oil spill of Naphtha, MS, Crude (or similar light oils with fire hazard)
occurring in any area and the oil is entering surface drain. There is an
imminent danger of oil going out of the refinery.
• Catastrophic failure of any of the Storage Tanks.
• If any of the oil spill is above 100 MT.
• Oil Spill due to any abnormal occurrence in wharf and/or OSTT.
FIVE • Oil Tanker capsizing or running aground.
The requirement and level of response in each of the category will vary. Though theoretically
there is a danger of fire in every oil spill, the danger is more in lighter oils and very high fire
risk in case of Naphtha/MS oil spill. Situations where the fire risk is high will require
simultaneous activation of Fire emergency Plan. Proper precautions will have to be taken to
make sure that the personnel involved in managing such oil spills be aware of such dangers
and are well protected and prepared. In case there is a risk of MS/Naphtha going out of the
Refinery, the fire risk is much higher and the impact also will be very high.
The above category is not showing the fire risk ranking. The Categories are arrived at
considering the oil breakthrough out of the Refinery and its impact outside the refinery.
NOTE:
• As stated in the preface of the plan, the oil spill response plan is a sub plan under the On-Site
Emergency Plan. At any time during any oil spill event it can be declared as Onsite
emergency by the incident controller with authorization from Head Refinery. Once it is
declared as Onsite emergency all the requirements of response as per the Onsite emergency
plan will have to be fulfilled from that time onwards apart from the requirements under
NOSDCP when applicable.
• In the event of a fire resulting during the oil spill, the Fire emergency has to be given
precedence over the oil spill emergency. But simultaneously resources must be directed
towards carrying out containment, source arresting and recovery of the leaked out oil as it
will reduce the severity of fire. And during such time the response organization will be as per
the Fire emergency manual.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.9 GUIDELINES FOR IMPLEMENTING THE ELEMENTS OF OIL SPILL

RESPONSE PLAN
No two oil spill events can be considered totally identical. Their origination, magnitude, after
effects, resource requirements for response etc. can be vastly different. The dynamics
involved in handling the on-shore oil spill are quite different from an Off-shore oil spill. The
effectiveness in handling will depend upon many elements. Satisfying resource requirement,
though very important, is not the only element in. achieving effectiveness. Keeping abreast of
the roles and practicing their execution at certain intervals enables improving the response
capability and quality. Therefore it is important to conduct mock drills and exercise at certain
intervals. These exercises not only help to understand the roles better but also are tools for
further improving the Plan strategies itself based on the work-front experience.
Preparedness of each role player for playing his role to the fullest is dependent upon the
psychological and resource adequacy. The resources have to be adequate and they have to be
available in a manner that they can be rapidly deployed. Backup arrangement is also needed
to mobilize additional resources in case required. The methodology adopted to deploy the
resources nevertheless enhances the effectiveness of response. A well coordinated, rapid and
on target response in the initial stages can make things easier to manage in subsequent stages.
The following guidelines for implementing each of the philosophy element of an Oil Spill
Response will help in understanding the direction in which the O.S.R.A. has to act:
33.9.1 To identify and Stop the Source leak:
• If a leak is occurring in the Process Unit area where OWS facilities are provided, from oil
spill point of view it is not of imminent danger (surely there is a risk of Fire). Such an event
can become an oil spill scenario if it prolongs or if it is of a catastrophic nature. It is the
rapidity of activities like isolating, de-pressuring and taking shutdown of the respective
section which will be important in stopping source leak.
• A pipeline leak in an Offsite area where there are no OWS facilities and which is unpaved,
theoretically the oil spill scenario starts from the moment the leak starts. For source leak
stoppage, usage of clamps with rubber packing etc. should be resorted to. These Kits are
available in Fire-House and with Maintenance Department. If leak does not stop, system will
need to be isolated and de-pressured. A Tank Bottom Leak will require decision to pump-out
the Tank contents.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
33.9.2 To Contain the oil spill:
• First Step in containment is to prevent the entry of the oil into the surface drain. This may not
be fully possible every time but efforts have to be made to achieve this to the maximum. This
will require deployment of Flexible Absorbent or containment Booms all around the oil
pool/patch which has started developing due to the leak. Based on the surface contour and
presence of other hurdles at the area, the boom invariably will leave some gaps. These gaps
will have to be packed using absorbent pads, pillows or such other packing material.
• The adjacent Surface drains have to be blocked, towards upstream and downstream of the oil
spill area, using baffle plates. Requisite grooves arrangement has been provided (or are being
provided) at some locations in each of the Surface drain to enable such baffle insertion. It will
be possible to insert such baffles and fully block the surface drain only in case of dry weather
and when there is no water flow in the drain. In case of wet weather or water flow case,
underflow-overflow baffle combination will have to be suitably inserted to allow water flow
to go through and retain the oil. In such cases, traces of oil are expected to breakthrough and
measures must include close monitoring of the situation.
• It will also help if protective block-baffles are provided at a distance after the first block-
baffle in the surface drain this will act as secondary containment and thus will enable that
much cushion in the response activity with respect to recovery of the spilled oil.
• Depending on the severity, boom and baffle should be deployed at the respective surface
drain' outlet leaving the refinery.
• In case the above mentioned equipment is not available, methods like usage of sand bags, hay
filters can -be used. But these have disadvantage that they cannot be re-used and end up as
hazardous waste and their disposal becomes a problem.
33.9.3 To recover the oil spill:
• Recovery of spilt oil will require equipment which can be pressed into service at a short
notice. These may be Gully sucker, Oil skimmers and in some cases manual bailout may be
required.
• Usage of oil skimmers is generally not possible in shallow depths. In such cases gully suckers
should be used.
• Gully sucker is versatile equipment and can be used in most cases.
• A floating suction mesh attachment helps in improving the effectiveness of a gully sucker.
• Recovered oil from a floating skimmer will need to be stored in a vessel close to the skimmer
operation area. Gully Sucker is mobile truck and can transport the oil to a distance location
for unloading the same.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
• Refinery has two gully suckers which can be used simultaneously to increase the recovery
capacity.
33.9.4 To treat the breakthrough oil (which is going out of containment) spill:
• Only Treatment possible for break-through oil is application of dispersant. The dispersant can
only be applied to relatively lesser quantities of oil-which is breaking through in the form of
streaks.
• If there is a sheet of oil escaping, the application of dispersant has no use and in such cases,
the containment area should be extended. .
• A dispersant does not have the capability to disperse the entire oil body to which it is applied.
It has an efficiency ranging from 30 to 60 %.
• For applying dispersant, either a pump can be used or it can be sprayed using an eductor on
the Fire water hose with nozzle.
33.9.5 For working area house keeping/cleaning:
• This is to enable smooth functioning of the personnel involved and equipment and maintain
the ergonomics. A person should be nominated by the I.C. & E.M.C. to generally look after
this aspect so that the frontline personnel involved in the actual activity of oil spill
management have a manageable work-front available for them.
• The person who looks after the house keeping aspects must be in close contact with all the
OSRAs and interact with them so that his activities are managed in a manner to suit their
requirements.
• After the completion of the entire oil spill response activity a final mop up and area
inspection to restore to original condition is necessary.
33.9.6 To ensure Safety during the entire activity:
• Emergency Fire and Safety Controller must nominate one of his representatives to look after
this aspect.
• This representative should interact, prompt and advise the participating personnel in the
safety aspects of their execution activity.
• The execution area may have lot of non standard accesses movement paths which the
participating personnel will have to encounter. Proper prompting and interaction at the time
of activity will help in avoiding injuries.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 33
PLANT NAME: CDU II
Chapter Rev No: 0
• Road closure should be suitably done with respect to the roads in close proximity to the oil
spill area.
• Personnel protective equipment should be provided.
33.9.7 To help in restoring the Damage to the Environment:
• This activity will generally mean the finishing touches in case of the area cleanups after the
event has fully come in control.
In case any birds, animals are affected action shall be taken to treat them in the veterinary
hospitals. Affected trees shall be cleaned
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
ANNEXURES
34.1 UNIT MASTER BLIND LIST:
34.1.1 UNIT LIMIT BLIND LIST:
EAST BATTERY LIMIT BLIND LIST:
FIRST PLATFORM:
S no Size Specification Description rating

1. 6” B7A HVGO R/D 150#
2. 6” A1A BITUMEN TO HFO LINE 150#
3. 3” A9A AW TO MEROW 150#
4. 6” B7A HVGO HOT FEED TO FCCU-II 300#
5. 8” A1A HFO R/D 300#
6. 6” A1A OLD BITUMEN R/D 150#
7. 3” A2A LVGO TO DSL 150#
8. 6” A1A KERO R/D 150#
9. 6” A1A KERO R/D TO DSL 150#
10. 6” A1A DIESEL TO STORAGE 150#
11. 4” A1A DIESEL TO LDO 150#
12. 3” A1A KERO TO LDO 150#
13. 3” A1A KERO TO FO 150#
14. 6” B1A SR TO IFO 300#
15. 8” A1A SLOP Header 150#
16. 1 ½” A1A HWW TO MEROX 150#
17. 4” A1A KERO TO FO 150#
18. 3” B1A FO RETURN LINE 300#
19. 2” A9A CAUSTIC LINE 150#
20. 6” A1A SRN TO MS 150#
21. 6” A1A SRN R/D TO STG 150#
22. 3” B1A FO SUPPLY 300#
23. 3” B1A CDU-I SR TO BBU 300#
24. 6” A1A OTN TO STORAGE 300#
25. 3” A1A NAPHTHA TO 11-C-05 300#
26. 3” B4F SLOPCUT TO PDU 300#
27. 6” Redundant line CTU RCO LINE 300#
28. 2” B1A HOT DIESEL TO FCCU-II 150#
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
29. 3” A9A CAUSTIC TO 11-V-04 150#

30. 2” B1A LPG TO VAPORISER 300#
31. 4” A3A FCCU-II MAB COND. TO 11-V-04 150#
32. 3” B1A LPG R/D 300#
33. 2” A9A CAUSTIC TO 11-V-07 150#
34. 8” B1A RFO LINE 300#
SECOND PLATFORM:
S no Size Specification Description rating
1. 6” B1A SR FROM CDU-3 300#
2. 6” A1A BITUMEN NEW R/D LINE 300#
3. 3” A1A HN TO SRN 150#
4. 2” DRINKING WATER LINE
5. 3” A1A HN TO DSL 150#
6. 2”/3” A3A 11-E-18 condensate to PP 150#
7. 3”/2” A9A CAUSTIC FROM MEROX 150#
8. 4” B1A SR TO LDO 300#
9. 8” A1A FUEL GAS LINE 150#
10. 3” A1A LVGO TO HVGO R/D 150#
11. 3” A1A LVGO TO LDO 150#
12. 4” B1A STRIPPED WATER FROM MEROX 300#
13. 3” B1A EFFLUENT WATER TO SWSU 300#
14. 4” A1A CUTTER 150#
15. 2” J3A INST. AIR 150#
16. 4” A3A YARD AIR 150#
17. 4” A2A SERVICE WATER 150#
18. 4” A3A BCW SUPPLY 150#
19. 4” A3A BCW RETURN 150#
20. 4” A1A 11-V-03 GAS TO FCCU-II 150#
21. 3” A1A HWO TO TK 17 150#
22. 12” A2A TANK FARM LP STEAM 150#
23. 12” A1A OFF GAS
24. 6” B7A FCCU HOT FEED 300#
25. 4” A3A DM WATER 150#
26. 4” A3A BFW 300#
27. 3” A1A HN TO TK 124 150#
28. 6” B1A SR TO VBU TK 150#
29. 10” A2A LP STEAM 150#
30. 8” D2A HP STAEM 600#
31. 12” B2A MP STEAM 300#
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
32. 4” A1A MEROX FLARE KOD TO OTN 150#

33. 3” A1A SRN TO FCCU 300#
34. 3” B4F RCO TO FCCU-II 300#
35. 3” A1A 11-V-01 TO FCCU-II 150#
36. 6” A3A BCW RETURN 150#
37. 4” A1A KERO TO FO (OM&S) 150#
38. 20” A1A FLARE 150#
THIRD PLATFORM:
S no Size Specification Description Rating

1. 14” A1A SR TO VBU TK 300#
2. 10” A1A SR TO CDU-III 300#
3. 8” B3F CIRCULATING OIL 300#
4. 8” B3F CIRCULATING OIL RETURN 300#
5. 6” A1A KERO TO ATP 150#
6. 3” A1A HN TO ATP 150#
FOURTH PLATFORM:

1. 10” B1A HOT DIESEL TO DHDS 150#
2. 4” A1A PG HN TO STG 150#
WEST BATTERY LINES:

1. 10” A1A FEED LINE FROM TANK FARM 150#
2. 12” A2A TANK FARM LP STEAM 150#
3. 4” A3A BCW SUPPLY LINE 150#
4. 4” A3A BCW RETURN LINE 150#
5. 10” A1A CBD INLET V/V 150#
6. 4” A1A CBD PUMP DISCH. 150#
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.2 INDIVIDUAL EQUIPMENT BLIND LIST:
34.2.1 CDU-II PUMPS BLIND LIST:
S. No PUMP SERVICE BLINDS SIZE & RATING SPEC

1 11-PM-01A/B CRUDE Suction 10” X 150 A1A
Discharge 10” X 300 B1A
Warm up 1”X300 B1A
2 11-PM-02A/B CRUDE Suction 12” X150 A1A
Discharge 10” X300 B1A
3 11-PM-03A/B/C DIESEL Suction 8” X150 A9A
Discharge 6” X300 B7F
Warm up ¾ ”X300 B7F
4 11-PM-04A/B KERO Suction 8”X150 A9A
Product Discharge 6”X300 B7F
5 11-PM-05A/B Heavy Suction 6”X150 A1A
Naphtha Discharge 3”X150 A1A
Warm up ¾ ”X150 A1A
6 11-PM-06A/B Top Reflux Suction 12”X150 A1A
Discharge 8”X300 B1A
7 11-PM-07C/D Diesel CR Suction 10”X150 A4F
Discharge 8”X300 B4F
8 11-PM-08A/B KERO CR Suction 16”X150 A9A
Warm up ¾ ”X300 B7A
9 11-PM-08C/D KERO CR Suction 10”X 300 B7A
booster Discharge 10”X300 B7A
Warm up ½”X300 B7A
10 11-PM-09A/B Top pump Suction 16”X150 A1A
around Discharge 10”X300 A3A
Warm up ¾ ”X300 A3A
11 11-PM-10A/B RCO Suction 12”X150 A4F
Discharge 8”X300 B4F
Warm up ½”X300 B4F
12 11-PM-11A/B LPG Suction 8”X150 A1A
Discharge 6”X150 A1A
13 11-PM-12A/B Wash water Suction 4” X 150 A3A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
S. No PUMP SERVICE BLINDS SIZE & RATING SPEC

14 11-PM-13A/B/C Caustic Suction 1”X150 A9A
injection Discharge ¾”X300 B7A
15 11-PM-14A/B/C Ammonia Suction 1”X150 A9A
injection Discharge 1”X300 B7A
16 11-PM-15A/B Filmer Suction ¾”X150 A9A
Discharge ¾”X300 B7A
17 11-PM-16A/B DMF Suction ¾”X150 A9A
Discharge ¾”X300 B7A
18 12-PM-01A/B SR Suction 12”x 150 A4F
Discharge 8”x300 B4F
Warm up 1” B4F
Vent 2”X300 B1A
19 12-PM-02A/B Slop cut Suction 6”x150# A4F
Discharge 4”x 300# B4F
Warm up 1”X300 B4F
Vent 2”X300 B1A
20 12-PM-03A/B HVGO Suction 16” x 150# A4F
Discharge 10” x 300# B4F
Warm up 1”X300 B4F
Vent 2”X300 B1A
21 12-PM-04A/B LVGO Suction 8” x 150# A1A
Discharge 6” x 300# B1A
Vent 2”X300 B1A
22 12-PM-05A/B HWO Suction 2”x150# A1A
Discharge 1 ½” x150# A1A
23 12-PM-06A/B HWW Suction 3” x150# A9A
Discharge 2” x150# A9A
24 12-PM-07A/B Tempered Suction 10” x150# A3A
water Discharge 8” x150# A3A
25 12-PM-08A/B Vac. Suction ¾” X150. A9A
neutralizer Discharge ¾”X300 B7A
26 10-PM-01A/B Suction 4”X150 A9A
27 10-PM-03A/B Suction 2”X150 A3A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.2.2 EXCHANGERS BLIND LIST:
S. Exchanger Service blinds size & rating spec

