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Assignment 2

This document provides an assignment to estimate the concentration of compounds in an unknown sample (Sample X) by comparing it to chromatograms of standard mixtures of known concentrations. Students are asked to use the peak height and width data from Figure 1 and Table 1 to calculate the concentration of each compound in Sample X. The assignment is due on December 20th before noon and should follow the specified formatting guidelines. It is a group assignment with 3-4 students per group. Plagiarism will result in a zero mark.

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Solehah Omar
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0% found this document useful (0 votes)
77 views2 pages

Assignment 2

This document provides an assignment to estimate the concentration of compounds in an unknown sample (Sample X) by comparing it to chromatograms of standard mixtures of known concentrations. Students are asked to use the peak height and width data from Figure 1 and Table 1 to calculate the concentration of each compound in Sample X. The assignment is due on December 20th before noon and should follow the specified formatting guidelines. It is a group assignment with 3-4 students per group. Plagiarism will result in a zero mark.

Uploaded by

Solehah Omar
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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CEV444 (Sep 2017 – Jan 2018) 1

Assignment 2

ASSIGNMENT 2

(PO1, CO1, C6)

 Content
Figure 1 is overlaid chromatograms of GC analysis for three different standard mixtures (various
concentrations) consist of similar compounds as well as one unknown sample. Estimate the
concentration of each compound in Sample X.
(Note: Use “peak width on baseline, WB” value = 0.15 min for all peaks)

Figure 1
CEV444 (Sep 2017 – Jan 2018) 2
Assignment 2

Table: Calibration data of standard solution and sample X

A B C D
Concentration (mol %)
Standard 1 32 15 36 17
Standard 2 34 21 26 19
Standard 3 33 16 31 20
Peak height (pA)
Standard 1 650 175 750 320
Standard 2 850 585 710 360
Standard 3 725 300 730 400

Sample X 425 715 735 170

 Reminder
 This assignment is group assignment (Number of members for each group is 3 – 4).
 Marks will be deducted for late submission of report after the due date.
 0 mark will be given for any form of cheating and plagiarism of report.
 Submission Date: 20th December 2017 (Wednesday) before 12.00 pm (the assignment
need to be submitted to the respective lecturer).

 Format
X
 Font : Arial, Font size: 11 (1.5 spacing)
 Page setup : Top: 0.75”, Bottom: 0.75”, Left: 1” and Right: 0.75”
 Paper size : A4

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