No
1. 11-E-01 Crude/ HN i) Crude inlet valve downstream flange 10” X 300 B1A
ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) HN inlet valve downstream flange 3” X 150 A1A
iv) HN outlet valve upstream flange 3” X 150 A1A
v) Crude inlet cutter line 1” X 150 A9A
vi) Crude to CBD 1 ½ “ X 150 A1A
vii) HN to CBD 1“ X 150 A1A
2. 11-E-02 Crude/ i) Crude inlet valve downstream flange 10” X 300 B1A
KERO ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) KERO inlet valve downstream flange 6” X 300 B1A
iv) KERO outlet valve upstream flange 6” X 300 B1A
vii) KERO to CBD 1“ X 150 A1A
Diesel ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) Diesel inlet valve downstream flange 6” X 300 B1A
iv) Diesel outlet valve upstream flange 6” X 300 B1A
v) Diesel to 11-E-23A upstream flange 6” X 300 B1A
vi) Crude inlet cutter line 1” X 150 A9A
vii) Crude to CBD 1 ½ “ X 150 A1A
viii) Diesel to CBD 1“ X 150 A1A
4. 11-E-04A/B Crude/ i) Crude inlet valve downstream flange 10” X 300 B1A
TPA ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) TPA inlet valve downstream flange 10” X 150 A1A
iv) TPA outlet valve upstream flange 12” X 150 A1A
vii) TPA to CBD 1“ X 150 A1A
KERO ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) KERO inlet valve downstream flange 6” X 300 B1A
iv) KERO outlet valve upstream flange 6” X 300 B1A
vii) KERO to CBD 1“ X 150 A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
Diesel ii) Crude outlet valve upstream flange 10” X 300 B1A
iii) Diesel inlet valve downstream flange 6” X 300 B1A
iv) Diesel outlet valve upstream flange 6” X 300 B1A
vii) Diesel to CBD 1“ X 150 A1A
7. 11-E-07 Crude/ i) Crude from 11-E-06 valve downstream 10” X 300 B1A
LVGO flange
ii) Crude from 11-PM-02A valve downstream 10” X 300 B1A
flange
iii) Crude to Desalter valve upstream flange 10” X 300 B1A
iv) Crude to 11-E-08 valve upstream flange 10” X 300 B1A
v) LVGO inlet valve downstream flange 4” X 300 B1A
vi) LVGO outlet valve downstream flange 4” X 300 B1A
vii) Crude inlet cutter line 1” X 150 A9A
viii) Crude to CBD 1 ½ “ X 150 A1A
ix) LVGO to CBD 1“ X 150 A1A
8. 11-E-08 Crude/ i) Crude inlet valve downstream flange 8” X 300# B1A
Diesel ii) Crude outlet valve upstream flange 8” X 300# B1A
product iii) Diesel product inlet valve downstream 6” X 300# B1A
flange
iv) Diesel product outlet valve upstream flange 6” X 300# B1A
v) CBD inlet crude inlet
vi) Diesel product to CBD 1 ½” X150# A1A
1” X 150# A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
9. 11-E-09 Crude / i) Crude inlet valve downstream flange 8”X 300# B1A
KERO CR ii) Crude outlet valve upstream flange 8” X 300# B1A
iii) Crude inlet from 11-E-11 at 11-E-11 valve 8” X 300# B1A
downstream flange
iv) KERO CR inlet valve downstream flange 12” X 300# B7A
PG mode
v) KERO CR inlet valve downstream flange 12” X 300# B7A
BH mode
vi) KERO CR outlet valve upstream to control 12” X 300# B7A
valve flange
vii) KERO CR outlet to 11-C-01 valve upstream 12” X 300# B7A
flange
viii) Crude inlet to CBD 1 ½ “ X150 # A1A
ix) KERO CR inlet to CBD. 1 ½ “ X150 # A1A
10. 11-E-10 Crude/ i) KERO product inlet valve downstream 6“ X300 # B7A
KERO flange
product ii) KERO product outlet valve upstream flange 6“ X300 # B1A
iii) Crude inlet valve from 11-E-11 downstream
flange 8“ X300 # B1A
iv) Crude outlet valve from 11-E-09
downstream flange 8“ X300 # B1A
v) Crude outlet shell flange
vi) CBD drain 8“ X300 # B1A
1 ½ “ X300 # A1A
11. 11-E-11 Crude/ i) Crude inlet valve from 11-E-10 bypass 8” X 300# B1A
KERO CR downstream flange
ii) Crude inlet valve from 11-E-08 downstream 8” X 300# B1A
flange
iii) Crude outlet valve upstream flange 8” X 300# B1A
iv) KERO CR inlet from 11-E-09 and 11-E-25 12” X 300# B7A
inlet valve downstream flange
v) KERO CR inlet valve downstream flange 10” X 300# B7A
vi) KERO CR outlet valve upstream flange
vii) KERO CR outlet valve upstream flange 10” X 300# B7A
12” X 300# B7A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
12. 11-E-12 Crude/ i) Crude inlet valve downstream flange 8” X 300# B1A
iii) Diesel product inlet valve downstream 6” X 300# B7A
flange
iv) Diesel product outlet valve upstream flange 6” X 300# B1A
v) Diesel CR from 11-E-13 valve downstream
flange 8” X 300# B7A
vi) Diesel inlet to CBD
vii) Crude inlet to CBD 1 ½ ” X 150# A1A
1 ½ ” X 150# A1A
13. 11-E-13A/B Crude/ i) Crude inlet valve downstream flange 8” X 300# B1A
Diesel CR ii) 11-E-13 inlet bypass valve downstream 8” X 300# B1A
iii) Crude outlet valve at 11-E-14 upstream 8” X 300# B1A
iv) At 11-E-14 and 11-E-15 bypass valve 8” X 300# B1A
upstream flange
v) Diesel CR inlet downstream flange 8” X 300# B7A
vi) Diesel product inlet downstream flange 6” X 300# B7A
vii) Diesel CR outlet valve upstream flange 8” X 300# B7A
viii) Diesel product outlet valve upstream 6” X 300# B7A
ix) Crude to CBD 1 ½” X150 A1A
x) Diesel CR to CBD 1 ½” X150 A1A
14. 11-E-14A/B Crude / i) Crude inlet valve downstream flange 8” X 300# B7A
iii) 11-E-13 crude bypass valve downstream 8” X 300# B7A
flange
iv) Diesel inlet valve downstream flange 6” X 300# B7A
v) Diesel outlet valve upstream flange 6” X 300# B7A
vi) Diesel CR inlet valve downstream flange 8” X 300# B7A
vii) Diesel CR outlet valve upstream flange
viii) Crude inlet and outlet to CBD 8” X 300# B7A
ix) Diesel inlet to CBD 1 ½ ” X 150# A1A
1 ½ ” X 150# A1A
15. 11-E-15A/B Crude / i) Crude inlet valve downstream flange 8” X 300# B7F
Diesel CR ii) Crude outlet valve upstream flange 8” X 300# D7F
iii) Diesel CR inlet valve downstream 8” X 300# B4F
iv) Diesel CR outlet valve upstream flange 8” X 300# B7A
v) Diesel CR inlet to CBD 1 ½ ” X 150# A1A
vi) Crude inlet and outlet to CBD 1 ½ ” X 150# A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
16. 11-E-16 Crude / SR i) Crude inlet valve downstream flange 8” X 600# D7A
ii) Crude outlet valve upstream flange 8” X 600# D7A
iii) SR inlet valve downstream flange 8” X 300# B4F
iv) SR outlet valve upstream flange 8” X 300# B4F
v) Crude inlet to CBD 1 ½” X 150# A1A
vi) Crude outlet to CBD 1 ½” X 150# A1A
vii) SR inlet to CBD 1 ½” X 150# A1A
viii) SR outlet to CBD 1 ½” X 150# A1A
17. 11-E-18 Wash i) Water inlet flange 4”X300# B1A
water / LP ii) Wash water outlet flange 4”X300# B1A
iii) LP steam inlet flange 2”X150# A3A
iv) LP outlet(condensate) 2”X150# A3A
v) Wash water to CBD 1 ½”X150# B1A
18. 11-E-19 Stabilizer i) Stabilizer feed inlet to 11-E-19 6” X300# B1A
feed / SRN ii) Unstabilized naphtha to stabilizer from 11-E- 6”X300# B1A
No isolation 19
valves iii) SRN inlet 6” X300# B1A
iv) SRN outlet 6”X300# B1A
v) SRN to CBD 2”X150# A1A
vi) Unstabilized naphtha to CBD 1”X150# A1A
19. 11-E-25 Stabilizer i) Naphtha to reboiler flange (2 no’s) 10”X300# B1A
reboiler ii) Naphtha from reboiler flange (2 no’s) 10”X300# B1A
iii) KERO CR to reboiler inlet flange 10”X300# B7A
iv) KERO CR outlet flange from reboiler 10”X300# B7A
v) KERO CR to CBD 2”X150# A1A
vi) Naphtha to CBD 1 ½”X150# A1A
20. 11-E-40A/B Crude/ i) Crude inlet valve downstream flange 8”X300# D7A
circulating ii) Crude outlet valve upstream flange 8”X300# D7A
oil iii) Circulating oil inlet valve flange 8”X300# B4F
iv) Circulating oil outlet valve upstream flange 8”X300# B4F
v) Crude in let to CBD
vi) Cutter inlet to crude line 1 ½”X 150 A1A
vii) Circulating oil to CBD 1” X 150 A1A
viii) Cutter to Circulating oil 1 ½”X 150 A1A
1”X 150 A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
21. 12-E- Crude/ i) Crude inlet valve downstream flange 8”X300# B1A
01A/B/C KERO CR ii) Crude outlet valve upstream flange 8”X300# B1A
iii) KERO CR inlet valve flange 8”X300# B7A
iv) KERO CR outlet valve upstream flange 8”X300# B1A
v) SR to shell inlet 10”X300# B4F
vi) SR from shell outlet line 10”X300# B4F
vii) Cutter to crude 1”X150 A1A
viii) Crude to CBD 2 nos 1”X150 A1A
ix) Cutter to KERO CR 1”X150 A1A
x) KERO CR to CBD 1 ½”X150 A1A
22. 12-E-02 Crude/ i) Crude inlet valve downstream flange 6”X300# B1A
HVGO ii) Crude outlet valve upstream flange 6”X300# B1A
iii) HVGO inlet valve downstream flange 6”X300# B7A
iv) HVGO outlet valve upstream flange 6”X300# B7A
v) Cutter to crude 1 ”X150 A1A
vi) Crude to CBD 2 nos 1 ½”X150 A1A
vii) Cutter to HVGO 1 ”X150 A1A
viii) HVGO to CBD 2 nos 1 ½”X150 A1A
23. 12-E-03 Crude/ SR i) Crude inlet valve downstream flange 8”X300# B1A
ii) Crude outlet valve upstream flange 8”X300# B1A
iii) SR inlet valve downstream flange 8”X300# B4F
iv) SR outlet valve upstream flange 8”X300# B7A
vi) Crude to CBD 2 nos 1 ½”X150 A1A
vii) Cutter to SR 1 ”X150 A1A
viii) SR to CBD 2 nos 1 ½”X150 A1A
24. 12-E-04 Crude/ i) Crude inlet valve downstream flange 8”X300# B7A
HVGO ii) Crude outlet valve upstream flange 8”X300# B7A
v) HVGO vertical line valve 6”X300# B7A
vi) Cutter to crude 1 ”X150 A1A
vii) Crude to CBD 2 nos 1 ½”X150 A1A
viii) Cutter to HVGO 1 ”X150 A1A
ix) HVGO to CBD 2 nos 1 ½”X150 A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No
25. 12-E-05A/B Crude/ i) Crude inlet valve downstream flange 8”X300# B7A
HVGO ii) Crude outlet valve upstream flange 8”X300# D7A
vi) Crude to CBD 2 nos 1 ”X150 A1A
vii) Cutter to HVGO 1 ”X150 A1A
viii) HVGO to CBD 2 nos 1 ”X150 A1A
26. 12-E-06A/B Crude/ SR i) Crude inlet valve downstream flange 8”X300# D7A
ii) Crude outlet valve upstream flange 8”X300# D7A
iii) SR inlet valve downstream flange 8”X300# B4F
iv) SR outlet valve upstream flange 8”X300# B4F
v) RCO inlet valve downstream flange 8”X300# A1A
vi) RCO outlet valve upstream flange 8”X300# A1A
vii) cutter to Crude side 1 ”X150 A1A
viii) crude to CBD 1 ½”X150 A1A
ix) cutter to shell side 1 ”X150 A1A
x) SR to CBD 1 ½”X150 A1A
27. 12-E-10 HVGO i) HVGO inlet 6”X300 B7A
steam gen ii) HVGO outlet 6”X300 B7A
iii) MP steam outlet 2 nos 2”X300 B2A
iv) BFW inlet 2”X300 B2A
v) Cutter to HVGO 2”X 150 A1A
vi) HVGO to CBD 1 ½ “ X150 A1A
28. 12-E-10A HVGO i) HVGO inlet 6”X300 B7A
steam gen ii) HVGO outlet 6”X300 B7A
iii) MP steam outlet 2 nos 2”X300 B2A
iv) BFW inlet 2”X300 B2A
v) Cutter to HVGO 1”X 150 A1A
vi) HVGO to CBD 1 “ X150 A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
COOLERS AND CONDENSERS:
S. COOLER/ SERVICE BLINDS SIZE & SPEC

No CONDESERS RATING
1. 11-E-17 A/B Atmos O/h i) Vapor inlet valve down stream flange 16”X 150 A3A
vapors ii) 2” service water line
iii) Condenser outlet valve to drum 2”X150 A9A
upstream flange 8”x150 A9A
iv) To CBD
v) Gas make up flanges 2 nos 1 ½” X150 A1A
vi) Salt water inlet valve 2”X 150 A9A
vii) Salt water outlet flange 10” J5A
viii) Salt water reverse inlet valve 10” J5A
ix) Salt water reverse outlet flange 10” J5A
10” J5A
2. 11-E-17 C/D Atmos O/h i) Vapor inlet valve down stream flange 16”X 150 A3A
upstream flange 8”x150 A9A
iv) To CBD
10” J5A
3. 11-E-17 E/F Atmos O/h i) Vapor inlet valve down stream flange 16”X 150 A3A
upstream flange 8”X150 A9A
iv) To CBD
10” J5A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No CONDESERS RATING
4. 11-E-17 G/H Atmos O/h i) Vapor inlet valve down stream flange 16”X 150 A3A
upstream flange 8”X150 A9A
iv) To CBD
10” J5A
5. 11-E-20 A/B stabilizer i) Stabilizer vapors to condenser inlet 6”X150 A1A
O/h vapors ii) LPG from condensers 4”X150 A1A
iii) to flare 1”X150 A1A
iv) make up or depressuring line 1 ½”X 150 A1A
v) Salt water inlet valve downstream 8” J5A
flange
vi) Salt water outlet valve upstream flange 8” J5A
vii) Salt water reverse inlet valve
viii) Salt water reverse outlet flange 8” J5A
8” J5A
6. 11-E-20 C/D stabilizer i) Stabilizer vapors to condenser inlet 6”X150 A1A
O/h vapors ii) LPG from condensers 4”X150 A1A
iii) to flare 1”X150 A1A
iv) make up or depressuring line 1 ½”X 150 A1A
v) Salt water inlet valve downstream 8” J5A
flange
vi) Salt water outlet valve upstream flange 8” J5A
vii) Salt water reverse inlet valve
8” J5A
7. 11-E-21 SRN i) SRN inlet valve downstream flange 6”X300 B1A
ii) SRN outlet valve upstream flange 6”300 B1A
iii) Take off to FCCU-II 3”X300 B1A
iv) SRN to CBD 1 ½ “X150 A1A
v) Salt water inlet valve 6” J5A
vi) Salt water outlet flange 6” J5A
vii) Salt water reverse inlet valve 6” J5A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No CONDESERS RATING
8. 11-E-22 LVGO i) LVGO inlet valve downstream flange 4”X300 B1A
ii) LVGO outlet valve upstream flange
iii) LVGO to CBD 4”X300 A1A
iv) Cutter to LVGO 2”X150 A1A
v) Salt water inlet valve 1”X150 A1A
vi) Salt water outlet valve 6” J5A
6” J5A
9. 11-E-22A LVGO i) LVGO inlet valve downstream flange 4”X300 B1A
ii) LVGO outlet valve upstream flange
iii) LVGO to CBD 4”X300 A1A
iv) Cutter to LVGO 1 ½ ”X150 A1A
v) Salt water inlet valve 1”X150 A1A
vi) Salt water outlet valve 6” J5A
6” J5A
10. 11-E-23 Diesel i) DSL from 11-E-03 or KERO from 11- 6”X300 B1A
E-02 inlet valve downstream flange
ii) DSL/KERO to CBD
iii) Cutter to DSL line 1 ½”X150 A1A
iv) t/o to 11-E-24 1”X150 A1A
v) to DSl storage 6”X300 B1A
vi) salt water inlet valve downstream 6”150 A1A
flange 6” J5A
vii) salt water outlet valve upstream flange
6” J5A
11. 11-E-23A Diesel i) Dsl from 11-E-03 inlet valve 6”X300 B1A
ii) t/o to FCCU-II 2”X150 A1A
iii) DSL to CBD 1 ½”X150 A1A
iv) Cutter to DSL 1”X150 A1A
v) DSL to storage 6”X150 A1A
vi) Salt water inlet valve 6” J5A
vii) Salt water outlet valve 6” J5A
12. 11-E-24 KERO KERO from 11-E-02 6”X300 B1A
Cutter to KERO 1”X150 A1A
Kero from 11-E-24 outlet 6”X300 B1A
KERO to CBD 1”X150 A1A
Salt water inlet valve 6” J5A
Salt water outlet valve 6” J5A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No CONDESERS RATING
13. 11-E-24A KERO KERO from 11-E-02 6”X300 B1A
Kero from 11-E-24 outlet 6”X300 B1A
KERO to CBD 1”X150 A1A
14. 11-E-26 Heavy HN from 11-E-01 inlet valve 3”X150 A1A
Naphtha HN to CBD 1”150 A1A
HN from 11-E-26 3”X150 A1A
15. 12-E-08 A Tempered i) tempered water from 12-E-09A-D-inlet 8”X150 A3A
water ii) tempered water outlet valve
iii) salt water inlet valve 8”X150 A3A
iv) salt water outlet valve 10” J5A
v) salt water reverse inlet valve 10” J5A
vi) salt water reverse outlet valve 10” J5A
10” J5A
16. 12-E-08 B Tempered i) tempered water from 12-E-09A-D- 8”X150 A3A
water inlet
ii) tempered water outlet valve 8”X150 A3A
iii) salt water inlet valve 12” J5A
iv) salt water outlet valve 12” J5A
v) salt water reverse inlet valve 12” J5A
vi) salt water reverse outlet valve 12” J5A
17. 12-E-09A/B SR/ i) SR from 12-E-01 A/B/C inlet valve 6”X300 B1A
Tempered downstream flange
water ii) SR to run down. 6”X300 B1A
iii) SR to CBD 2 nos 1 ½”X150 A1A
iv) Tempered water inlet valve 6”X150 A3A
v) Tempered water out let valve 6”X150 A3A
vi) Tempered water to OWS ¾”X 150 A3A
18. 12-E-09C/D SR/ i) SR from 12-E-01 A/B/C inlet valve 6”X300 B1A
Tempered downstream flange
water ii) SR to run down. 6”X300 B1A
iii) SR to CBD 1 ½”X150 A1A
iv) Tempered water inlet valve 6”X150 A3A
v) Tempered water out let valve 6”X150 A3A
vi) Tempered water to OWS ¾”X 150 A3A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES

No CONDESERS RATING
19. 12-E-11 LVGO i) LVGO inlet valve downstream flange 4”X 300 B1A
ii) LVGO from 11-E-22/22A inlet
iii) LVGO outlet 4”X300 B1A
iv) LVGO to CBD 4”X300 B1A
v) Cutter to LVGO line 1 ½”X150 A1A
vi) Salt water inlet flange 1”X 150 A1A
6” J5A
20. 12-E-12A HVGO i) HVGO inlet from 12-E-04 6”X300 B7A
ii) HVGO outlet r/d 6”X300 B7A
iii) Bypass valve from 12-E-12B 6”X300 B7A
iv) HVGO from 12-E-10/10A 6”X300 B7A
v) VGO to CBD 1 ½ ”X150 A1A
vi) Cutter to VGO line 1”X150 A1A
vii) Salt water inlet flange 6” J5A
viii) Salt water outlet flange 6” J5A
21. 12-E-12B HVGO i) LVGO inlet from 11-E-07 valve 4”X 300 B7A
downstream flange
ii) LVGO outlet 4”X300 B7A
iii) HVGO inlet from 12-E-04 6”X300 B7A
iv) HVGO outlet r/d 6”X300 B7A
v) Bypass valve from 12-E-12A 6”X300 B7A
vi) VGO to CBD 1 ½”X150 A1A
vii) Cutter to VGO line 1”X 150 A1A
viii) Salt water inlet flange 6” J5A
Salt water outlet flange 6” J5A
34.2.3 Heaters Blind List:
11F01 ENTRY BLIND LIST:
S. No DESCRIPTION SIZE RATING SPEC

1. To install b/m on FO to individual burners(12nos) ¾“ 300 B1A
2. FG c/v 1st block valve downstream flange and bypass valve 6 ‘’ 150 A1A
upstream flange
3. 4’’ yard air to decoking at pillar no 26 4 ‘’ 150 A3A
4. Soot blowing steam valve at down stream flange 4 ‘’ 300 B2A
5. LP smothering steam to take valve down stream flange 4 ‘’ 150 A2A
6. Di -sulphide gas line valve at up stream valve down stream ¾ ‘’ 300
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
flange
7. Hot well off gas line 3 ‘’ 150 A1A
8. Atomizing steam take off valve down stream flange 3 ‘’ 300 B2A
9. Super heater steam out let flange 6’’ 300 B2A
10. Super heater steam in let flange 10’’ 300 B2A
11. Pass A control valves upstream block valve downstream 6’’ 300 B7A
flange & its bypass valve upstream flange
12. Pass B control valves upstream block valve downstream 6’’ 300 B7A
13. Pass C control valves upstream block valve downstream 6’’ 300 B7A
14. Pass D control valves upstream block valve downstream 6’’ 300 B7A
15. Pass A out let flange at heater 6’’ 300 B7A
16. Pass B out let flange at heater 6’’ 300 B7A
17. Pass C out let flange at heater 6’’ 300 B7A
18. Pass D out let flange at heater 6’’ 300 B7A
19. Purge steam (for each pass flow) 4 no’s 2” 300 B2A
12F01 ENTRY BLIND LIST:
S. No DESCRIPTION SIZE RATING SPEC

1. Fuel gas line take off valve flange (2 no’s) 3” 150 A1A
2. Atomizing steam take off valve downstream flange 3” 300 B2A
3. Soot blowing steam take off valve down stream flange 4” 300 B2A
4. Smothering steam take off valve down stream flange 6” 150 A2A
5. FG line at EBL valve down stream flange 6“ 150 A1A
6. FO supply mass flow meter Downstream valve and bypass 3” 300 B1A
valve downstream ( 2nos)
7. FO return downstream of SDV 3’’ 150 B1A
8. Turbulising steam (4 no’s) 2” 300 B2A
9. Purge steam (4no’s) 2” 300 B2A

10. Pass –A control valves upstream block valve downstream 4” 300 B4F
11. Pass –B control valves upstream block valve downstream 4” 300 B4F
12. Pass –C control valves upstream block valve downstream 4” 300 B4F
13. Pass –D control valves upstream block valve downstream 4” 300 B4F
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
14. Radiation out let (4 no’s) 8” 300 B2G

15. 4” yard air to decoking 4” 150 A3A
16. Service water and steam combined line to APH 3” 150 A1A
Columns Blind List:
11C01 BLIND LIST:
S. No. DESCRIPTION SIZE& RATING SPEC

1. TOP OUTLET 24”X150 A3A
2. VENT 3”X150 A9A
3. REFLUX 6”X150 A1A
4. SAFETY VALVE TAKE-OFF (BOILER MAKER) 14”X150 A1A
5. TPA RETURN 12” X150 A1A
6. TPA TAKE OFF (2 no’s) 14”X150 A1A
7. HEAVY NAPHTHA VAPOR RETURN 8”X150 A1A
8. SIDE DRAW (HEAVY NAPHTHA) 6”X150 A1A
9. KERO VAPOR RETURN 12”X150 A9A
10. KERO CR RETURN 12”X150 A1A
11. SIDE DRAW (KEROSENE) 18”X150 A9A
12. DIESEL VAPOR RETURN 14”x150 A4F
13. DIESEL CR RETURN 14”x150 A4F
14. PFD VAPOR TO COLUMN 10”X300 B1A
15. SIDE DRAWOFF (DIESEL) 14”X150 A4F
16. DESALTER AND PFD RV OUTLETS 10”X150 A1A
17. OVERFLASH DRAW 6”X150 B4F
18. OVERFLASH RETURN 6”X150 B4F
19. FEED WITH COMPANION FLANGE 24”X300 B4F
20. BOTTOM STEAM 8”X300 B2A
21. BOTTOM OUTLET 12”X300 A4F
22. UTILITY CONNECTION 1 ½” X150 B4F
11C02 BLIND LIST:

1 FEED HEAVY NAPHTHA 6”X150 A1A
2 BOTTOM OUTLET OF HEAVY NAPHTHA 6”X150 A1A
3 TOP OUTLET HEAVY NAPHTHA 8“X150 A1A
4 VENT 2”X150 A9A
5 UTILITY CONNECTION 1 ½”X150 A9A
6 STRIPPING STEAM HEAVY NAPHTHA 4”X300 B2A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
11C03 BLIND LIST:

1 FEED KEROSENE 12”X150 A9A
2 BOTTOM OUTLET KEROSENE 8”X150 A9A
3 TOP OUTLET KEROSENE 12”X150 A9A
4 VENT 2”X150 A9A
5 UTILITY CONNECTION 1 ½ ”X150 A9A
6 STRIPPING STEAM KEROSENE 6”X300 B2A
11C04 BLIND LIST:

1 FEED DIESEL 12”X150 A4F
2 BOTTOM OUTLET DIESEL 8”X150 A9A
3 TOP OUTLET DIESEL 14”X150 A4F
4 VENT 2”X150 A9A
5 UTILITY CONNECTION 1 ½ ”X150 A9A
6 STRIPPING STEAM DIESEL 6”X300 B2A
11C05 BLIND LIST:

1. VAPOR TAKEOFF 10”X150 A1A
2. RV TAKE OFF 6”X300 A1A
3. VENT 2”X300 A1A
4. REFLUX FLOW 4”X300 A1A
5. FEED ENTRY 6”X300 B1A
6. REBOILER RETURN 18”X 300 B1A
7. REBOILER DRAW OFF 16”X300 B1A
8. SRN DRAWOFF 6”X300 B1A
9. MP STEAM CONNECTION 1 ½ “X 300 A2A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
12C01 BLIND LIST:

1. TOP OUTLET 36”X150 A1A
2. VENT 4”X150 A1A
3. SAFEY VALVE 10”X150 A1A
4. LVGO REFLUX 4”X150 A1A
5. LVGO DRAWOFF 10”X150 A1A
6. HVGO CR+LVGO IR 8”X150 A3A
7. HVGO DRAWOFF 18”X150 A4F
8. HVGO IR 6”X150 A4F
9. SLOPCUT DRAWOFF 8”X300 A4F
10. PUMP OUT VENT 3”X300 B4F
11. FEED 52”X300 B6A(C*)
12. LP STEAM 3”X300 A2A
13. QUENCH RETURN 6”X300 B7A
14. BOTTOM OUTLET 12”X300 A4F
15. UTILITY CONNECTION 1 ½ ”X300 A4F
32.4.5 Vessels blind list:
11-V-01 BLIND LIST:

1 OVERHEAD NAPHTHA FROM 11-E-17A-H 12”X 150 A9A
2 RV TO FLARE 4”X 150 A9A
3 TAKE OFF TO FLARE OR MAKEUP 6”X 150 A9A
4 VENT 2”X 150 A9A
5 REFLUX DRAW OFF 12”X150 A1A
6 BOOT TAKEOFF 3“X150 A9A
7 DRAIN 1 ½”X150 A9A
11-V-02 BLIND LIST: DESALTER:

1. FEED INLET 10”X300 B1A
2. FEED OUTLET 10”X300 B1A
3. FEED OUTLET BOTTOM 8”X300 B1A
4. RELIEF VAVLE TAKE OFF 10“X300 B1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
5. DESLUDGING WATER LINE UP (3 NOS) 2“X300 B1A

6. VENT 3”X300 B1A
7. EFFLUENT WATER TAKE OFF (2 NOS) 2”X300 B1A
8. LP STEAM 2”X300 A2A
9. BOTTOM DRAIN ¾”X 300 B1A
10. DRAIN 6”X300 A1A
11. TRI-COCKS ¾” X300 B1A
11-V-03 BLIND LIST: STABILIZER OVER HEAD DRUM
S NO DESCRIPTION SIZE& RATING SPEC

1. VAPORS FROM 11-E-20A-D 8”X150 A1A
2. RV TAKE OFF 1 ½”X150 A1A
3. STABILISER OFF GAS TO FUEL GAS 4”X150 A1A
4. BYPASS LINE TO CONTROL VALVE 3”X150 A1A
5. SPLIT CONTROL VALVE RETURN 3”X150 A1A
6. VENT 2”X150 A9A
7. UTILITY CONNECTION 1 ½”X150 A1A
8. BOOT TAKE OFF 2”X150 A1A
9. LPG PUMP SUCTION 8”X150 A1A
11-V-04 BLIND LIST: DESALTER WATER TANK

1 DM WATER MAEK UP 3”X150 A3A
2 DRAIN 3”X150 A3A
3 VENT 2”X150 A3A
4 SUCTION TO WASH WATER PUMPS 4”X150 A3A
5 MAB CONDENSATE 4”X150 A3A
6 TOP DRAIN 3”X150 A3A
11-V-05 BLIND LIST: DECOKING POT:

1 SERVICE WATER INLET 3”X150 A3A
2 VENT 20”X150 A9A
3 INLET 18”X300 B7A
4 DRAIN 6”X150 A9A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
11-V-06A/B BLIND LIST: AMMONIA SOLUTION TANKS

1 AMMONIA FEED 1 ½”X150 A3A
2 SERVICE WATER 2”X150 A3A
3 OVERFOLW 1”X150 A9A
4 DRAIN ¾”X150 A9A
5 SOLUTION TO 11-PM-14A/B/C 1”X150 A9A
6 COMMON CONNECTION TO DRUMS 1”X150 A9A
11-V-07A/B BLIND LIST: CAUSTIC TANKS:

1 CAUSTIC INLET 3”X150 A9A
2 SERVICE WATER MAKE UP 1 ½”X150 A3A
3 VENT 2”X150 A9A
4 AIR INLET 2”X150 A3A
5 CAUSTIC MAKE UP 2”X150 A1A
6 VENT 1”X150 A9A
7 TAKE OFF TO PUMP SUCTION 1”X150 A9A
8 DRAIN ¾”X150 A9A
9 OVERFLOW 2”X150 A9A
11-V-08 BLIND LIST: CBD DRUM

1 CBD INLET 8”X150 A1A
2 PUMP SUCTION MANWAY
3 SERVICE WATER INLET 4”X150 A3A
4 COOLING WATER INLET 3” J5A
5 COOLING WATER OUTLET 3” J5A
6 VENT
7 LP STEAM INLET 2”X150 A2A
11-V-10 BLIND LIST:

1 CRUDE BOTTOM DRAW OFF 14”X 300 B7A
2 CRUDE INLET 10”X300 D7A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
3 PFD VAPOR OUTLET TO 11-C-01 10”X300 B1A

4 RELIEF VALVE 8”X300 B1A
5 VENT 3”X300 B1A
6 DRAIN 6”X300 B1A
7 CUTTER CONNECTION 4”X300 A1A
8 DRAIN TO OWS 3”X300 B1A
12-V-01 BLIND LIST:

ST
1. 1 STAGE EJECTOR CONDENSATE 4”X150 A1A
2. 2ND STAGE EJECTOR CONDENSATE 4”X150 A1A
3. 3RD STAGE EJECTOR CONDENSATE 3”X150 A1A
4. UN-CONDENSABLE GAS 8”X150 A1A
5. OFF GAS TAKE OFF 8”X150 A1A
6. VENT 2”X150 A1A
7. HOT WELL WATER TAKEOFF (2 NOS) 2”X150 A9A
8. HOT WELL OIL TAKE OFF 2”X150 A1A
9. WATER MAKE UP 3“X150 A1A
10. UTILITY CONNECTION 1 ½ “X150 A1A
11. DRAIN 2”X150 A9A
12-V-02 BLIND LIST:

1 TEMPERED WATER INLET 10”X150 A3A
2 TEMPERED WATER OUTLET TO 12-PM- 12”X150 A3A
07A/B
3 OVERFLOW 3”X150 A3A
4 DM WATER MAKEUP 2”X150 A3A
5 TEMPERED WATER PUMP RETURN 3”X150 A3A
6 LP STEAM TO DRUM 1 ½”X150 A2A
12-V-3 BLIND LIST:

1 1ST INLET FEED 2”X150 A3A
2 2ND INLET 2”X150 A3A
3 VENT 4”X150 A3A
4 SYPHON LOOP 2”X150 A3A
5 STEAM CONDENSATE 2”X150 A1A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
10-V-01 BLIND LIST:

1 SRN TO 10-V-01 3”X150 A9A
2 SRN OUTLET TO 10-V-02 6”X150 A1A
3 RELIEF VALVE 3”X300 A1A
4 VENT 2”X300 B1A
5 CAUSTIC TAKEOFF 6”X150 A9A
6 UTILITY CONNECTION ½”X150 A9A
10-V-02 BLIND LIST: NAPHTHA WASH WATER DRUM

1 SRN FROM 10-V-01 6”X150 A1A
2 RELIEF VALVE 3”X300 A1A
3 VENT 2”X300 B1A
4 SRN TAKE OFF 6”X 150 A1A
5 WATER MAKE UP 6”X150 A1A
6 UTILITY CONNECTION ½”X150 A9A
34.3 LIST OF VENDOR MANUALS:
The following vendor manuals are available in CDU II.

i) Desalter manual
ii) EIL design Package
iii) ZEECO burner Manual
iv) DCS Operating Manual
v) APC manual
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.4 START-UP & SHUTDOWN CHECK LISTS:
34.4.1 CDU-II START-UP CHECK LIST:
Pre start up check list:
S. No Activity Responsibility Sign Time Remarks

1. Information given to P&U for
consumption of BCW, Senior
STEAM(MP/LP),BFW,DMW,FO AND supervisor
UNBOOSTED COOLING WATER
2. Information given to FCCU-2/FCCU-R for Senior
consumption of FG supervisor
3. Ensured portable pilot igniter in charged
PO
condition.
4. information given to MEROX for Senior
consumption of FLUSHING OIL supervisor
5. information given to CPP for consumption Senior
of power supervisor
6. Information given to PSS-20 for readiness Senior
of all motors. supervisor
7. information given to TPH for readiness of Senior
SLOP TANK and FEED BOOSTER supervisor
8. Senior
good housekeeping done
supervisor
9. Senior
availability of instrument air
supervisor
10. Senior
ensured availability of all critical pumps
supervisor
11. readiness of FIRE WATER atmos "A/B"
12. readiness of utilities
atmos "A/B"
(BCW,STEAM,DMW,BFW)
13. check for readiness of FG and effective FO
atmos "A/B"
circulation for atmos heater
14. check for readiness of FG and effective FO
vac "A/B"
circulation for vac heater
15. readiness of feed PH neutralization dosing
system, feed de-emulsifier system, atmos
atmos "A/B"
O/H PH neutralization dosing and atmos
O/H filmer injection.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
16. readiness of SRN caustic and water wash

atmos "A/B"
system
17. readiness of vac O/H PH neutralization
vac "A/B"
dosing
18. readiness of CBD pump vac "A/B"
19. ensured CBD level is under control vac "A/B"
20. ensured U/L feed B/V in closed condition vac "A/B"
21. ensured cooling water to O/H condenser atmos "A/B"
22. ensured stripping steams B/V's are closed atmos "A/B"
23. ensured atmos heater stack damper in open
atmos "A/B"
condition
24. ensured atmos heater is in natural draft atmos "A/B"
25. ensured vac heater stack damper in open
vac "A/B"
condition
26. Ensured vac heater is in natural draft. vac "A/B"
27. ensured BFW to steam gens are isolated vac "A/B"
28. ensured availability of pilot flames in
atmos "A/B"
atmos heater
29. ensured availability of pilot flames in vac
vac "A/B"
heater
30. proved clear SR and HVGO R/D's vac "A/B"
31. ensured atmos column bottom level is
atmos "A/B"
under control
32. ensured atmos column O/H accumulator
atmos "A/B"
level in under control
33. Ensured all DCS software switches are in
paner officer
start up mode.
34. ensured vac column bottom level is under
vac "A/B"
control
35. ensured steam traps on atmos stripping
atmos "A/B"
steam header are working condition
36. atmos heater pass FCV's and atmos
atmos "A/B"
column O/H PCV stroke checked
37. vac heater pass FCV's stroke checked vac "A/B"
38. ensured atmos stripper levels are pumped atmos
out "A/B"/PO
39. ensured vacuum is broken with FG vac "A/B"
40. ensured vac. Column vent in closed
vac "A/B"
position.( for breaking vacuum)
41. PPE box checking and found ok vac "A/B"
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
Atmos start up check list:
S. No Activity Responsibility Sign Time Remarks

1. Ensured tempered water coolers are in
service Vac "A/B"
2. Maintain atmos column pr at 0.5
kg/cm2 PO
3. Checked line up of feed circuit Atmos "A/B"
4. Checked line up of RCO circuit for feed
circulation Atmos "A/B"
5. Checked for any leaks on flanges of
feed and RCO circuits Atmos "A/B"
6. 1st phase condensate drained and from
exchangers and columns (after one
hour circulation and half an hour
settlement) Atmos "A/B"
7. Ensured atmos column bottom level
gauge glass indication tallying with the
level transmitter Atmos "A/B"/PO
8. Ensured all instruments are working on
feed and RCO circuits Atmos "A/B"
9. 2nd phase condensates drained from
exchangers and columns (after one hour
circulation and half an hour settlement) Atmos "A/B"
10. Line up of cooling water to overhead
condensers atmos "A/B"
11. ensured atmos heater in natural draft Atmos "A/B"
12. Ensured heater FG line deblinded Atmos "A/B"
13. Checked pilot flame healthiness in
atmos heater Atmos "A/B"
14. Checked main gas flame healthiness in
atmos heater Atmos "A/B"
feed passes of atmos heater Atmos "A/B"
16. Allowed COT to raise at the rate of 400
c/hr PO
17. Allowed atmos column Flash Zone
temp at 1200 c for about two hours to
remove condensate PO
18. Ensured tempered water temp operates
in between 600 c and 800 c Vac "A/B"/PO
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
19. Ensured feed pump suction temp

operates below 550 c Atmos "A/B"/PO
feed and RCO circuits at 2500 c of
atmos heater COT (hot bolting if
required) and hold for 2hrs for temp
profile of the column Atmos "A/B"
atmos heater inlet and outlet at 2500 c
COT (hot bolting if required) Atmos "A/B"
22. Checked atmos column bottom level,
overhead accumulator H/C and
interface levels are tallying with
corresponding level transmitters Atmos "A/B"/PO
23. Ensured that after each makeup of
atmos column bottom level feed B/V at
U/L is in isolated condition Atmos "A/B"
24. Ensure all circulating reflux pump
suction lines are free off condensate Atmos "A/B"
25. Lined up circulating reflux circuits to
column Atmos "A/B"
26. Lined up product circuits to slop Atmos "A/B"
27. Lined up atmos water to MEROX Atmos "A/B"
28. Ensured atmos heater pass O/L' s are
below 2600 c with 50 c imbalance Atmos "A/B"
29. Ensured atmos heater skin temp's are
below 5000 C and arch temp is below
8000 C Atmos "A/B"
30. place overhead condensers in service (if
condensers inlet temp >650 C) Atmos "A/B"/PO
31. FEED CUT IN TO ATMOS SECTION Atmos "A/B"/PO
32. Maintained pass flows above 50 m3/hr Atmos "A/B"
33. Increased atmos heater cot to 3500c Atmos "A/B"
34. Increased atmos column pressure to 2.0
kg/cm2 Atmos "A/B"
35. Start up mode switches kept back to
normal and RCO routed to vac heater
after introduction of bottom stripping
steam Atmos "A/B"/PO
36. Atmos O/H temp controlled below 1350
c by using top reflux and routed un- Atmos "A/B"/PO
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
stabilized naphtha to slop

37. Started KERO CR bypassing stab
reboiler after KERO stripper senses
level Atmos "A/B"/PO
38. Route Un-stabilizer Naphtha stabilizer
and ensure bottom level is below 70%.
39. Route KCR thru reboiler and stab
bottoms lined up to R/D and maintain
stabilizer pressure @ 8.5Kg/Cm2g. Atmos "A/B"
40. Maintained stab vapor line temp below
600 c by using stab reflux and LPG
lined up to R/D Atmos "A/B"/PO
41. Started DSL CR Atmos "A/B"/PO
42. Started TPA Atmos "A/B"/PO
43. Started HN product to slop Atmos "A/B"
44. Started KERO product to slop Atmos "A/B"
45. Started DIESEL product to slop Atmos "A/B"
46. Adjusted all other process parameters
suited to the type of feed PO
47. Introduced stripping steams to strippers
after removal of condensate PO
48. HN routed to diesel R/D Atmos "A/B"
49. KERO routed to diesel R/D Atmos "A/B"
50. Diesel routed to diesel R/D (ensured
diesel color is good) Atmos "A/B"
51. Routed product samples to LAB Atmos "A/B"
52. Feed booster placed I/S Atmos "A/B"/PO
53. Desalter pressured up (ensured that pass
flows are not Cascaded with total flow)
at 10 kg/cm2 Atmos "A/B"/PO
54. Power to Desalter energized Atmos "A/B"
55. Desalter effluent water lined up to
MEROX Atmos "A/B"
56. Wash water (service water/DMW)
injection to Desalter started Atmos "A/B"
57. Interface level counter checked with LT Atmos "A/B"/PO
58. Ensured Desalter PT tallying with local
PG Atmos "A/B"/PO
59. Demulsifier injection started Atmos "A/B"
60. Atmos O/H neutralizer injection started Atmos "A/B"
61. Atmos O/H filmer injection started Atmos "A/B"
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
62. HN to SRN/DIESEL R/D Atmos "A/B"/PO

63. KERO to KERO R/D Atmos "A/B"/PO
64. Commission PFD as per procedure. Atmos "A/B"/PO
Vac. Section start-up check list:
S.No Activity Responsibility Sign Time Remarks

1. Lined up vac bottom circuit for
circulation Vac "A/B"
2. Lined up BFW to HVGO steam
generators Vac "A/B"
3. ensure vac. Heater in natural draft Vac "A/B"/PO
4. Checked pilot flame healthiness in vac
heater Vac "A/B"
5. Checked main gas flame healthiness in
vac heater Vac "A/B"
6. Allowed Cot to raise at rate of 400 C/hr PO
7. Checked for any leaks on flanges of vac
column at 2500 C Vac "A/B"
8. Lined up cooling water to surface
condensers Vac "A/B"
feed passes of vac heater Vac "A/B"
VAC heater inlet and outlet at 2750 C of
COT Vac "A/B"
VAC column at 2750 C of COT Vac "A/B"
12. Ensured HW level tallying with LT Vac "A/B"/PO
13. Ensured all instruments are in working
condition on vac column and bottom
circuit Vac "A/B"/PO
14. Ensured all pump suction lines are free
off condensate Vac "A/B"
15. Lined up LVGO and HVGO R/Ds to
HVGO R/D tank Vac "A/B"
16. Lined up HWO to slop Vac "A/B"
17. Lined up HWW to MEROX Vac "A/B"
18. Ensured vac heater pass O/L's are Vac "A/B"
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
below 2750 C with 50 C imbalance

19. Ensured vac heater skin temp's are
below 5700 C and arch temp is below
7760 C Vac "A/B"
20. Ejector lined up (1A/B/C,
2A/B/C,3A/B/C) Vac "A/B"
21. FEED CUT IN TO VAC SECTION Vac "A/B"/PO
22. Maintained pass flows above 18 m3/hr PO
23. SR routed to RFO/HFO Vac "A/B"
24. Vacuum pulled Vac "A/B"/PO
25. HWW routed to MEROX Vac "A/B"
26. HWO routed to slop Vac "A/B"
27. Increased vac heater COT to 3850 C PO
28. HVGO product routed to SLOP Vac "A/B"
29. Slop cut routed to SR Vac "A/B"
30. Adjusted all other process parameters
suited to type of feed PO
31. Vac O/H neutralizer injection started Vac "A/B"
32. Vac O/H filmer injection started Vac "A/B"
33. Routed product samples to LAB Vac "A/B"
34. LVGO product routed to HVGO R/D
TK Vac "A/B"
35. HVGO product routed to HVGO R/D
TK Vac "A/B"
36. HW off gases routed to 11-F-01 and
vent closed Vac "A/B"/PO
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.4.2 CDU-II PLANNED SHUTDOWN CHECKLIST:
S no Activity required / done/ not Sign Time Remarks

not done
required
1. Clearance to be taken from manager &
YSF
2. Information to be given to CPP
3. Information to be given to SS20
4. Information to be given to P& U for the
expected reduction of BCW,
Steam(MP/LP),BFW, DMW, FO &
Cooling water consumption
5. Information to be given to TPH for
readiness of slop tank
6. Information to be given to FCCU-II,
VRCFP & DHDS before the removal of hot
feed
7. Information to be given to FCCU’s for the
expected reduction of FG consumption.
8. Information to be given to MEROX for the
expected reduction of stripped water flow
consumption.
9. Ensured readiness of CBD pump
10. Ensured all hot work permits stopped.
11. Ensured readiness of Fire water
12. Reduce feed rate gradually from 500 m3/hr
to 430 m3/hr. and accordingly adjust other
parameters like Heater firing, stripper
levels, Reflux drum levels etc
13. Slowly increased the PFD pressure to
ensure no vaporization.(PFD pressure C/V
closed fully)
14. After PFD level reduced to about 20%, PFD
by-pass valve to be opened
15. 11-PT-02B turbine speed reduced slowly
(informed power plant), Level C/V to be
closed fully.
16. 11-C-01 tray 14 shell V/V from PFD vapor
line to be closed
17. 11-E-40 crude side to be bypassed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
18. Reduce feed rate from 430 M3/Hr to 350

M3/Hr slowly.
19. Simultaneously product R/D flows & CR
flows to be reduced (first TPA, DSL CR,
then KERO CR)
20. Hot feed to FCCU-II to be taken out
21. 12-E-12 top cooler changed over to HVGO
mode from LVGO CR mode.
22. 12-E-06 A/B changed over to SR mode
from RCO mode.
23. Disulphide off gas to 11-F-01 taken out &
line blinded
24. Desalter water injection reduced slowly &
finally taken out
25. Desalter to be taken out
26. R/D flows & CR flows further to be
reduced in atmos. & vac. column
27. 12-F-01 COT slowly reduced.FO & FG trip
bypass taken in manual
28. Hot well off gas to 11-F-01 no. 17, 18, 19
and 20 burners to be taken out & vented to
atmosphere.
29. Off gas line to burners to be blinded
30. When the Vac. furnace COT reduced to 300
deg C, furnace is taken out from balanced
draft & placed in natural draft. First stack
damper opened, then ID fan stopped, then
DODs opened & simultaneously air flow to
furnace reduced & finally FD fan stopped
31. Slop cut to be taken out from CDU-I cooler
box (tk.4) & line cutter flushed
32. When Vac. furnace COT reduced below
300 deg C, all the fires to be taken out.
33. FG & FO line to furnace blinded
34. BFO kept under circulation
35. take out vac. Feed
36. ejector steam flow to be taken out & lines
blinded
37. Vac. column product pumps (LVGO &
HVGO) to be stopped after the levels came
down. Pump d/s & R/D v/v closed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
38. Slop cut to be recycled back to 12-F-01

until the level came down. Then slop cut
pump to be stopped.
39. Vac. section kept under circulation. 12-C-
01 bottom --12-PM-01 -- 12-F-01—12-C-
01
40. remove FG blind to vac. Column
41. FG introduced in vac. column to maintain
positive pressure
42. Feed slowly reduced from 350 m3/hr to 250
m3/hr. At this flow rate feed booster pump
11-PM-02B stopped
43. Diesel to DHDS taken out
44. All the chemical injections taken out
45. When atom. Furnace COT came down to
270-280 deg C furnace to be taken out from
balanced draft to natural draft. First stack
damper opened, then ID fan stopped, then
DODs opened & simultaneously air flow to
furnace reduced & finally FD fan stopped
46. As the KERO CR flow came down to 200
m3/hr, KERO CR booster pump stooped.
47. All fires to be taken out from atmos.
Furnace and pilot burners
48. All the product pumps & CR pumps
stopped except top reflux pump
49. Pump d/s V/Vs & R/D V/Vs closed.
50. Reflux pump stopped when reflux drum
level came down. Pump d/s V/Vs closed
51. Atmos. Column bottom & strippers
stripping steams stopped & shell B/Vs
closed.
52. Stabilizer feed C/V to be closed
53. CDU-I unstabilized naphtha to be taken out
and v/v to be closed
54. reduce stabilizer bottom level to minimum
SRN C/V to be closed
55. When stabilizer reflux drum level came
down LPG pump to be stopped. Pump d/s &
R/D V/Vs closed.
56. Atmos. Section kept under circulation.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
57. unit limit feed v/v to be closed

58. 11-C-01 Bottom—11-PM-10 B—SR
circuit—11-PT-01B—11-F-01 (by-passing
Desalter & PFD ) –11-C-01
59. Cutter to be taken at the top of vac. column
& LVGO level build up, pumped out by
LVGO pump & again put back into vac.
Column
60. Build up HVGO level and pump out to slop
& the whole HVGO circuit to be cutter
flushed & again put back to vac. column.
61. Build up slop cut level with cutter and
pump out the level to SR After that pumps
to be stopped. D/S & R/D V/Vs closed
34.5 LEL DETECTORS STATUS:
S No. TAG. No. LOCATION TYPE REMARKS
1 HCD1001 Stabilizer reflux pumps (11-PM-11A/B south side) HC

2 HCD1002 DL1503 boot drain point/ OWS HC
3 HCD1003 11-F-01 FD fan suction HC
4 HCD1004 12-F-01 FD fan suction HC
5 HCD1005 South east of Atmos Over head drum HC
6 HCD1006 North east of Atmos Over head drum HC
7 HCD1007 South east of over head condensers HC
8 HCD1008 North east of over head condensers HC
9 HCD1009 Top of 11-V-04 wash water drum HC
10 HCD1010 South west of 11-V-04 wash water drum bottom HC
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.6 INSTRUMENT AIR FAIL TO OPEN CONTROL VALVES IN CDU-2
S. No. CONTROL VALVE DESCRIPTION

NUMBER
1. 11DPV301 Atomizing Steam to FO DP
2. 11FV101 Vac. split control valve
3. 11FV204 Kero to diesel
4. 11FV301 11F01 Pass1
5. 11FV302 11F01 Pass2
6. 11FV303 11F01 Pass3
7. 11FV304 11F01 Pass4
8. 11FV403 Reflux
9. 11FV404 DSL C/R
10. 11FV405 Kero C/R
11. 11FV406 Top Pump Around CR
12. 11FV501 Stab. RX.
13. 11LV101 Desalter interface level
14. 11LV902 PFD level
15. 11PV101 PFD bypass SDV
16. 11PV105 Desalter pressure
17. 11PV409B Makeup control valve
18. 11PV501B Stab makeup.
19. 11PV902 PFD pressure
20. 12DPV103 12F01 Atm. steam & FO
21. 12FV101 12F01 Pass1
22. 12FV102 12F01 Pass2
23. 12FV103 12F01 Pass3
24. 12FV104 12F01 Pass4
25. 12FV109 Slop cut Recycle
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
26. 12FV201 Hot LVGO RX Flow

27. 12FV202 Hot HVGO Rx
28. 12FV203 Cold HVGO Rx.
29. 12TR201 SR Quench
30. 12FV205 LVGO top reflux
31. 12LV301 12E10 level
32. 12LV302 12E10A level
33. 12PV207 Ejector pressure
34. 12TV103 Cold SR to VBU
35. 13FV106 Air to BBU reactor
NOTE: All shutdown valves (SDVs), will close and all STACK DAMPERS and DOD’s
will open during instrument air failure.
34.7 DCP CYLINDERS, FIRE HOSE REELS AND SAFETY SHOWERS

LOCATIONS:
DCP LOCATION
BOX NO.
1. West of CSS - 20
2. North West of MOI
3. East of 11 - F - 1
4. South of 11 -F - 1
5. East of 11 - F - 1 (FD Fan)
6. South of 11 - E - 21
7. South of 11 - E - 14 AB
8. West of De Salter
9. West of Unit
10. East of Field Room
11. North of Vac Heater

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
12. East of 12 - PM - 01A
13. East of 11 - PM - 09A
14. East of 12 - PM - 04A
15. East of 13 - PM - 02B
16. Near 11 - PM - 12B
17. West of 11 - PM - 02A
18. South of 1st Floor (11 - V - 01)
19. South of 1st Floor (11 - V - 01)
20. South of Column (2nd Floor)
21. South of 2nd Floor(11-E -17E/F)
22. South of 2nd Floor(11-E-20A/B)
23. North Floor near 12 - E - 07A
24. 3rd Floor Vac Column
25. Top Floor Vac Column
26. Near 12 - E - 7C
27. Atmos Heater
28. Vac Heater
29. Vac Heater (12 - F -1)
30. Atmos Heater Top
31. Atmos Column (8th Landing)
32. Extreme Top on 11 - C -01
33. One CO2 extinguisher at field room
FIRST AID FIRE HOSE REELS
HR. No LOCATION
1. South of 11 - F - 1 (ID Fan)
2. South of 11 - E - 12
3. East of De Salter Drum

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
4. South West Corner
5. South West of 11 - PM - 02A
6. North of 11 - PM - 02A
7. Near 12 - E - 01 A/ B
8. Near 12 - PM - 04B
9. East of 13 - KM - 01B
10. North of Vac Column
11. North of Vac Heater
12. East of Vac Heater
13. West of Vac Heater
14. West of Vac Column
15. O/H Condenser 1st Floor

South of 11 - V - 03
16. O/H condenser 2nd Floor
S/E of 11 - E - 17 E/F
17. Near O/H Condenser North of 12 - E - 07A
18. South of 11-F-01 (ID FAN)
19. South of 11-E-16
SAFETY SHOWERS
Safety shower number Location

1 12-F-01 Heater Area - East Side
2 Chemicals Pump Area- North Side
3 10-PM-01A/B Caustic Pump Area – South Side
4 11-F-01 Heater Area - East Side
5 10-V-01 & 10-V-02 Area - North Side
6 BBU Compressor Area- Towards North side

OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.8 AUTO IGNITION TEMPERATURES:
The following are the auto ignition temperatures of the products handling:
S no Liquid Auto ignition temperature

1 Crude 500-850 °F
2 LPG 466.1 °C
3 Naphtha 232 °C
4 Motor spirit 280-456 °C
5 Kerosene 280 to 456 °C
6 ATF 230 °C
7 Diesel 257 °C
8 LDO 257 °C
9 JBO/MTO 253 °C
10 Fuel Oil 360 cst 487 °C
11 Fuel Oil 180 cst 500 °F
12 Bitumen >300 °C
13 Sulphur 232 °C
14 H2S 260 °C
15 Methane 537 °C
16 Ethane 515 °C
17 Ethylene 543 °C
18 Butane 420 °C
19 Propane 450 °C
20 Propylene 472 °C
21 Carbon monoxide 700 °C
34.9.1 A. Provision of Corrosion Coupons, Corrosion Probes

1. Corrosion Probes
Loop Line Line Piping
S. No. Tag Location Service
No. Description size Class
10"-P-11-319-
1 11-CP-301 13 Crude 10" D9A/CS
D7A-Ih Crude to Atmos Furnace
14"-P-11-410- Diesel CR + Product drawoff A4F/P5(5
2 11-CP-401 52(B) Diesel 14"
A4F-Ih line Cr)
3 12-CP-202 72 8"-P-12-222- LVGO Pump 12-P-04 A/B LVGO 8" A1A/CS
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
A1A-It Suction Line

6"- P-12-318- HVGO exchanger 12-E-05A/B
4 12-CP-301 76(E) HVGO 6" B7A/CS
B7A-It Outlet
16"-P-12-214- HVGO pump 12-P-03A/B A4F/P5(5
5 12-CP-203 73(A) HVGO 10"
A4F-It suction line Cr)
2. Corrosion Coupons
10"-P-11-319-
1 11-CC-301 13 Crude 10" D9A/CS
D7A-Ih Crude to Atmos Furnace
14"-P-11-410- Diesel CR + Product drawoff A4F/P5(5
2 11-CC-401 52(B) Diesel 14"
A4F-Ih line Cr)
8"-P-12-222- LVGO Pump 12-P-04 A/B
3 12-CC-202 72 LVGO 8" A1A/CS
A1A-It Suction Line
6"- P-12-318- HVGO exchanger 12-E-05A/B
4 12-CC-301 76(E) HVGO 6" B7A/CS
B7A-It Outlet
16"-P-12-214- HVGO pump 12-P-03A/B A4F/P5(5
5 12-CC-203 73(A) HVGO 10"
A4F-It suction line Cr)
6"-P-12-208- Slopcut pump 12-P-02A/B A4F/P5(5
6 12-CC-201 83 Slopcut 6"
B4F-It Suction Cr)
12"-P-12-201- Vac Residue pump 12-P- Vacuum A4F/P5(5
7 12-CC-204 73(A) 12"
A4F-It 01A/B pump section Residue Cr)
B. VR improvement schemes
1. ER Probes
8"-P-11-437-2- Light
1 CPI 1401 26 O/L of 11-E-17E/F 8" A9A
A9A Naptha
12"-P-11-437- Light
2 CPI 1402 26 I/L of 11-V-01 12" A9A
A9A Naptha
Vac O/H
4"-P-12-247-1-
3 CPI 2201 68 O/L of 12-E-7A condensat 4" A1A
A1A
e
2. PH Meter
1"- O/L hotwell drum near 12-LV- Sour
1 PH 2201 88 1" A9A
-A9A 201 Water
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
34.9.2 FSM: PROCESS /LOCATION DETAILS FOR CDU2
S Location Servic State Lin Parameters Pipi Max Probe Corroive Ben
constituent d
l e e ng flow metallu
N Siz Operating Design clas rgy
conditions conditions T/Hr
o e s/
Pressu Temper Pressu Temp Met
ature eratur
re re allur
Deg.C e
Kg/cm Kg/cm gy
Deg.
2g 2g
C
FSM (FOR MONITORING NAPHTHENIC ACID CORROSION)
1 Atmos furnace 11-F- Crude Vapor 6” 3.5 350- 4.8 400 B4F 112. Not Sulphur, H2S On
(ppm), CO2 elbo
01 Radiation outlet + 378 / P5 6 applica (ppm), Naph w
first elbow Liqui (5Cr ble Acid
6”-P-11-314-B4F-Ih d )
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
2 Atmospheric Crude Vapor 24” 3.5 350- 4.8 400 B4F 450 Sulphur, H2S -
(ppm), CO2
Transfer line + 378 / P5
(ppm), Naph
24”-P-11-318-B4F-Ih Liqui (5Cr Acid
d )
3 Vacuum furnace 12- Reduce Vapor 8” 50 410 3.5 / 425 B2G 62 Sulphur, H2S On
(ppm), CO2 elbo
F-01 Radiation outlet d + mm Full /P9
(ppm), Naph w
first elbow Crude Liqui Hg Vacuu (9Cr Acid
8”-P-12-115-B2G-Ih Oil d abs m )
Standing instructions No 32
Procedure for monitoring online ER probes, PIN matrixes and Corrosion coupons for High
Acid crudes in CDU-II
Objective: To monitor the system corrosion and keep it in the limited values while
processing HAC in the unit.
Background: CDU-II was designed for BH Crude. Later it was planned to process HAC
in CDU-II for getting better margins. During the 2010 T&I, projects had installed
corrosion probes, corrosion coupons, PH meter and Pin Matrix in CDU-II for
monitoring the corrosion factor when processing HAC. Monitoring the above
parameters and injecting the chemicals with proper dosage will reduce the corrosion
factor of lines and equipment’s.
Scope: This standing instructions is generated for monitoring the probes and injecting
the chemicals with proper dosage for reducing the corrosion factor when processing the
HAC in CDU-II.
Responsibility: The overall responsibility to implement these guidelines rests with the
unit shift in charge.
Standing Instructions:
The following are to be observed while processing HAC crudes in CDU-II :
1. PIN matrix device: In CDU-II ROXAR group had installed pin matrix devices in
11F01 pass B inlet and outlet lines and 12F01 pass B outlet lines for monitoring
the corrosion factor. Dedicated PC is provided in MOI for monitoring the
corrosion rates. Actual corrosion rate will display and there are calculated in
time bound period. Maximum allowable corrosion factor is 5mils/year.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
2. ER probes: These were installed in the following locations for monitoring the
corrosion rate during processing HAC. Below are the locations where corrosion
probes are installed in CDU-II.
S.No Tag Location Service
1 CI301 Crude to Atmos furnace Crude

2 CI400 Disel CR+Product drawoff line Diesel
3 C2202 LVGO pump 12-P-04 A/B suction line LVGO
4 C2301 HVGO exchanger 12-E-5 A/B outlet HVGO
5 C2203 HVGO pump 12-P-3 A/B suction line HVGO
6 C1401 11E17E/F O/L Naphtha
7 C1402 11V01 I/L Naphtha
8 C2201 12E07O/L VAc. O/H

9 PH2201 Hotwell water Sour water
In every shift the readings are to be noted (0400hrs, 1200hrs and 2000hrs) and
corrosion rate to be calculated.
a) The following calculations are to be done once in the shift for measuring the corrosion
rate (mils/yr):
For Example: value of C1402 at 31st Dec at 0400hrs :736076mil.
Value of C1402 at 31st Dec at 1200hrs: 7.6114mil
Corrosion rate = (present value –previous value)*365*24/(diff in hrs)
= (7.6114-7.6076)mil*365*24/8= 4.161mil/yr.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
When the value of ER probe reaches 9.5mil(ER probe range 0-10 mil), it has to be
informed to Tech-PAD for the replacement of the probe.
If the corrosion rate is more than 5mils/yr, the chemical dosing should be increased.
Corrosion rate and pH of the overhead system should be controlled by increasing
corrosion inhibitor and caustic injection to Desalter. HAC chemical dosing should be
increased to control the corrosion rate of side stream products. The HAC chemical
dosage rates will be provided by Tech-PAD.
The following tags are to be monitored and rate at which the value decreases implies
corrosion rate and proper action to be taken. To reduce the corrosion rate the chemical
injections are to be introduced and the following are the locations where chemicals
are introduced.
Injection point Diluent Source of diluent Diluent flow

tag
Suction of Crude booster pumps 11P02A Crude Crude from common F1604
discharge of 11P01A/B
Diesel CR and Product common draw off Diesel 11-E-03 (Dsl/crd) down F1605
line from 11C01 stream
Suction of RCO pumps 11P10 A/B. Diesel 11-E-03 (Dsl/crd) down F1606
stream
Suction of LVGO pumps 12P04 A/B HVGO 12-E-10/10A to 12-C-01 F2607
Suction of HVGO pumps 12P03 A/B HVGO 12-E-10/10A to 12-C-01 F2608
Suction of SR pumps 12P01 A/B HVGO 12-E-10/10A to 12-C-01 F2609
If the dosing rate reaches maximum limit but the corrosion rate does not come down,
it has to be informed to Tech-PAD for further advice.
b) Atmos water and hot well water pH are to be maintained between 5.5 and 6.5. Online
monitoring devices are installed to check HWW pH (PH2201) and high and low
values alarms were provided at 5.5 and 6.5. Corrective actions need to be taken in
case the value deviate from the given range. The main aim to maintain the pH
between 5.5 and 6.5 is when pH is acidic more corrosion takes place and leads to
depletion of pipelines and equipment. If pH is above 7, then salts will form and plug
the Overhead Condensers.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
3. Corrosion coupons: indicates the corrosion in a particular stream. These are monitored
in field. The coupons should be removed once in a month with the help of
maintenance (raise respective job card) and send to lab for weighment for pre-
determined period. The difference in weight of the corrosion coupon will be
monitored by Technical (PAD and inspection). The corrosion coupons are inserted at
the following locations:
S.No Tag Location Service

1 11-CC-301 Crude to Atmos furnace Crude
2 11-CC-401 Disel CR+Product drawoff line Diesel
3 12-CC-202 LVGO pump 12-P-04 A/B suction line LVGO
4 12-CC-301 HVGO exchanger 12-E-5 A/B outlet HVGO
5 12-CC-203 HVGO pump 12-P-3 A/B suction line HVGO
6 12-CC-201 Slop cut 12-P-02 A/B suction Slopcut
7 12-CC-204 VR pump 12-P-01 A/B pump section Vac residue
4. Corrective actions:
• Prior to changing over to HS( 1hr before spiking/ switch), the following
chemical injection rates are to be maintained:
S.No Chemical Dosage rate Lt/hr Pump max Pump

w.r.t crude feed flow stroke
rate
1. DMF 5PPM 10 12 80%
2. Ammonia 2PPM 24 20 50%
with 2
pumps
3. Filmer 3PPM 5.5 10 50%
4. Caustic 5PPM 58 75 80%
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 34
PLANT NAME: CDU II
Chapter Rev No: 0
ANNEXURES
Caustic should be introduced downstream of desalter and injection should start along
with the crude changeover activity.
The above dosage rates are to maintained to ensure minimal corrosion in the system.
However the dosage rates can be optimized based on the actual corrosion rate.
• In addition to the above, wash water rate of 5 to 6% on crude rate should be

maintained and mix valve DP to be maximized (target value: 05 Kg.cm2)
• If pH is less or more 6.5, ammonia dosage is to be increased or decreased
respectively.
While processing HAC, the HAC chemical (EC1245A) has to be introduced at the target
locations mentioned in the table.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
UTILITY SYSTEMS
Introduction to Utility System

The supply of utilities is common to CDU / VDU and BBU. The Utility System consists of
Instrument Air (IA)
Plant Air (PA)
once through cooling (Sea) Water
Bearing Cooling Water
Service Water (WS)
DM Water (DMW)
Boiler Feed Water (BFW)
Tempered Water (TW)
LP Steam
MP Steam
HP Steam
Fuel Oil (FO)
Fuel Gas (FG)
Flushing Oil (FLO).
Flare system
35.1.1 INSTRUMENT AIR SYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
The existing compressed air system at MEROX plant has an installed capacity of
15,000 m3/hr and comprises three big Elliott air compressors, each of capacity 5000 m3/hr. A
2" Instrument Air header supplies IA to CDU/VDU-II and BBU. The header is provided with
an isolation valve and a spectacle blind. IA is used as motive force for pneumatically
operated control valves and for the operation of 11-F-01 and 12-F-01 soot blowers. A
pressure gauge 11-PG-709, a temperature gauge 11-TG-708, a low pressure switch 11-PAL-
703 and a flow integrator 11-FQ-705 are provided on the header.
35.1.2 PLANT AIR SYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
A 4" plant air header supplies plant air to the entire unit. The header is provided with
an isolation valve and a spectacle blind for positive isolation at the battery limit. A number of
utility points are provided from this header. Dedicated 4" & 2" tapings are taken from main
header for decoking of Atmospheric Furnace & Vacuum Furnace, respectively. A 2" tapping
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
is provided to 11-V-07 A/B (Caustic solution tanks) for agitation. There is a provision to
route Plant Air to the Instrument Air header at the unit limit. There is also a provision to route
Plant Air to BBU reactor through 13-PIC-102. A pressure gauge 11-PG-710, a temperature
gauge 11-TG-709, and a flow integrator 11-FQ-708 are provided on the header.
35.1.3 ONCE-THROUGH COOLING (SEA) WATER SYSTEM

(Refer P&ID 10- 1100-E-201-1 Rev.6):
The cooling water requirement is met by the Once-through Cooling Water System in
which sea water is used. Sea water is supplied in two headers to the unit. One header of
30” size, known as the un-boosted water header, caters to the cooling water requirement at
the ground level and its supply pressure is 2.5 kg/cm2 g. The other header is a 24” one, known
as the boosted water header, caters to the cooling water requirement to the overhead
condensers and its supply pressure is 3.5 kg/cm2 g. The connected salt water booster pumps
(11-P-17 A/B) are there in FCCU-II.
Each of the supply headers is further bifurcated as follows
30” header into two headers of 26” and 18”
26” header into two headers of 18” and 26”
Both the return headers join one 36” header and go out of the unit to WWTP. There is
battery limit isolation with blinding facility for both the supply and return headers. A pressure
gauge 11-PG-701 and a temperature gauge 11-TG-702 are provided on the return header.
The following coolers have been provided with supply and return headers:
10” line to / from 11-E-17A to H
8” line to / from 11- E- 20A to D
6” line to / from 11-E-21
6” line to / from 11-E-23/23A
6” line to / from 11-E-21A
6” line to / from 11-E- 24/24A
6” line to / from 11-E- 22/22A
18” line to / from 12-E-07A/B/C
10” line to / from 12-E-12B
6” line to / from 12-E-12A
12” line to / from 12-E-08 A/B
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
35.1.4 BEARING COOLING WATER SYSTEM

(Refer P&ID 10-1100-E-201-2 Rev.6):
Circulating bearing cooling water is used for pump gland and bearing cooling, turbine
oil coolers etc., where use of sea water is prohibited. The BCW system for VREP-I caters to
the requirement in CDU/VDU-II, FCCU-II, PP-II, MEROX, air compressors, off sites and
PRU.
A bearing cooling water system with 2 cooling tower cells near the IFO system of the
refinery complex meets the additional bearing cooling water requirement of units in VREP-
II.A 4” BCW supply line and 4” and 6” return headers cater to the entire load of the unit.
There is a battery limit isolation valve with a spectacle blind. Pressure gauges 11-PG-
720/721, temperature gauges 11-TG-716/717 are provided on the supply and return headers
respectively.
35.1.5 SERVICE WATER SYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
Service water is required mainly for cleaning and washing. A 4" service water header
caters to the entire unit. It is provided with an isolation valve along with a spectacle blind at
battery limit. A pressure gauge 11-PG-711, a temperature gauge 11-TG-710, and a flow
integrator 11-FQ-709 are provided on the header at the battery limit.
The service water header supplies water to various hose stations in the plant, 11-V-05
(decoking pot), CBD drum (11-V-08), Caustic solution vessels (11-V-07 A/B) for dilution of
concentrated Caustic solution, Ammonia solution tanks (11-V-06 A/B), LVGO product / CR
pumps (12-P-04 A/B), Crude Charge pump (11-P-01 A/B) suction, to air pre-heaters (11-E-
27, 12-AP-01) and to BBU off-gas quench drum (13-V-02). Service water is also provided
for steam blow down drum (12-V-03), as makeup to Desalter water drum (11-V-04), to the
suction of 11-P-06 A/B (for washing 11-V-01) and to other equipment within the unit.
35.1.6 DM WATER SYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
A 4" header caters to the DM water need for the entire unit. It is provided with an
isolation valve and a spectacle blind at the battery limit. A pressure gauge 11-PG-714, a
temperature gauge 11-TG-713, and a flow integrator 11-FQ-706 are provided on the header at
the battery limit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
DM water is used as Desalter wash water in (11-V-04) and in the tempered water
drum (12-V-02) for level make-up.
35.1.7 BOILER FEED WATERSYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
A 3” BFW line caters to the entire load of the unit. It is provided with an isolation
valve and a spectacle blind in the battery limit. A pressure gauge 11-PG-13, a temperature
gauge 11-TG-712, and a flow integrator 11-FR/FQ-710 are provided on the header at the
battery limit. It serves the following points
1” line for de-superheating the steam exit of Atmospheric furnace
2” line for HVGO CR steam generators 12-E-10/10A
The line then goes to the Bitumen plant to supply BFW to the steam generators. And splits
into
2” line for BBU steam generators 13-E-01A/B, 13-E-03/03A.
1 ½” line to BBU reactor top.
35.1.8 LP STEAM SYSTEM

(Refer P&ID 10-1100-E-203 Rev.5):
A 6” LP Steam header caters to the requirement of the entire unit. The header is
provided with isolation valves and spectacle blind. A pressure gauge 11-PG-712, a
temperature gauge 11-TG-711, and a flow recorder / integrator 11-FR/FQ-707 are provided
on the header at the B/L. A 4” steam line is provided on the superheated MP steam line from
the Atmospheric Furnace. This line is to be used only when the LP steam header is low or
when the superheated MP steam temperature is more than 375 °C.
The following connections are provided on the header.
4” line to 11-E-18
6” line as snuffing steam to 11-F-01
6” line as snuffing steam to 12-F-01
3” & 1 ½” line to 12-C-01
2” header for the pumps 11-P-09 A/B, 12-P-03 A/B, 11-P-05 A/B, 12-P-04 A/B (1” each)
4” line to 11-C-01
4” & 2” line to 11-V-08
2” line to biturox reactor.
1” line to bitumen pumps 13-PM-01A/B.
1” take off to the BBU sample point.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
Use of LP steam is mainly as follows:

1. Sample point purging
2. Heating medium for exchangers (for heating products with LP steam)
3. Body steam for steam out of columns
4. Quench steam for pump mechanical seal
5. Snuffing steam of fired heaters / furnace
6. Soot blowing of fan blades
7. Heat Tracing of process lines
8. Dilution of vented hydrocarbons from vent systems
9. Steam smothering and utility
10. Dead end of CBD headers
35.1.9 MP STEAM SYSTEM

(Refer P&ID 10-1100-E-202 Rev.7):
MP steam for CDU/VDU-II is supplied from Power Plant-II. A 12" medium pressure steam
header caters to the entire unit. The header is provided with isolation valves and spectacle
blind. A pressure gauge 11-PG-705, a temperature gauge 11-TG-705, a flow recorder /
integrator 11-FR / FQ-702 and a low pressure alarm 11-PAL-701 are provided on the header
at the battery limit.
MP steam serves mainly following purposes:
Atmos Heater (11-F-01)

a) 10” line for superheating
1. 4” line for Soot blowing Steam
2. 6” line for Decoking Steam
3. 4” line for Atomising Steam
4. 4” line for purging steam
b) Vacuum Heater (12-F-01)

1. 4” line for Soot blowing Steam
2. 4” line for Decoking Steam
3. 3” line for Atomising Steam
4. 4” line for purging steam
5. 4 nos. 2” lines for tubulising steam
c) 6” line as motive fluid in steam ejectors (12-J-01, 02 & 03 A/B/C)
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
d) As velocity steam to each pass in 12-F-01

e) Utility Hose Stations (for use in equipment in hot services under shut down /maintenance)
f) In BBU,
2” take off to Reactor
2” take off to seal pot and quench drum
1” take off to BBU product pumps 13-PM-03A/B
2” take off to BBU product turbine 13-GT-01.
Utility Hose Stations (for use in equipment in hot services under shut down
/maintenance)
From the 12” header, a 10” tapping has been taken along to which the MP steam
produced by the HVGO CR steam generators 12-E-10/10A and Bitumen feed / product
cooler 13-E-01A/B joins and gets superheated in the 11-F-01 convection bank. The total
steam generated by the above steam generators is measured and integrated by 11-FQ-712.
A pressure gauge (11-PG-719) and a temperature gauge (11-TG-715) are provided on

the generated header. The superheated steam temperature from the Atmospheric Furnace can
be controlled by injecting BFW through 11-TCV-303, and is used to control the degree of
superheating.
The temperature can also be controlled by allowing more MP steam into the
superheating coil and the excess MP steam can be diverted to the LP header through a 4” line
by manually operating a globe valve. At the time of refractory drying, superheated steam can
be vented to the Atmosphere through a silencer. Safety valves are also provided on this
header at 11-F-01 top.
This superheated steam is used as stripping steam for Heavy Naphtha, Kerosene and
Diesel Strippers and also for the Atmospheric Column Bottom.
35.1.10 HP STEAM SYSTEM

(Refer P&ID 10-1100-E-202 Rev.7):
An 8” HP steam header caters to the need of the entire unit. The header is provided
with isolation valves and spectacle blind. A pressure gauge 11-PG-708, a temperature gauge
11-TG-767, a flow recorder / integrator 11-FR/FQ-704 and a low pressure alarm 11-PAL-702
are provided on the header at the battery limit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
The following connections are provided on the header.

1. 6” line to 11-P-01B turbine
35.1.11 FUEL GAS SYSTEM

(Refer P&ID 10-1100-E-202 Rev.7):
An 8” fuel gas header caters to the need of the entire unit. It is provided with a double
block valve and a spectacle blind at the battery limit. A pressure gauge 11-PG-707, and a
flow integrator 11-FR/FQ-703 are provided on the header at the battery limit.
The following connections are provided on the header

1. 6” line to 11-F-01 (with a separate flow recorder and integrator)
2. 3” line to 12-F-01 (with a separate flow recorder and integrator)
3. 3” line to the Atmospheric overhead reflux drum (11-V-01)
4. 3” line u/s of 1st stage vacuum ejectors
Fuel gas being produced in various units is routed to the Sulphur Recovery Units for
removal of H2S. The sweet fuel gas is then routed to the FG distribution network in FCCU-I
(R), and FCCU-II. The FG produced within the CDU/VDU-II unit is routed to FCCU-II in a
FG supply header of 4” size at the battery limit and is provided with double block valve and
spectacle blind.
35.1.12 FUEL OIL SYSTEM

(Refer P&ID 10-1100-E-202 Rev.7):
A 3” fuel oil supply and return header caters to the entire need of the unit. It is
provided with isolation valves and spectacle blinds at the battery limit. Pressure gauges 11-
PG-706/703 and temperature gauges 11-TG-706/703 are provided on the supply and return
headers respectively at the battery limit.
The following connections are provided on the header

3” supply to 11-F-01, with flow recorder and integrator 11-FR/FQ-305
2” supply to 12-F-01, with flow recorder and integrator 12-FR/FQ-105
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
The return headers have a globe valve, an SDV and a flow recorder and integrator 11-
FR/FQ-306 and 12-FR/FQ-106.Within the CDU/VDU unit, FO is supplied to the
Atmospheric and vacuum Furnaces through 3" & 2" headers respectively with circulating
lines back to the return headers. Constant circulation is necessary in the FO lines to prevent
congealing in the headers which may occur during idle conditions.
35.1.13 FLUSHING OIL SYSTEM (FLO)

(Refer P&ID 10-1100-E-204 Rev.7 & 10-1100-E-205 Rev.7):
Flushing oil (FLO) is normally with boiling range and properties comparing well with
gas oil. It is used as a flushing medium for displacing heavy congealing and viscous material
from equipment & piping during unit shut-down or other maintenance jobs requiring cleaning
of equipment from such hydrocarbons. It is also used as a shaft lubricant in 13/3-GT-01.
35.1.14 TEMPERED WATER SYSTEM

(Refer P&ID 10-1200-E-104 Rev.5):
The tempered water system serves the SR coolers (12-E-09A/B and 12-E-09C/D) and
the bitumen product coolers (13-E-02A/B and 13-E-02C). The purpose is to make sure that
SR and bitumen product rundowns are maintained above their pour points, else there are
chances of plugging and congealing of the lines. A 1” take off from the discharge of
tempered water pump (12-PM-07A/B) serves the SR pumps (12-PM-01A/B) for cooling the
pump bearings. The tempered water system is a closed loop, wherein, the spent tempered
water from the coolers exchanges the excess heat with the sea water in tempered water
coolers (12-E-08A/B), and then it is pumped back into 12-V-02. In order to account for
evaporation losses in the drum, a 1” DM water make up line has been provided from DM
water tank (11-V-04).
35.1.15 FLARE SYSTEM:

(Refer P&ID 10-1100-E-202 Rev.7):
In the event of abnormal operating conditions or emergencies, the hydrocarbon

operating system may get pressurised. In order to prevent this from shooting up and crossing
design limit of respective system / equipment and causing accident and / or equipment
damage, it may become necessary to relieve same amount of non condensable hydrocarbon
vapours to a system that renders them harmless. For this header is provided for collection of
relieved vapours in the unit to which all relevant equipment are connected. PSV’s of the
vessels of hydrocarbon service are all connected to 24” flare header. Flare lines are designed
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 35
PLANT NAME: CDU II
Chapter Rev No: 0
UTILITY SYSTEMS
for a pressure of 3.5 kg/cm2 g. and temperature of about 200 °C. Flare lines to be tested
pneumatically because of line support considerations. Entry of steam and condensate in flare
header to be avoided as it may lead to extinguishing of main flare flame.
The following from CDU/VDU-II are routed to flare header.

1. Atmospheric overhead accumulator (11-V-01) PSV
2. Atmospheric Column top pressure controller (11-PV-409B)
3. Stabiliser column PSV
4. Stabiliser reflux drum (11-V-03) PSV
5. Stabiliser reflux / LPG product pump seal pot
6. LPG pumps and Stabiliser reflux pump casing vents
7. Overhead Naphtha accumulator pressure control vent
8. Stabiliser overhead condenser shell vents.
There is a provision to measure the mass flow rate of the flare gases, which is indicated by
FX-801 on the DCS panel. There is also a SOP provision at the dead-end of the flare header
in the unit.
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
CDU-II INSTRUMENT TAGS DESCRIPTION:
S no Tag no Description
1. LI-1101 Desalter water interface level control
2. LI-1404 HN stripper level control (11-C-02)
3. DL-0101 SRN water wash drum interface level (10-V-02)
4. LI-2202 Column bottom level control
5. LI-3102 13-E-01 BFW level control
6. LI-3108 13E-03 BFW level control
7. LI-3402 13-E-03A Steam gen.
8. DL-1406 11-V-01 Reflux drum boot interface control
9. DL-2201 Hot-well level water control
10. LI-1502 Stabilizer reflux drum level control
11. LI-2203 Slop cut level control
12. LI-2204 HVGO level control
13. LI-2205 LVGO level control
14. LI1701 CBD Level
15. L2206 Hot-well oil level control
16. LR-1902 PFD level control
17. LR-1401 11-C-01 bottom level control
18. LI-2201 12-C-01 bottom level
19. LI-1103 Desalter wash water tank level control
20. LI-1403 KERO stripper level control (11-C-03)
21. LI-1402 Diesel stripper level control (11-C-04)
22. LI-1405 11-V-01 Reflux drum level control
23. LI-1501 Stabilizer bottom level control
24. LI-2301 12-E-10 BFW level control (MP Steam gen.)
25. LI-2302 12-E-10A BFW level control
26. LI-3107 Quench drum level control
27. DL-1503 11-V-03 boot water level (LPG Drum)
28. LI-2401 Temperature water drum level
29. LI1101A Agar probe-
30. LI1101B Agar probe-
31. LI1101C Agar probe-
32. DP1301 11F01 Atomizing steam DP control
33. DP2103 12F01 Atomizing steam DP control
34. L2201 12C01 Bottom Level
35. LI1902 PFD Level
36. LR1401 Atmos Column bottom level
37. LI-3102 13-E-01 BFW level control
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
38. LI-3108 13E-03 BFW level control

39. LI-3402 13-E-03A Steam gen.
40. LI-3107 Quench drum level control
41. AI3401 Capillary DPT of Bit. Viscosity meter
Level switches
42. LL1401 Atmos Column bottom level low

43. LH1401 Atmos Column bottom level high
44. LL2201 Vac bottom low switch
45. LH2201 Vac. Column bottom high
46. LL2203 Vac. Column HVGO level low
47. LL2204 Vac. Column LVGO level low
48. LL1501 Stabilizer bottom level low
49. LH1501 Stabilizer bottom level high
50. LL1902 PFD level low
51. LH1902 PFD level high
52. LL2202 Vac. Slop cut level low
53. LL2401 Tempered water low
54. LH2401 Tempered water high
55. LL11P11A LPG pump seal level switch A
56. LL11P11B LPG pump seal level switch B
57. LSL1101 Desalter level switch
58. LL3001 Bit agitator Seal pot LS
59. LL3401 BBU reactor level high
60. LH3401 BBU reactor level low
Flow transmitters:
S no Tag no Description Location

1. On 11-C-01,O/F Loop KERO LCV
F1402R Over flash Flow Platform(P/F)
2. FI2100 RCO to 12-F-01 East of 11PM 10A
3. FR2101 RCO to Pass A South of Pass A C/v
4. FR2102 RCO to Pass B South of Pass B C/v
5. FR2103 RCO to Pass C South of Pass C C/v
6. FR2104 RCO to Pass D South of Pass D C/v
7. FR2109 Slop cut Recycle East of 12PM01A
8. FR2202 Hot HVGO CR to 12C01 12PM01B Suction to CBD,OWS Line.
9. FR2203 Cold HVGO CR to 12C01 Opposite to12PM05A
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
10. FR2301 SR to BBU feed flow East of Bitumen K.O. Pot near 13PM03B
11. South of 11PM05B near slop cut PDU
FR2304 Slop cut to SR manifold
12. F2401R SR R/D Flow South of 12PM 04 A/B
13. F2402R HVGO R/D to Tank West of 11PM 05B behind HVGO LCV
14. FR2402 HVGO Hot feed to FCCU II Opp. to LPG Reflux C/V
15. F2406R SR to HFO Near HFO/RFO 3 way C/V
16. F2408Q HVGO to LDO East of 12E11
17. FR1101 Total crude flow -Vac section Between 12-E-01A/B/C Bell Cover Side
18. FI1102 Desalter Wash Water Flow 11-E-18 West side
19. FR1103 HN to DSL R/D 11-E-26 West
20. F1104R Total Crude Flow to Unit South of 11PM01A
21. F1105R Crude split Flow to Atoms section West of 11PM 11B
22. F1106R LP Steam to 11-E-18 East of 11-E-18
23. FR1107 HN to SRN R/D East of 11-E-26
24. F1201R SRN R/D Flow East of SRN Cooler
25. FR1202 DSL R/D to Tank Between 11PM 8C/D
26. FR1203 KERO R/D to Tank 11PM 8D discharge V/V
27. FR1204 KERO R/D to DSL KERO R/D to DSL C/V
28. F1205Q KERO R/D to LDO South of KERO to LDO V/V
29. F1206Q KERO to FO South of KERO to FO Loop
30. F1207Q DSL to LDO East of 11PM 8C
31. FR1301 Crude to Pass A North of PassA C/V
32. FR1302 Crude to Pass B North of Pass B C/V
33. FR1303 Crude to Pass C North of Pass C C/V
34. FR1304 Crude to Pass D North of Pass D C/V
35. F1307R Atomizing Steam flow Atomizing steam C/V
36. FR1308 F.G. Supply to 11F01 North of FO Return SDV 5th from East
37. FR1401 11-C-01 Bottom S/Steam South of 11PM 4A
38. FR1403 Top Reflux South of 11PM 4A
39. FR1404 DSL CR to 11-C-01 South of DSL CR C/V
40. FR1405 KERO CR to 11-C-01 Desalter RV
41. FR1406 TPA to 11-C-01 South of TPA C/V
42. FR1407 DSL Stripping Steam Behind 11-C-01 RV steam T/O,V/V
43. FR1408 KERO Stripping Steam Behind Top Reflux C/V
44. FI1409 HN Stripping Steam Behind 11-C-01 RV Steam T/o, V/V
45. F1450R Atmos Water to 11V04 North of 11V04, Out of two East one
46. FR1501 Stabilizer Reflux flow West of 12PM7B
47. FR1502 LPG R/D to MEROX East of 11PM11A
48. FR1503 Stabilizer Feed flow Behind DL1406 C/V
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
49. FR1504 KERO CR to 11E25 Between 11PM8A&8B

50. F1505 Cdu-1 Naphtha to 11C05 South of 11PM8A
51. F1701Q Salter water flow to CDU Located at FCCU-2
52. F1702R MP steam to unit North of 11F01 F.O.C/v 1st from east
53. F1703R F.G. Flow to Unit Near 12F1 F.O. C/V 3rd from East
54. F1704R HP steam flow to unit Near 11F1 F.O. C/V 3rd from East
55. F1705Q Inst. Air flow 12 F 1 F.O C/V 5th from East
56. F1706Q D.M Water North of 11F1 F.O,C/V 4th from East
57. F1707R L.P steam to Unit North of 11F 1` F.O,C/V 2nd from East
58. F1708Q Plant Air to Unit South of 12F1 F.O,C/V 2nd from East
59. F1709Q Service Water to Unit South of 12F1 F.O ,C/V 4th from East
60. F1710Q B.F.W to Unit South of 12F1 F.O,C/V 2nd from East
61. F1711Q Salt water to FCCU Located at FCCU-2
62. F1712R Total MP steam generated West of 11F01 Pass' C ' C/V
63. FR1801 AGO South of 12PM02A
64. FR1805 NGL North of SR Quench C/v
65. FR1820 Air to 11F01 On APH 3rd Platform from landing
66. F1902R PFD Crude to 11-F-01 North of 11-V-01
67. FR3501 DSL to DHDS West of TPA , C/V
68. F4218Q Tank farm steam East of 11PT2B
69. 11FI9301 KERO to FO (OM&S) West of MOI
70. F2107R 12F01FG Volumetric Flow South of 12F01 F.O. Supply C/V
71. FR2107 F.G.to 12F01 South of F.O. Supply C/v
72. F2108R Atomizing steam to 12F01 Southof12F01Atomizing Steam C/V
73. FR2201 Hot LVGO CR to12C01 Below 12C01, Opp. to Hot LVGO CR C/V
74. FR2204 Quench to 12C01 West of 11PM004B behind Quench C/V
75. F2207R MP steam to 12C01 Ejector Behind ejector steam C/V East of 11PM09A
76. F2302R Steam generated from 12E10 West of blow down
77. F2302A Steam generated from 12E 10A North of 11V04 out of two East one
78. F2303R SR From 12E03 O/H of 11PM05A/B
79. F2305B BFW to 12E 10A North of 11V4 out of two West one
80. F2403R LVGO R/D North of 12PM4 A/B
81. FR2404 LVGO R/D to DSL/LDO West of 12E11
82. FR2405 SR to RFO U/L 1st stage P.F south corner
83. F2407Q SR to LDO West of U/L Slop manifold
84. FR2520 12F01Combustion air Between DOD no1&no2
85. F2650R Hot well water to 11V04 North of 11V04manifold,Out of two West one
86. FR2205 Cold LVGO CR to 12C1 North of DSL CR C/V
87. F2206 Hot well oil R/D Near slop manifold EBL
88. 12FT23 12 E 10 A BFW FT
89. FT0104
90. FR2404A Hot LVGO to FCCU-II Behind 12-PM-04A/B
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
91. FR1101 Total crude flow -Vac section Between 12-E-01A/B/C Bell Cover Side
92. FI1102 Desalter Wash Water Flow 11-E-18 West side
93. FR1103 HN to DSL R/D 11-E-26 West
94. F1104R Total Crude Flow to Unit South of 11PM01A
Pressure transmitters:
1. PI2101 F.O. Supply Pressure Control South of 12F01FOsupply C/v
2. PI1301 FO Supply to 11F01,Pr, North of 11F01 FO Supply C/V
3. P1101 11PM 01A/B discharge Pressure East of 11PM 01A
4. P1410R 11-C-01Flash Zone Pressure On 11-C-01,Desalter RV
5. Behind 11F01 Safety Shower out of two
P1801 11F01 FD Discharge Pressure south
6. Behind 11F01 Safety Shower out of two north
P1802 APH Air Outlet Pressure one
7. P1803 Flue gas APH I/L Pressure 11F01 APH 4th P/F, from landing
8. P1804 Flue gas APH O/L, Pressure West of 11F01, Opp. D0d 5,1st from North
9. P1901R PFD I/L, Pressure PFD , LCV U/s, B/V
10. P2202R 12C01, Flash zone Pressure East of Surface condensers P/F
11. P2501 12F01 FD Discharge Pressure Opposite to DOD no.1 4th from south
12. P2502 APH Air outlet Pressure Opposite to DOD No1 ,3rd from south
13. P2503 Flue gas APH I/L, Pressure On 12F01 APH 4th Platform from landing
14. P2504 Flue gas APH O/L Opposite to DOD no.1 5th from south
15. 11F01 ID Fan Suction Pressure
PH1807 Indication North of 11F01 ID Fan
16. PH1807A 11F01IDFan Suction Pressure high Adjacent toPH1807South
17. Opposite to DOD no.1, 6th and 7th from
PH2507 ID fan suction Pressure high south
18. Opposite to DOD no.1, 6th and 7th from
PH2507A ID fan suction Pressure high south
19. PI1105 Desalter Pressure Control South of 10PM 3B
20. PI1409 11C01 Top Pressure 11C01 Top
21. PI1501 Stabilizer bottom Pressure 11C5 2nd P/F from Bottom
22. 11F01FDFan discharge Pressure
PL1806 Low West of 11F01, Opp. DOD 5
23. PL2506 FD fan Discharge Pressure Low Opposite to DOD no1,1st from south
24. PR1409A Atmos O/H gas to flare 11 C 01 Top
25. PR1409B FG make up to Atmos column. 11 C 01 Top
26. PR1501A Stabilizer Pr Controller North of 11E20A to D
27. PR1501B Stabilizer Pr Controller North of 11E20A to D
28. PR1808 11F01 Pressure Control 11F01SB Air V/v P/f west
29. PR1809 11F01Pressure Control(switch) 11F01SB Air V/v P/f west
30. PR1902 PFD Pressure Controller PFD PCV
31. PR2202R 12C01 Flash zone pressure 12C01 Vac Column
32. PR2206 12C01TopPressure Control 12C01 RV P/F
33. PR2207 12C01 Ejector Pressure East of 11PM09A
34. PR2508 12F1 Pressure Control North of 12F1 soot blowing P/F
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
35. PO2509 12F1 Arch Pr trip

Temperature indications:
1. T1101 Desalter I/L, Temp Mix valve D/s near shell flange
2. T1102 Desalter O/L Temp Crude O/L D/s shell flange
3. T1103 11 E 07 Crude O/L Temp Near 11 E 23 A Bell cover
4. T1104 HN R/D Temp On O/L, of 11 E 26
5. T1201 SRN R/D Temp East of 11 E 26
6. T1202 DSL R/D Temp At the d/s of DSL r/d c/v
7. T1203 KERO R/D Temp O/H 11PM08D
8. T1205 11 E 09 KERO CR return South of 11E09,U/S of I/L Shell flange
9. Just below SB P/F, On it's O/L to Common Line 1st
T1306 PASS A Radiation O/L from east
10. T1307 Pass B Convection O/L Soot blowing P/F north side 2nd from east
11. Just below SB P/F on it's O/L to common line 2nd from
T1311 Pass B Radiation O/L east
12. T1312 Pass C convection O/L Soot blowing P/F north side 4th from east
13. Just below SB P/F, on it's O/L to common line,4th
T1316 Pass C Radiation O/L from east
14. T1317 Pass D Convection O/L Soot blowing P/F north side 3rd from east
15. Just below SB PF, on it's O/L to common line,3rd from
T1321 Pass D Radiation O/L east
16. T1322 Heater O/L, Temp On Transfer Line to 11C01 Shell flange
17. T1324 MP Super heated steam temp On Super heat steam O/L, Soot blowing P/F
18. T1332 11E16 Crude O/l, Temp 11E16 Crude O/L,V/V
19. T1334 Pass A Decoking I/L Temp Near burner platform 1st from east
20. T1335 Pass B Decoking I/L Temp Near burner platform 2nd from east
21. T1336 Pass C Decoking I/L Temp 3rd from east
22. T1337 Pass D decoking I/L Temp 4th from east
23. T1338 Pass A Decoking O/L Just near elbow swing portion before coil o/l
24. T1339 Pass B Decoking O/L Same as above 2nd from east
25. T1340 Pass C Decoking O/L Same as above 1st from west
26. T1341 Pass D Decoking O/L Same as above 2nd from west
27. T1401R 11 C 01 Flash Zone Temp On 11 C 01, Near Desalter Rv
28. T1402A RCO D/O Temp RCO D/O Shell flange D/s,
29. T1402R DSL D/O Temp Near D/O, Shell flange
30. T1403R KERO d/o Temperature U/S of KERO LCV bypass valve
31. T1404R HN d/o TEMP At the d/s o/f d/o shell flange
32. T1406 11C01 Top temperature On 11C01 Vapor line
33. T1407 DSL stripper d/o temp. O/H of 11PM10B
34. T1408 KERO stripper d/o Temp. D/O shell flange
35. T1409 HN stripper d/o Temp. D/O shell flange
36. T1410 11-V-01 drum Temp. On HC i/l to 11v01 u/s of shell flange
37. T1411 TPA d/o Temperature On TPA d/o south side at 11c01
38. T1412 DSL CR return Temp. DSL CR shell flange
39. T1413 KERO CR Return Temp KERO CR Shell flange, u/s
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
40. T1414 TPA Return Temp TPA Return. Line Shell flange, u/s west side
41. T1501 Stabilizer Feed Temp. 11C5 Feed I/L shell flange
42. T1502 11 C 05 Flash zone Temperature Above11c5 SOP Shell flange
43. T1503 Stabilizer Bottom Temp control Adjacent toT1501
44. T1505 Reboiler Naphtha O/L temp Both T/O,of11E25Join&going to11C05
45. T1506 Reboiler Naphtha I/L, Temp Before splitting to Two streams & entering to 11E25
46. T1507 11E25KeroCRO/L Temp Reboiler C/V D/S
47. T1509 Stabilizer REFLUX drum Temp On11pm11A/B Suction line, before splitting to pumps
48. T1510 Stabilizer Top temp control On11C05Vapor line
49. T1901R PFD I/L Temp. U/S of PFD LCV
50. T1902R PFD O/L Temperature 11PT2B Discharge D/s V/V
51. T1C01 11E1 Crude I/L Temp D/S of 11E01 Crude I/L V/V
52. T1H010 11E01HN I/L O/Hof11E01at the U/SV/V of HN
53. T1H100
54. T1H11 11E11KERO CR I/L At the U/S of11E11KERO I/L Shell flange
55. T1H12 11E12DSL O/L At the D/S of 11E12 DSL O/L B/V
56. T1H140 11E14A/B DSL O/L
57. T1I01 11E1 Crude O/L, Temp D/S of 11E01 Crude O/L V/V
58. T1I02 11E2 Crude O/L, Temp D/S, of O/L,V/V
59. T1I03 11E3,Crude O/L, Temp D/S, of O/L V/V
60. T1I04 11E4, Crude O/L, Temp U/S, of I/L to 11E5
61. T1I05 11E5,Crude O/L Temp O/L, of D/S B/V
62. T1I06 11E6,Crude O/L, Temp U/S, of O/L,B/V
63. T1I07 11 E 07 CRUDE O/L D/S of Crude O/L B/V of 11E07 to Desalter
64. T1I08 11E08Crude O/L At the D/S of 11E08 Crude O/L V/v
65. T1I09 11E09 Crude O/L Located at 11E12 Crude I/L Shell flange U/S
66. T1I10 11E10 Crude O/L Located near11E09 Crude I/L Shell flange U/S
67. T1I11 11E11 Crude O/L Located near11E10Crude I/L Shell flange U/S
68. T1I12 11E12 Crude O/L At the U/S of11E12 Crude O/L V/v
69. Located at 11E14A/B, on 11E13 Crude O/L to
T1I13 11E13 Crude O/L 11E14A/B Crude I/L valve U/S
70. Located at 11E15A/B, on 11E14Crude O/L to
T1I14 11E14A/B Crude O/L 11E15A/B Crude I/L valve U/S
71. T1I15 11E15A/B Crude O/L At the D/S of 11E15 A/B Crude O/L V/V
72. T1R01 11E01 HN O/L At the D/S of 11E01 HN O/L V/V
73. T1R02 11E02 KERO O/L Located near 11E24,At the U/S of KERO I/L V/V
74. T1R03 11E03 DSL O/L Located near 11E23,At the U/S of DSL I/L V/V
75. T1R05 11E05KERO O/L At the U/S of11E02 KERO I/L Shell flange
76. T1R07 11E07LVGO O/L At the D/S of 11E07LVGO O/L V/V
77. T1R08 11E08DSL O/L At the D/S of 11E08DSLO/L V/V
78. T1R10 11E10KERO O/L At the D/S of 11E10KERO O/L V/V
79. Near West of 11E12 On 11E11O/L to 11PM8C/D
T1R11B 11E11 KERO CR O/L Suction
80. T1R13 11E13 DSL O/L At the D/S of 11E13DSL O/L V/V
81. T1R14 11E14A/B DSL O/L At the D/S of 11E14DSL O/L V/V
82. T1R15 11E15A/B DSL CR O/L At the D/S of 11E15DSLCR0/LV/V
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
83. T1R16 11E16SR I/L At the U/S of 11E16 SR I/L V/V

84. T2101 RCO to 12F1 I/L Temp O/H of RCO, Manifold
85. T2102 Pass A ,convection O/L Convection O/L,P/F
86. T2106 Pass A Radiation O/L Decoking elbow P/F
87. T2107 Pass B Convection O/L At Convection O/L P/F
88. T2111 Pass B Radiation O/L Temp Decoking elbow platform
89. T2112 Pass C Convection O/L At convection O/L, platform
90. T2116 Pass C Radiation O/L Near Decoking elbow P/F
91. T2117 Pass D Convection O/L Convection O/L,P/F
92. T2121 Pass D Radiation O/L Decoking elbow P/F
93. T2122 Vac. Furnace O/L Temp. Transfer line Ext. Portion
94. T2134 Pass A Decoking I/L On Decoking elbow swing P/F,1st from west
95. T2135 Pass B Decoking I/L On Decoking elbow swing P/F, 2nd from west
96. T2136 Pass C Decoking I/L On Decoking elbow swing P/F, 3rd from west
97. T2137 Pass D, Decoking I/L On Decoking elbow swing P/F, 4th from west
98. T2138 Pass B Decoking O/L On decoking elbow swing west side 1st from bottom
99. T2139 Pass A Decoking O/L On Decoking elbow swing west side 2nd from bottom
100. T2140 Pass C Decoking O/L On Decoking elbow swing East side 2nd from bottom
101. T2141 Pass D, Decoking O/L On Decoking elbow swing Eastside 1st from bottom
102. T2202 SR Quench Temp. SR Quench to12C01Shell flange
103. T2203R 12C01, Flash zone Temp. Surface condensers P/F
104. T2204 Slop cut D/O O/H of 12PM 02A/B
105. T2205 HVGO D/o O/H of 12PM02A/B
106. T2206 Hot HVGO CR Temp. D/S of Strainer
107. T2207 LVGO D/O LVGO D/O Shell flange
108. T2208 Cold HVGO CR Temp. D/S of Strainer
109. T2209 12C01 Top Temp. On Vapor line-RV P/F
110. T2210 Cold LVGO CR Temp. D/S of LVGO CR Strainer
111. T2301 MP Steam Temp. from 12E10 O/H of 12E10
112. T2302 MP Steam from 12E10A O/h of 12E10A,D/s of Check V/v
113. T2303 SR R/d to Bitumen
114. T2305 12E06A/B, Crude O/L Temp. 12E06A/B Crude O/L V/v D/s
115. T2401 SR R/D Temp. 12E09A/B,C/D,SR O/L near HFO,RFO C/V U/S
116. T2402 12E11 LVGO O/L Temp. On 12E11O/LLVGO to R/D,O/h of Sample Point
117. T2403 HVGO O/L from 12E12 On HVGO R/d near 12E12A/B O/L
118. T2404 HVGO R/D Temp. On HVGO R/D near 12E12A/B O/L
119. T2405 Temp. Water Drum Temp 12E08A/B O/L to drum near G/G P/F
120. T2406 SR R/d to IFO Adjacent to 12PM07B on SR to IFO line
121. T2501 Comb. air APH O/L, On APH air O/L
122. T2506
123. T2C010 12E01 Crude I/L At the U/S of 12E01A/B Crude I/L V/V
124. T2H01
125. T2H040
126. T2H050
127. T2H060 11E16 SR O/L At the D/S of 11E16 SR O/L V/V
128. T2I01B 1201A/B/C Crude O/L 2,tags at 12E01A/B,C O/L
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
129. T2I02 12E02 Crude O/L At the U/S of 12E03 Crude I/L V/V
133. T2R01 12E01 SR O/L
134. T2R02 12E02 HVGO CR O/L At the D/S of 12E02 HVGO O/L V/V
135. T2R03 12E03 SR O/L At the D/S of 12E03 SR O/L V/V
136. T2R04 12E04 HVGO O/L At the D/S of 12E04 HVGO O/L V/v
137. T2R05 12E05 HVGO O/L At the d/sof12E05HvgoO/L V/v
138. T2R06 12E06A/B SR O/L At the U/S of 12E03 SR I/L V/V
139. TH1701 CBD I/L, Temp High Upstream of CBD I/L, V/V
140. TH1702 CBD Drum Temp On CBD Drum
141. TH1801 Comb air O/L, Temp high Same as above
142. Furnace ID Fan flue gas temp.
TH1802 high Near ID fan suction
143. TH1804 Flue gas APH O/L Temp Near I.D fan suction
144. TI1402 Over flash Liquid Temp On O/F Loop , S/Steam Shell V/V Platform
145. TR1301 Furnace COT controller On11F01Passes O/L Common Header
146. TR1403 11C01 Top Temp. Control On 11C01 Vapor line shell flange D/S
147. TR2133 Furnace COT controller On Transfer line Ext. Portion
148. TR2201 12C01 Bottom Temp. O/H of cold LVGO FT or 12C01 SW corner pillar
149. TR2302 12E10HvgoTemp.control 12E10 HVGO C/v
150. Below SD P/F Adjacent toT1805,Out of two north
TX1302 Flue gas convection O/L Temp. isT1805& South is TX1302
151. T1301R Below convection Temp.
152. T1325 Arch Temp Just below soot blower NO.3
153. T1326 Arch Temp West of 11F01 soot blowing P/F
154. T1327 Fire Box Temp Near Burner No4 T/o V/V
155. T1328 Fire Box Temp Between burner No 11 T/O, V/V
156. T1329 Fire Box Temp Between No.7&8 Burner
157. T1330 Fire Box Temp Near No7 Burner peep hole
158. T1331 Flue gas convention O/L South of T1325
159. T1333 Below stack damper Temp
160. Comb air O/L Temp high from
T1801 APH APH 2nd platform
161. T1804 Flue gas APH O/L Temp Flue gas APH O/L Temp
162. T1805 Flue gas APH I/L Temp Below damper P.F North one
163. T1806 Stack Temp Above damper
164. T2123 Arch Temp Below soot blower no.7
165. T2124 Arch Temp Blow Soot blower no.2
166. T2125 Fire box From south --->north second peephole
167. T2126 Fire box From south-->north 7th peephole
168. T2127 Fire box Behind no3 burner v/v
169. T2128 Fire box Behind no10 burner v/v
170. Just above SD West side, In between FG T/O to
T2129 Ex. Convection Temp. APH&FG from ID fan discharge to stack
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
171. T2132R Flue gas Convection I/L Between SBno.7&8 1st from north
172. T2501 On APH air O/L Combustion air APH O/L,
173. T2504 Flue gas APH O/L Temp
174. T2505 Flue gas APH I/L Temp
175. T2506 Stack Temp
176. TH1801 Combustion air O/L, Temp high Combustion air O/L, Temp high
TH1802 high Furnace ID Fan flue gas temp. high
178. TH2501 Flue gas APH Temp. high Combustion air O/L, Temp high
TH2502 high
TL1803 low
TL2503 low
182. Below SD P/F, Adjacent toT1805,Out of two north
TX1302 Flue gas convection O/L Temp. isT1805& South is TX1302
183. T2131R Flue gas Convection I/L Between Soot Blower no.1&2
184. T1303 Pass A Skin Temp. Below1st stage soot blowing P/F South side
185. T1304 Pass A skin Temp. N.E.corner,belowNo1SB P/F
186. T1305 Pass A skin Temp. East of Burner No 12
187. T1308 Pass B Skin Temp. East side, below No1SB P/F
188. T1309 Pass B Skin Temp. SE corner,belowNo1 SB P/F
189. T1310 Pass B Skin Temp. Between BurnerNo12& No1 T/O V/v
190. T1313 Pass C Skin Temp. SW corner below No1 SB P/F
191. T1314 Pass C Skin Temp. NW corner belowNo1SB P/F
192. T1315 Pass C Skin Temp. West of burner No1 V/v
193. T1318 Pass D skin Temp South side below 1st stage soot blowing P/F
194. T1319 Pass D skin Temp S/w corner below 1st stage soot blower
195. T1320 Pass D skin Temp Between burner no 12 &1 V/V, adjacent no1v/v
196. 12F01West,O/H of 4th peep hole (from south),out of
T2103 Pass A Skin Temp. two south one
197. 12F01West,O/Hof no4& no5 Peep holes 1st P/F from
T2104 Pass A Skin Temp. Top
198. T2105 Pass A Skin Temp. Same Location,3rd P/F from Top
199. 12F01West,O/H of 4th peep hole (from south),out of
T2108 Pass B Skin Temp. two north one
200. T2109 Pass B Skin Temp O/H of 4&5 peephole on west 2nd from Top
201. T2110 Pass B Skin Temp Same location 4th from Top
202. T2113 Pass C Skin Temp South of SB. No 5 2nd from south
203. T2114 Pass C Skin Temp O/H of no.7burner operating v/v 1st from Top
204. T2115 Pass D Skin Temp Same location 3rd from Top
205. T2118 Pass D Skin Temp South of S.B no.5 1st from south
206. T2119 Pass D Skin Temp O/H of no7 burner operating v/v 2nd from top
207. T2120 Pass D skin Temp Same location 4th from Top
208. T3108 Bitumen Compressor Discharge On Bitumen Compressor Discharge header
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
Temp.
209. T3109 Bitumen R/D temperature At the O/L of 13E02A/B to 13E02C
210. T3402 Reactor Temp. West of Reactor 2nd P/F, Out of two, Top one
211.
T3403 Reactor temperature middle. West of Reactor 2nd P/F, out of two,2nd one
212. West of Reactor 1st P/F,O/H of LP Steam to Reactor
T3404 Reactor Bitumen Temperature V/V
213. T3405 Reactor Waste gas Temp. On Reactor top, south side, near Pr. Gauge
Trip instruments:
S no Tag Description type

1. 11PH807A 11F01IDFan Suction Pressure high Transmitter
2. 11PL806 11F01FDFan discharge Pressure Low Transmitter
3. 12PL506 FD fan Discharge Pressure Low Transmitter
4. 12PO509 12F1 Arch Pr trip Transmitter
5. 11PO809 11F01Pressure Control(switch) Transmitter
6. 11-PAL-301 11F1 fuel oil pressure low Switch
7. 11-PAL-303 11F1 fuel gas pressure low Switch
8. 12-PAL-106 12F1 fuel oil pressure low Switch
9. 12-PAL-108 12F1 fuel gas pressure low Switch
10. 11FR301 Crude to Pass A Transmitter
11. 11FR302 Crude to Pass B Transmitter
12. 11FR303 Crude to Pass C Transmitter
13. 11FR304 Crude to Pass D Transmitter
14. 12FR101 RCO to Pass A Capillary
15. 12FR102 RCO to Pass B Capillary
16. 12FR103 RCO to Pass C Capillary
17. 12FR104 RCO to Pass D Capillary
18. 11PH807A 11F01IDFan Suction Pressure high Transmitter
19. 11PL806 11F01FDFan discharge Pressure Low Transmitter
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
Control valves:
S no Tag no Description
1. 10DL101 Wash water drum interface
2. 10FV104 SRN to MS
3. 11DL406 11V01 interface
4. 11DPV301 Atomizing Steam to FO DP
5. 11FV101 Vac. split control valve
6. 11FV102 Desalter water
7. 11FV103 HAN to Diesel
8. 11FV107 HAN to SRN
9. 11FV202 DSL R/D
10. 11FV203 KERO to MEROX
11. 11FV204 KERO to diesel
12. 11FV301 11F01 Pass1
13. 11FV302 11F01 Pass2
14. 11FV303 11F01 Pass3
15. 11FV304 11F01 Pass4
16. 11FV308 11F01 FG flow
17. 11FV3501 DSL to DHDS
18. 11FV401 11C1 Bottom stripping steam
19. 11FV403 Reflux
20. 11FV404 DSL C/R
21. 11FV405 KERO C/R
22. 11FV406 Top Pump Around CR
23. 11FV407 Diesel striping steam
24. 11FV408 KERO stripping
25. 11FV409 HN Striping steam
26. 11FV501 Stabilizer REFLUX
27. 11FV502 LPG to MEROX
28. 11FV503 Stabilizer feed
29. 11FV504 KERO C/R to Reboiler
30. 11FV805 Natural Gas to 11C01
31. 11LV101 Desalter interface level (located at MEROX )
32. 11LV103 11V04 level
33. 11LV402 DSL stripper level
34. 11LV403 KERO stripper level
35. 11LV404 HN stripper level
36. 11LV501 Stabilizer level
37. 11LV902 PFD level
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
38. 11PV101 PFD bypass SDV

39. 11PV103 Steam
40. 11PV105 Desalter pressure
41. 11PV301 11F01 FO Pressure
42. 11PV402 Turbine Auto cut Steam
43. 11PV408 Steam
44. 11PV409A flare control valve
45. 11PV409B Makeup control valve
46. 11PV501A Stabilizer pressure to FCCU
47. 11PV501B Stabilizer makeup.
48. 11PV902 PFD pressure
49. 11SDV301A SDV-11F1 Fuel oil supply
50. 11SDV301B SDV-11F1 Fuel oil return
51. 11SDV303 11F01 Fuel Gas
52. 11TV303 BFW to super heated MP steam coil
53. 12DL201 Hot water level
54. 12DPV103 12F01 Atm. steam & FO
55. 12FV101 12F01 Pass1
56. 12FV102 12F01 Pass2
57. 12FV103 12F01 Pass3
58. 12FV104 12F01 Pass4
59. 12FV107 12F01 FG flow
60. 12FV109 Slop cut Recycle
61. 12FV201 Hot LVGO REFLUX Flow
62. 12FV202 Hot HVGO Rx
63. 12FV203 Cold HVGO Reflux
64. 12FV204 MC1 Quench
65. 12FV205 LVGO top reflux
66. 12FV301 SR to 12E3 (CDU-I SR & BBU)
67. 12FV402 FCCU Hot feed
68. 12FV404 LVGO to DSL
69. 12FV404A Hot feed to FCC
70. 12FV405 SR+ Slop
71. 12LV202 12C01 Bot. level
72. 12LV203 Slop cut level
73. 12LV204 HVGO level
74. 12LV205 LVGO level
75. 12LV301 BFW
76. 12LV302 12E10A level
77. 12PV101 12F01 FO Pressure
OPERATING MANUAL
PLANT NO: 10, 11 & 12
Chapter No: 36
PLANT NAME: CDU II
Chapter Rev No: 0
INSTRUMENT TAGS
78. 12PV206 12C01 Top pressure

79. 12PV207 Ejector pressure
80. 12SDV102A 12F01 FO Supply
81. 12SDV102B 12F01 FO Return
82. 12SDV105 12F01 Fuel Gas
83. 12SDV900 HW Off gas to vent
84. 12SDV901 HW Off gas to 12F01
85. 12TV102 Tempered water CV
86. 12TV103 Cold SR to VBU
87. 12TV302 HVGO 12E10
88. 12TV303 HVGO, 12E10, Temperature

CDU II Operating Manual PDF

Uploaded by

Copyright:

Available Formats

CDU II Operating Manual PDF

Uploaded by

Document Information

Original Title

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

CDU II Operating Manual PDF

Uploaded by

Copyright:

Available Formats

OPERATING MANUAL

PLANT NO: 10, 11 & 12

SECTION B: TABLE OF CONTENTS

FROM REV DATE

FROM REV DATE

FROM REV DATE

33 Chemical/HC spillage Handling 478 0 31-03-2012

FROM REV DATE

Name P N VARA PRASAD

Designation DIVISION HEAD- PRODUCTION

This is to certify that this Operating Manual is current and accurate.

SECTION D: DOCUMENT CONTROL

1. The administrative sections (Chapter 1 of PSM/GL/4.1) are approved by Division

Name P N VARA PRASAD

SECTION E : REVISION OF THE OPERATING MANUAL

1. This Operating Manual is revised for the following :

2. The revision of the Operating Manual is done in two stages :

Name P N VARA PRASAD

II. SECTION F : LIST OF ABBREVIATIONS

Designation DIVISION HEAD-

SECTION G: LIST OF COPY HOLDERS

List of the Controlled Copy holders are as given below:

S.NO COPY TYPE DESIGNATION OF THE COPY HOLDER

1 Original Division Head-Production Block

2 Controlled Unit Manager, CDU II Unit DCS, Field room

Approved By Name P N VARA PRASAD

SECTION H: RECORD OF REVISIONS TO THE MANUAL

3. The Standing Instructions are issued by the Respective Division Head-Operations.

Name P N VARA PRASAD

SECTION I: PART-I: STANDING INSTRUCTIONS - IN USE

9. ADM/OPRN/PRODN/ Empty oil & chemical drums March’ Standing Instructions

PART-II: RECORD OF STANDING INSTRUCTIONS CANCELLED

Approved By Name P N VARA PRASAD

The facilities put up under VREP-I are listed below:

Crude Pre-heating in process heat exchangers and desalting of crude in Desalter.

Heating of pre-heated crude oil in Atmospheric Fired Heaters.

The products from CDU can be routed as follows:-

1) Stabilizer off Gas to FCCU-II

2) LPG to the Amine Treating Unit (ATU)

The VDU products are routed as follows:-

3.1.1 ELECTRICAL DESALTER:

Crude Basrah Bombay high

3.1.2 DISTILLATION UNIT:

Product TBP cut range °C Temperature °C Pressure,

Product TBP cut range °C Temperature °C Pressure,

3.2 Equipment Design Basis:

3.2.1 ELECTRIC DESALTER :

Design inlet chloride as NaCl 85.601 mg/l

3.2.2 ATMOSPHERIC DISTILLATION COLUMN:

3.2.2.2 Over flash and bottom stripping steam:

3.2.2.3 Heat removal:

Diesel CR 5.0 MM K.cal/hr

3.2.2.4 Top Reflux:

3.2.3 NAPHTHA STABILISER:

3.2.4 NAPHTHA CAUSTIC/ WATER WASH SYSTEM:

3.2.5 VACUUM DISTILLATION COLUMN:

3.2.5.1 Number of stages:

3.2.5.2 Flash zone temperature:

3.2.5.3 Tower pressure: