AccuPyc II Series Operator Manual

ACCUPYC® II SERIES
GAS DISPLACEMENT PYCNOMETER
OPERATOR MANUAL
134-42800-01
Jan 2016
(Rev A)
Trademarks
AccuPyc is a registered trademark of Micromeritics Instrument Corporation.

Micromeritics is a registered trademark of Micromeritics Instrument Corporation.
Scientech is a registered trademark of Scientech, Inc.
Windows is a registered trademark of Microsoft Corporation.
Copyright
The software described in this manual is furnished under a license agreement and may be used or
copied only in accordance with the terms of the agreement.
Copyright © 2014 - 2016. Micromeritics Instrument Corporation. All rights reserved.

Warranty
WARRANTY
MICROMERITICS INSTRUMENT CORPORATION warrants for one year from the date of shipment each
instrument it manufactures to be free from defects in material and workmanship impairing its usefulness under normal
use and service conditions except as noted herein.
Our liability under this warranty is limited to repair, servicing and adjustment, free of charge at our plant, of any
instrument or defective parts when returned prepaid to us and which our examination discloses to have been
defective. The purchaser is responsible for all transportation charges involving the shipment of materials for warranty
repairs. Failure of any instrument or product due to operator error, improper installation, unauthorized repair or
alteration, failure of utilities, or environmental contamination will not constitute a warranty claim. The materials of
construction used in MICROMERITICS instruments and other products were chosen after extensive testing and
experience for their reliability and durability. However, these materials cannot be totally guaranteed against wear
and/or decomposition by chemical action (corrosion) as a result of normal use.
Repair parts are warranted to be free from defects in material and workmanship for 90 days from the date of shipment.
No instrument or product shall be returned to MICROMERITICS prior to notification of alleged defect and
authorization to return the instrument or product. All repairs or replacements are made subject to factory inspection of
returned parts.
MICROMERITICS shall be released from all obligations under its warranty in the event repairs or modifications are
made by persons other than its own authorized service personnel unless such work is authorized in writing by
MICROMERITICS.
The obligations of this warranty will be limited under the following conditions:
1. Certain products sold by MICROMERITICS are the products of reputable manufacturers, sold under their
respective brand names or trade names. We, therefore, make no express or implied warranty as to such
products. We shall use our best efforts to obtain from the manufacturer, in accordance with his customary prac-
tice, the repair or replacement of such of his products that may prove defective in workmanship or materials.
Service charges made by such manufacturer are the responsibility of the ultimate purchaser. This states our
entire liability in respect to such products, except as an authorized person of MICROMERITICS may oth-
erwise agree to in writing.
2. If an instrument or product is found defective during the warranty period, replacement parts may, at the dis-
cretion of MICROMERITICS, be sent to be installed by the purchaser, e.g., printed circuit boards, check
valves, seals, etc.
3. Expendable items, e.g., sample tubes, detector source lamps, indicator lamps, fuses, valve plugs (rotor) and
stems, seals and O-rings, ferrules, etc., are excluded from this warranty except for manufacturing defects.
Such items which perform satisfactorily during the first 45 days after the date of shipment are assumed to be
free of manufacturing defects.
Purchaser agrees to hold MICROMERITICS harmless from any patent infringement action brought against
MICROMERITICS if, at the request of the purchaser, MICROMERITICS modifies a standard product or
manufactures a special product to the purchaser’s specifications.
MICROMERITICS shall not be liable for consequential or other type damages resulting from the use of any of its
products other than the liability stated above. This warranty is in lieu of all other warranties, express or implied,
including but not limited to, the implied warranties of merchantability or fitness for use.
AccuPyc II Series Operator Manual

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Contact Us
CONTACT US
Micromeritics Instrument Corporation
4356 Communications Drive
Norcross, GA / USA / 30093-2901
Phone: 1-770-662-3636
Fax: 1-770-662-3696
www.Micromeritics.com
---------------
U.S. Inquiries
U.S. Sales Phone: 1-770-662-3636
[email protected]
---------------
Quotes, Orders, and Customer Satisfaction

Customer Service Phone: 1-770-662-3636
[email protected]
---------------
U.S. Instrument Service Department

U.S. Service Department Phone: 1-770-662-3666
[email protected]

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134-42800-01 (Rev A) — Jan 2016
About this Manual
ABOUT THIS MANUAL

The following icons may be found in this document:
NOTE - Notes contain important information pertinent to the subject matter.
CAUTION - Cautions contain information to help prevent actions that may damage the
analyzer or components.
WARNING - Warnings contain information to help prevent actions that may cause per-
sonal injury.
KEYPAD FUNCTION- - The keypad icon indicates the section is applicable only when
using the keypad.

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Table of Contents
Warranty i
Contact Us ii
About this Manual iii
1 About the AccuPyc II 1 -1

About the TEC Module 1-2
Asphalt Density Application 1-3
About the FoamPyc Module 1-3
Instrument Components 1 -5
Equipment Options 1 -7
Configuration Options 1 -8
Power Analyzer On and Off 1 -9
Specifications for AccuPyc II 1 - 11
2 Data Entry with Keypad 2-1

About the Display 2-1
About the Keypad 2-2
Cancel an Analysis 2-5
Manual Mode 2 -6
Transmit 2 -7
Analysis Parameters 2 -7
Review Data 2 - 11
View Data Results 2 - 13
Print a File 2 - 13
3 About the Software 3 -1

Menu Structure 3 -1
Common Fields and Buttons 3 -2
Option Presentation 3 -5
File Status, Description, Extension, and Location 3 -7

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Keyboard Shortcuts 3-8
Sample Default File 3-9
Analyzer Status 3-9
Show Instrument Log 3-9
Show Instrument Schematic 3 - 10
Show Status 3 - 11
Print, List, or Export Files 3 - 12
Open a File 3 - 14
Uninstall the Software 3 - 15
4 About Sample Files 4 -1

Create Sample Files 4 -1
Sample Cup 4 -4
Material Parameters 4 -5
5 About Parameter Files 5 -1

Parameter Files Directory 5 -1
Analysis Conditions 5 -2
FoamPyc Application 5 -4
Report Options 5 -5
Collected Data 5 -7
6 Perform an Analysis 6 -1
Prepare and Load a Sample 6 -1
Perform an Analysis 6 -3
QuickStart Analysis 6 -7
Sequence Analysis 6 -8
Review Analysis 6 -9
7 About Reports 7 -1
Open and Close Reports 7 -1
Start Reports 7 -1
SPC Report 7 -2

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Regression Report 7-3
Control Chart Report 7-6
Report Features and Shortcuts 7-9
Graph Features and Shortcuts 7 - 13
Graph and Sample Overlays 7 - 18
Generate Multiple Graph Overlays 7 - 18
Generate Multiple Sample Overlays 7 - 19
Report Examples 7 - 21
Combined Report 7 - 21
Summary Report 7 - 22
Tabular Report 7 - 23
Graph Report 7 - 24
Overlay Report 7 - 25
Equilibration Report 7 - 26
Sample Log Report 7 - 27
8 Selected Reports 8 -1
Combined Report 8 -1
Density and Volume Table 8 -1
Density vs Cycle Number Trend Plot 8 -2
Density vs Time Trend Plot 8 -3
Equilibration Report 8 -4
Options Report 8 -5
Pressure and Volume Table 8 -5
Sample Log Report 8 -6
Summary Report 8 -6
Tabular Report 8 -7
Total Pore Volume vs Temperature 8 -8
Volume vs Cycle Number Trend Plot 8 -8
9 Diagnostics using the Software 9 -1
10 About Calibration 10 - 1

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Calibrate using the Software 10 - 1
Calibration Report 10 - 1
Calibrate Temperature Offset 10 - 2
Calibrate Zero Cell Volume 10 - 3
Calibrate Zero Pressure 10 - 4
Reset Pressure Calibration 10 - 5
Calibrate Volume Scale 10 - 6
Verify Operation 10 - 10
Load Calibration from File 10 - 11
Save Calibration to File 10 - 11
Calibrate using the Keypad 10 - 12
Calibrate Function 10 - 12
Calibration Data 10 - 12
Calibrate Volume 10 - 13
Reset Pressure Calibration 10 - 14
Review Calibration 10 - 15
Temperature 10 - 17
Zero the Pressure Transducer & Chamber Volume 10 - 17
Load Calibration Data from a USB Stick 10 - 18
Copy Calibration Data to a USB Stick 10 - 18
11 Hardware 11 - 1
Add Analysis Module to Control Module 11 - 1
Analytical Balance 11 - 3
Printer Setup 11 - 3
12 Maintenance and Troubleshooting 12 - 1

Chamber Cap O-Ring 12 - 3
Check the Cell and Expansion Chambers for Leaks 12 - 5
Clean the Dust Filter 12 - 7
Clean the Pycnometer 12 - 8
Guidelines for Connecting Gases 12 - 9
Replace a Gas Cylinder 12 - 10

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Regulator Pressure 12 - 13
Recover From a Power Failure 12 - 14
Reset the Pycnometer 12 - 15
13 Parts and Accessories 13 - 1
A Calculations A-1
Analysis A -1
Asphalt Density A -3
Calibration A -4
FoamPyc Methods A -5
Geometric Volume and Active Area A -7
Percent Porosity A -7
Resin Volume A -8
Run Precision A -8
SPC Report Variables A -9
Specific Gravity A - 10
Total Pore Volume A - 10
Total Solids Concentration A - 11
B Error Messages for the 1340 AccuPyc B-1
C Multigas Option C-1
D MultiVolume Insert Option D-1
E RS-232 Pin Assignment E-1
F Sample Volume Equation Derivation F -1
G TEC Module G -1
H Temperature Controlled AccuPyc H-1

Attach a Circulating Bath H -1

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Add Analysis Modules to a Temperature Controlled Module H -2
I Transmitted Data I -1
J Installation Instructions J-1

Handling System Components J-1
Gas Requirements J-2
Pycnometer Set up J-2
Pycnometer Configuration J-2
Set the TEC Temperature J-5
Temperature Controlled Module Hardware Setup J-5
Connect Keyboard J-5
Gas Connection J-6
Connect the Analyzer to the Computer J-8
Configure the Pycnometer using the Keypad J-9
Analytical Balance J - 17
Connect an Ethernet Switch J - 18
Brightness Control J - 18
Software Installation J - 19
Start the Application J - 22
Specify Unit Selections J - 23
Reinstall or Modify the Software J - 23
Install Analyzer Software Upgrade using a Media Device J - 24
Uninstall the Software J - 25
Index Index - 1

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1 About the AccuPyc II
1 ABOUT THE ACCUPYC II
The AccuPyc II is an easy to use, fully automatic gas displacement pycnometer. It determines
density and volume by measuring the pressure change of helium within calibrated volumes. It also
reports the chamber temperature at the end of the requested cycles. The AccuPyc II can be operated
using the analysis program installed on an attached computer, or if no computer is attached to the
pycnometer, the keypad can be used to start and run analyses. If using the keypad, the analyzer may
be operated in English, French, German, Italian, or Spanish. The application is available in English
only.
The AccuPyc II consists of a control module and an analysis module. When ordering a single unit,
the control module is built into the same unit as the analysis module for convenience. The analysis
modules are also available in a standalone configuration, allowing multiple analysis modules to be
attached to a single controlling unit. A maximum of five analysis modules can be installed to one
controller (six total). Each module has its own gas connection. The pycnometer can be controlled by
either:
l a 32-bit Windows interface. The operational status of the pycnometer can be continually mon-
itored in the application. If the Windows interface is used, the keypad is disabled.
l the keypad if not running the 32-bit Windows interface. A separate keyboard and printer
can be attached to the pycnometer using USB ports.

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ABOUT THE TEC MODULE

See TEC Module on page G - 1
Density measurements at specific temperatures are required for certain applications. The AccuPyc II
Thermo Electric Cooling (TEC) Module maintains an accurate temperature control during analysis
using the principle of Peltier cooling.
TEC Modules, also known as Peltier coolers, are solid-state heat pumps that utilize the Peltier effect
to move heat. By passing a current through the TEC Module, heat is transferred from one side of the
module to the other, typically producing a heat differential of approximately 40° C.
The transferred heat is then removed from the system through the combination of a heat sink and
fan, cooling the system to maintain a set temperature for accurate analysis.
TEC systems feature:
• fast dynamic response

• long-life
• no moving parts
• no use of refrigerants or circulated liquids/antifreeze

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Asphalt Density Application
ASPHALT DENSITY APPLICATION

The AccuPyc II TEC Module can measure asphalt density using disposable cups to limit cross-
contamination of samples.
This solution can be closely correlated (< 0.15% difference) to results obtained with ASTM Test
Method D70-09. The AccuPyc asphalt density measurement is completed much faster than the
ASTM method while virtually eliminating operator error. The Peltier thermoelectric cooling control
(15 to 36 °C) provides stability for handling of samples.
Performing an asphalt density measurement requires the AccuPyc II Asphalt application and
disposable sample cups.
ABOUT THE FOAMPYC MODULE

A FoamPyc option for measuring open and closed cell foam materials is available for both standard
and temperature controlled pycnometers. This unit can be ordered initially with the FoamPyc
application installed, or can be upgraded from the standard AccuPyc with a software enhancement
via USB media. Configuration options are:
l 100 cm3 nominal cell volume (recommended)

l 10 cm3nominal cell volume
The FoamPyc option performs analyses on materials such as polystyrene, urethane, and rubber
foams using five different methods:
l Method A. Measures the closed cell fraction and corrects for the cells damaged while cutting the
sample to the necessary size and shape. This is accomplished by using either the average cell dia-
meter or the cell chord length (as defined in ASTM method D-3576) and the measurements of the
sample to determine the volume of the cut cells. This volume is deducted from the total volume of
the open cells measured by the pycnometer.
l Method B. Corrects for the cut cells by using two separate measurements. For the 2nd meas-
urement, the sample is recut to double the amount of cut surface. The observed difference in cut
open cell volume is applied as a correction to the initial measured volume. This method offers the
distinct advantage that no assumptions are needed about the relative amounts of open and
closed cells.
l Method C. Does not correct for cut cells. It is used for materials with predominantly open cells
where good accuracy can be achieved without correction. The accuracy level deteriorates as the
percentage of closed cells increases.
l Method D. Is a compressibility test. The fill pressure is increased incrementally over the sample
with each repeat of the P1,P21 ) cycle. The apparent variation of the measured sample volume
1 ) Where P1 is the initial pressure to which the sample is charged, and P2 the final pressure after
expansion.

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with the average pressure is determined. This test is an approximate indication. It is not intended
to be an exact measure of the volume compressibility.
l Method E. Is a cell fracture test; a perfectly rigid foam is assumed. First, a P1,P2 cycle is per-
formed at the lower of two specified P1 pressures, and the results stored. A second cycle is per-
formed at a higher specified value of P1, then a third cycle identical to the first cycle is performed.
The difference between the volume of the sample on the first measurement and on the third meas-
urement is reported as the volume of fractured cells. It is assumed that cells fracture by exposure
to the highest pressure (2nd cycle) so that when the third measurement is made, the measured
sample volume has decreased from the first cycle by the amount of the closed cell volume which
was fractured.
The 100 cm3 AccuPyc II has been designed and tested to follow the procedure in ASTM Method D
6226 for FoamPyc analyses. The 10 cm3 and 350 cm3 units can be used for some types of foam
materials; however, analyses on these AccuPycs will not conform to the ASTM method. The 1 cm3
AccuPyc II cannot be used to perform FoamPyc analyses.
The FoamPyc software also provides the capability to perform analyses in the Standard mode of
operation. This is especially convenient for users who have upgraded to the FoamPyc method from
the standard method. For example, a 100 cm3 AccuPyc on which FoamPyc analyses are performed
and a 1 cm3 analysis module attached on which standard analyses are performed.

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Instrument Components
INSTRUMENT COMPONENTS
FRONT
The sample chamber, located on the top panel, is where the sample container is placed for analysis,
or the standard for calibration.
The sample chamber should remain capped except when inserting or removing a sample. When left
uncapped, water vapor adsorbs on the inner surface of the chamber or the chamber temperature
becomes unstable; either condition can affect analysis results. If water vapor accumulates in the
chamber, the pycnometer must be purged.
The standalone control module, often used for the Glove Box pycnometer, does not contain a
sample chamber.
Component Description
Active indicator A blue LED which illuminates when an operation is in progress. It is included
on all analysis modules. It is not included on standalone control modules.
Display window Displays Remote Operation when the Windows application is being used.
The AccuPyc can be operated in the keypad mode when the Windows applic-
ation is closed.
Keypad Not used with AccuPyc software application.
Power indicator A green LED which illuminates when the analyzer is powered on.

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REAR
Analysis module Used to connect up to five analysis modules to the initial control / analysis mod-
connector ule. Each module contains analysis module input and output connectors.
Brightness con- Used to adjust the brightness of the display. See Brightness Control on
trol page J - 18.
Dust filter (not (For 2000 cm3 units and high pressure units only.) Traps sample dust to pro-
shown) tect internal valves.
Ethernet port Provides for setting up for e-mailing reports, sending data to a web browser,
or interfacing with the AccuPyc Windows application.
Gas inlet port Use to connect the analysis gas; helium is recommended. If multiple analysis
modules are attached, each module contains a gas inlet port. Multiple gases
can be attached using the Multigas option. See Multigas Option on page C
- 1.
On/Off switch For powering the analyzer on and off.
Power connector For connecting the power source to the instrument.
RS-232 port Used to transmit data only when using the keypad function. Also used to con-
nect to the analytical balance.
USB connectors Use for connecting a keyboard, printer, or balance to the instrument.

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Equipment Options
EQUIPMENT OPTIONS
HIGH PRESSURE CORE PYCNOMETER

Gas pycnometry is recognized as one of the most reliable techniques for obtaining skeletal volume
and density. The fully automatic AccuPyc High Pressure pycnometer provides high speed, high
precision volume measurements and density determinations on intact or crushed shale core
samples.
The high pressure pycnometer:
l Operates at a pressure of up to 500 psi to provide a better diffusion of the gas into the rock.
l Has a stainless steel sample chamber with a volume of 3100 cm .
l Has a sample chamber that can accommodate a 48 mm (1.85 in.) diameter core of up to 60 mm
(2.40 in.) in length.
LARGE VOLUME CORE PYCNOMETER

The AccuPyc Large Volume pycnometer sample chamber addresses the specific needs of
operations that require pore volume knowledge of intact drilling cores. This instrument eliminates the
need to break core samples into smaller pieces prior to analysis.
The large volume pycnometer:
l Has a large sample chamber with a volume of approximately 2000 3 cm .

l Has a sample chamber that can accommodate a 95 mm (3.74 in.) diameter core of up to 278 mm
(10.9 in.) in length.
MULTIVOLUME INSERTS
The MultiVolume option is used to analyze smaller sized samples. Options are:
l 1 cm3 nominal cell volume; contains a 0.1 cm3 cup

3 3 3
l 10 cm nominal cell volume; contains 1 cm and a 3.5 cm cups
3 3 3
l 100 cm nominal cell volume; contains 10 cm and 35 cm cups
3 3 3
l 2000 cm nominal cell volume, contains 650 cm and 1300 cm cups
Each kit includes inserts, reference standards, and sample cups.

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MULTIGAS OPTION.
The Multigas Option allows connection of up to four gases to one analyzer. See Multigas Option
on page C - 1.
CONFIGURATION OPTIONS
For best fit with a sample, the AccuPyc II is available in multiple configurations.
All sample chamber volumes are nominal unless otherwise specified.
l 1 cm3sample chamber
3
l 10 cm sample chamber
3
3
3
3
l 100 cm High Pressure sample chamber
Best fit means the sample nearly fills the sample chamber and, therefore, optimizes the precision of
the results.
GLOVE BOX
Provides for analysis of samples in which a controlled environment is required.
Options Description
Configuration l 1 cm3 sample chamber
3
3
3
l 2000 cm
3 sample chamber
l 100 cm
3 High Pressure sample chamber
This unit consists of two separate modules. The controller is placed outside the glove box, while the
analysis module is placed inside the glove box. Up to six analysis modules may be placed in the glove
box, all controlled by one external control module.

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Power Analyzer On and Off
TEMPERATURE CONTROLLED MODULE

Provides for the attachment of an external circulating bath.
Options Description
Configuration l 10 cm3 sample chamber
l 100 cm3 sample chamber
The temperature controlled unit is specifically designed for temperature sensitive materials. This unit
is ideally suited for laboratories in which ambient temperature varies during normal work hours, or in
which subambient cooling is required.
POWER ANALYZER ON AND OFF
It is important that a constant temperature be maintained inside the unit because a

change in temperature could alter analysis results. We recommend that the pycnometer
remain powered on at all times to maintain thermal stability.
Do not power off the analyzer while initialization is in progress. Doing so may damage
the instrument.
When the analyzer is powered on, after a few seconds, the system vents automatically and the
green indicator light on the front panel illuminates. Allow approximately 30 minutes for the analyzer
to warm before performing analyses. For analyses that require very precise results, allow the
analyzer to warm a minimum of two hours. If running the analyzer with a computer:
Power ON the equipment in the following order:
If running the analyzer with a computer:
1. Computer
2. Monitor
3. Printer
4. Analyzer
If running the analyzer without a computer:
1. Analyzer

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Power OFF the equipment in the following order:
If running the analyzer with a computer:
1. Analyzer. Allow any analyses in progress to complete prior to powering off.

2. Exit the analysis program. Failure to do so could result in loss of data.
3. Computer
4. Monitor
5. Printer
If running the analyzer without a computer:
1. Allow any analyses in progress to complete prior to powering off the analyzer.
2. Printer
3. Analyzer

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Specifications for AccuPyc II
SPECIFICATIONS FOR ACCUPYC II

Characteristic Specification
Analysis
Precision Reproducibility typically to within 0.01% of the nominal full scale cell
chamber volume. Reproducibility guaranteed to within ±0.02% of the
nominal full scale volume on clean, dry, thermally equilibrated samples
using helium in the 15° to 35 ºC range (15° to 50 ºC for temperature
controlled models).
Accuracy Accurate to within 0.03% of reading, plus 0.03% of sample capacity
Electrical
Voltage 90 to 264 VAC
Power 30 VA
Frequency 50 to 60 Hz
Environment
Temperature Stable between 15° and 35 ºC (59° to 96 ºF)
Temperature controlled AccuPyc - temperature stability is dependent
upon specifications of the installed circulator. Recommended range:
15° to 50 ºC (59° to 122 ºF)
Humidity 20 to 80% relative, non-condensing
Gases
Research grade helium or nitrogen is recommended. If unavailable, use helium with a dew point of
-67 ºC (-88 ºF) or lower. Carbon dioxide, dry air, or argon can also be used for different applic-
ations. A multigas option is available for connection of multiple gases.
Physical
Analysis Module Height. 17.9 cm (7.0 in.)
(1, 10, 100 cm3) Width. 22.2 cm (8.7 in.)
Depth. 36.2 cm (14.3 in.)
Weight. 7.9 kg (17.4 lbs)
Weight - High Pressure Unit. 8.2 kg (18.1 lbs)
Analysis Module Height. 25.9 cm (10.2 in.)
(350 cm3) Width. 22.2 cm (8.7 in.)
Depth. 36.2 cm (14.3 in.)

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Analysis Module Height. 43 cm (17 in.)
(2000 cm3) Width. 27 cm (10.6 in.)
Depth. 36.2 cm (14.3 in.)
Weight. 26 kg (57 lbs)
Control Module Height. 17.9 cm (7.0 in.)
Width. 27.3 cm (10.7 in.)
Depth. 36.2 cm (14.3 in.)
Control Analysis Mod- Height. 17.9 cm (7.0 in.)
ule Width. 27.3 cm (10.7 in.)
Depth. 36.2 cm (14.3 in.)
TEC Module Height. 27.3 cm (10.7 in.)
Width. 28.7 cm (11.3 in.)
Depth. 36.1 cm (14.2 in.)
Weight. 13.8 kg (30.5 lbs.)
Printers
Requirements l must be USB 2.00 (or newer)
lmust have a printer language supported by one of the printer drivers
l cannot be host based
Supported printers Canon Bubble Jet Epson ESCP HP PCL 3

Postscript Epson ESCP Raster HP PL 6XL
Epson ESCP2
Sample Chamber
1 cm3 chamber ID: 1.15 cm (0.45 in.)
Depth: 1.1 cm (0.44 in)
Depth: 3.93 cm (1.55 in)
Depth: 6.17 cm (2.43 in)
Depth: 13.94 cm (5.49 in)
Depth: 26 cm (10.2 in)

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Specifications for AccuPyc II
Computer Requirements
l Operating System. Windows 7 Professional or higher operating system is recommended for

the best user experience.
l Desktop Installation Required. The application should not be installed on a network drive
with shared access. Multiple users cannot operate the application at the same time.
l 10 Base T Ethernet Port. If the computer is to be connected to a network, two Ethernet ports
are required. If more than one Ethernet based unit is connected to the same computer, an eth-
ernet switch will also be required.
l Read/Write Permissions. All users of the application will need Read / Write permission to all
directories and subdirectories where the application is installed.

l Drives. CD-ROM drive and thumb drive.
In keeping with a policy of ongoing product improvement, specifications are subject to change
without notice.

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2 Data Entry with Keypad
2 DATA ENTRY WITH KEYPAD

Data can be entered into the system using either a:
l Keypad (or a keyboard). Used if a computer with the analyzer software installed is not con-
nected to the analyzer. In this case, any section of this manual referring to software can be omit-
ted. All instructions specific to the keypad are designated with the icon specified in the section
About this Manual on page iii. Also see Configure the Pycnometer using the Keypad on
page J - 9.
l Computer. Used if the computer with analysis software is installed and connected to the analysis
module. In this case, this section of this manual can be skipped.
ABOUT THE DISPLAY

The display provides information about the analyzer and the current operation. During operations,
different types of information are shown in lines two, three, and four. Line one always displays the
unit and serial number. If the Alt key is pressed, the 3 in 10 cm3 will change to a + (plus sign). This is
an example of the display when the analyzer is in an idle state, or the Reload prompt.
Line Description
First Displays the unit number, serial number, and nominal cell volume of
the selected unit. Up to five analysis modules may be attached; though
the initial module, containing the keypad and display, will control all
units.
Second At the Reload prompt, manual control, or an automatic operation, this
line contains three characters, separated with dashes. The first
character represents the Fill valve, the second represents the Expand
valve, and the third represents the Vent valve.
Valve states: X = Closed, O = Open
During user interface, this line shows the command currently in use.
Third Displays status of the current operation, or Reload when in an idle
state. When the Reload prompt is displayed, this line may also contain
an asterisk (*), indicating there is a message in the queue. During cer-
tain functions (such as Setup), this line contains a prompt for additional
information.

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Line Description
Fourth At the Reload prompt, shows the current pressure and temperature
alternately, where:
l P = Pressure
l T = Temperature
This line is also used to choose options, enter information, or provide
information about the current operation.
ABOUT THE KEYPAD
A keyboard can be connected to the USB port on the rear panel of the AccuPyc II. Com-
mands can be entered from either the keypad or the keyboard.
Most keys on the keypad perform one primary and one alternate function. The primary function of
any key is indicated by the number or command on the face of the key. The alternate function is
indicated by the command above the key. The top right corner of the display screen will show a +
(plus sign) when the Alt key is pressed and the alternate function mode is entered. See About the
Display on the previous page.
To select the:
lPrimary function. Press only the key. Primary functions are labeled on the key face. For
example; press 4 to enter the number 4.
l Alternate function. Press Alt, then press the key. Alternate functions have blue labels above
the key. For example; press Alt + 4 to start an analysis. If the Alt key is pressed accidentally,
pressing it a second time will cancel its function.
The alternate functions for keys 7 (FILL), 8 (EXPAND), and 9 (VENT) are executed differently.
Press Alt + 1 first to enter Manual mode then press the alternate key. For example: press Alt + 1 +
7 to manually control the Fill valve. Press Alt + CLEAR to exit Manual mode.
Functions can be entered from the keyboard.

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About the Keypad
Keypad and Keyboard Functions

Keypad Key Sequences Description
Function Keypad Keyboard
Decimal (.) . . Enter a decimal point, a dash for sample or
instrument ID, a slash for date, or a colon for
time
Number keys ( 0 0-9 0-9 Enters the numbers 0 through 9
through 9 )
Calibrate Alt + . Ctrl + O Calibrates the pycnometer.
(decimal)
Zero Alt + 0 Ctrl + Z Zeroes the pressure transducer.
Manual Alt + 1 Ctrl + Y Provides manual control to open and close
valves.
l Fill (Key 7)
l Expand (Key 8)
l Vent (Key 9)
The state of the valve is shown on the second

line of the display, where X=Closed and
O=Open.
Alt + CLEAR exits manual mode.

Set Up Alt + 2 Ctrl + U Display or edit:
l Analysis parameters
l Report options
l Calibration data
l Data transmission parameters
l Unit types
l Operating language
l Date and time

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Keypad and Keyboard Functions (continued)

Keypad Key Sequences Description
Function Keypad Keyboard
Transmit Alt + 3 Ctrl + T Transmits analysis or calibration data. Trans-
mits a partial report if an automatic operation is
in progress.
Analyze Alt + 4 Ctrl + A Performs an analysis.
Review Alt + 5 Ctrl + R Review completed analysis or calibration data.
Print Alt + 6 Ctrl + P Prints an analysis or calibration report. If an
automatic operation is in progress, prints a par-
tial report.
Unit Alt + N/A Selects unit (when multiple analysis modules
CHOICE + are attached).
(unit num-
ber)
Escape Alt + CLEAR Esc Discards all data entered in the current mode
and returns to display mode. Cancels an auto-
matic operation in progress. Exits manual
mode.
CHOICE CHOICE Ctrl + N Display the next message when in display
mode.
Display the next multiple choice item when in
command mode.
CLEAR CLEAR Ctrl + X Clear a message when in display mode.
Clear an entry when in command mode.
ENTER ENTER Enter or Ctrl + Complete an entry or begin an action.
M
SAVE SAVE Ctrl + W Save the information and return to display
mode.

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Cancel an Analysis
CANCEL AN ANALYSIS
To cancel an analysis, press Alt + CLEAR.
Press ENTER within five seconds to cancel the operation. A notification that the automatic operation
has been canceled will be displayed.
When canceling an operation, messages are displayed indicating that termination is in progress. The
termination process, which vents the system, takes about 30 seconds and returns to the Reload
prompt.
To view the data that have been collected, press CHOICE.
The following prompt is displayed if no cycles have been completed.

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MANUAL MODE
Press Alt + 1 to enter manual mode, allowing manual control of the Bypass, Fill, Expansion, and
Vent valves.
The Bypass valve is only available on the 2000 cm3 units and the High Pressure Core
Pycnometer units.
Display Text Description

Manual When Manual is shown, manually open and close the Fill, Expansion,
and Vent valves by pressing:
l 5 - Opens and closes the Bypass valve

l 7 - Opens and closes the Fill valve
l 8 - Opens and closes the Expansion valve
l 9 - Opens and closes the Vent valve
The three characters in the second line of the display show the state of
the valves (Fill, Expansion, Vent). X = Closed. O = Open.
Press SAVE to exit Manual mode and return to display mode.
Prolonged opening of all three valves at one time may cause excessive loss of helium.

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Transmit
TRANSMIT
The AccuPyc RS-232 interface transmits report data to a computer using the standard ASCII file
format. Reports may be transmitted in a single column format or a spreadsheet format. See
Transmitted Data on page I - 1.
Press Alt + 3 to transmit report data.
Press Alt + CLEAR to cancel report data transmission.
ANALYSIS PARAMETERS
This option enables specific analysis and calibration parameters. Although the Setup Type is shown
as Analysis Parameters, these same prompts are used to specify calibration parameters. The
pycnometer is shipped with default values; however, these settings may be modified to meet
laboratory requirements.
After each selection, press Enter to display the next prompt. If data results are to be e-mailed
automatically after analysis, specify e-mail parameters in Setup Reports on page J - 14.
Enter appropriate analysis and report parameters for the current analysis. The chosen or specified
parameters in Set Up determine what prompts and information are displayed for the analysis.

Setup Type? Press ENTER to accept Analysis Parameters.
Analysis Parameters
Number of Purges: Key in the number of purges to be performed. Purging cleans the
sample cell and expansion chambers before an analysis begins. The
greater the number of purges, the cleaner the sample will be when
analyzed.
The range is 0 to 999. For calibration, 10 is sufficient.

Purges fill pressure Key in the fill pressure. For most applications, the default of 19.500
psig is adequate. Typically, the greater the fill pressure, the easier it is
to measure the volume precisely. However, a lower pressure may be
required for some samples.
The range in psig is 0 to 19.850.

The range in kPag is 0 to 136.86.
High Pressure sample chamber:
The range in psig is 0 to 500.

The range in kPag is 0 to 3450.

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Number of Cycles Key in the number of cycles to be performed. A cycle is a series of
functions which equal to a single volume measurement.
The range is 1 to 999. For calibration, 10 is sufficient.

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Analysis Parameters

Cycle fill pressure Key in the fill pressure. For most applications, the default of 19.500
psig is adequate.
The range in psig is 0 to 19.850.

The range in kPag is 0 to 136.86.
The range in psig is 0 to 500.

The range in kPag is 0 to 3450.
P1, P2 end by? Choose the manner in which to end the pressure measurement. Press
[selection] CHOICE to make a selection.
The available options are Equilibrate and Fixed interval.

Equilibration Rate: Select Equilibrate at the P1, P2 end by? prompt. Pressure
(Does not display for measurement will end when the entered rate is obtained. Key in the
Fixed Intervals) equilibration rate.
A high rate will produce faster results, but results may not be as
precise as desired. The lowest rates may cause errors when some
materials (such as those with appreciable vapor pressures or
organics) are analyzed.
The default setting is 0.0050 psig/min.

The range in psig/min is 0.0001 to 9.0000.
The range in kPag/min is 0.0007 to 62.0500.
The range in psig is 0.001 to 99 minimum (the default is 0.05)

Interval Time: (Does Select the Fixed interval at the P1, P2 end by? prompt. Pressure
not display for measurement ends when the specified time is reached. Key in the
Equilibrate) interval time.
The range is 10 to 99999 seconds.

Use Run Precision? Allows early termination of the analysis when certain criteria are met.
l Yes. The analysis terminates after five consecutive cycles are

within the specified tolerance. Always request a large number (50 to
99) of runs. The number of runs is determined through the Number
of Cycles option. With a small number of runs, the analysis stops
when the selected number is reached, even if the specified tol-
erance has not been met.
l No. Run Precision is not used.

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Percent Full Scale: This prompt only displays if Yes is selected for Run Precision and
more than five cycles have been requested.
Enter the run precision volume tolerance which is expressed as a

percentage of nominal cell volume (sample capacity).
The range is 0.01% to 50.00%.

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Review Data
REVIEW DATA
The Review function allows review of and editing of the results of the last operation – analysis or
calibration – along with its entered parameters. It is important to review and print the report before
starting another operation. Data are no longer available for review on the display when another
operation is started; however, data results are saved in the control module and can be reviewed
using a web browser.
Review Data with a Web Browser
Data results for the last five analyses are saved in the control module for each attached unit. These
results can be viewed by accessing a web browser. To use this feature, connect to a network.
1. Press Alt + 2 to access Setup. Then press CHOICE until Communications is displayed.
2. Press ENTER to display a prompt showing that the IP Address mode is DHCP.
The display may show Specify, depending on how the IP address was assigned.
3. Press ENTER to view the assigned address on the display. If the address was specified, the
display shows IP Address? and the entered address. This line is editable since it is specified
and not assigned automatically. An assigned address cannot be edited.
4. Make a note of the IP address.
5. Press Alt + CLEAR to return to the Reload prompt.
6. Access the web browser and type in the IP address.
7. Press Enter to display the serial number(s) of the attached unit(s).
8. Click on the serial number of the unit containing the data to review. A window displaying the
data files for the last five analyses, and for the zero (slope) and volume offset files is displayed.

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The files are in .HTML format and are assigned the name used as the Sample ID. If sample
identifications are not used, Untitled is assigned and appended for each file.
9. Click the file to view the data results. The progress of a current operation can be monitored by
reloading the page.
10. Use the File > Print option to print a copy of the results.

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View Data Results
VIEW DATA RESULTS

Press Alt + 5 to view data results.
Reports are generated after analysis and calibration, and remain available for viewing or printing
until another automatic operation (other than zero) is performed. When an automatic operation is
performed, data from the previous operation are no longer available for viewing on the display.
A display report is always generated regardless of the specified destination and contains:
l Analysis. The average density (or volume) and the deviation from the mean.
l Calibration. Average cell (or expansion volume) and the deviation from the mean.
PRINT A FILE
Press Alt + 6 to print a report of the last operation; analysis or calibration. If Alt + 6 is pressed during
an automatic operation, a partial report is printed.
Reports are generated after analysis and calibration, and remain available for viewing or printing
until another automatic operation (other than zero pressure) is performed. Previously generated
reports are deleted whenever a new automatic operation begins.
For each attached analysis module, the data for up to five analyses are stored in the control module.
These data sets can be viewed using a web browser when connected to a network.
An asterisk next to a cycle number indicates that it has not been included in calculations.
l Analysis. Volume, density, deviation for each cycle, an average of all cycles, the date and time
the analysis was started and completed, and the temperature of the cell chamber.
l Calibration. Cell and expansion volumes and deviations for each cycle, an average of all cycles,
and the date and time the calibration started and completed.

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3 About the Software
3 ABOUT THE SOFTWARE

The AccuPyc II Pycnometer’s unique run precision reports data from five consecutive runs that are
within a user-specified tolerance. This feature allows early termination of analyses, thereby
decreasing the number of runs needed for accurate results.
Analysis provides the measurement of sample volume, from which density can be derived
automatically if the sample mass is entered. The unit comes preprogrammed with default conditions
and ready to perform analyses. It can be reprogrammed to meet specific needs. Analyses can be
modified by entering the number of purges and purge fill pressure, number of cycles and cycle fill
pressure, equilibration rate, and run precision. Modifying these parameters allow control of the
primary portions of the analysis; purge and run.
When the PC software is not running, the AccuPyc II can be operated in keypad mode. For example;
if the computer is inoperative for some reason, analyses can be performed using the keypad.
If running the FoamPyc module, an option to select a Standard method is available so that analyses
on other types of sample materials can be performed.
See Installation Instructions on page J - 1 for hardware installation, software installation, and
software upgrade instructions.
MENU STRUCTURE
All program functions use standard Windows menu functionality. The title bar contains a Unit
Number. If multiple units (analyzers) are installed, ensure the appropriate unit is selected before
continuing.
Main Menu Bar Options

Option Description
File Use to manage files used by the application — such as sample files, ana-
lysis conditions files, report options files, etc.
Unit [n] Use to perform analyses, calibrations, and other analyzer operations. Unit
[n] displays on the menu bar for each analyzer attached to the computer.
Reports Use to run reports and view the results.
Options Use to edit the default method, specify system configuration, specify units,
and change presentation options.
Window Use to manage open windows and display a list of open windows. A check-
mark appears to the left of the active window.
Help Provides access to the operator manual and information about the ana-
lyzer.

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COMMON FIELDS AND BUTTONS

The fields and buttons in the following table are located in multiple windows throughout the analyzer
application and have the same description or function. Fields and button descriptions not listed in this
table are found in tables in their respective sections.
Common Fields and Buttons Table

Field or Button Description
Add Log Entry Use to enter information to appear in the sample log report that cannot
be recorded automatically through the application. Click the button
again to enter multiple log entries.
Autoscale When enabled on report parameters windows, allows the x- and y-
axes to be scaled automatically. Autoscale means that the x- and y-
ranges will be set so that all the data is shown. If Autoscale is not selec-
ted, the entered range is used.
Axis Range On report parameters windows, the From / To fields are enabled when
Autoscale options are not selected. Enter the starting and ending val-
ues for the x- and/or y-axes.
Bar Code Enter bar code reader information if a bar code reader is connected to
the computer’s USB port. If a bar code reader is not used, this alpha-
numeric field can be used to enter additional information about the
sample, such as a sample lot number, sample ID, etc.
Browse Searches for a file.
Cancel Discards any changes or cancels the current process.
Close Closes the active window.
Close All Closes all active windows. If changes were made and not yet saved, a
prompt displays for each changed file providing the option to save the
file.
Comments Enter comments about the sample or analysis. Comments display in
the report header.
Delete When working with report parameters, Delete removes the selected
report. Deleted reports will have to be regenerated if deleted in error.
Destination Select the report destination.
Preview. Previews the predefined report on the screen.
Print. Sends the report to the default printer.
Copies. Select the number of copies to print. This field is only enabled
when Print is selected.
File. Select the destination directory. Enter a new file name in the File

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Common Fields and Buttons
Common Fields and Buttons Table (continued)

name field, or accept the default. Select to save the file as a report
system (.REP), a spreadsheet (.XLS), a portable document format
(.PDF), or an ASCII text (.TXT) file format.
Edit When working with report parameters, highlight the item in the Selec-
ted Reports list box and click Edit to modify the report details.
Exit If a file is open with unsaved changes, a prompt displays providing the
option to save the changes and exit or to exit the application without
saving the changes.
Export Exports data in a sample information file as a .REP, .TXT or .XLS file.
When saved to a file, the data can be imported into other applications.
File name Select a file from either the Name column or from the library.
From / To When working with report parameters windows, enter the From and
To range for x- and/or y-axes.
List Provides the option to create a list of sample or report options file
information, for example, file name, date / time the file was created or
last edited, file identification and file status.
Name column A list of files in the selected directory or library.
Next Click to move to the next window or next step.
OK Saves and closes the active window.
Open Opens the selected file. Alternatively, double click the file name in the
Name column to open the file.
Prev Click to move to the previous window.
Preview Previews predefined reports. Click the tabs at the top of the window to
preview each selected report. When an analysis has not been run on a
sample, this button is disabled.
Print Sends the report to the selected destination (screen, printer or file).
Remove Click to remove an item from the list.
Replace Click to select another file where the values will replace the current
file’s values.
Replace All Click to select another .SMP file where the values will replace all val-
ues for the active Sample Information file. The original file will remain
unchanged.

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Common Fields and Buttons Table (continued)

Report Click to display a window to specify report output options.
Start Date. Displays a calendar to select the start date for the report.
Preview. Previews the predefined report on the screen.
Print. Sends the report to the default printer.
Copies. Select the number of copies to print. This field is only enabled
when Print is selected.
File. Select the destination directory. Enter a new file name in the File
name field, or accept the default. Select to save the file as a report
system (.REP), a spreadsheet (.XLS), a portable document format
(.PDF), or an ASCII text (.TXT) file format.
Save Saves changes to the active window.
Save As Saves a file in the active window under a different file name.
Start Starts the report, test, analysis, or operation.
Table buttons Use to modify the table contents.
Insert. Inserts one row above the selected row.
Delete. Deletes the selected row.
Clear. Clears all table entries and displays only one default value.
Append. Inserts one row at the end of the table.

View Instrument Log For use by a Service Technician. Operators should use Unit [n] >
Show Instrument Log.
View Operation. Use to display the current mode of operation.
Instrument Log. Use to display recent analyses, calibrations, errors

or messages.
Instrument Schematic. Use to display a schematic of the analyzer

system.

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Option Presentation
OPTION PRESENTATION
Options > Option Presentation
Use to change the way sample files and parameter files display: Advanced, Basic, or Restricted.
Each display option shows sample information and options differently.
Option Presentation Display Table

Presentation Display Description
Advanced Displays all parts of sample information and parameter files. Navigate
to parameter windows by selecting the tabs across the top of the win-
dow.
Basic Displays sample information in a single window. This display option is
used after the parameter files have been created. The previously
entered or default parameter files are then accessible using drop-
down lists.
Restricted Displays the sample information file in a single window similar to the
Basic display option with certain functions disabled. A password is set
when the Restricted option is selected. That same password must be
entered to change to the Basic or Advanced display option. This dis-
play type is typically used in laboratories where analysis conditions
must remain constant — such as the pharmaceutical industry. The
Advanced option is not available at the bottom of the window when
using the Restricted display option.
If the AccuPyc II TEC application is installed, additional fields for inserting values for the sample cup
can be displayed. Go to Options > Option Presentation > Show Cup Properties to enable
these fields.
Specify or change the default option presentation by selecting Options > Option
Presentation, or select Basic or Advanced from the drop-down list at the bottom of the
window.
The following examples show the same sample information file in Advanced and Basic display. Basic
and Restricted displays will look the same.

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A sample information file must be created for each analysis. The file can be created prior
to or at the time of analysis. The sample information file identifies the sample, guides the
analysis, and specifies report options.

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File Status, Description, Extension, and Location
FILE STATUS, DESCRIPTION, EXTENSION, AND LOCATION

In the File Selector window, the Mic Description column and the Mic Status column display file
description and file status. The File Selector incorporates standard Windows features for resizing
windows, reordering and repositioning columns, and right clicking an entry to display a menu of
standard Windows functions.
File Status and Description Table

File Status Description
Analyzing Sample information files that are currently being used for analysis.
Complete Sample information files used in an analysis that has been completed.
No Analysis Sample information files which have not been used to perform an ana-
lysis.
File Type, Extension, and Location Table

File Type File Name Default Location
Extension
Analysis conditions .ANC Param Directory
Report options .RPO Param Directory
Sample cup .CUP Param Directory
Sample information .SMP Param Directory
The following file types are available when printing or exporting reports:
Spreadsheet .XLS
Unicode .TXT

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KEYBOARD SHORTCUTS
Shortcut keys can be used to activate some menu commands. Shortcut keys or key combinations
(when applicable) are listed to the right of the menu item.
Certain menus or functions can also be accessed using the Alt key plus the underlined letter in the
menu command. For example, to access the File menu, press Alt + F, then press the underlined
letter on the submenu. For example, Alt + F opens the File menu, then press O to access the File
Selector for opening files.
If the underscore does not display beneath the letter on the menu or window, press the
Alt key on the keyboard.
Keyboard Shortcut Table

F1 Opens the online help operator manual.
F2 Opens the File Selector window.
F3 Opens the File Selector window listing analysis conditions files.
F5 Opens the File Selector window listing report options files.
F6 Cascades open windows.
F7 Tiles all open application windows.
F8 Start a report.
F9 Close all open reports.
Alt + F4 Exit the program.
Shift + F2 List sample information files.
Shift + F3 List analysis conditions files.
Shift + F5 List report options files.

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Sample Default File
SAMPLE DEFAULT FILE

Options > Sample Defaults
A Sample Default determines the default sample identification format and sequence number. A
Sample Default is a template of specifications that go into a newly created sample file. It allows for
the definition of complete sets of parameters for each type of sample commonly analyzed, so that
only a single selection is required for each new sample file created.
When Sample Default files are created and saved, use the Replace All button when on a sample
file to replace values in the open file with values from the Sample Default file. Sample defaults can be
created and saved for sample files (.SMP), analysis conditions files (.ANC), and report options files
(.RPO).
ANALYZER STATUS
SHOW INSTRUMENT LOG
Unit [n] > Show Instrument Log
Use to display a log of recent analyses, calibrations, errors, or messages.
Instrument Log Fields and Buttons Table

Field Description
Analysis / Select the logs to display.
Calibration /
Message [selection]
For fields and buttons not listed in this table, see Common Fields and But-
tons on page 3 - 2.

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SHOW INSTRUMENT SCHEMATIC

Unit [n] > Show Instrument Schematic
Use to display an analyzer schematic. To operate the valves and elevator from this window, manual
control must be enabled (Unit [n] > Enable Manual Control).
Analyzer Schematic Icon Table

Icon or Symbol Description
Open Valve. Green indicates an open valve.
Closed Valve. Yellow indicates a closed valve with manual control enabled.
Closed Valve. White indicates a closed valve with manual control not enabled
Sample Chamber.
Expansion Chamber.
Pressure and temperature readings. Displays for either the expansion

chamber or the sample chamber, depending on the unit configuration.
Gas flow direction.

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Show Status
Instrument Schematic Shortcut Menus
Each manually controlled schematic component has a shortcut menu displaying the operations
available for that particular component. To access the shortcut menu, hover the mouse pointer over
the component and right click.
Schematic Shortcuts Table

Schematic Shortcut Available Options:
Icon
Valve options Close. Closes the selected valve.
Open. Opens the selected valve.
SHOW STATUS
Unit [n] > Show Status
Use to show the current status for each port. If multiple units are attached to the computer, go to Unit
[n] > Show Status for the indicated unit.
Sow Status Fields and Buttons Table

Cycles The current cycle and the number of cycles requested. For example, 2
(current) of 10 (requested).
Density Last computed density and standard deviation, if applicable.
Elapsed Time The elapsed time of the current step.
Equilibration The measured equilibration rate and the limit.
Operation The operation, task, and the step in progress.
Pressure The pressure in the sample chamber.
Sample The name of the sample file being analyzed.
Temperature The temperature of the sample chamber.
tons on page 3 - 2.

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PRINT, LIST, OR EXPORT FILES

File > Print > [File Type]
File > List > [File Type]
File > Export > [File Type]
File Print, List or Export Fields and Buttons Table

Date Range Click to filter by a date range.
Directories: Displays directories where files are found.

c:\...\data
Export Type (Export fea- Cycle Data. Exports as five columns containing the elapsed time, P1
ture only) (fill pressure), P2 (expansion pressure), Volume, and Temperature.
P[n] Equil Data. Exports as one column of equilibration data.

File name Enter the name of a new sample file.
File Type (Export feature Select either .XLS or .TXT.
only)
Files Displays the files that fit the search criteria.

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Print, List, or Export Files
File Print, List or Export Fields and Buttons Table (continued)

Status To filter by file status, select a status from the drop-down list.
All. Displays all files
Analyzing. Sample information files that are currently being used for
analysis.
Complete. Sample information files used in an analysis that has been

completed.
No Analysis. Sample information files which have not been used to

perform an analysis.
tons on page 3 - 2.

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OPEN A FILE
File > Open > [File Type]
When working with an existing file, it is recommended that a copy of the file be used
rather than the original.
Fields and buttons will vary depending on the file type selected.

Date Range Click to filter by a date range.
Directories: Displays directories where files are found.

c:\...\data
File name Enter the name of a new sample file.
Files Displays the files that fit the search criteria.

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Uninstall the Software

Status To filter by file status, select a status from the drop-down list.
l All. Displays all files

l Analyzing. Sample information files that are currently being used for
analysis.
l Complete. Sample information files used in an analysis that has been
completed.
l No Analysis. Sample information files which have not been used to per-
form an analysis.
tons on page 3 - 2.
UNINSTALL THE SOFTWARE

When the software is uninstalled, only the files required to run the application are removed.
Parameter files, sample files, reports, calibration files, and data files are not removed.
1. Insert the Setup media into the media drive.

2. Select the Uninstall option.
3. Follow the prompts.

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4 About Sample Files
4 ABOUT SAMPLE FILES

Sample files include the information required by the analyzer to perform analyses and collect data. A
sample file identifies the sample, guides the analysis, and specifies report options and may be
displayed in either Advanced, Basic, or Restricted presentation display mode.
A sample information file consists of parameter sets; however, parameter sets can also stand alone.
A sample information file may be created either prior to or at the time of analysis.
Parameter files allow for repeated use of parameter sets. For example, if the same analysis
conditions exist for multiple analyses, an Analysis Conditions file containing the recurring conditions
can be created. When the sample file is created, the Analysis Conditions file can be selected for the
analysis conditions. Once it becomes part of the new sample file, the new file can be edited as
needed without affecting the original Analysis Conditions file.
The analysis software contains a default method. A method is a template for sample files that
contains the parameters to be used for an analysis. When a new sample information file is created,
all the parameters are filled with the values in the default method.
Specify or change the default option presentation by selecting Options > Option
Presentation, or select Basic or Advanced from the drop-down list at the bottom of the
window.
CREATE SAMPLE FILES

Options > Option Presentation > [Advanced / Basic / Restricted]
File > New Sample > [.SMP File]
File > Open > [.SMP File]

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Each analysis must be linked with a sample information file before the analysis can proceed. A
sample information file can consist of parameter files; however, parameter files can also stand alone.
See About Parameter Files on page 5 - 1.
The values specified in the parameter portions of the default sample file are saved as the defaults for
new sample files. To navigate from one set of parameters to another, select the parameter tab
across the top of the window.
The Basic and Restricted formats use predefined parameter files to create a sample information file.
When using the Basic option presentation, switch to Advanced to edit parameter file
values. When using the Restricted option presentation, parameter files cannot be
edited.
Sample File Fields and Buttons Table

Cup mass * [text box] Enter the cup mass.
Geometry ** [button] Enter material properties when using the FoamPyc Method.
User Computed. Select to enter the geometric volume and when

using Method A, the Active Area. Active Area is the total geometric
surface area of the sample - excluding any sides that contain a skin.
Compute. Select the shape of the sample and enter the dimensions.
Number of Pieces. The number of pieces making up the sample.

Material Properties See Material Parameters on page 4 - 5.
[button]
Operator [text box] Enter operator identification information. This field label may have
been renamed or may not display if modified in Options > Sample
Defaults.
Sample [text box] Enter a sample description.

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Create Sample Files
Sample File Fields and Buttons Table (continued)

Sample cup * Select a sample cup file from the drop down list or click Edit to create
[drop-down box] and save a new file for sample cup properties. See Sample Cup on
the next page.
Sample mass Enter the sample mass.
[text box]
Submitter [text box] Enter submitter identification information. This text box may have been
renamed or may not display if modified in Options > Sample
Defaults.
User Parameters These fields are primarily used for the SPC (Statistical Process Con-
[group box] trol) reporting to specify sample characteristics or its manufacturing
process but may be used for other data by entering specific analysis
conditions or sample criteria. The entered parameters display on the
Summary Report. This option may not display (or may have a different
field label) if modified in the through Options > Sample Defaults.
* Option displays only in the Asphalt application.
** Option displays only in the FoamPyc application.
tons on page 3 - 2.

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SAMPLE CUP
Options > Option Presentation > Show Cup Properties
File > Open > [.CUP File]
(or click the Sample Information tab when in Advanced option presentation)
Use to set the sample cup mass and density.
Sample Cup Properties Fields and Buttons Table

Density [text box] Enter the density of the sample cup.
Mass [text box] Enter the sample cup mass.
Sample Cup [text box] Enter a description of the sample cup.
tons on page 3 - 2.

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Material Parameters
MATERIAL PARAMETERS
File > Open > [.SMP File]
Material parameters are used to report porosity or total solids concentration when using the
Standard analysis method.
Material Parameters Fields and Buttons Table

Bulk Density / Envelope Dens- Calculated from a volume that includes pores.
ity [selection]
Liquid Density [text box] Density of the liquid.
Solids Density [text box] Density of the solid sample.
tons on page 3 - 2.

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5 About Parameter Files
5 ABOUT PARAMETER FILES

Parameter files allow for repeated use of parameter sets. For example, if the same analysis
conditions exist for multiple analyses, an Analysis Conditions file containing the recurring conditions
can be created. When the sample file is created, the Analysis Conditions file can be selected for the
analysis conditions. Once it becomes part of the new sample file, the new file can be edited as
needed without affecting the original Analysis Conditions file.
The following file types can exist as part of the sample information file as well as individual parameter
files:
File Type File Extension

Analysis Conditions .ANC file extension
Material Parameters .MTP file extension
Report Options .RPO file extension
Sample Cup .CUP file extension
PARAMETER FILES DIRECTORY

Options > Parameter Files Directory
Use to select the location for the predefined parameter files displayed in the drop-down lists when
using the Basic or Restricted option presentation. This configuration option is not available if using
the Restricted option presentation.
The system default directory is the recommended location for saving report options files.
The default directory is ..\param, if accessed from the top-level installation directory.

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ANALYSIS CONDITIONS
File > Open > [.ANC File]
(or click the Analysis Conditions tab when in Advanced presentation option)
Analysis conditions specify the data used to guide an analysis.
Analysis Conditions Fields and Buttons Table

Analysis Conditions Displays the description of the file. If this is a new file, the description
[text box] specified in sample defaults is displayed.
Analysis gas [text box] The gas to be used for analysis gas (helium is recommended).
Analysis method See FoamPyc Application on page 5 - 4.
[selection]
Cycle fill pressure Enter the fill pressure for the cycles. Typically, the default of 19.500
[text box] psig is appropriate for most samples.
End equilibration by: Rate. Equilibration ends when the rate of pressure change drops
[group box] below the entered amount.
Time. Equilibration ends when the specified time interval is attained.

Number of cycles The number of cycles to be performed. A cycle is a series of func-
[text box] tions which equals to a single volume measurement.
Number of purges The number of purges to be performed. A higher number of purges
[text box] will mean a cleaner sample.

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Analysis Conditions
Analysis Conditions Fields and Buttons Table (continued)

Percent full scale Enabled when Use run precision is selected. Enter the run precision
[text box] volume tolerance which is expressed as a percent of nominal cell
volume (sample capacity).
Purge fill pressure The purge fill pressure (in psig or kPa). For FoamPyc analyses, the
[text box] typical pressure is 3.5 psig. For analyses on standard samples, the
measured volume is more precise if a greater fill pressure is used.
The default of 19.500 is appropriate for most standard analyses.
Some materials, such as organic polymers, may require a lower
pressure in order to limit permeability into the sample matrix.
The default is 500 psig for the High Pressure sample chamber.
Record P1 equilibration Record first. Enter the number of cycles to be recorded at the
data [check box] beginning of the analysis.
Record P2 equilibration
data [check box] Record last. Enter the number of points to be recorded at the end
of equilibration.
Use run precision Select to use run precision. This feature provides early termination
[check box] of the analysis when certain criteria are met. The analysis ter-
minates after five consecutive cycles are within the specified tol-
erance. Typically, a large number (50 to 99) of cycles is requested. If
a small number of runs is selected, the analysis stops when the
entered number is reached even though the specified tolerance has
not been met. If fewer than five cycles are requested, this feature is
disabled.
tons on page 3 - 2.

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FOAMPYC APPLICATION
File > Open > [.ANC File]
Analysis Methods
Selection Required Action
Standard Select Record equilibration data then enter the criteria (if recording equilibration
data).
A, B, or C Enter the Resin density.
D Enter the initial and final pressure, and the pressure increment.
Enter Resin density.
E Enter the Low pressure and the Fracture pressure.
Enter Resin density.

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Report Options
REPORT OPTIONS
File > Open > [.RPO File]
(or click the Report Options tab when in Advanced presentation display)
See Selected Reports on page 8 - 1
If using the FoamPyc application, reports for all FoamPyc Methods are fixed
and cannot be created or selected from within the application.
Report options specify the types of reports to be generated from an analysis and allow for
customization of reports such as axis scale, axis range, and column headings.
Report Options files can be customized to accommodate standard analysis requirements. Reports
can be generated automatically after each analysis or at any time during or after an analysis. A report
generated during an analysis only includes data collected up to the time of the report.
Report Options files may be defined to include overlay options. This system allows the overlay of up
to 8 plots of different samples onto a plot of the same type or overlay one plot type onto a different
plot type from the same analysis.
Report Options Fields and Buttons Table

Overlays [button] Click to open the Graph Overlay Samples window. Click Browse to
select sample files to overlay into a plot.

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Report Options Fields and Buttons Table (continued)

Report Options Displays the description of the file. If this is a new file, the description
[text box] specified in sample defaults is displayed.
Selected Reports Select the report names to include in the report.
[selection]
Show graphic Use to show a graphic on the report header.
[check box] Height / Width. Enter the height and width of the selected graphic.
These values determine the graphic appearance on the generated
report.
Show report title Select and enter a report title to appear on the report header.
[check box]
tons on page 3 - 2.

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Collected Data
COLLECTED DATA
The Collected Data tab displays after an analysis has been completed.
Collected Data Fields and Buttons Table

Cell Volume [text box] Nominal cell volume for the unit or for the selected insert.
Chamber Insert Select the chamber insert size, if applicable. Options will vary depend-
[selection] ing on the type of unit being used.
Values in the Volume column are recalculated automatically if the
Chamber Insert selection is changed.
Expansion Volume Expansion volume for the current unit or for the selected insert.
[text box]
Pressure Table Displays information collected during analysis:
Columns l Elapsed Time
l P1 Pressure (fill)
l P2 Pressure (expansion)
l Volume
l Temperature

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Collected Data Fields and Buttons Table (continued)

l Exclude. Click the cell for each cycle to exclude in the average cal-
culations. An x in the cell indicates the cycle will be excluded.
Excluded parameters are marked with an asterisk (*) in the gen-
erated report.
tons on page 3 - 2.

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6 Perform an Analysis
6 PERFORM AN ANALYSIS
An analysis can be performed from either the computer application or directly from the keypad on the
analyzer.
See Handling System Components on page J - 1
PREPARE AND LOAD A SAMPLE
FOAMPYC METHODS
FoamPyc Methods are intended to conform to the procedures detailed in ASTM Test Methods D-
6226 and D-3576. Prepare samples according to the methods outlined in these procedures. Once
the sample is prepared and placed into the sample chamber, see Perform an Analysis above.
STANDARD METHOD
Samples must be properly prepared to obtain accurate results. Samples must be free of moisture in
order to obtain true sample mass and to avoid the distorting effect of water vapor on the volume
measurement. The following procedures are recommended; however, modifications may be
necessary for some materials:
lHeat-sensitive materials may have to be dried by long-time exposure to silica gel, freeze drying,
etc.
l Materials having a low melting point may be dried using the purge process. In this case, do not
weigh the sample and cup until after the purge and analysis have been completed.
Avoid exposure of the dried sample to atmospheric moisture during each step of the preparation
process. This means weighing as rapidly as possible and installing in the instrument without
unnecessary delay.
Keep the cap on the cell chamber except when actually inserting or removing a sample.
If the chamber remains uncapped, water vapor will adsorb on the inner surface of the
chamber and temperature instability will occur; either condition can affect analysis res-
ults.
1. Weigh the empty sample cup.

2. Place as large a quantity of sample as is possible in the cup (cup should be two-thirds full).
Pack powders and fluffy materials (if permissible) to obtain maximum sample weight in the
cup.
3. Place the sample cup with sample in a drying oven. The amount of time the sample must be
heated depends on the material and the temperature it will tolerate; this may have to be estab-
lished by other tests.

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4. Remove the sample cup from the oven and transfer it to a desiccator provided with active
desiccant. Allow it to cool until near room temperature. Minimize air exposure of the sample.
5. Use this equation to determine the sample mass. (If volume only is to be measured, skip this
step.)
Masssample = Masssample+cup – Masscup
6. Remove the cell chamber cap, place the sample cup (with sample) into the cell chamber, then
replace the cap.
It is best not to lay the cap down while loading the sample. Immediately replace the cap when
the sample is loaded. This will prevent particles from accumulating on the greased surface
(see Handling System Components on page J - 1 for guidelines on handling system
components).
7. If using a temperature-controlled AccuPyc, perform the following steps before proceeding,
see Perform an Analysis on the previous page.
a. Power on the bath circulator and specify the temperature for analysis. (Refer to the man-
ufacturer manual for instructions on operating the bath circulator.)
b. Allow the temperature to stabilize to the set temperature. Observe the temperature
reading on instrument schematic.
8. If using a TEC module, ensure the temperature reading has stabilized at the specified point.

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Perform an Analysis
PERFORM AN ANALYSIS
PERFORM AN ANALYSIS USING THE SOFTWARE

Unit [n] > Sample Analysis
After the sample has been properly prepared and loaded into the sample chamber, start the
analysis.
1. Select the sample file to run and click OK. To select a different sample file, click Browse and
locate the correct file. If sample file parameters exist in another file, rather than re-enter them
again, click Replace to locate and replace parameters in the current file with those of the selec-
ted file.
2. Edit or enter information for the analysis.
3. Click Report after analysis to generate reports automatically when the analysis is complete.
On the Report Settings window, select the report destination. Click OK to return to the pre-
vious window.
4. Click Export after Analysis analysis to have data exported automatically after the analysis.
Or, if exporting equilibration or cycle data, data can be exported after the analysis using the
File > Export.
5. Ensure the correct Chamber Insert is selected.
6. Click Start to start the analysis. A window displays data as they are collected. A short delay is
encountered before the port status at the bottom of the window changes from the Idle state.

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7. If running a FoamPyc analysis, a message displays indicating the sample should be cut.
a. Remove the sample chamber cap, then remove the cap before performing the next
step.
b. Cut the sample and return it to the cup.
c. Remove the cap, place the cup back into the sample chamber. Replace the cap.
d. Click OK to complete the second analysis.

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Perform an Analysis
PERFORM AN ANALYSIS USING THE KEYPAD

Prerequisites:
l specify analysis and report parameters

l prepare and load sample
The prompts that display for an analysis depend on the options selected in Setup >Analysis
Parameters and Report Options; therefore, the analysis may not display all of the prompts
referenced in this procedure.
1. Press Alt + 4 to display the Sample ID prompt. Enter an appropriate identification. Press .
(decimal) to insert a dash.
2. Press ENTER to display the Description prompt.
Most users display this prompt only when a keyboard is attached to the pycnometer.
3. Press ENTER to display the Sample Mass prompt. At the Anls Display Mode prompt in the
Setup > Report Options choose Density. Enter the sample mass.
4. If an analytical balance is connected to the module, press the appropriate button on the bal-
ance to transfer the sample mass while this prompt is displayed.
5. Press ENTER to display the Chamber Insert prompt if using an insert. Press CHOICE until
the appropriate insert is displayed, then press ENTER.
6. Press ENTER to begin the analysis. Operational status messages display during analysis.
7. When the analysis has finished, the pycnometer beeps three times and the display returns to
the Reload prompt.
Do not remove the cell chamber cap when the pycnometer is pressurized. The sample
may be discharged from the chamber.
8. Ensure the pressure reads approximately 0 (zero), then remove the cell chamber cap and
remove the sample from the chamber.
9. Replace the cell chamber cap or load another sample.
Analyze Sample ID: Enter sample identification for the current analysis. Sample ID can be
up to 20 numbers and dashes. Press . (decimal) to insert a dash.
Analyze Enter the description for the current sample. A prompt for Line 2 of the
Description Line 1: description is displayed.

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Analyze Sample Mass: Enter a value for the sample mass. Displays only when Density is
selected for Analysis display mode. It does not display if Volume is
selected.
The range is 000.0000 to 10000.0000 g.
The range for the 2000 cm3 AccuPyc is 000.0000 to 25000.0000 g.
This field will also accept input from a connected analytical balance.
While this prompt is displayed, press the appropriate button on the
analytical balance to transfer the mass (refer to the manufacturer’s
manual for the appropriate command).
Analyze Chamber Select the insert to be used.
insert?
l None, 0.1 cm3 (for 1 cm3 unit)
l None, 3.5 cm3, 1.0 cm3 (for 10 cm3 unit)
l None, 35 cm3, 10.0 cm3 (for 100 cm3 unit)
l None, 650 cm3, 1300 cm3 (for 2000 cm3 pycnometer)
Press CHOICE until the appropriate insert is displayed or None if an
insert is not being used.
Analyze Cup Mass? Enter the mass of the sample cup.
Analyze ENTER. Starts the analysis. The analysis begins and operational
[ENTER] to start status messages are continually displayed during analysis
[ESCAPE] to cancel
ESCAPE. Cancels the analysis.
For keypad and/or keyboard functions or commands not listed in this table,
see About the Keypad on page 2 - 2.

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QuickStart Analysis
QUICKSTART ANALYSIS
Unit [n] > QuickStart Analysis
Use to analyze a series of samples of the same type and same analysis conditions. Sample files will
be created using default values.
QuickStart Analysis Fields and Buttons Table

Analysis Conditions Select the Analysis Conditions file to be used for analysis. See Ana-
lysis Conditions on page 5 - 2.
Chamber Insert Select the chamber insert size to be used in this analysis.
Export after analysis Exports reports automatically to the specified destination and in the
selected format when the analysis is complete.
Material Parameters Click to verify or change the material properties to be used for analysis.
See Material Parameters on page 4 - 5.
Report after analysis Generates reports automatically to the specified destination when the
analysis is complete.
Report Options Select the Report Options file to be used for analysis. See Report
Options on page 5 - 5.
Sample Displays the sample description specified in the Sample Defaults.
Sample Cup Select the sample cup properties file to be used for analysis. See
Sample Cup on page 4 - 4.
Sample Mass Enter the sample mass.
tons on page 3 - 2.

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SEQUENCE ANALYSIS
Unit [n] > Sequence Analysis
Use to analyze the same sample using up to eight different sample files.
Sequence Analysis Fields and Buttons Table

Chamber Insert Select the chamber insert to be used for analysis.
Clear Removes all entries from the Sample Files list box.
Export After Analysis Exports reports automatically to the specified destination and in the
selected format when the analysis is complete.
Insert Click to browse and select a file to be added to the sequence analysis.
The selected file displays in the Sample Files list box.
Pause between ana- When using multiple sample files and this option is selected, the sys-
lyses tem will return to the sample selection window after each analysis.
When the previous analysis completes, click Start to run the next ana-
lysis. As each analysis is run, the sample file is removed from the
Samples Files list box.
Remove Select a file in the Samples Files list box then click Remove to delete
the file from the list.
Replace Select a file in the Samples Files list box then click Replace to sub-
stitute a sample file for the selected one.

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Review Analysis
Sequence Analysis Fields and Buttons Table (continued)

Report After Analysis Generates reports automatically to the specified destination when the
analysis is complete.
tons on page 3 - 2.
REVIEW ANALYSIS
Keypad Function
The Review function allows review of the results of the last analysis operation. Press Alt + 5 to
review or edit analysis results. The analysis information can also be edited through the prompts. The
prompts that display during the analysis review depend on the options selected in Setup > Analysis
Parameters and Report Options.
1. Press Alt + 5 to display the Sample ID prompt containing the sample identification.
2. Press ENTER to display the Description prompt containing an additional description. This
prompt typically is not used unless a keyboard is connected to the analyzer.
3. Press ENTER to display the Sample Mass prompt containing the sample’s mass.
4. Press ENTER. The Start prompt containing the start date and time of the analysis is dis-
played.
5. Press ENTER. The End prompt containing the ending date and time of the analysis is dis-
played.
6. Press ENTER. The first of the prompts containing data is displayed. The [n] displayed in the
example prompts represents the cycle number.
7. Continue pressing ENTER to view data. Press CHOICE to exclude data from report cal-
culations. An asterisk will display indicating that it will be excluded. Press CHOICE again to
remove the asterisk.
8. Press SAVE to return to the Reload prompt.
9. Press Alt + 6 to print report results.
Sample ID: Identification entered for the analysis.
(sample identification)
Sample Mass: Sample mass for the analysis (if Density was chosen as Analysis
(mass) display mode).
Temperature: Sample chamber temperature.
(sample chamber temp)

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Start: Time and date the analysis began.
(time) (date)
Time: HH:MM:SS
Date: DD/MM/YY
End: Time and date the analysis completed.
(time) (date)
Time: HH:MM:SS
Date: DD/MM/YY
Dn[n] = (density) Density or Volume (depending on the selection made for Analysis
Dv[n] = (deviation) display mode).
or [n]: cycle number.
V[n] = (volume) Press CHOICE to exclude the displayed density (or volume) from the
Dv[n] = (deviation) calculated average. An asterisk indicates that it has been excluded.
Press CHOICE again to remove the asterisk. Each time CHOICE is
pressed to exclude (or include) the value, a new deviation is calculated
and displayed.
Press SAVE to return to the Reload prompt. Press SAVE to

automatically recalculate the collected data and update data reduction
messages in the queue.
For keypad and/or keyboard functions or commands not listed in this table,
see About the Keypad on page 2 - 2.

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7 About Reports
7 ABOUT REPORTS
Review this section for information on the Reports menu options as well as customizing and running
reports.
Reports can be generated for data:
l collected on a sample that has completed analysis

l collected on a sample currently being analyzed
OPEN AND CLOSE REPORTS

Reports > Open Report. > [.REP File]
Reports > Close Reports
START REPORTS
Reports > Start Report
Starts the selected report. Select a file from the Files list. Ensure the selected file has a status of
either Complete or Analyzing.

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7 About Reports
SPC REPORT
Reports > SPC Report Options
Use to generate reports with various SPC (Statistical Process Control) options. All selected
variables must be computed for each sample file used in an SPC report; therefore, it is more efficient
to select only the necessary variables.
The selected items display as graph variable selections in Reports > Regression Report and
graph selections in Reports > Control Chart. If additional report options are required, click More.

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Regression Report
REGRESSION REPORT
Reports > Regression Report
Use to generate a Statistical Process Control (SPC) Regression report to determine the
interdependency between two variables. Up to three dependent variables (y-axis) may be plotted
against a single independent variable (x-axis). The degree of correlation between the variables is
also reported.
Regression Report Fields and Buttons Table

Autoscale [check box] When enabled, allows the x- and y-axes to be scaled automatically.
Axis Range [text box] Enter the beginning and ending values for the x- and y-axis ranges.
These fields are disabled if Autoscale is selected.
Label data [check box] Use to label the points on the plot to correspond with the values in the
sample files.

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7 About Reports
Regression Report Fields and Buttons Table (continued)

Recalculate archived Use to have archived SPC values recalculated ensuring any changes
SPC results [check box] made to the SPC Report Options are included in the new report. This
option lengthens the time required to generate the report.
If this recalculation option is enabled and sample files from

an earlier application version are selected, it is recom-
mended that copies of the archived sample files be used
rather than the original. Selecting this option will make
some archived sample files unreadable by the original
application.
When this option is selected, the following message displays:
Saving the recalculated SPC data may render some files

unreadable by the original application. Saving the SPC
data speeds up future SPC reports.
If Do not show me this message again is selected, the mes-

sage cannot be redisplayed without Micromeritics assist-
ance.
The first time this option is used, the time it takes to generate the report
is lengthened. The second time the report is generated, if using the
same sample files used in the initial calculation, it is recommended that
this option not be selected since the data was recalculated previously.
If a sample file is added or removed from the report after the initial
recalculation, this option should be selected again to ensure the data
from the newly added or removed sample file is recalculated.
Samples [button] Select additional sample files to add to the report.
Save as Default [button] Click to save selected report options as default report settings.
report.
[check box]
Tabular report Generates a tabular report of the included samples. A tabular report
[check box] contains the numeric values contributed by each sample.

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Regression Report
Regression Report Fields and Buttons Table (continued)

X- and Y-Axis Variable Use to designate the x- and y-axes variables. The variables in the
[drop-down box] drop-down lists are those selected in the Reports > SPC Report
Options window. Use these options to plot the regression of up to
three y-axis variables against the x-axis variable.
tons on page 3 - 2.

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7 About Reports
CONTROL CHART REPORT

Reports > Control Chart
Generates a Statistical Process Control (SPC) control chart report which plots the changes in a
statistic.
Control Chart Fields and Buttons Table

Graph [n] [button] Defines the y-axis of each graph.
Statistic. Displays the SPC variables selected on the Reports >

SPC Report Options window. The selected variable will be plotted
against time. This selection also becomes the y-axis label.
Autoscale. Allows the y-axis to be scaled automatically. To specify a

range, deselect this option and enter a range in the From and To fields.
Center Line. Displays placement options for the center line in the
graph. Choose Entered to specify placement of the line.
Limit Lines group box. Displays limiting lines options. Lines can be
placed at some multiple of the standard deviation or at specified
positions (Entered). When Entered is selected, enter the High limit and
Low limit fields with appropriate values.

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Control Chart Report
Control Chart Fields and Buttons Table (continued)

Recalculate archived Use to have archived SPC values recalculated ensuring any changes
SPC results [check box] made to the SPC Report Options are included in the new report. This
option lengthens the time required to generate the report.
If this recalculation option is enabled and sample files from

an earlier application version are selected, it is recom-
mended that copies of the archived sample files be used
rather than the original. Selecting this option will make
some archived sample files unreadable by the original
application.
When this option is selected, the following message displays:
Saving the recalculated SPC data may render some files

unreadable by the original application. Saving the SPC
data speeds up future SPC reports.
If Do not show me this message again is selected, the mes-

sage cannot be redisplayed without Micromeritics assist-
ance.
The first time this option is used, the time it takes to generate the report
is lengthened. The second time the report is generated, if using the
same sample files used in the initial calculation, it is recommended that
this option not be selected since the data was recalculated previously.
If a sample file is added or removed from the report after the initial
recalculation, this option should be selected again to ensure the data
from the newly added or removed sample file is recalculated.
Report [button] Generates the report.
Samples [button] Select additional sample files to add to the report.
report.
[check box]
Tabular report Generates a tabular report of the included samples. A tabular report
[check box] contains the numeric values contributed by each sample.

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7 About Reports
Control Chart Fields and Buttons Table (continued)

X Axis Order by Select the order in which x-axis statistics are placed. Sort by:
[group box]
Time. Time the files were analyzed.
File name. Alphanumeric order.
Date. Date the files were analyzed.
Minutes. Minutes elapsed from the first file placed on the list, which is
the earliest-analyzed file.
Days. Number of days elapsed from the first file placed on the list,
which is the earliest-analyzed file.
tons on page 3 - 2.

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Report Features and Shortcuts
REPORT FEATURES AND SHORTCUTS

Reports can be customized and manipulated using the toolbar, shortcut menus, the zoom feature, or
axis cross-hairs.
l After analysis, reports can be viewed, printed, and/or copied and pasted into other documents.
l The report zoom feature provides the viewing of fine graph details and the ability to shift the axes.
l All reports contain a header displaying file statistics.
If configured, the report header can also contain a graphic and/or a title.
l Tabular and graphical reports contain sample and analyzer statistics such as analysis date / time,
analysis conditions, etc.
l The headers contain notes of sample file changes occurring after analysis.
l Summary report headers contain the same information as tabular and graphical reports with the
exception of notes.

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7 About Reports
REPORT HEADER SHORTCUTS

Display header shortcuts by right clicking in the report header.
If configured, the report header can also contain a graphic and a title.
l Tabular and graphical reports contain sample and instrument statistics — such as analysis date,
analysis time, analysis conditions, etc.
l The headers contain notes of sample file changes occurring after analysis.
l Summary report headers contain the same information in tabular and graphical reports with the
exception of notes.
Report header Shortcut Field and Button Table
Copy header as text Use to copy the report header as text. Text is copied to the clipboard
and then can be pasted into other documents.
Edit Use to edit the report title and/or graphic in the report header.

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Report Features and Shortcuts
REPORT TOOLBAR
The Report window has a toolbar on the right portion of the window and selectable tabs at the top of
the report header. To view a specific report, either select the tab or the report in the Reports list box,
then click Show.
Report Toolbar Fields and Buttons Table

Default Style [button] Specify default report parameters for fonts and curve properties.
Delete [button] Deletes the selected report in the Reports list box. Deleted reports will
have to be regenerated if deleted in error.
Hide [button] Hides (or temporarily removes) the selected report from the tabbed
view. The report name remains in the Reports list box.
Print [button] Displays the Print window for report output.
Reports [group box] Contains a list of all generated reports. The same reports display as
tabs at the top of the report header unless the report has been hidden
using the Hide button.
Show [button] Displays the selected or hidden report in the Reports list box.
tons on page 3 - 2.

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7 About Reports
TABULAR REPORT FEATURES AND SHORTCUTS

Display tabular report shortcuts by right clicking in the body of the tabular report. Column shortcuts
require right clicking on the column to be modified.
Tabular Reports Shortcut Options and Descriptions Table

Align column Select to change the column alignment to either left, right, or centered.
Copy table as text Use to copy the report contents to the clipboard as tab-delimited text. It
can then be pasted into another document.
Edit title Use to edit the report title and/or title font attributes. Click Font to
modify font attributes.
Move column Right click the column to be moved. Select Move column on the short-
cut menu and select Left or Right for the move.
Rename column Right click the column to be renamed. Select Rename column on the
shortcut menu and enter the new column name.
Resize column Right click the column to be resized. Select Resize column on the short-
cut menu and enter the new column width in inches.
Show column Displays a list of all columns. Click a column to add a checkmark to
show the column or remove the checkmark to hide the column.
Table data font Right click in the report data. Select Table data font on the shortcut
menu.
Table header font Right click in the report data. Select Table header font on the shortcut
menu.
tons on page 3 - 2.

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Graph Features and Shortcuts
GRAPH FEATURES AND SHORTCUTS

Display graph report shortcuts by right clicking in the body of the graph report.
Graph Shortcuts Options and Description Table

Autoscale Returns the report to full view after using the zoom feature.
Copy as Metafile Copies the report data as a metafile (.WMF) .
Copy as Text Copies the report data to the clipboard. It can then be pasted into other
software programs as tab-delimited columns or copied as an overlay
onto another graph.
Edit axis Use to edit the selected axis properties.
Autoscale minimum / maximum. To manually specify minimum /

maximum autoscale, deselect the option and enter the new amount in
the text box.

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7 About Reports
Graph Shortcuts Options and Description Table (continued)

Grid lines. Use to change how to display major / minor grid lines.
Invert scale. Use to invert the scale.
Linear / Logarithmic. Select the option to scale the graph as linear or

logarithmic.
Scale font. Use to modify the font for the scale label. Deselect Use
default font to enable font options.
Title. Use to edit the selected axis label.
Title font. Use to modify the font for the selected axis label. Deselect
the Use default font to enable font options. Select new font attributes
for the report data. To return to the default fonts, enable Use default
font.
Edit curve Use to edit selected curve properties.
Color. Click to change the curve color.
l Curve group box. Use to change the interpolation, point style and
pen style for the selected curve. These options are disabled if Use
default fill style is selected in the Histogram group box.
l Histogram group box. Enabled only if Histogram is selected in
the Style drop-down list. Use to specify the type of fill, fill color and
label position for the selected curve.
Label. Select where the graph point labels will display (left, right,
center, etc.) on the SPC report.
Style. Use to select another style for the collected data curve.
Title. Use to change the title of the selected curve.

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Graph Shortcuts Options and Description Table (continued)

Use default thickness. Uses the default curve thickness. Deselect to
enter a new thickness number in the Thickness text box.
Edit legend Use to change the legend location and font. Click Font to modify font
attributes. Deselect the Use default font to enable font options. Select
new font attributes for the report data. To return to the default fonts,
enable Use default font.
Edit title Use to change the graph title and font. Click Font to font attributes.
Deselect the Use default font to enable font options. Select new font
attributes for the report data. To return to the default fonts, enable Use
default font.
Hide curve Hides selected curve.
Redraw Sets the axis boundaries to the original view. This option also removes
cross-hairs.
Show curve Displays a list of all curves. Select the curve to display.
tons on page 3 - 2.

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7 About Reports
AXIS CROSS-HAIR
Left click on the graph to view the cross-hair coordinates.

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GRAPH GRID LINES

Options > Graph Grid Lines
Use to select how grid lines appear on reports. This menu option is not available if using Restricted
option presentation.
Graph Grid Lines Fields and Buttons Table

Grid Line Styles [selec- Select if the major and/or minor grid lines should appear as solid or dot-
tion] ted lines.
X-Axis / Y-Axis [selec- Select major and/or minor lines to display in reports for the logarithmic
tion] and linear scales. Deselect this option to remove the grid lines.
tons on page 3 - 2.
ZOOM FEATURE
Use the zoom feature to examine graph details. Click, hold, and drag the left mouse button on the
graphical area to be enlarged. A box will display in the area to be enlarged.

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7 About Reports
GRAPH AND SAMPLE OVERLAYS

Use the graph overlay functions to compare multiple graph options. Graphical lines are differentiated
by the use of varying colored symbols outlined on a legend. Overlays may be generated in two ways:
l Multiple Graph Overlays. Overlay two different types of graphs from one sample.
l Multiple Sample Overlays. Overlay graphs of the same type with that of the current plot.
This feature is available only when using Advanced option presentation. Go to Options
> Option Presentation > Advanced.
GENERATE MULTIPLE GRAPH OVERLAYS

1. Go to Options > Option Presentation and ensure there is a checkmark to the left of
Advanced.
2. Go to File > Open > Sample Information and open the sample file.
3. On the Report Options tab, in the Selected Reports list box, highlight the graph to be used for
multiple overlays, then click Edit.
4. Click the down arrow to the right of the Overlay field and select a graph. This selection will over-
lay the graph selected in the Y-axis field.

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Generate Multiple Sample Overlays
5. Click OK then click Save.

6. Go to Reports > Start Report. Select the report destination in the Settings group box. Select
the overlay file name in the Files list box, then click OK.
7. In the pop-up Selected Reports list box, reports can be added or removed by double clicking
the entry. Selected reports as indicated by a checkmark to the left. Click OK.
8. Reports display in a tabbed format. Click each tab to view each report.
GENERATE MULTIPLE SAMPLE OVERLAYS
Use a copy of a file rather than the original file when performing a sample overlay.
1. Go to Options > Option Presentation and ensure there is a checkmark to the left of
Advanced.
2. Go to File > Open > Sample Information and open the sample file.
3. On the Report Options tab, in the Selected Reports list box, select the reports to be used by
double clicking the report name. This places a checkmark to the left of each selected report.
4. Highlight the graph to be used for multiple overlays, then click Edit.
5. On the overlay window, click the down arrow to the right of the Overlay field and select the
Overlay Samples Select other options as needed, then Click OK.
6. In the Report Options tab, click Overlays.

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7 About Reports
7. Om the Graph Overlays window, click Browse to locate and select which graphs are to be
overlaid. Click OK.
8. Go to Reports > Start Report. Select the report destination in the Settings group box. Select
the overlay file name in the Files list box, then click OK.
9. In the pop-up Selected Reports list box, reports can be added or removed by double clicking
the entry. Selected reports as indicated by a checkmark to the left. Click OK.
10. Reports display in a tabbed format. Click each tab to view each report.

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Report Examples
REPORT EXAMPLES
COMBINED REPORT

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7 About Reports
SUMMARY REPORT

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Tabular Report
TABULAR REPORT

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7 About Reports
GRAPH REPORT

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Overlay Report
OVERLAY REPORT

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7 About Reports
EQUILIBRATION REPORT

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Sample Log Report
SAMPLE LOG REPORT

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8 Selected Reports
8 SELECTED REPORTS
COMBINED REPORT
The Combined Reports option creates a single report from all selected reports. The Combined
Report contains no breaks between reports and no headings. Highlight the report, then click Edit to
edit report details.
DENSITY AND VOLUME TABLE
Density and Volume Fields and Buttons Table

Columns 1 though 7 Select a variable for each column.
[drop-down box]
Name [text box] Enter the name of the report.
Summary Data Select the average, standard deviation, and coefficient of variation
[group box] (C.V.) for report parameters.

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8 Selected Reports
Density and Volume Fields and Buttons Table (continued)

tons on page 3 - 2.
DENSITY VS CYCLE NUMBER TREND PLOT
There are four types of graphical reports available. Report titles are based on the parameters
selected for the X-axis and Y-axis.
Density vs Cycle Number Trend Plot Fields and Buttons Table

Autoscale x-axis When enabled on the report parameters windows, allows the x- and y-
Autoscale y-axis axes to be scaled automatically. Autoscale means that the x- and y-
[check box] ranges will be set so that all the data is shown. If Autoscale is not selec-
Overlay [drop-down box] Select overlay plot options.
l A second Y-axis can be selected to overlay with the variable in the
Y-Axis field, or
l Select Overlay Samples to overlay data of the type selected in the

Y-Axis field with the same type of data contained in other sample
files. To select other sample files, go to the Report Options tab and
click the Overlays button.

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Density vs Time Trend Plot
Density vs Cycle Number Trend Plot Fields and Buttons Table (continued)
Plot curve Select to display how data are plotted.
Plot points
[check box]
Show +/- Select to place two horizontal lines on the graph. The top line will be
[check box] placed at a point relative to the average and standard deviation of the
data. The bottom line will be placed at the point entered in the adjacent
field.
Show Average Select to show the average of all cycles. A horizontal line is placed at
[check box] the average point for the cycles.
Show Min Select to show the average of all cycles. Horizontal lines are placed at
Show Max the entered limits.
[check box]
Show Reference Select to show a horizontal line placed at a reference point specified in
[check box] the adjacent field.
X-Axis [check box] Variables available for the X-axis.
Y-Axis [check box] Variables available for the Y-axis.
tons on page 3 - 2.
DENSITY VS TIME TREND PLOT
The Density vs Cycle Number Trend Plot and the Volume vs Cycle Number are identical unless
otherwise noted. See Density vs Cycle Number Trend Plot on the previous page.

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8 Selected Reports
EQUILIBRATION REPORT
This report is available only if the Record equilibration data option was selected on the Analysis
Conditions tab.
Equilibration Report Fields and Buttons Table

Autoscale x-axis When enabled on the report parameters windows, allows the x- and y-
Autoscale y-axis axes to be scaled automatically. Autoscale means that the x- and y-
[check box] ranges will be set so that all the data is shown. If Autoscale is not selec-
From cycle [text box] Enter the beginning report cycle.
Report every Enter which cycle to report.
[text box]
Overlay cycles Select to overlay the number of cycles entered in the Report total of
[check box] field.
Overlay samples Select to overlay the last cycle in the current file with the last cycle con-
[check box] tained in other files. Click Overlays on the Report Options tab to select
the other sample files.
Plot curve Select to display how data are plotted.
Plot points
[check box]
Report quantity Select a variable to be reported.
[drop-down box]
Report total of [text box] Enter the number of cycles for this report. Enter up to 8 cycles.
Report every Enter time between cycles. Up to 60 seconds can be entered.
[text box]

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Options Report
Equilibration Report Fields and Buttons Table (continued)

Show plot [check box] Generates a plot (graph) for the Report quantity field selection.
Show table [check box] Generates a tabular report for the Report quantity field selection.
tons on page 3 - 2.
OPTIONS REPORT
The Options report provides information on the sample, its material properties, and analysis
conditions. This report cannot be edited.
PRESSURE AND VOLUME TABLE
The Pressure and Volume Table and the Density and Volume Table are identical unless otherwise
noted. See Density and Volume Table on page 8 - 1.

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8 Selected Reports
SAMPLE LOG REPORT

The Sample Log report displays:
l Automatic operations
l Information entered using Add Log Entry on the Sample Information tab
l Warnings and/or errors which occurred during analysis
The Sample Log Report cannot be edited.
SUMMARY REPORT
The Summary Report provides a condensed listing of data results. Select the type of information to
include in the report. If Pass/Fail is selected, the Min and Max fields are enabled. Enter the minimum
and maximum values for the pass / fail.

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Tabular Report
TABULAR REPORT
Tabular Report Fields and Buttons Table

Columns 1 through 7 Select a variable to appear in each column.
[drop-down box]
Selections applicable only to the Asphalt configuration:
l Volume (60 °F)

l Density (60 °F)
l Specific Gravity (60 °F)
l Volume (60 °F) Deviation
l Density (60 °F) Deviation
l Specific Gravity (60 °F) Deviation
Name [text box] Enter a name for the report.

Summary Data Select options for reporting the average, standard deviation, and coef-
[group box] ficient of variation (C.V.).
tons on page 3 - 2.

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8 Selected Reports
TOTAL PORE VOLUME VS TEMPERATURE
The Total Pore Volume vs Temperature and the Density vs Cycle Number Trend Plot are identical
unless otherwise noted. See Density vs Cycle Number Trend Plot on page 8 - 2.
VOLUME VS CYCLE NUMBER TREND PLOT
The Volume vs Cycle Number and the Density vs Cycle Number Trend Plot are identical unless
otherwise noted. See Density vs Cycle Number Trend Plot on page 8 - 2.

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9 Diagnostics using the Software
9 DIAGNOSTICS USING THE SOFTWARE

Unit [n] > Diagnostics
Performs a leak test for the analysis module.
Diagnostic Test Fields and Buttons Table

File name [text box] Shows a status bar of steps complete once the test begins.
Next [button] Starts the next test.
Report after test Automatically generates reports to the selected destination when the
[check box] test is complete.
Sequence Sequence number assigned to the test.
Test [drop-down box] Select the appropriate test from the drop-down list.
tons on page 3 - 2.

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10 About Calibration
10 ABOUT CALIBRATION
The pycnometer volume should be calibrated every time it is restarted. Cell volume and expansion
volume in the set up parameters are updated automatically upon calibration. Run an analysis with an
empty cup to see how close the average volume is to 0. It should be ±0.05% of full scale. If it is not
within ±0.05% of full scale, calibration is required.
If calibrating using the keypad, see Calibrate using the Keypad on page 10 - 12.
CALIBRATE USING THE SOFTWARE

CALIBRATION REPORT
Unit [n] > Calibration > Calibration Report
1. Select the type of chamber insert used.

2. Select the report destination.
3. Click OK to generate the report.

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CALIBRATE TEMPERATURE OFFSET

Unit [n] > Calibration > Temperature
Opens the Calibrate Temperature Offset box.
Calibrates the temperature offset. Use an external reference device to determine the sample cell
temperature. Enter the value in the field, then click Done.
A Calibration report is not generated for the temperature offset. The entry is recorded in the
Instrument Log. To view the log, go to Unit [n] > Show Instrument Log.
1. Enter the current sample cell temperature.

2. Click Done. Temperature reading will be adjusted to the entered temperature.

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Calibrate Zero Cell Volume
CALIBRATE ZERO CELL VOLUME

Unit [n] > Calibration > Zero Cell Volume
Use to calibrate the cell volume offset.

Analysis Conditions Specify conditions for the calibration.
Click Replace to replace the values with those from an existing

Analysis Conditions file. See Analysis Conditions on page 5 - 2.
Cell Volume Current cell volume (without an insert) or the volume of the selected
insert.
Expansion Volume Current expansion volume, and the date and time of calibration.
Insert l None
1 cm3 unit 3
l 0.1 cm
If None is selected, place an empty sample cup in the chamber.

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Insert l None
10 cm3 unit 3
l 3.5 cm
Insert l None
1.0 cm3and 100 cm3 l 35 cm
3
unit 3
l 10 cm
Insert l None
350 cm3 and 2000 cm3 l Large
units
l Small
tons on page 3 - 2.
CALIBRATE ZERO PRESSURE

Unit [n] > Calibration > Zero Pressure
This option zeros the pressure transducer reading.
Click Start to calibrate the pressure offset.

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Reset Pressure Calibration
RESET PRESSURE CALIBRATION

Unit [n] > Calibration > Reset Pressure Calibration
This procedure resets the pressure calibration to the factory default settings.
This option can be used when the pressure appears not to be reported correctly by the analyzer. For
example: a zero, negative, or unreasonably high reading is being consistently reported. Resetting to
nominal may restore normal pressure readings but a proper calibration should be performed.
A popup warning indicates that when this option is used, the previous pressure calibration is lost and
the nominal calibration is used.
Temperature and volume calibrations are not affected by a reset of the pressure cal-
ibration.
Click OK. The nominal calibrations may be sufficient. However, it is recommended to contact your
Micromeritics Service Representative and schedule a proper pressure calibration as soon as
possible since data accuracy may be compromised.

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CALIBRATE VOLUME SCALE

Unit [n] > Calibration > Calibrate Volume
Calibrates the cell volume offset and expansion volume.
Although the instrument is calibrated prior to shipment, the pycnometer should be recalibrated to
laboratory atmospheric and environmental conditions.
1. On the pressure regulator, turn the pressure control knob clockwise to set the regulator pres-
sure at 21.500 psig (low pressure gauge). For a High Pressure sample chamber con-
figuration, set regulator pressure 20 psi above cycle and fill pressure.
2. Remove the chamber cap and place an empty cup into the sample chamber, then replace the
cap. If an insert is being used, place the insert sample cup into the chamber.
Wear latex or nitrile, powder-free gloves to prevent transfer of oil from hands when
handling sample cups, calibration standards, and inserts. See Handling System
Components on page J - 1.
3. Go to Unit [n] > Calibration > Calibrate Volume.

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Calibrate Volume Scale
4. Enter the volume of the calibration standard (located on the outside of the calibration stand-
ards case shipped with the instrument) in the Volume of Calibration Standard field.
The value recorded on the case for a 10 cm3 pycnometer is the sum of the two standards, and
on a 350 cm3 pycnometer, the sum of the three standards.
5. Select the Measured option.
6. Click Analysis Conditions to specify calibration parameters. Click Replace and select the
file calstd.anc. The values in the current file will be replaced with those contained in the selec-
ted file. Click OK, then click OK again to return to the Calibrate Volume Scale window.
7. Click Start to begin the first phase of the calibration (volume offset). Status messages display
until this phase is complete. When the phase has finished, a prompt display indicates to insert
the calibration standard.
8. Remove the sample chamber cap, then remove the sample cup from the chamber. Place the
cap back onto the chamber while placing the standard into the cup.
9. Tilt the sample cup and allow the standard to roll gently into the cup to prevent denting of the
cup.

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l one standard is shipped with the 1-, 100-, and 2000 cm3 pycnometers
l two are shipped with the 10 cm3 pycnometer
l three are shipped with the 350 cm3 pycnometer
10. Remove the sample chamber cap, place the sample cup back into the chamber, and replace
the cap. Turn the cap clockwise to tighten.
11. Allow the standards to reach thermal equilibrium with the pycnometer.
l Wait 10 minutes for 1- and 10 cm3 pycnometer
3
l Wait 15 minutes for the 100 cm pycnometer l
Wait 20 minutes for the 350 cm3 pycnometer l

30 minutes for the 2000 cm3 pycnometer
12. Click Continue to complete the second phase of the calibration (volume scale). Status mes-
sages display until the calibration is complete.
13. Click Done to accept the new values, then click OK.
14. Do not remove the standard from the sample chamber until the operation is verified. See
Verify Operation on page 10 - 10.
Calibrate Volume Scale Fields and Buttons Table
Analysis Conditions Specify conditions for the calibration.

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Calibrate Volume Scale
Calibrate Volume Scale Fields and Buttons Table (continued)

Click Replace to replace the values with those from an existing
Analysis Conditions file.
Cell Volume Displays the current cell volume (without an insert), or the volume of
[group box] the selected insert.
Continue [button] Place the standard into the sample cup and click Continue to com-
plete the volume scale calibration.
Expansion Volume Displays the current expansion volume, and the date and time of cal-
[group box] ibration.
Insert [group box] l 1 cm3 unit None, 0.1 cm3
l 10 cm3 unit None, 3.5 cm3
l 1.0 cm3100 cm3 unit None, 35 cm3, 10 cm3
l
3 3
350 cm and 2000 cm units None, Large, Small
If None is selected, pace an empty sample cup in the chamber.
Previous / Entered / Select the method for calibrating the cell and expansion volumes.
Measured
[check box] Previous. Uses the current values.
Entered. Enables the fields for the cell and expansion volumes.
Measured. Measure the cell and expansion volumes using a

reference standard.
Start [button] Begins the first segment of the volume offset calibration. Status mes-
sages are shown as the calibration proceeds. When the volume offset
calibration is complete, a prompt displays indicating to insert the stand-
ard.
Volume of Calibration The volume of the standard used for the previous calibration.
Standard [text box]
tons on page 3 - 2.

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VERIFY OPERATION
Verify operation of the pycnometer by performing an analysis on the calibration standard to ensure
that the pycnometer is operating properly.
1. Go to Unit [n] > Sample Analysis.

2. Click OK, then Yes to create a new sample file.
3. Click Replace and select the refanly.smp file. The values in the current file will be replaced
with those contained in refanly.smp. Click OK.
4. Click Report After Analysis. Select the Report after analysis option, then click OK.
5. Click Start to begin the analysis.

6. Compare the value displayed for the average volume to the value recorded on the calibration
standards case. These two values should agree plus or minus the tolerance obtained using
the following calculation:
Tolerance = (chamber volume * 0.0003) + (Value recorded on Standards case * 0.0003)

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Load Calibration from File
Example: calculate the tolerance for a 10 cm3 pycnometer with a value of 6.372242
recorded on the case as :
Tolerance = (10 * 0.0003) + (6.372242 * 0.0003) = 0.003 + 0.0019116726 = 0.005
If the values do not agree, a leak may be indicated. Check the system for leaks. Then repeat
steps 1 through 6. If the values continue to disagree, contact your Micromeritics service
representative. See Diagnostics using the Software on page 9 - 1.
7. Remove the standards and place them back into the case.
LOAD CALIBRATION FROM FILE

Unit [n] > Calibration > Load from File
Use to load a previously saved calibration file.
It is recommended that the current calibration settings be saved using Unit [n] > Calibration >
Save to File prior to loading another calibration file. When loading a previously saved calibration file,
a backup of the current file is created and saved as [SN]last.cal. The backup file is overwritten each
time a new one is created.
Changing the calibration may affect the analyzer’s performance.
SAVE CALIBRATION TO FILE

Unit [n] > Calibration > Save to File
Use to save the current calibration settings to a backup file which can later be reloaded using Unit
[n] > Calibration > Load from File menu option.
The default file naming convention for calibration files can be used or the file name can be changed.
The default file name of 0217-2013-04-25.CAL is interpreted as:
0217 is the analyzer serial number

2013-04-25 is the date the calibration file was saved
.CAL is the file name extension

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CALIBRATE USING THE KEYPAD

CALIBRATE FUNCTION
This command performs a full volume slope and offset calibration. Press ALT + . (decimal) to
access the Calibrate function.

Calibration Type? Press CHOICE until the option is displayed, then press ENTER.
Volume
l Volume
l Temperature
l Pressure
l Copy to an external device
l Load from an external device
l Reset Pressure Calibration
CALIBRATION DATA

Setup Type? Press CHOICE until Calibration Data is displayed, then press ENTER.
Calibration Data
Calibration Data Select Yes at the Request insert prompt in Report Options. Press
Chamber Insert? CHOICE until the appropriate insert is displayed, then press ENTER.

Calibration Data Displays the cell volume determined during calibration Cell volumes
Cell Volume: can also be entered at this prompt. Press ENTER.
The range is 0.01 to 999.0000 cm3.

Calibration Data Displays the expansion volume determined during calibration. Press
Expansion Volume: ENTER.

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Calibrate Volume
CALIBRATE VOLUME
Place an empty cup into the sample chamber for Cal1 (volume offset). If using an insert, place the
insert and its appropriate sample cup into the sample chamber.

Calibration Type? Press ENTER to accept Volume (default) and display the next prompt.
Volume
Calibrate Volume Press CHOICE until the appropriate insert is displayed, then press
Chamber insert? ENTER. Yes must be selected for the Request Insert prompt in
Report Options for this prompt to display.

Calibrate Volume Enter the volume of the calibration standard to be used in the
Volume of Cal Std: calibration (located on the outside of the calibration standards case).
Some pycnometers require and are shipped with multiple standards.
In this instance, the value recorded on the case is the sum for all
standards and is the one that should be entered at the prompt. Press
ENTER.

Calibrate Volume Press ENTER to begin the calibration or Alt + CLEAR to cancel. The
[ENTER volume offset is calibrated first (Cal1). When the first calibration is com-
plete, the pycnometer beeps three times and the next prompt is dis-
played.
Insert Cal Std Place the calibration standard in the cup in the sample cell chamber
[ENTER] to start and replace the chamber cap. Press ENTER to calibrate the
temperature offset (Cal2). Calibration continues and operational
status messages are continually displayed. After the operation is
complete, the pycnometer returns to the Reload prompt.
For best results, sample volume should be approximately equal to the

volume of the calibration standard. Therefore, if calibrating the 10 cm3
pycnometer for use with smaller sample volumes, use only one
standard. If using one standard, enter half of the value at the Volume of
cal std prompt. Press Alt + CLEAR to cancel the operation.

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RESET PRESSURE CALIBRATION
Contact a Micromeritics service representative and schedule a proper pressure cal-

ibration since data accuracy may be compromised.
This option can be used when the pressure is suspected of not being reported correctly by the
analyzer. For example: a zero, negative, or unreasonably high reading is being consistently
reported. Resetting to nominal may restore normal pressure readings but a proper calibration should
be performed.

Calibration Type? Press CHOICE until the desired option is displayed, then press
Reset Pressure Cal ENTER.
Reset Pressure cal? Resets the pressure calibration to nominal values. Temperature and
[Yes / No] volume calibrations are not affected. Nominal values may be sufficient.
Schedule a proper pressure calibration as soon as possible, then
press CHOICE.
Select Yes to reset the calibration to nominal values. Press ENTER.
Select No to contact your service representative to schedule a proper

pressure calibration. Press ENTER.

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Review Calibration
REVIEW CALIBRATION
The Review function reviews the results of the last calibration operation.
The sample cell volume and the expansion cell volume are used for calculating the sample volume.
The cell volume and expansion volume are updated automatically when the pycnometer is
calibrated.
The prompts that display during a review of calibration data depend on the options specified in Setup
> Analysis Parameters and Report Options.
1. Press Alt + 5 to display the Chamber Insert prompt from which the insert can be selected (if
used).
2. Press ENTER to display the volume of the calibration standard. This volume can be edited
from this prompt.
3. Press ENTER to display the Which Chamber prompt.
4. Press CHOICE to select whether to view the results for the sample chamber or the expansion
chamber.
5. Press ENTER to display a prompt showing the starting time and date.
6. Press ENTER to display a prompt showing the ending time and date.
7. Press ENTER to display the first of the prompts containing data. The [n] in this example rep-
resents the cycle number.
8. Continue pressing ENTER to view all of the data. Press CHOICE to exclude data from report
calculations. An asterisk will display indicating that it will be excluded.
9. Press SAVE to return to the Reload prompt
10. Press Alt + 6 to print report results.
Chamber insert? Displays the insert selected for the calibration or None if an insert was
(insert) not used. If the selection is incorrect, press CHOICE until the correct
one is shown, then press ENTER.


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Volume of Cal Std: Displays the volume of the calibration standard that was used for the
(volume) calibration. Press ENTER.
Which Chamber? Select to view calibration data for the sample cell chamber or the
(chamber type) expansion chamber. Press CHOICE until the chamber is displayed,
then press ENTER.
The chamber type options are Cell volume and Expansion volume.
Start: Displays the time and date the calibration began. Press ENTER.
(time) (date)
Time: HH:MM:SS
Date: DD/MM/YY
End: Displays the time and date the calibration completed. Press ENTER.
(time) (date)
Time: HH:MM:SS
Date: DD/MM/YY
Cell[n] = (volume) Displays the Volume, depending on the chamber type selected (Cell
Dv[n] = (deviations) volume or Expansion volume).
or [n] represents the cycle number.
Exp[n] = (volume) Press CHOICE to exclude the displayed density (or volume) from the
Dv[n] = (deviations) calculated average. An asterisk next to the density indicates it has
been excluded. Press CHOICE again to remove the asterisk and have
it included.
Each time CHOICE is pressed to exclude or include the value. A new

deviation is calculated and displayed.
Press ENTER to view the values for the next cycle.
Press SAVE to return to the Reload prompt. Press SAVE to

automatically recalculate collected data and add all data reduction
messages back into the queue.

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Temperature
TEMPERATURE
This operation typically is performed by a Micromeritics service representative.
Press Alt + ., then press CHOICE until Temperature is displayed.

Calibrate Temperature Enter the temperature obtained from a reference temperature sensor.
Temperature: Press ENTER to automatically return to the Reload prompt. Press ALT
+ CLEAR to cancel the operation.
ZERO THE PRESSURE TRANSDUCER & CHAMBER VOLUME

The pressure transducer zeroes automatically before each cycle in an analysis or calibration;
therefore, it is not necessary to zero the unit for these operations. Typically, this function is not
required unless manually performing analyses for an extended period of time.
Press Alt + 0 to access the Zero function.

Zero Type? Allows zeroing of the pressure transducer or the volume offset. Press
Pressure CHOICE until the option is displayed, then press ENTER. If choosing
Pressure, the next prompt is not displayed. Choices are Pressure and
Volume. Ensure the sample chamber is empty if selecting Volume.
Zero Volume? Displays when Volume is selected. Select Yes at the Request insert
Chamber insert? prompt in Report Options. Press CHOICE until the appropriate insert is
None displayed, then press ENTER.
Does not display for l None, 0.1 cm3 (for 1 cm3 unit)
Pressure 3 3 3
l None, 3.5 cm , 1.0 cm (for 10 cm unit)
Zero Volume Press ENTER to begin the zero operation or Alt + CLEAR to cancel
[ENTER] to start the operation.
[ESCAPE] to cancel
If zeroing the Volume, the purges and cycles specified in the current
or analysis parameters are used to calculate the volume offset.
Zero Pressure After the operation is complete, the pycnometer returns to the Reload
[ENTER] to start prompt.
[ESCAPE] to cancel

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LOAD CALIBRATION DATA FROM A USB STICK

Calibration Type? Press CHOICE until the option is displayed. Press ENTER.
Load from USB Stick
Insert USB stick Insert the USB device into the USB connector on the rear panel of the
and press [ENTER] unit. Press ENTER.
Local cal for SN: Key in the serial number. Press ENTER.
Calibration for Display the unit for which calibration information has been copied.
SN (nnnn) copied
Remove USB stick Remove the USB stick. The system automatically returns to the
Reload prompt. This prompt appears immediately after the Calibration
for SN prompt.
COPY CALIBRATION DATA TO A USB STICK

Calibration Type? Press CHOICE until the option is displayed. Press ENTER.
Copy to USB Stick
Insert USB stick Insert the USB device into the USB connector on the rear panel of the
and press [ENTER] unit. Wait a few seconds, then press ENTER.
Calibration for Display the unit for which calibration information has been copied.
SN (nnnn) copied
Remove USB stick Remove the USB stick. The the Reload prompt displays. This prompt
appears immediately after the Calibration for SN prompt.

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11 Hardware
11 HARDWARE
ADD ANALYSIS MODULE TO CONTROL MODULE

Additional analysis modules provide the ability to increase productivity and/or provide a means for
analyzing different size samples concurrently. Multiple analysis modules can be connected to an
integrated controller / analysis module.
If connecting to a temperature controlled unit, see Add Analysis Modules to a Temperature

Controlled Module on page H - 2.
Diagram Components
A Separate power cord for external power supply. Connect cable to wall outlet.
B External power supply
C Hardwired 8-pin mini-DIN power cable for external power supply.
D 8 pin mini DIN cable.
E Power adapter DIN port.
F Power adapter.
G Module Connection - 8-pin mini-DIN OUT port to connect next analysis module.
H Module Connection - 8-pin mini-DIN IN port to connect the control module or pre-
viously connected analysis module (not shown).
I Hardwired power mini-DIN cable for power adapter.

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11 Hardware
Exit the application before powering off the analyzer.
If installing an external TEC module, it is suggested that the TEC system be installed
first, to allow time for temperature to stabilize at the desired temperature, while the
AccuPyc is being installed. The TEC module has a separate power cord and external
power supply.
1. Power OFF the control module.

2. Connect one external power supply cable to the back of the new unit and another external
power supply cable to each power adapter.
3. Connect a power cable to each external power supply.
4. Attach one end of the DIN cable (provided in the module accessories kit) to the connector
labeled Module Connection on the back of the new unit.
5. Attach the other end of the DIN cable to the separate power adapter.
6. Attach the hardwired power adapter cable to the lower connector labeled Module Connection
on the back of the analysis module.
7. Plug the external power supply cables into electrical wall outlets.
8. Power ON the control module. If running the application software, start the application.
9. Verify the unit is recognized:
l If running the application software, Unit
[n] menus are added to the menu bar
for each analysis module connected.
l If using the keypad for analysis, press

Alt + CHOICE + 2 to access the addi-
tional analysis module. Unit [n] appears
in the upper left corner of the display.
10. Calibrate the pycnometer. See Calibrate using the Keypad on page 10 - 12 or Calibrate
using the Software on page 10 - 1.

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Analytical Balance
ANALYTICAL BALANCE
The analytical balance tested by Micromeritics is Scientec® model #ZSA120.
An analytical balance can be connected to a serial port on the computer and used to transfer the
sample’s mass via a third-party software directly to the AccuPyc II application. Refer to the balance
manufacturer’s operator’s manual for transmission instructions.
1. Connect the analytical balance to the RS-232 port on the rear panel of the analyzer.
2. Go to Options > Configure Balance to connect and set up an RS-232 balance to the ana-
lyzer.
Configure Balance Fields and Buttons Table

Enable / Disable Select to enable or disable the attached balance.
Serial Parameter Used to set the baud rate, parity, data bits, and stop bits. This field
should not require modification from the default values.
Serial Port Select which serial port is used to connect the balance to the analyzer.
PRINTER SETUP
If using the Keypad only, see Printer Setup on page J - 10. This step is not required if using the
software.

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12 Maintenance and Troubleshooting
12 MAINTENANCE AND TROUBLESHOOTING

The instrument has been designed to provide efficient and continuous service; however, certain
maintenance procedures should be followed to obtain the best results over the longest period of
time. When unexpected results occur, some common operational problems not indicated on the
window and their respective causes and solutions are provided:
Power indicator did not illuminate when analyzer was powered ON.
Cause A: Power or DIN cables not fully inserted.

Action A: Verify cable connections and connect any loose cable ends into proper outlets.
Cause B: No power at outlet.
Action B: Test the outlet. If there is no power, contact electrician.
Cause C: Plug prongs bent so that contact not made at outlet.
Action C: Unplug the power cable and re-plug into outlet. If indicator does not illuminate,
have electrician adjust prongs or replace outlet or plug.
Cause D: Power cord damaged.
Action D: Have electrician check cord using test meter. Replace if defective.
Cause E: Loose internal connection, broken wire, or failure of internal power supply.
Action E: Contact a Micromeritics Service Representative for repair or replacement
information.
Specified pressure not reached or maintained.
Cause A: Chamber cap not properly closed.

Action A: Close chamber cap by turning fully clockwise.
Cause B: Chamber cap contains dust or debris or the O-ring is not properly greased.
Action B: Using a lint free tissue, clean the chamber cap and the rim of the cell chamber.
Lightly grease the chamber cap O-ring. See Chamber Cap O-Ring on page
12 - 3.
Cause C: The chamber cap O-ring is not properly seated.
Action C: Check the chamber cap. Ensure that the O-ring is properly seated and that it
contains no scratches or cuts.
Cause D: The chamber cap O-ring is cut or scratched.
Action D: Replace the O-ring in the chamber cap. See Chamber Cap O-Ring on page
12 - 3.
Cause E: Gas leaks in the cell chamber or expansion chamber.
Action E: Check the pycnometer for leaks. See Check the Cell and Expansion Cham-

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134-42800-01 (Rev A) — Jan 2016
bers for Leaks on page 12 - 5 .

Cause F: The helium tank is low on gas or empty. Tank pressure should be at least 200
psi above regulator pressure.
Action F: Check tank. Minimum recommended pressure is 200 psig above regulator pres-
sure. See Regulator Pressure on page 12 - 13.
Cause G: The shutoff valve on the gas cylinder is closed.
Action G: Ensure that the valve is open.
Cause H: The Zero offset (of pressure transducer) is too low.
Action H: Check offset by opening chamber cap. If pressure is negative (displayed on
instrument schematic), run a new zero offset. See Zero the Pressure Trans-
ducer & Chamber Volume on page 10 - 17.
Cause I: Dust filter on 2000 cm3 unit is clogged or leaking to atmosphere.
Action I: Clean the dust filter. See Clean the Dust Filter on page 12 - 7.
Helium drained from tank.
Cause A: Leaks in the gas line connection.

Action A: Pressurize the system. Close, then open the gas cylinder shutoff valve. If the
needle on the pressure gauge falls abruptly, a leak in the gas line connections
may be indicated. Check all gas line connections.
Cause B: Pycnometer was left in Manual mode with all the valves open or the fill valve
open and chamber cap off.
Action B: Close all valves, then attach a new tank of helium.
Unit will not equilibrate, or results are not reproducible.
Cause A: Sample outgassing.

Action A: Prior to analysis, remove moisture and contaminants from the sample. See Pre-
pare and Load a Sample on page 6 - 1.
Cause B: Dust filter on 2000 cm3 unit is clogged or leaking to atmosphere.
Action B: Clean the dust filter. See Clean the Dust Filter on page 12 - 7.
Cause C: Defective cap O-ring.
Action C: Check cap O-ring for defects. Regrease or replace the O-ring, if necessary.
Cause D: Debris on valves.
Action D: With manual mode enabled and with the cap installed, open all valves. With
helium flowing through the pycnometer, open and close the expansion valve
repeatedly for approximately one minute. This will remove sample con-
tamination, which may cause a leak, from the valve seat. Repeat the process for
the vent valve with the inlet and expansion valves open.

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Chamber Cap O-Ring
CHAMBER CAP O-RING

The cell chamber cap contains an O-ring that requires routine maintenance. The chamber cap O-
ring should be greased at the beginning of each period of use.
Fine fibers and particles between the O-ring and its sealing surfaces can cause leaks, as can
scratches or cuts in the O-ring or in the metal surfaces.
GREASE THE CHAMBER CAP O-RING

1. Turn the chamber cap counter-clockwise and lift it from the chamber.
2. Place the chamber cap on a clean surface with the O-ring side exposed.
3. Use a small drop of Dow Corning high vacuum grease (or equivalent).
4. Distribute the grease evenly and completely around the O-ring groove.
5. Replace the chamber cap.

6. If recalibrating the pycnometer, allow the pycnometer to warm up for 30 minutes before cal-
ibrating.
REPLACE THE CHAMBER CAP O-RING

1. Use a pointed tool and carefully remove the O-ring from its groove in the cap. A small niche is
provided at the groove for placement of the tool.

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134-42800-01 (Rev A) — Jan 2016
Do not to scratch the metal surface of the chamber cap. Scratches could result in an
imperfect seal.
2. Clean the groove in the chamber cap using a small brush or lint-free tissue moistened with iso-
propyl alcohol.
3. Allow the chamber cap to dry thoroughly.
4. Use a small drop of Dow Corning high vacuum grease (or equivalent).
5. Grasp the O-ring with the two greased fingers. Distribute the grease evenly and completely
around the O-ring.
Apply the grease sparingly. Too much grease may alter cell volume while too little
grease results in an imperfect seal and leaks.
6. Place the O-ring back into the groove on the cap and, with the greased index finger, gently
press it back into position.
7. Ensure the O-ring groove is properly greased. See Grease the Chamber Cap O-Ring on
the previous page.
8. Replace the chamber cap.

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Check the Cell and Expansion Chambers for Leaks
CHECK THE CELL AND EXPANSION CHAMBERS FOR LEAKS

This procedure should be performed in a temperature-stable environment after the pycnometer has
been allowed to warm for at least two hours. Before performing this procedure, check the chamber
cap to ensure that it is not the source of leaks. It should be free from particles, the O-ring should be
properly seated, and should not contain excessive grease.
CHECK FOR LEAKS USING THE SOFTWARE
Before performing this procedure, check the chamber cap to ensure that it is not the
source of leaks. It should be free from particles, the O-ring should be properly seated,
and it should not contain excessive grease.
Unit [n] > Diagnostics

See Diagnostics using the Software on page 9 - 1
CHECK FOR LEAKS USING THE KEYPAD
Before performing this procedure, check the chamber cap to ensure that it is not the
source of leaks. It should be free from particles, the O-ring should be properly seated,
and it should not contain excessive grease.
Check the cell and expansion chambers for leaks.
1. Allow the pycnometer to equilibrate thermally in a room with a stable temperature.

2. Press Alt + 1 to enter Manual mode.
3. If the system was previously open, manually purge the system before proceeding:
a. Press 8 to open the Expansion valve and 9 to close the Vent valve; X - O - X.
b. Press 7 to open the Fill valve. Once the sample chamber fills to the appropriate pres-
sure, press 7 to close the Fill valve.
c. Press 9 to open the Vent valve; X - O - O.

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d. Repeat this procedure two or three times.

e. Press 8 to close the Expansion valve; X - X - O.
4. Press 7 to open the Fill valve; O - X - O.
5. Fill the sample chamber to 19.5 psig.
6. Press 7 to close the Fill valve; X - X - O.
7. Observe the pressure display. After an equilibration period (about 20 to 30 seconds), the pres-
sure should not decrease more than 0.007 psig (0.048 kPag) or increase more than 0.02 psig
(0.14 kPag) in a two minute span.
lIf the pressure does not decrease more than 0.007 psig (0.048 kPag) or increase more
than 0.02 psig (0.14 kPag) in a two minute span, proceed to step 8.
l If the pressure decreases more than 0.007 psig (0.048 kPag) or increases more than 0.02
psig (0.14 kPag) in a two minute span, temperature instability or a leak may be indicated.
Vent the system, then repeat steps 4 through 7 several times to verify that a leak is indic-
ated. If a leak is indicated, call a Micromeritics Service Representative.
8. Press 9 to close the Vent valve, 8 to open the Expansion valve, and 7 to open the Fill valve;
O - O - X.
9. Fill the chambers to 19.5 psig.
10. Press 7 to close the Fill valve; X - O - X.
11. Observe the pressure display. After an equilibration period (about 20 to 30 seconds), the pres-
sure should not decrease more than 0.007 psig (0.048 kPag) or increase more than 0.02 psig
(0.14 kPag) in a two minute span.
If the pressure decreases more than 0.007 psig (0.048 kPag) or increases more than 0.02
psig (0.14 kPag) in a two minute span, temperature instability or a leak may be indicated. Vent
the system, then repeat steps 8 through 11 several times to verify that a leak is indicated. If a
leak is indicated, call a Micromeritics Service Representative.

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Clean the Dust Filter
CLEAN THE DUST FILTER
Applicable only to 2000 cm3 units and 100 cm3 high pressure units.
Dust from the sample may be carried into the instrument plumbing. A dust filter protects the valves,
minimizing valve leaks.
1. Press Alt+1 to enter Manual mode.

2. Close the Fill valve. Open the Expansion and Vent valves to ensure that the system is not
under pressure.
3. At the lower rear of the instrument, remove the two screws which hold the dust filter cover and
remove the cover plate.
4. Remove the spring and the filter. Remove the small O-ring inside the filter port.
5. Clean all parts with alcohol. The filter may require sonication to dislodge dust. It should be
replaced if it becomes severely clogged.
6. Inspect the O-rings before re-assembly. A very thin coating of vacuum grease may be used.
7. Re-assemble.
8. Check for leaks:
a. Fill the system with gas.
b. Open Expansion valve.
c. Check for leaks by applying a leak detecting liquid around the dust filter cover.

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CLEAN THE PYCNOMETER

The exterior casing of the pycnometer may be cleaned using a clean cloth, dampened with isopropyl
alcohol (IPA), a mild detergent solution, or a 3% hydrogen peroxide solution.
Do not immerse the pycnometer or the power cord in any liquids. Doing so could result
in electrical shock to personnel or damage to the unit.
Do not allow liquid to penetrate the casing of the pycnometer. Doing so could result in
damage to the unit.

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Guidelines for Connecting Gases
GUIDELINES FOR CONNECTING GASES

l Place gas cylinders within 6 feet (2 m) of the gas inlets of the instrument. Using gas line extenders
on gas cylinders located in remote areas may degrade gas quality and reduce pressure. Gas lines
are typically five to six feet long. Place the cylinders close enough to allow for proper connection at
the analyzer inlet.
l Use a retaining strap (or other appropriate tether) to secure the gas cylinder.
l Always use the gas lines provided with the analyzer. It is very important that proper gas lines are
used with the analyzer.
o Do not use polymer tubing for the gas line.

o Do not use flexible gas lines. Some flexible lines may appear to be appropriate, such as those
with a herringbone covering, but the line may be coated internally with a polymer.
l Long gas lines, such as those used with gas cylinders placed in remote areas, must be evacuated
for an extended period of time to remove ambient gases. When possible, avoid placing gas cyl-
inders in remote locations. It is always better to have gas cylinders located near the analyzer.
l Carefully route the gas lines from the cylinder to the analyzer avoiding overlapping or entangling
gas lines. This will help avoid confusion when maintenance is required.
l Label the gas line at the analyzer inlet for proper identification and maintenance.
l Replace gas cylinders before gas is depleted. It is best to replace a gas cylinder when the pres-
sure reads approximately 200 psi (1500 kPa) on the high pressure gauge. Contaminants
absorbed to the walls of the cylinder will desorb as the pressure decreases.
l Ensure the gas cylinder is closed before connecting to the analyzer.

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REPLACE A GAS CYLINDER
These instructions apply to working with inert gases only. When working with hazardous
gases, follow the safety procedures established by your lab.
A power failure can result in dangerous pressures in the sample chamber. When using
toxic or flammable gases, additional venting of the cabinet may be required.

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Replace a Gas Cylinder
DISCONNECT THE DEPLETED GAS CYLINDER

1. Close the regulator shut-off valve and gas cylinder shut-off valve by turning the knobs clock-
wise.
2. Disconnect the gas line from the regulator. Gas will be vented from the line. It is not necessary
to disconnect the gas line from the analyzer inlet if the cylinder will be replaced immediately
with one of the same type.
3. Open the gas regulator shut-off valve by turning the knob counter-clockwise. Gas will be ven-
ted from the regulator.
4. Turn the regulator control knob clockwise to open and vent any remaining gas. Both gauges
should read at or near zero. If not, make sure the gas regulator shut-off valve is open.
5. Close the regulator by turning the control knob counter-clockwise.
6. Use an appropriate wrench to loosen the nut at the regulator connector nut then remove the
regulator from the bottle.
7. Replace the protective cap on the depleted bottle. Disconnect the retaining strap and move
the bottle to an appropriate location.

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CONNECT A GAS CYLINDER

Regulator Pressure Settings
Analyzer Series Gauge should indicate
3Flex 15 psig (103 kPag)
AccuPyc 15 psig (103 kPag)
ASAP 15 psig (103 kPag)
AutoChem 5 psig (35 kPag)
AutoPore 45 - 50 psig (310 - 345 kPag)
Gemini 19.5 psig (134.4 kPag)
TriStar 15 psig (103 kPag)
Move the replacement bottle close to the analyzer and tether it into place. It is not necessary to
disconnect the gas line from the regulator or the analyzer.
1. Use an appropriate cylinder wrench to remove the protective cap from the replacement gas
cylinder. Place the protective cap in a secure location. It will be needed to recap the gas cyl-
inder when it is depleted and replaced.
2. Attach the gas regulator to the gas cylinder connector. Hand tighten the nut, then use an
appropriate wrench to tighten an additional 3/4 turn.
Over-tightening the fitting may cause a leak.
3. Check for leaks at the high-pressure side of the regulator and in the connector.
a. Turn the regulator control knob fully counter-clockwise.
b. Slowly open the gas cylinder shut-off valve, then quickly close it.
c. Observe the pressure on the high-pressure gauge for approximately one minute:
l If the pressure is stable, proceed with the next step.
l If the pressure decreases, tighten the regulator connector nut until it becomes stable.
If the pressure does not remain stable, remove the regulator and clean all contacts at
the regulator connection, then reinstall the regulator.
4. Purge the lines and set the regulator pressure.
a. If the gas line is not connected to the regulator and the instrument connect it now.
b. Fully open the gas bottle shut-off valve and the gas regulator shut-off valve.
c. Under manual control, open the fill, expand, and vent val

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Regulator Pressure
d. Adjust the regulator pressure control knob until the Purge fill or Cycle fill pressure,
whichever is higher, is shown on the regulator display.
e. Allow gas to flow for 30 seconds.
f. Close the fill, expand, and vent valves.
g. Turn the regulator control knob clockwise to increase pressure by 2 psi (15 kPa).
REGULATOR PRESSURE
SET REGULATOR PRESSURE WITH THE SOFTWARE
Tank pressure should be at least 200 psi above regulator pressure. Pressures less than
200 psig indicate the tank is low on gas. Analyses are terminated automatically if gas is
depleted.
For a High Pressure sample chamber configuration, set regulator pressure 20 psi above
cycle and fill pressure.
The Purge fill and Cycle fill pressures are specified in Analysis Conditions. Set the regulator
pressure at the higher of the two, plus 2.0 psig. For example; if the Purge fill pressure is set to 19.500
psig (134.445 kPag) and the Cycle fill pressure as 19.000 psig (131.000 kPag), set the regulator
pressure at 21.500 psig (148.237 kPag).
1. Go to Unit [n] > Enable Manual Control. Ensure a checkmark displays to the left of the
menu item. If the instrument schematic does not display, go to Unit [n] > Show Instrument

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134-42800-01 (Rev A) — Jan 2016
Schematic.
2. On the schematic, right click the Expansion and Vent valves and select Open for both. Then
open the Fill valve.
3. Adjust the regulator pressure control knob until the Purge fill or Cycle fill pressure, whichever
is higher, is shown on the regulator display. Tank pressure should be at least 200 psi above
regulator pressure.
4. On the schematic, close the Fill valve, then increase the regulator pressure by 2.0 psig (13.8
kPag).
5. Allow the pressure in the pycnometer to drop below 2.0 psig, then close the Expansion and
Vent valves.
SET REGULATOR PRESSURE WITH THE KEYPAD
Ensure the tank pressure for the gas regulator is at least 200 psig. Pressures less than
200 psig indicate the tank is low on gas. Analyses are terminated automatically if gas is
depleted.
The Purge fill pressure and cycle fill pressure are specified using Setup > Analysis Parameters. Set
the regulator pressure at the higher of the two (plus 2.0 psig). For example; if the purge filll pressure
is specified as 19.500 psig and the cycle fill pressure as 19.000 psig, then set the regulator pressure
at 21.500 psig.
1. Press Alt + 1 to enter Manual mode.

2. Press 8 (EXPAND) and 9 (VENT) to open the expansion and vent valves; the display will
show:
X-O-O
3. Press 7 (FILL) to open the fill valve; the display will show: O - O - O
4. Adjust the regulator pressure control knob until the Purge fill or Cycle fill pressure, whichever
is higher, is shown on the regulator display.
5. Press 7 to close the Fill valve, then increase the regulator valve by 2.0 psig. The display will
show: X - O - O.
6. Allow the pressure in the pycnometer to drop below 2.0 psig, then press 8 and 9 to close the
Expansion and Vent valves. The display will show: X - X - X
7. Press SAVE to return to the Reload prompt.
RECOVER FROM A POWER FAILURE

Setup parameters and collected data are recorded by the pycnometer in case of a power failure.
These settings will be available when power is restored. If an automatic operation was in progress
when the power failure occurred, it will be canceled when the pycnometer restarts.
Even though the pycnometer saves data during a power failure, any operation should be
restarted to ensure complete results.

12 - 14
134-42800-01 (Rev A) — Jan 2016
Reset the Pycnometer
RESET THE PYCNOMETER
Keypad Function
There are two ways to reset the Pycnometer.
l Hold the . key on the keypad during power ON. This erases data and setup parameters except for
printer and network settings.
l Hold 5 on keypad during power ON. This resets setup parameters, as well as printers and net-
work settings.

12 - 15
134-42800-01 (Rev A) — Jan 2016
13 Parts and Accessories
13 PARTS AND ACCESSORIES

Order system components and accessories using one of the following methods:
l Call our Customer Service Department at 1-770-662-3636

l Email orders to [email protected]
l Contact your local sales representative
Part Number Item and Description

Analyzer Equipment
134-00000-00 AccuPyc II, 10 cm3 capacity
134-00005-00 Control Module, no sample compartment
134-00010-00 AccuPyc II, flowing temperature control, 10 cm3 capacity
134-00020-00 AccuPyc II, flowing temperature control, 100 cm3 capacity
134-00030-00 AccuPyc II Glove Box, 10 cc capacity
134-00035-00 AccuPyc II TEC, 10 cc, Glove Box
134-00036-00 AccuPyc II TEC, 100 cc, Glove Box
134-00037-00 AccuPyc II 1340 500 psi, 100 cc Glove Box
134-00040-00 Analysis module, 10 cm3 capacity
134-00044-00 Analysis module, flowing temperature control, 10 cm3 capacity
134-00045-00 Analysis module, flowing temperature control, 100 cm3 capacity
134-00047-00 Analysis module 1340 TEC, 10 cm3
134-00048-00 Analysis module 1340 TEC, 100 cm3

13 - 1
134-42800-01 (Rev A) — Jan 2016

134-00049-00 Analysis Module 1340 500 psi, 100 cc
134-00050-00 AccuPyc II TEC, 10 cm3
134-00051-00 AccuPyc II TEC, 100 cm3
Cables
003-60623-00 Cable, 2 ft; for connecting analysis modules
003-60623-01 Cable, 25 ft; for connecting Control module to Glove box unit
003-63801-00 Ethernet cable, cross-over
003-63821-00 Null Modem Cable, for connecting Analytical Balance to Controller/Data Man-
agement Module
Calibration Kit
133-34900-00 Calibration Standard Kit, 10 cm3; contains two calibration standard and one
sample cup
134-34901-00 Calibration Standard Kit, 2000 cm3; contains one calibration standard and
one 2000 cm3 sample cup
133-34902-00 Calibration Standard Kit, 100 cm3; contains one calibration standard and one
100 cm3 sample cup
133-34903-00 Calibration Standard Kit, 350 cm3; contains 3 calibration standard and one
sample cup
Chamber Cap O-rings
004-25030-01 Chamber cap O-ring, 100 cm3 (500 psi model only)
004-25032-00 Chamber cap O-ring, 2000 cm3

13 - 2
134-42800-01 (Rev A) — Jan 2016

Dust Filter Components (for 2000 cm3 and 100 cm3 500 psi units only)
004-25006-00 O-ring, -006 70 DURO BUNA-N

004-25011-00 O-ring, -011 70 DURO BUNA-N
004-25312-00 Compression spring
004-27082-00 Filter, Line, 10 Micron
Equipment (Optional)
011-00000-00 Scientec Analytical Balance, model ZSA120
133-33604-00 MultiVolume Kit for 100 cm3 pycnometer; includes 10 cm3 and 35 cm3 inserts
and appropriate sample cups
133-33605-00 MultiVolume Kit for 10 cm3 pycnometer; includes 1 cm3 and 3.5 cm3 inserts
and appropriate sample cups
134-33605-00 MultiVolume Kit for 2000 cm3 pycnometer; includes 650 cm3 and 1300 cm3,
cups, inserts, and reference standards
134-33006-00 MultiVolume Kit for 1 cm3 pycnometer; includes 0.1 cm3 insert / sample cup
combination

13 - 3
134-42800-01 (Rev A) — Jan 2016

Filtered Cap Kits and Components
134-33011-00 Kit, 100 cc Filtered cap, 2 μm. Kit includes:
l 004-25030-00 (5 ea.) - O-ring, -030 70 DURO BUNA-N

l 133-25845-01 (1 ea.) - Sample cup, 100 cc, modified for paper filter cap
Internal diameter: 4.62 cm

Usable internal depth: 5.99 cm
l 134-25803-00 (1 ea.) - Filtered cap, 100 cc, 2 μm
134-33012-00 Kit, 10 cc Filtered cap, 0.5 μm. Kit includes:
l 004-25048-00 (5 ea.) - O-ring, BUNA-N, 14 mm ID × 1 mm wide

l 133-25805-03 (1 ea.) - Sample cup, 10 cc, modified for filter caps

l 134-25817-00 (1 ea.) - Filtered cap, 10 cc, 0.5 μm

13 - 4
134-42800-01 (Rev A) — Jan 2016


l 133-25805-03 (1 ea.) - Sample cup, 10 cc, modified for filter caps

l 004-25609-02 (5 ea.) - O-ring, -022, 70 BUNA-N

l 134-25837-00 (1 ea.) - Filtered cap, 100 cc, 35 cc Insert Multvol.
l 135-25804-00 (1 ea.) - Sample cup, 35 cc

Usable internal depth: 3.47 cm *

13 - 5
134-42800-01 (Rev A) — Jan 2016

134-33015-00 Kit, 3.5 cc Filtered cap, 10 μm. Kit includes:
l 004-25878-01 (5 ea.) - O-ring, BUNA-N DURO 70, 12 mm ID × 1 mm

wide
l 134-25820-00 (1 ea.) - Filtered cap, 3.5 cc
l 135-25805-00 (1 ea.) - Sample cup, 3.5 cc

REQUIRED: To be used in conjunction with the 10 cc

Multivolume Kit (Mic P/N 133-33605-00). Must be ordered
separately.

13 - 6
134-42800-01 (Rev A) — Jan 2016

134-33016-00 Kit, 1 cc Filtered cap, 0.5 μm. Kit includes:

l 133-09601-00 (1 ea.) - Tool, 1 cc and 0.08 cc filtered caps, 0.1 cc cup
l 133-25855-00 (1 ea.) - Sample cup, 1 cc

Usable internal depth: 1.12 cm **
l 134-25830-00 (1 ea.) - Filtered cap, 1 cc, 0.08 cc, 0.5 μm
REQUIRED: To be used in conjunction with the

0.08/1 cc Filter Cap Chamber Closure
Assembly (Mic P/N 134-34013-00 shown here).
Must be ordered separately.

13 - 7
134-42800-01 (Rev A) — Jan 2016


l 133-25855-00 (1 ea.) - Sample cup, 1 cc

l 134-25836-00 (1 ea.) - Filtered cap, 1 cc, 0.08 cc, 10 μm


13 - 8
134-42800-01 (Rev A) — Jan 2016

134-33018-00 Kit, 0.08 cc Filtered cap, 0.5 μm. Kit includes:

l 134-25802-00 (1 ea.) - Filtered cap cup, 0.08 cc

l 134-25830-00 (1 ea.) - Filtered cap, 1 cc, 0.08 cc, 0.5 μm


13 - 9
134-42800-01 (Rev A) — Jan 2016

134-33019-00 Kit, 0.08 cc Filtered cap, 10 μm. Kit includes:

l 134-25802-00 (1 ea.) - Filtered cap cup, 0.08 cc
l 134-25836-00 (1 ea.) - Filtered cap, 1 cc, 0.08 cc, 10 μm

Filtered Cup Assemblies (Optional)

133-25862-00 Filtered cup assembly, 10 cm3; used to constrain powdered samples
133-25863-00 Filtered cup assembly, 100 cm3; used to constrain powdered samples

13 - 10
134-42800-01 (Rev A) — Jan 2016

Filtered Cup Assembly Components (for 100 cm3 units only)
004-25299-00 O-ring, size -024 70 DURO BUNA-N

004-27055-00 Paper filter (100 pack)
133-25845-01 Sample cup, 100 cc, modified for paper filter cap
133-25901-00 100 cc sample cup filtered cap
133-25902-00 Spring clip for 100 cc sample cup cap
Gas Accessories
004-25549-00 Reducer, 1/8 in. tube × 1/4 in. tube
004-62150-580 Gas regulator, 1500 psig, CGA 580 (500 psi pycnometer only)
004-62230-58 Gas regulator, 30 psig, CGA 580
134-33020-00 Multigas Manifold; to connect multiple gases to the analysis unit
290-25846-00 Gas inlet line assembly
Keypad Template
134-42701-01 French template
134-42701-02 German template
134-42701-03 Spanish template
134-42701-04 Italian template
Operating Supplies
008-16045-00 High Vacuum grease, Dow Corning

13 - 11
134-42800-01 (Rev A) — Jan 2016

Power Accessories
003-40054-00 AC/DC power supply, external
003-40058-00 AC/DC external power supply, for TEC module on TEC instruments
003-60101-00 Power cord, US, Canada, Japan
003-60101-05 Power cord, Schuko, for European countries
134-34007-00 Power Adapter
Sample Cups
133-25805-00 Sample cup, 10 cm3 capacity
133-25805-02 Sample cup, 10 cm3 capacity, stainless steel
133-25805-03 Sample cup, 10 cm3 capacity, modified for filter caps
133-25845-01 Sample cup, 100 cm3 capacity, modified for paper filter cap
133-25855-01 Sample cup, 0.1 cc capacity

13 - 12
134-42800-01 (Rev A) — Jan 2016

134-25600-00 Sample cup, disposable, 3.3 cm3 capacity (qty. 50)
134-25802-00 Sample cup, .08 cc capacity for filter cap
134-25845-00 Sample cup, 100 cm3 capacity, stainless steel (500 psi model only)
134-25874-00 Sample cup, 2000 cm3 capacity (used with CorePyc)
Usable internal depth: 27.87 cm ***
134-25875-00 Sample cup, 1300 cm3 capacity (used with CorePyc MultiVolume kit)
134-25876-00 Sample cup, 650 cm3 capacity (used with CorePyc MultiVolume kit)
134-33007-00 Disposable Sample Cup Kit, for AccuPyc II (10 cm3) includes chamber insert
for 3.3 cm3 (nominal) disposable aluminum cups, calibration sphere, plus 50
disposable cups.
135-25804-00 Sample cup, 35 cm3 capacity (used with 100 cc MultiVolume kit)
135-25805-00 Sample cup, 3.5 cm3 capacity (used with 10 cc MultiVolume kit)

13 - 13
134-42800-01 (Rev A) — Jan 2016

Software and Manuals
134-20802-00 AccuPyc II Software for Windows
134-20804-00 AccuPyc II Software for Windows (with FoamPyc)
134-20808-00 AccuPyc II Software for Windows (Asphalt)
134-33005-00 Windows Upgrade for FoamPyc; includes software and operator manual
134-42800-00 AccuPyc II Series Operator Manual (includes keypad and software versions,
binder and dividers)
Depth listed is for solid materials. There is a small hole near the top of the cup to allow gas to
*
flow. This feature reduces the useful depth for powders by approximately 2 to 3 mm.
Depth listed is for solid materials. There is a small hole near the top of the cup to allow gas to
**
flow. This feature reduces the useful depth for powders by approximately 1 mm.
Depth listed is for solid materials. There is a lifting notch near the top of the cup. This feature
***
reduces the useful depth for powders by approximately 1.5 cm.

13 - 14
134-42800-01 (Rev A) — Jan 2016
A Calculations
A CALCULATIONS
l Calculations for the 1340 AccuPyc
http://www.micromeritics.com/Repository/Files/Calculations_-_AccuPyc_II_Series.pdf
ANALYSIS
For derivation, see the Sample Volume Equation Derivation section of the AccuPyc II Series
Operator Manual.
10, 100, AND 350 CM3 UNITS

Vx
Vs = Vc − P1
−1
P2
ms
ρs=
Vs
where
Vc = sample chamber volume

Vx = expansion chamber volume
Vs = sample volume
ms = sample mass
ρs = sample density
P1 = gauge pressure after fill
P2 = gauge pressure after expansion
1 CM3 AND 2000 CM3 UNITS

Vs = Vc − Vx P1 − 1
P 
  2 

ms
ρ =
s Vs

A-1
134-42800-01 (Rev A) — Jan 2016
A Calculations

where

Vs = sample volume
ms = sample mass
ρs = sample density
P1 = gauge pressure after fill
P2 = gauge pressure after expansion

A-2
134-42800-01 (Rev A) — Jan 2016
Asphalt Density
ASPHALT DENSITY
Sample volume at 60 °F is found by multiplying the measured volume by the asphalt volume
correction factor.
V(60) = α(T )Vmeasured
where
α(T )= 1.0211326242 − 3.548988118 × 10 4T + 4.498813 × 10−8T 2
and T is the analysis temperature in degrees Fahrenheit.
Sample density at 60 °F is
p(60) = m / V (60 )
Specific gravity at 60 °F is calculated by dividing the adjusted sample density by the density of water
at 60 °F.
SG(60) = p(60) ÷ ρH20 (60)
where
3
ρH20 = 0.990170 g / cm
Note that the density of water at the analysis temperature is not required for this calculation.

A-3
134-42800-01 (Rev A) — Jan 2016
A Calculations
CALIBRATION
Volume calibration uses the ultra-precise method of separate adjustments for the offset and scale
factor.
VOLUME OFFSET
Vc = Vcelprev − Vsampempty
−Vsampempty
is reported as the offset in volume calibration reports.
VOLUME SCALE 

Vc = Vcelprev  Vcalib 
V 
sampball 
 
 
Vx = Vexpprev  Vcalib 
V 
sampball 
 

 Vcalib 
V 
sampball 
  is reported as the scale factor in volume calibration reports.
where

Vcelprev = previously stored cell volume
V = average Vsamp from volume offset calibration analysis (no calibration ball)
sampempty
Vcalib = calibration ball volume

Vsampball = average Vsamp from volume scale calibration analysis (with calibration ball)
Vexpprev = previously stored expansion volume

A-4
134-42800-01 (Rev A) — Jan 2016
FoamPyc Methods
FOAMPYC METHODS
METHOD A: COMPUTED OPEN CELL FRACTION

GeomVol − Vs − VolCellsCutOpen
OpenCellPct = × 100
GeomVol
ResinPlusClosedCellPct = 100 − OpenCellPct
If cell measure is Chord Length,

ChordLength
VolCellsCutOpen = ActiveArea ×
1.14
If cell measure is Diameter,

CellDiam
VolCellsCutOpen = ActiveArea ×
1.4515
METHOD B: MEASURED OPEN CELL FRACTION

VolCellsCutOpen = Vs[1] − Vs[2 ]
ResinPlusClosedCellVol = Vs[1] + VolCellsCutOpen
OpenCellVol = GeomVol − ResinPlusClosedCellVol
ResinPlusClosedCellVol
ResinPlusClosedCellPct = × 100
GeomVol
OpenCellVol
GeomVol
where
Vs[1] = Vs from the first analysis (before recutting)

V [2] = V from the second analysis (after recutting)
s s
Vs[1] = Vs from the first analysis (before recutting)

A-5
134-42800-01 (Rev A) — Jan 2016
A Calculations
METHOD C: UNCORRECTED OPEN CELL FRACTION

OpenCellVol=GeomVol − Vs
OpenCellVol
GeomVol
METHOD D: COMPRESSIBILITY TEST

Quantities appended with [i] are for cycle i, where i goes from 1 up to the number of cycles.
Vsi − 1 − Vs[i]

∆V [i ] =
P1 P1[i − 1] − P1[i]
Vsi − 1 − Vs[i]

∆V [i ] =
P2 P2[i − 1] − P2[i]
AvgVolChangeP1 = avg(∆VP1[i ]) for all included i
AvgVolChangeP2 = avg(∆VP2 [i ]) for all included i

AvgVolChangeP1
PctAvgVolChangeP1 = × 100
GeomVol
AvgVolChangeP2
PctAvgVolChangeP2 = × 100
GeomVol
METHOD E: FRACTURE TEST

∆Vol = Vs[3 ] − Vs[1]
∆Vol
PctFracturedCells = × 100
GeomVol
where
Vs[1] = Vs for the first (prefracture) cycle

Vs[3] = Vs for the third (postfracture) cycle

A-6
134-42800-01 (Rev A) — Jan 2016
Geometric Volume and Active Area
GEOMETRIC VOLUME AND ACTIVE AREA

Geometric volume of the sample is calculated based on the sample shape; for Method A, Active area
is also calculated.
CUBE
3
GeomVol = EdgeLength × NumPieces
2
ActiveArea = EdgeLength × (6 − NumSk ins ) × NumPieces
CYLINDER
Diam2
GeomVol = π × × Height × NumPieces
4
π
ActiveArea = π × Diam × Height + 
2
× (2 − NumSk ins ) × NumPieces
× Diam 

 4

RECTANGLE
GeomVol = LongEdge × ShortEdge × RemainEdge × NumPieces
ActiveArea = [(LongEdge × RemainEdge × (2 − NumLargeSk ins ) + ShortEdge × RemainEdge ×

(2 − NumSmallSk ins ) + LongEdge × ShortEdge × (2 − NumRemainSk ins )] × NumPieces
PERCENT POROSITY
percent porosity = (ρs − ρ ) ÷ ρs

A-7
134-42800-01 (Rev A) — Jan 2016
A Calculations
RESIN VOLUME
ms
ResinVol =
ResinDensity
ResinVol
ResinVolPct = × 100
GeomVol
where
ms = sample mass
RUN PRECISION
Run precision requires at least five runs. Run precision criterion is met when the sample volumes
calculated for the four most recent previous runs fall within the specified error band for the current
run’s sample volume. The error band is a specified percentage of the nominal volume of the sample
chamber (1, 10, 100, 350 and/or 2000 cm3).
Vs[0] to Vs[4] are the five most recent sample volumes, Vs[4] being the most recent.
V
ErrBand = PctFullScale × nominal
100
where
Vnom- = nominal sample cell volume

inal
If
( Vs[i ] − Vs[4 ] ≤ ErrBand) for i = 0 to 3, run precision is achieved.

A-8
134-42800-01 (Rev A) — Jan 2016
SPC Report Variables
SPC REPORT VARIABLES
REGRESSION CHART VARIABLES

The line of best fit for the Regression Chart is calculated by the usual least squares method. 1 ) If
there is only a single point or all N points have the same x-value, there can be no line of best fit in the
standard form.
Σχi
χ =
N
Σ yi
y =
N
Slope =
(
Σ χi − χ )(yi − y )
(
Σ χi − χ 2 )
Intercept = y − Slope  x
The coefficient of correlation for this line is also calculated in the usual way. 2 )
σχ =
σy =
Cov(x, y ) =
( )(
Σ x i − x yi − y )
N
Cov(x, y )
Correlation Coeff =
σxσ y
1 ) BASIC Scientific Subroutines Vol II, by F.R. Ruckdeschel, Copyright 1981 BYTE
Publications/McGraw Hill, p. 16.
2 ) Mathematical Handbook for Scientists and Engineers, G.A. Korn and T.M. Korn, McGraw
Hill, Sec. 18.4. (1968)

A-9
134-42800-01 (Rev A) — Jan 2016
A Calculations
CONTROL CHART VARIABLES

Σyi
Mean =
N
Standard Deviation =
N−1
C. V.= StdDev
Mean
+ n σ = Mean + n Standard Deviation
− n σ = Mean − n Standard Deviation
SPECIFIC GRAVITY
SG = ρs ÷ ρw
where
ρw = water density at analysis temperature
TOTAL PORE VOLUME

Total pore volume is per gram of sample.
ρ − ρbulk
TotalPoreVol = s
ρs × ρbulk
where
ρbulk = entered bulk density

A - 10
134-42800-01 (Rev A) — Jan 2016
Total Solids Concentration
TOTAL SOLIDS CONCENTRATION

ρliq ρsol
WeightPctSolids = 1 − × × 100
ρs ρsol − ρliq
where
ρliq = entered liquid density ρsol
= entered solid density ρs =

sample density

A - 11
134-42800-01 (Rev A) — Jan 2016
B Error Messages for the 1340 AccuPyc
B ERROR MESSAGES FOR THE 1340 ACCUPYC

See Error Messages for the 1340 AccuPyc Keypad Only on page B - 21
2201 | Cannot execute report subsystem.
Cause: Start Report failed to execute the report subsystem (which is a separate
process).
Action: Restart the computer. If the problem persists, reinstall the application (this will
not affect any of your sample files). Contact a Micromeritics service rep-
resentative if this error message continues.
2204 | Communication attempt with [n] failed [n]. Please check application directory for
file.
Cause: A file necessary for reporting is missing.

Action: Re-install the software.
2401 | FATAL ERROR.
Cause: An internal processing and/or hardware error has occurred during

communication with the analyzer.
Action: Contact your Micromeritics service representative.
2430 | Error accessing file [n], error code = [n].
Cause A: Media may be damaged.

Action A: Clean the media drive. If this does not eliminate the problem, attempt operation
using a backup copy of the file.
Cause B: Hard disk may be damaged.
Action B: Contact your Micromeritics service representative.
Cause C: A software error occurred when the file was accessed.
Action C: Contact your Micromeritics service representative.
Cause D: The file name specified contains one or more invalid characters.
Action D: Enter a valid file name. Do not use characters such as * or ?. Refer to the oper-
ating system manual.
2431 | Error writing file [n], error code = [n].
Cause A: User logged onto a computer that does not have Write permissions.
Action A: Contact your IT department to change user permissions.

B-1
134-42800-01 (Rev A) — Jan 2016
Cause B: Insufficient hard disk to perform the operation.

Action B: Copy files not used regularly to the hard disk external media. Delete them from
the hard disk, and then try the operation again.
2432 | Invalid response from MMI ‘FILE_READ’ request.
Cause: An internal processing and/or hardware error has occurred.

Action: Contact a Micromeritics service representative if this error message continues.
2433 | New entries have been found in this directory. Refresh the directory information?
Cause: Several analyzer files (sample information, analysis conditions, adsorptive prop-
erties, or report options) have been added to this directory by some function
other than the analyzer program.
Action: Click Yes to update the directory information with data from each new file. This
operation may take a minute.
Click No to locate the file manually. This option may be feasible if a large
number of files have been copied into the directory and the file name is known.
2434 | File [n] — Subset [n] wrote wrong [n] of data, expected [n] bytes.

2436 | Path specification [n] is invalid.
Cause: An invalid path name and/or extension was entered.

Action: Type a valid path name (including the proper extension), then press Enter.
2437 | File name [n] does not exist.
Cause: The overlay file selected in the report option does not exist.
Action: Enter an existing file specification, or select a file name from the list box.
2439 | Could not register file.
Cause: An unexpected error occurred when trying to access a data file.

2440 | Subset not found.


B-2
134-42800-01 (Rev A) — Jan 2016
2441 | Seek within file failed.

2442 | Bad header in subset file.

2443 | Subset owner denied access.

2444 | Not a valid file format.

2445 | Subset wrote the wrong amount of data.

2446 | Error reading data.

2447 | Error writing data.
Cause: An unexpected error occurred when you tried to access a data file.
2448 | Basic Mode default parameter file directory [n] is invalid. Resetting to the install-
ation directory.
Cause: A working directory specified in the .INI file is invalid, has been moved, or has
been deleted.
Action: The installation directory will be substituted. The next time a file is opened, use
the directories list to move to the correct directory.
2448 | Default Adsorptive Properties directory [n] is invalid. Resetting to the installation

B-3
134-42800-01 (Rev A) — Jan 2016
directory.
been deleted.
2448 | Default parameter file directory [n] is invalid. Resetting to the installation directory.
been deleted.
2448 | Default report options directory [n] is invalid. Resetting to the installation dir-
ectory.
been deleted.
2448 | Default sample file directory [n] is invalid. Resetting to the installation directory.
been deleted.
2448 | Default script test file directory [n] is invalid. Resetting to the installation directory.
been deleted.
2448 | The reference file directory [n] cannot be used. Resetting to the installation dir-
ectory.
been deleted.
2448 | The z-table file directory [n] cannot be used. Resetting to the installation directory.

B-4
134-42800-01 (Rev A) — Jan 2016
been deleted.
2449 | This field does not contain a valid file specification.
Cause: An invalid file name was entered.

Action: See the description of file naming conventions in a Windows manual, then re-
enter the name.
2450 | Sample Defaults may not be edited while this operation is in progress. Do you
wish to save and close the Sample Defaults edit session?
Cause: An automatic analysis (an analysis in which sample files are created using the
defaults) was processing while editing the defaults.
Action: Finish the edit session of the defaults, close the window, then restart the
automatic analysis.
2452 | Attempt to write MICATTR.DIR in read only mode. [n]
Cause: The Read-Only attribute is turned on in the application’s MICATTR.DIR file (this
file exists in each folder containing sample or parameter files).
Action: Use Windows Explorer to access the folder containing the MICATTR.DIR file,
then disable the Read-Only option.
2453 | Attempt to append MICATTR.DIR in read only mode. [n]
Cause: The Read-Only attribute is turned on in the application’s MICATTR.DIR file (this
file exists in each folder containing sample or parameter files).
Action: Use Windows Explorer to access the folder containing the MICATTR.DIR file,
then disable the Read-Only option.
2454 | Too many selections for a print-to-file operation. Only the first (number) selections
will be processed. Please reselect the remainder.
Cause: Too many files were selected for this operation.

Action: Select only the number of files specified in the message.
2455 | Too many selections for an export-to-file operation. Only the first (number) selec-
tions will be processed. Please reselect the remainder.
Cause: Too many files were selected for this operation.

Action: Select only the number of files specified in the message.

B-5
134-42800-01 (Rev A) — Jan 2016
2456 | Insufficient file handles available. Application cannot continue.
Cause: More than 50 files are open at the same time.

Action: Refer to an operating system manual then set the limit for open files to 50 or
greater. Alternatively, close any unused open files.
2457 | Results cannot be displayed. More than [n] windows are currently displaying or
printing results.
Cause: Too many windows are open in the application.

Action: Close some of the open windows.
2458 | An instrument is performing a critical operation. Wait a few moments before exit-
ing the application.
Cause: An attempt was made to exit the application while the instrument was per-
forming a critical operation. This operation must be completed before the applic-
ation can be exited.
Action: Wait a short time and attempt to exit the application again.
2459 | An instrument is busy. A delay in restarting this application could result in loss of
new data. Continue with program Exit?
Cause: An attempt was made to exit the application while an analysis was in progress.
While this is possible, the data collected when the application is inactive will not
be permanently recorded until the application is re-started. A power failure to
the instrument could cause some data to be lost.
Action: If not concerned with the potential for loss of data should a power failure occur,
click Yes to continue; otherwise, click No.
2460 | Fatal Communications error on [n].
Cause: There was a fatal error in communication between the application and the
software in the instrument. All displays for that instrument will be closed.
Action: Ensure that the analyzer is connected to the computer on the communications
port configured in the Setup program. Stop and restart the analyzer software.
Contact your Micromeritics service representative.
2461 | No instruments are in operation. This application will unconditionally terminate.
Cause: At least one instrument must be active for the application to operate. The
initialization of all of the instruments configured with the Setup program has
failed. The application stops.
Action A: Usually this message is preceded by another message giving the reason for the

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instrument’s failure to initialize. Refer to the instructions for that message.

Action B: Ensure that the instrument is attached to the computer on the communications
port configured with the Setup program. Verify that the instrument's power
switch is in the ON position and that the light on the front panel is illuminated.
Contact a Micromeritics service representative if this error message continues.
2477 | [n] did not properly initialize.
Cause: The software was unable to initialize this instrument. This is usually caused by
one of the conditions listed in the previous error messages.
Action A: Run the Setup program and ensure that a valid port is specified; if not, specify a
valid one when prompted.
Action B: Reinstall the software, then restart application.
Action C: Contact a Micromeritics service representative if this error message continues.
2478 | Error copying sequential data segment.
Cause: An internal processing and/or hardware error occurred while accessing a

portion of a sample file.
Action: Confirm that the media being accessed does not contain errors. Contact your
Micromeritics service representative.
2479 | The instrument is busy performing an operation of which this application is

unaware. Do you want to cancel? [Yes, No]
Cause: During initialization of the application, the status of the analyzer was found to be
in a different state than expected.
Action: Click Yes to cancel the operation in process and allow the analyzer to reset,
then continue with initialization. Click Noto cancel the initialization process.
If this error message continues, verify that files in the application directory
structure are not being changed or removed.
2480 | File [n] cannot be analyzed. It is currently being edited.
Cause: An attempt was made to start an analysis using a file that is open for editing.
Action: Finish editing the file, save and close it, then start the analysis.
2481 | Error accessing the sample information file [n].
Cause: An unexplained error prevented access to this file.

Action: The hard disk drive may be corrupt. Run diagnostics.

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2482 | File cannot be opened for writing.
Cause: An attempt was made to open a file currently being used.

Action: Locate the application using the file (in the Micromeritics application, use the
Windows menu item to get a list of all open windows, one of which may contain
this file).
2483 | An analysis cannot be performed on [n]. It is open for editing and contains errors.
Cause: An attempt was made to use a sample file containing errors that is currently
open.
Action: Go to the window containing the file, correct the errors, then save it.
2484 | The edit session for [n] must be saved before the analysis. Save changes and con-
tinue with the analysis?
Cause: An attempt was made to start an analysis using a file that contains unsaved
changes and is open for editing.
Action: Click Yes to save the changes, then proceed with the analysis. Click No to
cancel the analysis, then continue editing the Sample Information file.
2485 | The service test file has an invalid status and cannot be used for this analysis.
Cause: The selected file has a status other than No Analysis.

Action: Select a different service test file, or create a new one and use Replace All to
copy parameters from the file originally selected.
2486 | Could not construct [n] report type. Program will terminate.
Cause A: Full rights to the application’s folders and files is required.

Action A: Contact a system administrator to have full rights granted.
Cause B: An internal processing and/or hardware error has occurred.
2487 | Could not start report generator. Error code [n]. Program will terminate.
Cause A: Full rights to the application’s folders and files is required.

Action A: Contact a system administrator to have full rights granted.
Cause B: An internal processing and/or hardware error has occurred.
2488 | File [n] cannot be opened for editing.

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134-42800-01 (Rev A) — Jan 2016
Cause: The specified file is being used in another edit operation.

Action: Check the Windows list to locate the other edit session.
2489 | File [n] cannot be opened for writing.
Cause: The specified file in a Save As operation is already open for edit.
Action: Select a different file for the Save As operation.
2490 | No ‘.INI’ file present. Application will terminate.
Cause: The ASCII .INI file containing initialization information and system options
information used during program startup does not exist.
Action: Restore the .INI file from back-up, or re-install the software.
2491 | Highlighted fields contain errors. Please correct the errors before dialog box.
Cause: The fields highlighted in red contain invalid entries. The window cannot be
closed until all errors are corrected.
Action: Check the entries, correct the errors, then close the window.
2492 | This field’s entry is invalid.
Cause: The highlighted field contains an invalid entry.

Action: Check the entry and correct the error.
2493 | An entry is required for this field.
Cause: This field requires a valid entry to proceed.

Action: Enter or select an appropriate value.
2494 | Value is out of the valid range.
Cause: The entered value in the highlighted field is outside the valid range of values.
Action: Check the entry, then either enter or select an appropriate value.
2495 | Value is out of the valid range. Enter a value between [n] and [n].
Cause: The entered value in the highlighted field is outside the valid range of values.
Action: Check the entry, then either enter or select an appropriate value.
2496 | Invalid number.

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Cause: An invalid number was entered in the highlighted field.

Action: Check the entry, then either enter or select a valid number.
2497 | This field contains an invalid character.
Cause: An invalid character was entered in the highlighted field.

Action: Check the entry, then enter valid characters.
2498 | The requested change to the Sample’s status is invalid at this time.
Cause: A request to change the file’s status, for example, from automatically collected
to manually entered could not be done.
Action: Contact your Micromeritics service representative. Record the name of the
sample file in which the problem occurred.
2499 | Sequence number must contain at least 3 digits.
Cause: An attempt was made to enter a sequence number that did not contain at least
three digits.
Action: Enter a sequence number that contains at least three digits.
2500 | All sample file names that can be created using the sequence number pattern
already exist. You may want to modify the next sequence number.
Cause: No more sample information files can be created using the currently entered file
name sequence number.
Action: Go to Options > Default Method, then enter another sequence number.
2501 | System resources have reached a dangerously low level. Please close some win-
dows to avoid the loss of data.
Cause: A large number of windows are open and consuming the system resources
available to all applications.
Action: Close one or more windows. Contact your Micromeritics service representative.
2502 | Error writing to file [n] during print. Error code [n].
Cause: An error occurred in the file being written to during a print operation.
Action: Ensure there is sufficient space on the drive containing the file.
2503 | Error converting file [n]. Cannot create DIO intermediate file.
Cause: An error occurred while printing a report to file.

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Action: An attempt was made to replace a file that is read only or the computer login
does not have permission to do so. Contact your IT Department.
2504 | Cannot create output file for sample [n].
Cause: There may be insufficient disk space.

Action: Ensure that sufficient space is available. Contact a Micromeritics service
representative if this error message continues.
2505 | Error logger cannot be initialized. Error code [n]. Program will exit.
Cause: An internal processing error has occurred.

2506 | Output device [n] is not installed. Printing cannot be accomplished.
Cause: An internal processing error has occurred.

2508 | Overlay [n] was not found. It will not be included in the reports.
Cause: The specified overlay file could not be found.

Action: Ensure the file specified as an overlay exists.
2509 | Error opening file [n]. Reports cannot be produced.
Cause: An error occurred while the program was opening a file necessary to the report
operation.
Action: Use the name given in the error message to investigate. Contact your Micro-
meritics service representative.
2510 | Error parsing reports from file [n]. Reports cannot be produced.
Cause A: One or more data entry fields in the sample file may contain an invalid character
(such as a single quote or double quotes).
Action A: Review the data entry fields (for example, the Sample field), then remove the
invalid character.
Cause B: The system was unable to create the usual temporary files during the report,
possibly due to insufficient disk space.
Action B: Check the space available on the hard disk.
Cause C: An internal processing error occurred.
Action C: Contact your Micromeritics service representative.

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2511 | Print job [n] has been canceled due to insufficient disk space. Delete unnecessary
files and restart the report.
Cause: The disk drive does not have required space for the temporary file.
Action: Delete unnecessary files from the disk. At least five megabytes of free space is
required for normal operation.
2512 | Print job [n] canceled.
Cause: The print job was canceled by the operator.

Action: None required.
2513 | Unable to read the calibration file [n].
Cause: An invalid calibration file was selected or cannot be read.

Action: Ensure the media containing the calibration file has no problems.
2514 | Unable to write the calibration file [n].
Cause: An attempt to save calibration data has failed due to possible media problems.
Action A: Ensure the destination location has no problems.
Action B: Choose an alternate media to save the calibration data.
2515 | Warning: Changing the calibration information will affect the performance of the
instrument. Only qualified service personnel should do this. Do you wish to proceed?
Cause: The process of performing a calibration operation was started.

Action: Calibration operations should only be done by or under the direction of qualified
service personnel.
2516 | Warning: Keeping a backup copy of the calibration data is recommended by Micro-
meritics. Would you like to do so now?
Cause: A calibration operation was performed and a backup copy is recommended.

Action: Go to Unit [n] > Calibration > Save to File to perform a calibration save
operation.
2517 | Canceling this dialog will reset the calibration state to what it was when this dialog
was first opened. Are you sure you want to cancel?
Cause: The calibration has not been accepted.

Action: If the calibration operation was successful, click Accept.
2520 | No data points available for reporting.

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134-42800-01 (Rev A) — Jan 2016
Cause: The selected sample file does not have collected data and cannot be used for
reporting.
Action: Select a different sample file.
2521 | Unable to program controller.
Cause: A hardware malfunction has occurred.

2522 | Invalid controller application file.
Cause: The application’s control file has been corrupted or deleted.

Action: Reinstall the analysis program.
2523 | Programming controller failed.

2524 | CRC check failed on programming controller.

2525 | Unknown error programming controller.

2526 | Controller download was not successful.

Action A: Contact your Micromeritics service representative.
2527 | Controller CRC error on boot block.

2528 | Controller DRAM error.


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2529 | Controller Com 1: error.

2530 | Controller Com 2: error.

2531 | Controller debug port error.

2532 | The instrument contains a different software version. Do you want to reset it?
Cause: The application has discovered a different version of software operating in the
analyzer.
Action: If there are no analyzers other than the one connected to the computer, click
Yes, then allow the updated software to load.
2533 | Analyzer initialization failed.

2534 | Error opening file[n] for printing. Error Code [n].
Cause: An error occurred in the selected file for print output.

Action: Ensure that sufficient disk space is available.
2548 | System status [n] [n].
Cause: There was a problem establishing communication with the analyzer.

Action: Ensure that the communications cable is seated firmly in the Ethernet slot at the
analyzer connection and the computer connection. Contact your Micromeritics
service representative.
2549 | Error accessing online manual file [n].
Cause: The operator’s manual file could not be located.

Action A: Reinstall the application.

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Action B: Copy the contents of the manual folder from the setup media to the application
directory.
2550 | Attempts to acquire the instrument’s status timed out.
Cause: There was a problem establishing communication with the analyzer.

Action: Ensure that the communications cable is seated firmly in the Ethernet slot at the
analyzer connection and the computer connection. Contact your Micromeritics
service representative.
2551 | Cannot access web page [n].
Cause: The Micromeritics web page for DFT models cannot be accessed. This could be
caused by an ISP problem of high internet traffic.
Action: Try the operation later.
6000 | An error occurred while loading the application control information. Data entry
cannot be performed. (Code [n]).
Cause: An error occurred accessing the control information disk file required by this
application.
Action: The disk drive may have failed or be corrupt. Run diagnostics on the disk drive.
6001 | Unable to establish the TCP connection with the instrument.
Cause: A communications problem between the computer and the analyzer has
occurred.
Action A: Check the cable connection between the computer and the analyzer
Action B: Go to Unit [n] > Unit Configuration and verify that the TCP/IP configuration
for the computer and the analyzer are correct.
Action C: Exit the application, and turn off the analyzer. Then turn on the analyzer and
restart the application. Contact a Micromeritics service representative if this
error message continues.
6002 | Configured serial number does not match instrument.
Cause: An incorrect serial number was entered when installing the software.
Action Exit the application. Access the Setup program and remove the incorrect ana-
lyzer. Then use the Add an Analyzer option in the Setup program to add the cor-
rect serial number for the controlling unit. Contact a Micromeritics service
representative if this error message continues.
6003 | The instrument [n] is not calibrated.

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134-42800-01 (Rev A) — Jan 2016
Cause: Calibration data for the selected unit was not found
Action: Go to Unit > Calibration. Select the appropriate Calibration menu item or load
a saved calibration.
6110 | Error accessing the sample information file [n].
Cause: There was an error opening a file.

Action: Code 5: There is a problem with the computer login permissions. Consult your
IT department.
Code 2: File not found. Select a different file name.
6111 | File [n] cannot be analyzed. It is currently being edited.
Cause: An open file was selected. This message is informational-only.

Action: Click OK to close the error message window. Then continue editing the file,
save and close it; or click Browse and choose a different file.
6112 | File [n] cannot be opened. It is currently being setup for analysis.
Cause: An open file was selected that is currently being used for analysis.
Action: Select a different file.
6113 | An analysis cannot be performed on [n]. It is open for editing and contains errors
Cause: The selected analysis file contains errors and is open for editing.
Action: Finish editing the file, save, and close it, or choose a different file. Then restart
the analysis.
6114 | The edit session for [n] must be saved before the analysis. Save changes and
proceed with the analysis?
Cause: An attempt was made to start an analysis using a file that contains unsaved
changes and is still open.
Action: Click Yes to save the changes and proceed with the analysis. Click No to can-
cel the analysis and continue editing the file, save and close it; or click Browse
and choose a different file.
6120 | Unable to read the calibration file [n].
Cause: The selected calibration file is not valid or cannot be read.

Action: Ensure the media containing the calibration file has no problems.
6121 | Unable to write the calibration file [n].

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134-42800-01 (Rev A) — Jan 2016
Cause: An attempt to save calibration data has failed due to possible media problems.
Action A: Confirm the media containing the calibration file has no problems.
Action B: Choose an alternate media to save the calibration data.
6122 | File contains calibration data for a different unit [n].
Cause: A calibration file from a different unit was loaded.

Action: Load a file for the current unit or go to Unit > Calibration and select the appro-
priate menu item.
6123 | The device has no calibration data for the selected insert.
Cause: A calibration report was produced for an insert that has not been calibrated.
Action: Perform a volume calibration for the insert or produce a report for a different
insert.
6126 | The cell and expansion volumes must be positive. Enter positive values and
recalibrate.
Cause: According to the calibration data, the cell volume or expansion volume for the
selected insert is zero or a negative value
Action: Perform these steps:
1. Select Setup > Calibration Data.

2. In the Cell volume field, enter the volume of the sample cell (or insert).
3. In the Expansion volume field, enter half of the sample cell volume.
4. Perform a volume calibration.
6127 | The entered calibration volume is < 10% of the cell volume. The resulting
calibration may be inaccurate.
Cause A: An incorrect volume was entered for the calibration standard.

Action A: Correct the volume entry.
Cause B: The calibration standard is too small for the cell.
Action B: Use a larger calibration standard.
6160 | Device in recognizable state. Analysis canceled.
Cause: The application was closed during an analysis. When the application was restar-
ted, the analysis had been canceled.
Action: None required. The data collected up to the point of cancellation is saved in the
sample file.

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6161 | The sample file [n] is already present in the sequence.
Cause: An attempt was made to insert an existing file into the Sample File list.
Action: None required. The same file cannot be inserted into the list multiple times.
6162 | The sequence list is full.
Cause: An attempt was made to add another file to the Sample File list for sequenced
analyses when the list already contains eight entries.
Action A: Run the sequence analysis with the current list and include the preferred file in
the next sequence analysis.
Action B: Remove one of the files from the list, then add the preferred file.
6163 | The sample file has an invalid status and cannot be used for analysis.
Cause: A sample file with a status other than No Analysis was selected.
Action: Select a sample file that has not been used in an analysis.
6164 | FoamPyc analyses cannot be done on a 1 cm3 unit.
Cause: An attempt was made to perform a FoamPyc analysis on a unit that does not
support it. FoamPyc analyses cannot be performed on a unit with a 1 cm3 or 2L
sample cell.
Action A: Start the analysis on a different unit.
Action B: Close the analysis window, open the sample file, and select Standard Method.
Then restart the analysis.
6165 | Failure to fill sample cup.
Cause: There was insufficient pressure to allow filling within five minutes during an ana-
lysis
Action: Increase the regulator pressure or, if there is insufficient helium in the tank,
obtain a new tank of helium.
6166 | Pressure overrange.
Cause A: A pressure overrange occurred during an analysis because the regulator pres-
sure is set too high.
Action A: Adjust the pressure so that it is equal to the higher of the two fill pressures spe-
cified in the analysis parameters plus 2.0 psig.
Cause B: A pressure overrange occurred during an analysis because an error occurred in
the pressure measurement electronics.

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134-42800-01 (Rev A) — Jan 2016
6167 | Pressure underrange
Cause: A pressure underrange occurred during an analysis because an error occurred

in the pressure measurement electronics.
6168 | Pressure failed to equilibrate.
Cause A: The sample being analyzed failed to equilibrate in 1000 seconds.

Action A: Check the system carefully for leaks following the instructions in the instrument
operator manual. Ensure the sample is properly prepared before performing an
analysis.
Cause B: Sample (foams, organics, etc.) absorbs helium slowly.
Action B: Set the equilibration rate to progressively higher values until reasonable equi-
libration times (15 sec to 120 sec) are achieved.
6169 | The instrument lost power during analysis.
Cause: A power failure occurred and when power resumed, the automatic operation
was canceled.
Action: Restart the automatic operation.
6170 | The measured volume is < 10% of the cell volume. Results may be inaccurate.
Cause: Not enough sample was placed in the sample cup to give an accurate reading.
Action: Rerun the sample using enough material to occupy the maximum amount of the
nominal cell chamber volume
6171 | Valve failed to respond.
Cause: The instrument valves failed to operate.

6200 | At least one report item must be selected. Press Cancel if you do not want a report.
Cause: No reports were selected in the Selected Reports list. No output could be pro-
duced.
Action: Ensure that at least one report is selected for the sample and re-submit the
sample for reporting, or click Cancel.
6201 | No data available in [n] for reporting.

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134-42800-01 (Rev A) — Jan 2016
Cause: The requested report file does not contain collected data.
Action: Use the file in an analysis before requesting reports.
6202 | Total solids concentration is invalid; liquid density is greater than or equal to solids
density.
Cause: A report was requested on a file containing invalid densities for Total Solids Con-
centration.
Action A: Specify appropriate densities for liquid and solids.
Action B: Do not request that total solids concentration be reported.

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ERROR MESSAGES FOR THE 1340 ACCUPYC KEYPAD ONLY

Press CHOICE to cycle through the messages and data. To delete the message, press CLEAR.
Messages that are not cleared will remain in the queue until the next analysis or calibration is
performed; at that time, any remaining messages will be cleared automatically.
l NN = Number of cycles completed

l ZZ = Number of cycles requested
Add Unit
Cause A: A new analysis module has been attached to the instrument where previously a
different module had been attached.
Action A: Press Choice and select Yes to add the new analysis module.
Cause B: An incorrect serial number was read by the analysis module.
Action B: Press Choice and select No to use the serial number and calibration inform-
ation stored in the command module. Contact a Micromeritics service rep-
resentative if this error message continues.
ANLSERR: Eq failure — NN/ZZ cycles completed
Cause A: The sample being analyzed failed to equilibrate in 1000 seconds.

Action A: Check the system carefully for leaks following the instructions in the instrument
operator manual. Ensure the sample is properly prepared before performing an
analysis.
Cause B: Sample (foams, organics, etc.) absorbs helium slowly.
Action B: Set the equilibration rate to progressively higher values until reasonable equi-
libration times (15 sec to 120 sec) are achieved.
ANLSERR: Fill failure — NN/ZZ cycles complete
Cause: There was insufficient pressure to allow filling within five minutes during an ana-
lysis
Action: Increase the regulator pressure or, if there is insufficient helium in the tank,
obtain a new tank of helium.
ANLSERR: Overrange — NN/ZZ cycles completed
Cause A: A pressure overrange occurred during an analysis because the regulator pres-
sure is set too high.

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Cause B: A pressure overrange occurred during an analysis because an error occurred in
the pressure measurement electronics.
ANLSERR: Underrange — NN/ZZ cycles completed
Cause: A pressure underrange occurred during an analysis because an error occurred

in the pressure measurement electronics.
Automatic operation has been canceled
Cause: The automatic operation has been canceled.

Action: Wait for the termination process to complete or end the termination process by
pressing Alt + CLEAR two more times.
CAL_ERR: Reset Pressure Cal. ?
Cause: The calibration information could not be read from the command or analysis
module.
Action A: Select Yes and press Enter to reset the pressure and temperature calibration
to nominal values. Resetting to nominal may restore normal readings but a
proper calibration should be performed by a service technician.
Action B: Select No to avoid resetting the calibration. The instrument will be unre-
sponsive.
CAL_ERR: Temperature Calibration Failed
Cause: The temperature calibration was unsuccessful.

CAL1ERR: Eq failure — NN/ZZ cycles complete
Cause: The empty cell chamber failed to equilibrate in 1000 seconds during the first
pass of calibration.
Action: Check the system for leaks.
CAL1ERR: Fill failure NN/ZZ cycles completed
Cause: There was insufficient pressure to allow filling within five minutes during the first

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Action: Open the tank valves if shut, increase the regulator pressure or, if there is insuf-
ficient helium in the tank, obtain a new tank of helium. Tank pressure should be
at least 200 psi above regulator pressure.
CAL1ERR: Overrange — NN/ZZ cycles completed
Cause A: A pressure overrange occurred during the first pass of calibration because the
regulator pressure is set too high.
Action A: Adjust the pressure so that it is equal to the higher of the two fill pressures
specified in the analysis parameters plus 2.0 psig.
Cause B: A pressure overrange occurred during the first pass of calibration because an
error occurred in the pressure measurement electronics.
CAL1ERR: Underrange — NN/ZZ cycles complete
Cause: A pressure underrange occurred during the first pass of calibration because an
error occurred in the pressure measurement electronics.
CAL2ERR: Eq failure — NN/ZZ cycles completed
Cause: The calibration standard failed to equilibrate in 1000 seconds during the second
Action: Check the system for leaks.
CAL2ERR: Fill failure — NN/ZZ cycles completed
Cause: There was insufficient pressure to allow filling within five minutes during the
second pass of calibration.
Action: Open the tank valves if shut, increase the regulator pressure or, if there is insuf-
ficient helium in the tank, obtain a new tank of helium. (Tank pressure should be
at least 200 psi above regulator pressure.)
CAL2ERR: Overrange — NN/ZZ cycles completed
Cause A: A pressure overrange occurred during the second pass of calibration because
the regulator pressure is set too high.
Cause B: Adjust the pressure so that it is equal to the higher of the two fill pressures spe-

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CAL2ERR: Underrange — NN/ZZ cycles completed
Cause: A pressure underrange occurred during the second pass of calibration because
an error occurred in the pressure measurement electronics.
DATA_ERR: Chamber volumes must be > 0
Cause: According to the calibration data, the cell volume or expansion volume for the
selected insert is zero or a negative value
Action: Perform these steps:
1. Select Setup > Calibration Data.

2. In the Cell volume field, enter the volume of the sample cell (or insert).
3. In the Expansion volume field, enter half of the sample cell volume.
4. Perform a volume calibration.
DATA_ERR: No data to compute
Cause A: An automatic operation was canceled before a complete cycle could be com-
pleted.
Action A: Restart the automatic operation.
Cause B: All the cycles have been excluded in review mode.
Action B: Return to review mode and include some cycles.
DTA_WRN: Cal std — 10% of full-scale
Cause A: You entered a value for the calibration standard that was less than 10% of the
nominal cell chamber volume. Resulting data may be inaccurate.
Action A: Be sure you enter the value recorded on the Calibration Standard case.
Cause B: You used an inappropriate calibration standard for the nominal cell chamber.
Action B: Use a calibration standard of sufficient size (calibration standards are available
from Micromeritics). The calibration standard should occupy at least 10% of the
nominal cell chamber volume and the more nearly filled the cell is, the better the
calibration.
DTA_WRN: Volume — 10% of full-scale
Cause: There was not enough sample placed in the sample cup to give an accurate
reading.
Action: Rerun the sample using enough material to occupy the maximum amount of the
nominal cell chamber volume.

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HW_ERR: Calibration could not be read
Cause: The calibration information could not be read from the command or analysis
module.
Action: Close the application and cycle power on the instrument. Contact a Micro-
meritics service representative if this error message continues.
MAN_ERR: Pressure overrange
Cause: The fill valve was left open until the maximum system pressure was exceeded.
Action: Close the fill valve and open the vent and expansion valves. Allow the pressure
to stabilize.
No A.C. Found
Cause: The control module cannot detect an analysis module.

No collected data to report, or all cycles excluded
Cause: You requested a report in which there is either no data available or data have
been excluded via review mode.
Action: Initiate an automatic operation or return to review mode and include at least one
cycle.
Printer port not responding
Cause: Printer port not responding

Action: Check to make sure the printer is properly connected to the pycnometer, is
turned on, and is online.
Queuing print job [ESCAPE] to cancel
Cause: Status message displayed when a report is being printed.

Action: None; this is a status message only.
Reset to factory defaults
Cause: The . (period) key was pressed at startup and the instrument was reset. Data
files and HTML reports have been erased. Setup options have been returned to
default values.
Action: Review setup options.
Sending line (line number) [ESCAPE] to cancel

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Cause: Status message displayed when data are being transmitted.

Action: None; this is a status message only.
SYS_ERR: Power Fail — NN/ZZ Cycles Completed
Cause: A power failure occurred and when power resumed, the automatic operation
was canceled.
Action: Restart the automatic operation if desired.
Transmission port not responding
Cause: The receiving device took longer than five seconds to acknowledge receipt of
data from the pycnometer.
Action: Make sure the receiving device is properly connected to the pycnometer RS-
232 port and is turned on. Verify that the serial I/O parameters controlling the
receiving device correspond with the data transmission parameters in the set up
mode.
Transmission port waiting for Xon
Cause: The receiving device stopped transmission by sending an Xoff, and hasn’t
resumed the transmission by sending an Xon.
Action: None; when the receiving device is ready for more data, it should send the
pycnometer an Xon.
TRN_ERR: Timeout failed to respond
Cause: The receiving device took longer than 10 seconds to acknowledge receipt of
data from the pycnometer.
Action: Make sure the receiving device is properly connected to the pycnometer RS-
232 port and is turned on. Verify that the serial I/O parameters controlling the
receiving device correspond with the data transmission parameters in the set up
mode.
Updating Unit [n] failed: Press [CLEAR]
Cause: One of the analysis modules has malfunctioned.

Action: Press CLEAR and follow the instructions displayed in the keypad window. After
disconnecting the faulty unit (as instructed), you may reconnect the control mod-
ule with the remaining analysis module(s) and continue using your system.
USR_ERR: Cal std 10% of full-scale

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134-42800-01 (Rev A) — Jan 2016
Cause: You tried to enter a calibration standard volume that is less than 10% of the nom-
inal full-scale volume.
Action: Enter a volume that represents at least 10% of the nominal cell chamber
volume.
USR_ERR: No data to review
Cause: You tried to review data for an automatic operation when there were no data to
review.
Action: Abandon request.
USR_ERR: Number of cycles must be ≥ 5
Cause: You tried to enable run precision without increasing the number of runs to at
least five.
Action: Increase the number of runs to five or abandon request.
USR_ERR: Out of range
Cause: You tried to enter a value that is out of the valid range.
Action: Enter a value in the specified range.
USR_ERR: Pressure overrange
Cause: A pressure overrange occurred but was left uncorrected.

Action: Return to manual mode and vent the system.
USR_ERR: Cal std 10% of full-scale
Cause: You tried to enter a calibration standard volume that is less than 10% of the nom-
inal full-scale volume.
Action: Enter a volume that represents at least 10% of the nominal cell chamber
volume.
USR_ERR: No data to review
Cause: You tried to review data for an automatic operation when there were no data to
review.
Action: Abandon request.
USR_ERR: Number of cycles must be ≥ 5
Cause: You tried to enable run precision without increasing the number of runs to at

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134-42800-01 (Rev A) — Jan 2016
least five.
Action: Increase the number of runs to five or abandon request.
USR_ERR: Out of range
Cause: You tried to enter a value that is out of the valid range.
Action: Enter a value in the specified range.
USR_ERR: Pressure overrange
Cause: A pressure overrange occurred but was left uncorrected.

Action: Return to manual mode and vent the system.

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134-42800-01 (Rev A) — Jan 2016
C Multigas Option
C MULTIGAS OPTION
The Multigas option enables the AccuPyc to use up to four different gases. The Multigas assembly
consists of:
l Valve assembly and two retaining screws

l Gas entrance tubing for connection from the analyzer to the valve assembly
l Gas supply tubing for four gases
INSTALL THE MULTIGAS ASSEMBLY
If a gas is attached to the gas inlet on the rear panel of the analyzer, close the gas cyl-
inder valve and remove the inlet tubing from the analyzer before installing the multigas
assembly. The gas can then be attached to one of the inlet valves on the assembly.
1. Remove the two retaining screws on the rear panel of the AccuPyc.
2. Position the valve assembly against the rear panel so that the retaining screw holes on the
valve assembly align with those on the rear panel of the analyzer.
3. Attach the valve assembly to the rear panel using the two screws included in the multigas kit.
4. Carefully cut and remove the cable ties holding the gas entrance tubing in position and remove
the ties.
5. Remove the protective caps from the ends of the gas entrance tubing, then remove the fer-
rules from the upper end of the tubing.
6. Remove the nut from the center port and slide it onto the end of the gas entrance tubing, then
replace the front and rear ferrules.
7. Insert the tubing into the center port of the multigas assembly. Use the nut to secure the tubing
to the assembly.
8. Insert the other end of the tubing into the gas inlet. Use the self contained swage nut to secure
the tubing to the inlet.

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C Multigas Option
CONNECT GASES
1. Connect one end of the gas supply tubing to the gas supply. See Instrument Components
on page 1 - 5.
2. Insert the other end of the tubing into one of the valve inlets on the multigas assembly.
3. The faceplate of the valve assembly contains four sections; one for each gas inlet on the
assembly. Write the name of the gas in the applicable section.
SELECT GASES
After installing the gases, use the knob to select the gas. Purge the gas lines when changing gases.

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D MultiVolume Insert Option
D MULTIVOLUME INSERT OPTION

The MultiVolume Insert option provides analysis of samples using smaller-sized sample chambers.
Wear latex gloves when handling inserts and sample cups. Oils from skin may con-
taminate the surface and affect analysis results. See Handling System Components
on page J - 1.
Equipment Description
AccuPyc 1 cm3 Includes a 0.1 cm3 insert/sample cup combination.
AccuPyc 10 cm3 Includes 1 and 3.5 cm3 inserts with corresponding sample cups and
appropriate calibration standards. Fritted filter lids are included for both
inserts.
AccuPyc 100 cm3 Includes 10 and 35 cm3 inserts with corresponding sample cups and
appropriate calibration standards. A fritted filter lid, which prevents the
escape of sample particles under rapid gas flow, is included for the 10
cm3 insert.
AccuPyc 2000 cm3 Includes 650 and 1300 cm3 cups, supporting inserts and calibration
standards. A tool is also included to allow removal of the supporting
inserts.
An insert changes the size of the sample chamber and requires its own sample cup. All inserts are
shipped with appropriate cups, with the exception of the 0.1 cm3 insert for the 1 cm3 unit. Because of
its size, the sample cup for the 0.1 cm3 insert is built-in. The appearance of the inserts and cups
varies.

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134-42800-01 (Rev A) — Jan 2016
This example shows a 10 cm3 cup and insert.
The inserts for the 2000 cm3 systems are installed and removed with a special tool.

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INSTALL AND REMOVE INSERTS AND SAMPLE CUPS

0.1 CM3 INSERT
The MultiVolume kit contains a special tool required to install the 0.1 cm3 inserts. The sample cup is
built into the 0.1 cm3 insert.
1 CM3 INSERT
The MultiVolume kit contains a special tool required to install the 1 cm3 inserts.
To Install the Insert
1. Remove the sample chamber cap and place on a clean work surface with the greased side
facing upward.
Contamination from airborne particles can occur rapidly. The chamber cap should be
left off the sample chamber for as little time as possible.
2. Place the insert into the sample chamber.

3. Use the handling tool to grasp the cup for placement in the insert. After placing the sample into
the sample cup, insert the tip of the tool into the cup and press down firmly. The handling tool
features an O-ring to grip the inside surface of the sample cup.
4. Place the cup into the insert, then tilt the tool to one side and remove it from the sample cup.

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134-42800-01 (Rev A) — Jan 2016
5. If using a fritted filter cap, place it onto the top of the insert.
6. Replace the sample chamber cap.
To Remove the Insert
facing upward.
2. Remove the fritted filter cap (if used).
3. Insert the handling tool into the sample cup until the sample cup is gripped by the O-ring.
4. Lift the sample cup out of the insert.
5. Pull the insert from the sample chamber.
6. Replace the sample chamber cap.
10, 3.5, AND 35 CM3 INSERTS

Remove the chamber cap and place the insert into the sample chamber. The insert should fit snugly
in the chamber. Place the appropriate sample cup into the well of the insert.
Do not force the insert or cup into the openings. This may damage the instrument, insert,
or sample cup.
Install the fritted filter cap (if used) before closing the sample chamber. A fritted filter cap is used to
constrict gas flow and is included with some inserts. The fritted filter cap for the 10 cm3 insert fits on
the top of the sample cup. The fritted filter caps for the 1 and 3.5 cm3 inserts fit on the top of the
insert. Fritted filter caps are not available for the 0.1 and 35 cm3 inserts.

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134-42800-01 (Rev A) — Jan 2016
CALIBRATE INSERT
An insert must be calibrated and its operation verified. Appropriate calibration standards are
included in the MultiVolume kits. For example, a 100 cm3 capacity AccuPyc with a 10 cm3 insert
must be calibrated with the 10 cm3 insert, cup, and calibration standards.
0.1 CM3 INSERT

Because of the size of the 0.1 cm3 insert, its calibration is performed in a different manner from that
of other inserts.
If the 1 cm3 pycnometer has not been calibrated recently, perform a calibration before
calibrating the 0.1 cm3 insert.
facing upward.
2. Place the insert into the sample chamber (the sample cup is built into the insert). Replace the
chamber cap.
3. Press Alt + 4 to access the Analyze function. Press ENTER until the Chamber Insert prompt
is displayed. Ensure that None is displayed.
4. Press ENTER to display the Analyze prompt. Press ENTER to begin the calibration.
5. After the calibration is complete, the Reload prompt is displayed.
6. Press CHOICE until the average measured volume is displayed. Record this value.
7. Press Alt + 2 to access Setup.
8. Press CHOICE until Calibration Data is displayed.
9. Press ENTER to display the Chamber Insert prompt.
10. Ensure that None is selected, then press ENTER to display the Cell Volume prompt.
11. Subtract the average volume of the 0.1 cm3 insert/cup (recorded in Step 6) from the cell
volume displayed in the prompt. Record this value.
12. Press ENTER to display the Expansion Volume prompt.
13. Record the value displayed for the expansion volume, then press ENTER to return to the Cal-
ibration Data prompt.
14. Press ENTER. The Chamber Insert prompt is displayed.
15. Press CHOICE until 0.1 cm3 is displayed, then press ENTER to display the Cell Volume
prompt. Enter the value recorded in Step 11.
16. Press ENTER to display the Expansion Volume prompt. Enter the value recorded in Step 12.
17. Press SAVE to save the information and return to the Reload prompt.
The pycnometer is now ready for analyses using the 0.1 cm3 insert/cup.

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134-42800-01 (Rev A) — Jan 2016
1, 10, 3.5, 35, 650, AND 1300 CM3 INSERTS

facing upward.
2. Place the insert and sample cup into the sample chamber. Replace the chamber cap.
3. Calibrate the insert. See About Calibration on page 10 - 1.
4. See Verify Operation on page 10 - 10.
OPERATING PARAMETERS USING THE KEYPAD

To operate using inserts, access the Chamber Insert prompt to select the appropriate MultiVolume
insert.
1. Press Alt + 2 to access the Setup function.

2. Press CHOICE until Report Options is displayed, then press ENTER.
3. Continue pressing ENTER until the Request Insert prompt is displayed.
4. Press CHOICE until Yes is displayed, then press ENTER.
5. Press SAVE to save the changes and return to the Reload prompt.
A Chamber Insert prompt will display during all normal operating procedures. For example, a
Chamber Insert prompt will display when starting a calibration or analysis.

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134-42800-01 (Rev A) — Jan 2016
E RS-232 Pin Assignment
E RS-232 PIN ASSIGNMENT

The AccuPyc is a standard DTE device. The RS-232 port can be used to connect an analytical
balance for transfer of sample weight, or for transmitting data to a computer. The receiving device
must be configured to interface with the RS-232 pin assignments. Any signals that are not listed in
the RS-232 Pin Assignment table are ignored.
RS-232 Pin Assignments

Pins Signal Description Data Direction
2 RXD Receive Data Into AccuPyc
3 TXD Transmit Data From AccuPyc
4 DTR Data Terminal Ready From AccuPyc
5 GND Ground N/A
6 DSR Data Set Ready Into AccuPyc
The AccuPyc uses the DTR and DSR signals for hardware flow control. Ensure that the serial
device provides these signals. For example, if attaching to a computer (also a DTE device), use a
null modem cable which includes the designated signals. If transmission problems occur, ensure that
the signals are set up properly. If the signals are correctly configured, contact the receiving device
manufacturer for assistance.

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134-42800-01 (Rev A) — Jan 2016
F Sample Volume Equation Derivation
F SAMPLE VOLUME EQUATION DERIVATION
10, 100, AND 350 CM3 UNITS

The AccuPyc II is a gas displacement pycnometer which measures the volume of solid objects of
irregular or regular shape whether powdered or in one piece. A greatly simplified diagram of the
instrument is shown below.
Sample volume is determined from the known cell and expansion volumes and from measured
pressures.
The cell and expansion chamber are initially at ambient pressure and the valve is closed. The cell is
then charged to an elevated pressure.
The ideal gas law gives:
P1(Vc − Vs ) = nc RT (1)
where
nc = moles of gas in the sample cell

R = the gas constant
T = temperature
Vc = cell volume
Vs = sample volume
Vx = expansion volume
P1 = initial cell pressure
Expansion volume:
PaVx = nx RT (2)

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134-42800-01 (Rev A) — Jan 2016
where
Pa = ambient pressure
nx = moles of gas in the expansion volume
When the valve is opened, the pressure falls to an intermediate value, P2, and mass balance yields:
P2( Vc − Vs + Vx ) = nc RT + nx RT (3)
Substituting from equations (1) and (2) into (3):
P2(Vc − Vs + Vx ) = P1(Vc − Vs ) + PaVx (4)
or
(P2 − P1 )(Vc − Vs ) = (Pa − P2 )Vx (5)
then
Pa − P2 (6)
Vc − Vs = V
P2 − P1
x
Adding and subtracting Pa in the denominator and rearranging gives
Pa − P2 (7)
−Vs = −Vc + V
P2 − Pa − P1 + Pa x
Dividing by (Pa - P2) in both the numerator and denominator
Vx (8)
Vs = Vc −
−1 −  P1 − Pa 
 Pa − P2
 

or
Vx (9)
Vs = Vc −
 P1 − Pa 
 P2 − Pa − 1
 

F -2
134-42800-01 (Rev A) — Jan 2016

Using gauge pressure defined as:
Pig = Pi − Pa (10)
equation (9) is rewritten as:
Vx (11)
Vs = Vc − P1g
−1
P2g
1 CM3 AND 2000 CM3 UNITS

The 1 cm3 and 2000 cm3 pycnometers operate by filling the expansion chamber while the sample
cell remains at ambient pressure. After P1 is equilibrated, the expansion valve opens to allow gas to
expand into the sample chamber and P2 is equilibrated.
For the 1 cm3 and 2000 cm3 pycnometers, equation (1) becomes
P1Vx = nx RT
and equation (2) becomes
Pa(Vc − Vs ) = nc RT
A derivation similar to that above yields the working equation for the 1 cm3 and 2000 cm3
pycnometers

V=V−V  P1g − 1 
s c x P 
 2g 

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G TEC Module

G TEC MODULE
This AccuPyc system has been modified to provide temperature control from 15 to 36 °C. The
system uses a thermoelectric control (TEC) system to heat or cool the AccuPyc. The temperature is
controlled using a digital temperature controller and a separate power system from the AccuPyc.
It is suggested that the TEC system be installed first, to allow time for temperature to stabilize at the
desired temperature, while the AccuPyc is being installed. See Add Analysis Module to Control
Module on page 11 - 1.
SET THE TEC TEMPERATURE

1. Power on the TEC module. The power switch is located near the power inlet.
The digital display of the temperature controller will show a test message while it starts up.
When the test message stops flashing, the current temperature displays. If the current
temperature and a message such as ErAt displays, press the P (Program) key on the front
panel of the controller. The ErAt message should stop and only the current temperature will
display.
2. Press P. SP 1 displays followed by the current setpoint (SP 1). Use the Up or Down key to
set the temperature.
3. Press P to accept the temperature. The controller will now start heating or cooling to achieve
the setpoint
The TEC module uses a fan to remove heat. The fan is located on the underside of the
instrument. The fan pulls air into the instrument and the air is exhausted through
ventilation slots on the rear panel. The exhaust slots must remain unobstructed.
Do not allow papers or other debris to be pulled across the fan as this will stop the
necessary air flow. The TEC system will be unable to control temperature, and may
become damaged.

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134-42800-01 (Rev A) — Jan 2016
G TEC Module
OPERATE THE TEC MODULE

When the TEC controller shows the correct temperature, there may be a small difference between
the temperature on the TEC unit and the AccuPyc display because two different sensors are being
used. The AccuPyc sensor and electronics are calibrated together to compensate for any
component differences between the sensor and the circuit board components. Micromeritics
considers the AccuPyc temperature display to be a more accurate reflection of the sample
temperature than the reading from the controller. The controller and the sensor used with the
controller cannot be calibrated.
The TEC controller may be adjusted to compensate for the small difference. If the AccuPyc
temperature is a little high, then reduce the setpoint of the TEC controller by the difference. Wait for
stabilization. Readjustment may need to be repeated until the correct AccuPyc temperature is
achieved.
The AccuPyc volume must be calibrated at the analysis temperature. Perform the volume calibration
in the normal way until it is time to insert the reference volume (sphere or spheres). After installing
the reference volume, wait at least 20 minutes to allow the volume to achieve the same temperature
as the AccuPyc. Then continue as normal.
When it is necessary to perform AccuPyc tests at a different temperature, re-calibrate the system
volume at the new temperature.
VOLUME CHANGE WITH TEMPERATURE FOR THE 10 CM3 ACCUPYC

The reference spheres supplied with the 10 cm3 AccuPyc are made from tungsten carbide. They
were measured at 20 °C. The spheres will change volume with temperature. The change is very
small and is shown in the following table. Every sphere is a slightly different size, and so the table
provides the factor to be used if the value used during calibration needs to be adjusted. Multiply the
volume provided with the reference spheres by the value in the right column.
3
Temperature (°C) Typical Volume (cm ), two balls Factor
15 6.37125 0.99991
20 6.37182 1.00000
25 6.37238 1.00009
30 6.37295 1.00018
35 6.37351 1.00027
For example, if the ball is 6.37182 cm3 at 20 °C but run at 50 °C, multiply the Volume × the Factor in
the table.
6.37182 x 1.00053 = 6.37520

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134-42800-01 (Rev A) — Jan 2016
G TEC Module
VOLUME CHANGE WITH TEMPERATURE FOR THE 100 CM3 ACCUPYC

The stainless steel calibration standard (ball) supplied with the 100 cm3 AccuPyc is made from 440
grade stainless steel. It was measured at 20 °C. Its volume will be higher when heated above 20 °C.
The following table uses the coefficient of thermal expansion of 440 grade stainless steel (0.0000101
m/m/degree C change) to provide the volume of the sphere at various temperatures.
Every ball is a slightly different size therefore the table provides the factor to be used if the value used
during calibration needs to be adjusted. Multiply the volume provided with the reference sphere by
the value in the right column.
3
Temperature (°C) Typical Volume (cm ) Factor
15 51.089712 0.99995
20 51.092292 1.000000
25 51.094872 1.000051
30 51.097452 1.000101
35 51.100032 1.000152
For example, if the ball is 51.092292 cm3 at 20 °C but run at 50 °C, multiply the Volume × the Factor
in the table.
51.092292 × 1.000303 = 51.107773

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G TEC Module
ASPHALT DENSITY MEASUREMENT

Samples can be analyzed in disposable cups. Any difference in the mass of the cups used for
calibration and analysis will be corrected for in the reported quantities. Performing an asphalt density
measurement requires the AccuPyc II Asphalt software and disposable sample cups.
Steps 1-9 do not need to be repeated for subsequent analyses.
1. Set the instrument temperature and allow 12 hours for equilibration.

2. Go to Options > Option Presentation. Select Show Cup Properties. Verify that a check-
mark displays to the left.
3. Label each disposable cup with a permanent marker and record its mass.
4. Place a disposable cup in the 3.3 cm3 insert and position the insert in the sample chamber.
5. Go to Unit [n] > Calibration > Calibrate Volume.
a. Enter the mass of the cup in the Cup mass field.
b. Enter the volume of the reference sphere in the Volume of calibration standard field.
c. Select the correct chamber insert.
d. Select Measured.
e. Click Start.
6. Insert the reference sphere when prompted and resume the calibration.
7. When the calibration is complete, remove the cup and reference sphere .
8. Prepare a sample in a different disposable cup and place it in the sample chamber.
9. Create a sample file for the analysis.
10. Go to Unit [n] > Sample Analysis and select the sample file created in the previous step.
11. Enter the mass of the cup in the Cup mass field.
12. Select the chamber insert that was used for calibration.
13. Click Start.

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134-42800-01 (Rev A) — Jan 2016
H Temperature Controlled AccuPyc
H TEMPERATURE CONTROLLED ACCUPYC

A temperature controlled AccuPyc must be connected to a circulating bath (not provided by
Micromeritics). Refer to the manufacturer operator manual for circulating bath operating instructions.
ATTACH A CIRCULATING BATH

The rear panel of the temperature controlled AccuPyc contains connections for a circulating bath.
Provided in the accessory kit are two (2) hose fittings and a four (4) foot length of tubing.
1. Power off the controlling unit.

2. Remove the plugs from the In port and the Out port.
3. Insert the provided hose fittings into each connector.

4. Cut the piece of 4 ft. tubing into two equal pieces of 2 feet each.
5. Install the tubing on the In and Out connectors.
6. Install the other end of the Out tubing to the Inlet connection of the bath circulator.
7. Install the other end of the In tubing to the Outlet connection of the bath circulator.
8. Set the temperature using the appropriate controls on the bath circulator.

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134-42800-01 (Rev A) — Jan 2016
H Temperature Controlled AccuPyc
ADD ANALYSIS MODULES TO A TEMPERATURE CONTROLLED MODULE
If using the Windows version of the AccuPyc II, exit the application before powering off
the analyzer.
1. Power OFF the controlling unit.

2. Connect the circulating bath. See Attach a Circulating Bath on page J - 5.
3. Connect one end of the module connector cable (provided in the analysis module accessories
kit) to the connector labeled Module Connection on the rear panel of the control module.
4. Connect the other end of the module connector cable to the lower connector labeled Module
Connector on the rear panel of the analysis module.
5. Power ON the analyzer. If using the Windows version of the AccuPyc II, start the application .
6. Calibrate the analysis module using the calibration kit shipped with the system. See About
Calibration on page 10 - 1.

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134-42800-01 (Rev A) — Jan 2016
I Transmitted Data
I TRANSMITTED DATA
Keypad Function
Analysis and calibration data can be transmitted in a single column or spreadsheet with data in
ASCII delimited format. Units are displayed as:
Data Units
Type Measurement
Date DD/MM/YY
Time HH:MM:SS
Pressure psig
Temperature °C
Elapsed Time seconds
ANALYSIS REPORT
Analysis Report - Spreadsheet
Record Description Form
Number
1 Version Number 20 characters
2 Serial Number 1 integer
3 Report type = analysis 8 characters
4 Start (reported on one line as ASCII comma delimited 8 characters (each)
data)
l 4a. Date
l 4b. Time
5 Stop (reported on one line as ASCII comma delimited 8 characters (each)

data)
l 5a. Date
l 5b. Time
6 Temperature 1 floating point

7 Description line 1 20 characters
8 Description line 2 20 characters

I-1
134-42800-01 (Rev A) — Jan 2016
I Transmitted Data
Analysis Report - Spreadsheet (continued)

Number
9 Sample IDs 20 characters
10 Sample mass 1 floating point
11 Number of purges 1 integer
12 Equilibration rate 1 floating point
13 Chamber Insert: 1 integer
l 0 = None
l 1 = 10 cm3 (100 cm3 unit)
1 cm3 (10 cm3 unit)

0.1 cm3 (1 cm3 unit)
l 2 = 35 cm3 (100 cm3 unit)
3.5 cm3 (10 cm3 unit)

14 Cell volume 1 floating point
15 Expansion volume 1 floating point
16 Average volume 1 floating point
17 Volume standard deviation 1 floating point
18 Average density 1 floating point
19 Density standard deviation 1 floating point
20 Number of runs 1 integer
21 Run precision 1 floating point
l 0 = Disabled
l 1 - Enabled
22 Percent full scale 1 floating point

23 Carriage return / Line feed
26 Run number and pressure (reported on one line as ASCII
comma delimited data)

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134-42800-01 (Rev A) — Jan 2016
I Transmitted Data
Analysis Report - Spreadsheet (continued)

Number
26a Run number 1 integer
26b P1 1 floating point
26c P2 1 floating point
26d Include in average calculation 1 integer
l 0 = Excluded
l 1 = Included
26e Elapsed time 1 unsigned integer

26f Volume 1 floating point
26g Volume deviation 1 floating point
26h Density 1 floating point
26i Density deviation 1 floating point
27 Temperature (all temperature data) 1 floating point
CALIBRATION REPORT
Calibration Report - Single Column
Number
3 Report type = calibration 11 characters
data)
l 4a. Date
l 4b. Time

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I Transmitted Data
Calibration Report - Single Column (continued)

Number
data)
l 5a. Date
l 5b. Time

7 Calibration standard size 1 floating point
9 Equilibration rates 1 floating point
l 0 = None
l 1 = 10 cm3 (100 cm3 unit)
1 cm3 (10 cm3 unit)

l 2 = 35 cm3 (100 cm3 unit)
3.5 cm3 (10 cm3 unit)

11 Average cell volume 1 floating point
12 Cell volume standard deviation 1 floating point
13 Average expansion volume 1 floating point
14 Expansion volume standard deviation 1 floating point
16 P1 (all P1 data) 1 floating point
17 P2 (all P2 data) 1 floating point
18 P1* (all P1* data) 1 floating point
19 P2* (all P2* data) 1 floating point
20 Include in average calculation 1 integer
l 0 = Excluded
l 1 = Included

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134-42800-01 (Rev A) — Jan 2016
I Transmitted Data
Calibration Report - Spreadsheet

Number
3 Report type = calibration 11 characters
data)
l 4a. Date
l 4b. Time

data)
l 5a. Date
l 5b. Time

7 Calibration standard size 1 floating point
9 Equilibration rates 1 floating point
l 0 = None
l 1 = 10 cm3 (100 cm3 unit)
1 cm3 (10 cm3 unit)

l 2 = 35 cm3 (100 cm3 unit)
3.5 cm3 (10 cm3 unit)

11 Average cell volume 1 floating point
12 Cell volume standard deviation 1 floating point
13 Average expansion volume 1 floating point
14 Expansion volume standard deviation 1 floating point

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I Transmitted Data
Calibration Report - Spreadsheet (continued)

Number
19 Run number and pressure (reported on one line as ASCII
comma delimited data)
19a Run number 1 integer
19b P1 1 floating point
19c P2 1 floating point
19d P1* 1 floating point
19e P2* 1 floating point
19f Include in average calculation 1 integer
l 0 = Excluded
l 1 = Included
19g Cell volume 1 floating point

19h Cell volume deviation 1 floating point
19i Expansion volume 1 floating point
19j Expansion volume deviation 1 floating point

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J Installation Instructions
J INSTALLATION INSTRUCTIONS
These instructions assume that the shipping cartons have been opened and their contents checked
and verified .
HANDLING SYSTEM COMPONENTS
CALIBRATION STANDARD
l Wear latex or nitrile, powder-free gloves to prevent transfer of oil from hands.
l Do not drop the standard into the sample cup. Roll the standard into the cup to prevent damage.
l Always return the standards to the case. Standards are unit specific.
SAMPLE CHAMBER CAP

l Wear latex or nitrile, powder-free gloves to prevent transfer of oil from hands.
l Keep the cap on the sample chamber except when inserting or removing the sample cup .
When left uncapped, the sample chamber temperature may become unstable and/or
water vapor will adsorb on the inner surface of the chamber. Either of these conditions
can affect analysis results.
l Avoid laying the chamber cap on a work surface. Debris may collect on the greased surface of the
O-ring which can also affect analysis results.
l When multiple analysis modules are connected, never interchange sample chamber caps. Caps
are unit specific.

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GAS REQUIREMENTS
The pycnometer uses helium or nitrogen (99.995% pure or better) to provide rapid, accurate
analyses. The cylinder containing helium must be fitted with a gas regulator set for 19-23 psig (131-
159 kPag). The pressure input to the pycnometer should never be greater than 25 psig (172 kPag).
Excessive pressures waste gas due to a protection device contained in the pycnometer that vents
the pycnometer to atmospheric pressure if pressure exceeds 35 psig (241 kPag).
This protection device is not installed on 2000 cm3 units.
Tank pressure should be at least 200 psi above regulator pressure.

The High Pressure sample chamber configuration inlet pressure should never be
greater than 520 psig (3580 kPag); there is no pressure relief.
Other inert, dry gases can also be used and may be more applicable for some applications.
PYCNOMETER SET UP
PYCNOMETER CONFIGURATION
Single Module Configuration

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Pycnometer Configuration
Control Module and Analysis Module Configuration
TEC Module Configuration
Diagram Components
A Separate power cord for external power supply. Connect cable to wall outlet.
B External power supply
C Hardwired 8-pin mini-DIN power cable for external power supply.
D 8 pin mini DIN cable.
E Power adapter DIN port.

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Diagram Components (continued)

F Power adapter.
G Module Connection - 8-pin mini-DIN OUT port to connect next analysis module.
H Module Connection - 8-pin mini-DIN IN port to connect the control module or pre-
viously connected analysis module (not shown).
I Hardwired power mini-DIN cable for power adapter.
Set Up Procedure
1. Unpack and inventory all boxed parts. Contact your Micromeritics Service Representative if
parts are missing or broken.
2. Place module(s) on work surface.
3. Connect separate power cable(s) to external power supply(s).
4. Connect external power supply(s) to power outlet on the module(s).
5. Connect power cable to wall outlet.
6. Toggle the module power switch to the ON position.
7. Check the power indicator on the front panel of the analyzer. The indicator will blink green to
indicate that power is applied to the analyzer. Once the application is running, the indicator will
stop blinking and remain illuminated.
8. On the keypad, press Alt + CHOICE + 2. Unit [n] appears in the upper left corner of the dis-
play.
9. Adjust the display brightness control using the Brightness Control button on the rear of the
analyzer.

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Set the TEC Temperature
SET THE TEC TEMPERATURE

See TEC Module on page G - 1
TEMPERATURE CONTROLLED MODULE HARDWARE SETUP
Setup a Single Temperature Controlled Module
See Pycnometer Configuration on page J - 2 for setup instructions. When complete, connect
the circulating bath.
Attach a Circulating Bath
The rear panel of the temperature controlled AccuPyc contains connections for a circulating bath.
Provided in the accessory kit are two (2) hose fittings and a four (4) foot length of tubing.
1. Power off the controlling unit.

2. Remove the plugs from the In port and the Out port.
3. Insert the provided hose fittings into each connector.

4. Cut the piece of 4 ft. tubing into two equal pieces of 2 feet each.
5. Install the tubing on the In and Out connectors.
6. Install the other end of the Out tubing to the Inlet connection of the bath circulator.
7. Install the other end of the In tubing to the Outlet connection of the bath circulator.
8. Set the temperature using the appropriate controls on the bath circulator.
CONNECT KEYBOARD
An optional USB keyboard can be connected to a USB port on the rear panel of the analysis module.
The keyboard is not provided by Micromeritics.

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GAS CONNECTION
These instructions are for connecting inert gases only. Follow the safety procedures
used by your laboratory for connecting hazardous gases.
Review Gas Requirements on page J - 2 prior to installing gas.
1. Attach an appropriate regulator to the gas cylinder or gas line, then tighten with a wrench.
Leave the gas bottle shutoff valve closed until instructed otherwise.
2. Attach the gas inlet line to the regulator, reducer fitting, or regulator expansion:
It is important to use the inlet tubing supplied with the analyzer. Gas lines made of mater-
ials other than copper or stainless steel can cause operational problems as well as inac-
curate data.
If Regulator has... Then...

1/4 in. outlet Attach the reducer fitting to the outlet of the regulator shutoff / isolation
valve
Tighten the nut finger-tight, then 1-1/4 turns with a wrench.
Continue with the steps given for the 1/8 in. outlet

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Gas Connection
If Regulator has... Then...

1/8 in. outlet Insert the gas tubing into the fitting.
Enure the tubing is seated fully inside the fitting.
Tighten the nut finger-tight
While holding the fitting body steady, tighten the nut with a wrench 3/4
turn.
Do not overtighten the fittings. Doing so can collapse the brass fitting and cause a leak.
Purge the regulator and inlet tubing to prevent contamination of the analysis gas.
a. Turn the regular shutoff valve clockwise to close.

b. Turn the pressure regulator control knob counter-clockwise to open.
c. Slowly turn the gas cylinder shutoff valve counter-clockwise to open, then quickly close it.
d. Observe the high-pressure gauge.
If the pressure decreases, tighten the nut connecting the regulator to the gas cylinder. If
the pressure is stable, proceed to the next step.
Ensure the gas supply equipment is adequately vented before performing the next step.
e. Turn the pressure regulator control knob clockwise until the low-pressure gauge indicates
19.500 psig (134.445 kPag).
f. Turn the regulator shutoff valve counter-clockwise to open.
g. Turn the gas cylinder shutoff valve counter-clockwise to open. Flow gas for 10 to 30
seconds, then close the valve.
h. Turn the gas regulator shutoff valve clockwise to close
i. Attach the other end of the copper tubing to the gas inlet on the rear panel of the pycno-
meter. Remove the inlet plug that shipped with the pycnometer.

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3. Turn the nut on the tubing clockwise until it is finger-tight. Then use a 7/16 in.(1 mm) wrench to
tighten the nut an additional 1/4 turn.
4. Open the gas cylinder and regulator shutoff valves.
5. Turn the regulator control knob until the low pressure gauge indicates 21.5 psig (148 kPag).
For a High Pressure sample chamber configuration, set regulator pressure 20 psi above cycle
and fill pressure.
CONNECT THE ANALYZER TO THE COMPUTER

If using the analyzer with the keypad or keyboard only, skip this section.
An Ethernet switch is required if connecting a different type of analyzer to the same computer as the
AccuPyc. If configuring multiple AccuPyc modules. they are connected together with only the
Control Module connected to the Ethernet switch. See Connect an Ethernet Switch on page J -
18.

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Configure the Pycnometer using the Keypad
CONFIGURE THE PYCNOMETER USING THE KEYPAD
If using the keypad to control analyses, follow these instructions for configuring the mod-
ule. If using the Windows application, skip this section.
Complete the installation process by configuring the module:
l Unit Types on page J - 13

l System Setup below
l Calibrate Volume on page 10 - 13
l Setup Reports on page J - 14
l Transmit on page 2 - 7
l Communications on the next page
SYSTEM SETUP
Press Alt + 2 to access the set-up function.
Display Description
Setup. Choose or enter parameters for analysis,
calibration, reporting, and data transmission.
Choices: Analysis Parameters, Report Options,

Calibration Data, Communications, Unit Types
Press CHOICE to display the set up type, then press

ENTER.
The parameters for each set up type are stored and used
to control the pycnometer until new ones are specified.
At the completion of each set up, the display returns to the Setup type? prompt.
l Press SAVE to save the information and return to the Reload prompt.
l Choose another set up type. Do not press SAVE until all parameters have been entered. The dis-
play will return to the Reload prompt.

l Press Alt + CLEAR to discard the information entered and return to the Reload prompt.

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PRINTER SETUP
Printers are connected to the AccuPyc II via a USB port. See Specifications for AccuPyc II on
page 1 - 11 for a list of supported printers. Using the keypad:
1. On the display, select Setup > Report Options.

2. Press ENTER until the Printer? prompt is displayed.
3. Press CHOICE until the appropriate printer driver is displayed.
COMMUNICATIONS
Use these instructions for keypad installations only. If a computer will be attached to the
module, skip this section. All setup functions will be done in the analysis software applic-
ation.
Communications enables specification of communications criteria, such as baud rate, parity, etc.

Setup Type? Press CHOICE until Communications is displayed.
Communications
Communications Enables selection of the manner in which the IP address is assigned.
IP Address? With an IP address, analysis results can be access via a web browser.
[choice] Typically, after an analysis (or calibration) is started, results from the
previous operation cannot be reviewed. However, results from five
analyses are stored in the controller. A web browser enables review of
these results. An IP address must exist for this operation. An IP
address can be detected and assigned automatically, or one can be
specified.
Ensure the Ethernet cable is plugged into the Ethernet port on the
analyzer and to the network. Choose DHCP to have an IP address
assigned automatically, or Specify to specify an address. Press
CHOICE until the option is displayed.
If using DHCP, an IP Address should be assigned within a minute.

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Communications Displays the first-time selection of DHCP.
Requesting Address *
[ENTER] to continue Press ENTER. The system automatically attempts to assign an IP
address. If the system is able to determine an address, the assigned
address is displayed.
Communications If an address cannot be determined, this prompt is displayed:

Requesting Address
[ESCAPE] to cancel
Press Alt + CLEAR to cancel the operation and return to the Reload
prompt. Contact your IT department, or choose the Specify option and
enter the appropriate information.
Communications Displays when the Specify option is selected. Enables entry of an
IP Address * appropriate IP address. This is a numerical field in the following format:
(user entered) nnn.nnn.nnn.nnn. Enter the address.
Communications Enables entry of the subnet mask number. Enter the subnet mask
Subnet Mask * number.
(user entered)
Communications The Gateway address is used for communicating outside the local
Gateway * network. The Gateway address is often the same as the IP address,
(user entered) with a “1” after the last dot instead of the last three characters
(nnn.nnn.nnn.1). Contact your IT department with any questions.
Communications When connected to a network, analysis or calibration results can be e-
E-mail Address: mailed automatically upon their completion. This prompt enables entry
of the e-mail address where results are to be sent.
If not using DHCP and the e-mail address is outside the local network,
specify a gateway address (see previous prompt). A keyboard is
required to type in the e-mail address.

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134-42800-01 (Rev A) — Jan 2016

Communications Enables entry of the numerical address of the SMTP server. If this
E-mail Server: address is unknown, contact your IT department.
IT may need to IT may need to configure the server to accept e-mail from the AccuPyc.
configure the server to The following information may be required:
accept email from the
AccuPyc. The following l IP address for the AccuPyc
information may be l Sender line: Micromeritics-1340
required:
l IP address for the

AccuPyc
l Sender line: Micro-
meritics-1340
Communications Press CHOICE to select proper baud rate.

Baud Rate?
Communications Press CHOICE to select 8 or 7.
Data Bits?
Communications Press CHOICE to select 1 or 2.
Stop Bits?
Communications Press CHOICE until the required option (None, Even, or Odd) is dis-
Parity? played.
Communications Transmits data through the Xon/Xoff protocol. Press CHOICE to select
Xon / Xoff Protocol? Disabled or Enabled.
* Does not display for DHCP.

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UNIT TYPES
If not using the analyzer software, these keypad prompts enable selection or entry of:
l units of measurement
l operating language
l current date and time

Set-up Type? Press CHOICE until Unit Types is displayed, then press ENTER.
Unit Types
Unit Types Enables selection of unit type for reports. Press CHOICE to select the
Pressure units? desired unit.
Options are:
l psig (pounds per square inch gauge)

l kPag (kilopascal gauge)
Unit Types Enables selection of operating language. Pressing SAVE is not

Language? required.
Error messages that may be in the message queue will remain in

English (or the current selected language). Error messages that occur
after selecting the language will display in that language.
Keypad overlays containing translations for the alternate functions are

available for each language. Choose the language.
Unit Types The date is entered in a two digit format for the day, month, and year.
Date (DD/MM/YY)? For example; to set the date for September 1, 2014, enter 01/09/14
(day/month/year). Use the . (decimal) key to enter a slash (/).
Unit Types The time (in 24 hour format) at which an analysis begins and ends is
Time (HH:MM:SS)? shown on all reports. The time shown on the display may not match the
current time.
The time is entered in a two digit format for the hour, minutes, and
seconds. For example; to set the time to 1:05 pm, enter 13:05:00
(hour:minutes:seconds). Use the . (decimal) key to enter a colon (:).

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SET DATE, TIME , AND LANGUAGE

1. On the keypad, press Alt + 2 to enter Setup mode.
2. Press Choice until Date displays, then press Enter and enter the current date.
3. Press Choice until Time displays, then press Enter and enter the current time.
4. Press Choice until Language displays, then press Enter and select the correct language.
SETUP REPORTS
The Report Options command enables the report mode (density or volume for analysis) and
specification of the report destination. After analysis or calibration, the display returns to the Reload
prompt. An asterisk (*) in the third line of the display indicates an error message exists.
A report is generated automatically to the destination selected at the Setup > Report Options as
follows:
l Printer. Report is automatically sent to the printer.

lTransmission line. Report is automatically sent through the serial line to an attached device for
this purpose.
l E-mail. Report is e-mailed to the address specified (when connected to a network).
To view report data by points, use the Review function. See Review Data on page 2 - 11.

Setup Type? Press CHOICE until Report Options is displayed.
Report Options

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Report Options Press CHOICE to select Density, Volume or Specific Gravity, the
Anls Display Mode? mode in which the analysis report will be displayed. When Density is
Density selected, a Sample Mass? prompt displays during the Analysis
function. Enter a value for the sample mass. For accurate data, the
sample mass must be entered when choosing Density.
Report Options A sample ID (identification) is a unique identifier of the sample. Using
Request Sample ID? sample IDs can help keep track of data from multiple analyses and
can be used as a date and time stamp. A Sample ID prompt displays
during the analysis operation, allowing entry of the identification when
after selecting Yes to this prompt. Press CHOICE to select Yes or
No.
Report Options Provides entry of additional descriptive information. This prompt
Request Description? typically is used when a computer keyboard is attached. All system
commands can be executed on the keyboard. Press CHOICE to
select Yes or No.
Report Options Provides automatic generating of a report after an analysis or cal-
Print Report? ibration. The type of printer is selected at the Printer? prompt. Press
CHOICE to select Yes or No.
Report Options Provides transmission of analysis or calibration data automatically
Transmit Report? after the operation. Press CHOICE to select Yes or No. See Trans-
mitted Data on page I - 1.
Report Options Select Yes at this prompt to automatically send an e-mail at the con-
E-mail Report? clusion of an analysis or calibration operation. An e-mail address and
server must be specified in order to select Yes. Press CHOICE to
select Yes or No.
Report Options Provides selection of the report printer. This is a system option and
Printer? does not have to be specified for each analysis (or calibration). It also
[printer name] applies for all units when multiple analysis modules are attached.
Press CHOICE to select the appropriate printer. See Printer Setup
on page J - 10.
Report Options Select the format of data to be used when transmitting reports. Press
Transmission Format? CHOICE to select either the Single Column format or the Spread-
sheet format. See Transmitted Data on page I - 1.
Report Options Prompts for a MultiVolume insert during analysis or calibration
Request Insert? operations. An insert is a device that can be placed in a sample
chamber, allowing use of a smaller sample cup for analysis of smaller
sample quantities. Inserts are available in MultiVolume Kits for the
1.0, 10, and 100 cm3 pycnometers. Press CHOICE to select Yes or
No.
If MultiVolume inserts are not used, select No.

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Report Options If Yes is selected, prompts user to enter the mass of the sample cup
Request Cup at start of analysis.
Mass?
Request Cup Mass? is only necessary if different size cups are used for cal-
ibration and analysis.

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Analytical Balance
CALIBRATION
See Calibrate Volume on page 10 - 13.
ANALYTICAL BALANCE
The analytical balance tested by Micromeritics is Scientec® model #ZSA120.
An analytical balance can be connected to a serial port on the computer and used to transfer the
sample’s mass via a third-party software directly to the AccuPyc II application. Refer to the balance
manufacturer’s operator’s manual for transmission instructions.
1. Connect the analytical balance to the RS-232 port on the rear panel of the analyzer.
2. Go to Options > Configure Balance to connect and set up an RS-232 balance to the ana-
lyzer.
Configure Balance Fields and Buttons Table

Enable / Disable Select to enable or disable the attached balance.
Serial Parameter Used to set the baud rate, parity, data bits, and stop bits. This field
should not require modification from the default values.
Serial Port Select which serial port is used to connect the balance to the analyzer.

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CONNECT AN ETHERNET SWITCH

An Ethernet switch is required to connect one or more analyzers and one computer.
BRIGHTNESS CONTROL
To adjust the display brightness:
1. Insert a small flat head screwdriver into the opening.

2. Rotate the screwdriver until it engages in the slot, then turn clockwise to darken and coun-
terclockwise to lighten.

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Software Installation
SOFTWARE INSTALLATION
The following prerequisites must be completed prior to installing the software:
l Operating System. Windows 7 Professional or higher operating system is recommended for the
best user experience.
l Desktop Installation Required. The application should not be installed on a network drive with
shared access. Multiple users cannot operate the application at the same time.
l 10 Base T Ethernet Port. If the computer is to be connected to a network, two Ethernet ports
are required. If more than one Ethernet based unit is connected to the same computer, an eth-
ernet switch will also be required.
l Read/Write Permissions. All users of the application will need Read / Write permission to all dir-
ectories and subdirectories where the application is installed.

l Drives. CD-ROM drive and thumb drive.
1. Configure an Ethernet port on the computer to communicate with the analyzer. The IP
address must be 192.168.77.100. Reference the computer operator manual for instructions
on changing the IP address.
2. Insert the installation media into the media drive. The program automatically starts the install-
ation. If the installation does not immediately start, navigate to the media drive, then locate and
double click the setup.exe file.
3. On the Ethernet Introduction window, verify that all prerequisites have been met.
a. If not, click Cancel and complete the steps, then restart the installation program. Do not
proceed with installation until these tasks have been completed.
b. If the prerequisites have been met, click OK.
4. On the New Installation window, verify that sufficient disk space is available to continue the
installation. If not, click Exitand free up the minimum required disk space. If the disk space is
OK, click Next to accept the default installation directory, or click Browse to change the install-
ation location.

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a. To add a shortcut to the desktop, select the Add the application icon to the Desktop.....
checkbox.
b. To allow all computer users access to the software application , select Install this applic-
ation for All Users.all users of the computer.
c. Click Next.
4. On the Analyzer Configuration window, select 1 for the number of analyzers to be installed
and enter the analyzer serial number in the text box.
10. On the Ethernet Ports window, select one option from the following table:

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Software Installation
If... Then...
the configured port is listed Select the port, then click Next.
the configured port is not listed Click Specify and enter the remaining portion of the
IP Address, then click Next.
The IP Address must be 192.168.77.100
11. If prompted to configure a balance, select either 0 or 1. The balance should be connected to
Com Port 1. The default parameters should be OK. If not prompted for a balance, skip this
step.

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12. On the Installation Complete window, click Finish.
START THE APPLICATION

To start the application, click the application shortcut on the desktop or select the application from the
Windows program list.

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Specify Unit Selections
SPECIFY UNIT SELECTIONS

Options > Units
Use to specify how data should appear on the application windows and reports. This menu option is
not available if using Restricted option presentation.
REINSTALL OR MODIFY THE SOFTWARE
If the computer is to be connected to a network, a second Ethernet port on the computer

must be used for that purpose.
The Setup program is located on the installation media. After initial software installation, if changes
need to be made to the analyzer setup, reinsert the Setup media and follow the prompts.
l Reinstall the software version [n]

l Add an analyzer
l Move an analyzer
l Remove an analyzer
l Change analyzer setup
l Reinstall calibration files for an analyzer
l Uninstall
l Reset security to default
To access the Setup program:

2. Locate and double click the Setup.EXE file.
If the IP address needs to be changed on the computer connected to the analyzer, refer
to the computer's operating system manual or the internet for instructions. The
IP address for the computer and the IP address specified in the setup program must
match. The IP address must be 192.168.77.100.

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INSTALL ANALYZER SOFTWARE UPGRADE USING A MEDIA DEVICE
Keypad Function
To install software upgrade on the AccuPyc II module:
1. Turn the On/Off switch on the rear panel in the Off ( O ) position.
2. Insert the USB stick containing the software update into one of the USB connectors on the
rear panel.
3. Place the Power switch in the On ( | ) position.
4. After approximately 1-2 minutes of initialization, the software starts to load. The following
prompt is displayed:
5. Once the software is successfully installed, the display will read:
6. Remove the USB stick and store in a secure location.

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Uninstall the Software
UNINSTALL THE SOFTWARE

When the software is uninstalled, only the files required to run the application are removed.
Parameter files, sample files, reports, calibration files, and data files are not removed.

2. Select the Uninstall option.
3. Follow the prompts.

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Index
INDEX B
Brightness Control J - 18
0
0.1 cm3 Insert C
calibrate D - 5
Calculations A - 1, A - 1
Active Area A - 7
1 Analysis A - 1
Asphalt Density A - 3
1, 10, 3.5, 35, 650, and 1300 cm3 Inserts Calibration A - 4
calibrate D - 6 for FoamPyc Methods A - 5
Geometric Volume A - 7
Percent Porosity A - 7
A Resin Volume A - 8
Run Precision A - 8
About this manual iii SPC report variables A - 9
AccuPyc, about 1 - 1 Total Pore Volume A - 10
Analysis Total Solids Concentration A - 11
Cancel 2 - 5 Volume Offset A - 4
Parameter Files 2 - 7 Volume Scale A - 4
Perform 6 - 1, 6 - 3 Calibrate
QuickStart 6 - 7 Insert
review 6 - 9 0.1cm3 D - 5
sequence 6 - 8 1, 10, 3.5, 35, 650, and 1300 cm3
Analysis Conditions Inserts D - 6
create parameter file 5 - 2 temperature offset 10 - 2
defined 5 - 2 using the keypad 10 - 12
FoamPyc Application 5 - 4 using the software 10 - 1
Analysis Module volume 10 - 13
Add to Temperature Controlled Unit H - 2 volume scale 10 - 6
Analytical Balance 11 - 3, J - 17 zero cell volume 10 - 3
Analyzer zero pressure 10 - 4
connect to computer J - 8 Calibration 10 - 1
schematic 3 - 10 Calculations A - 4
show status 3 - 11 copy data 10 - 18
status 3 - 9 data, keypad 10 - 12
Analyzing, file status 3 - 7 load data 10 - 18
Application. start J - 22 load from file 10 - 11
Asphalt Density Application 1 - 3 report 10 - 1
Asphalt Density Calculations A - 3 reset pressure 10 - 5, 10 - 14
Asphalt Density Measurement, TEC review 10 - 15
Modules G - 4 save to file 10 - 11
Axis Cross-hair 7 - 16 Temperature 10 - 17
verify operation 10 - 10

Index - 1
134-42800-01 (Rev A) — Jan 2016
Index
Zero the chamber volume (using the Equilibration Report

keypad) 10 - 17 report options 8 - 4
Zero the pressure transducer (using the Equipment Options 1 - 7
keypad) 10 - 17 Error Messages B - 1
Cell leaks Keypad B - 21
check for 12 - 5 Ethernet Switch, connect J - 18
check using software 12 - 5 Expansion Chamber
check using the keypad 12 - 5 check for leaks 12 - 5
Chamber Cap O-Ring 12 - 3 check for leaks using software 12 - 5
Circulating bath, attach H - 1, J - 5 check for leaks using the keypad 12 - 5
Collected Data 5 - 7
Combined Report
report example 7 - 21
F
report options 8 - 1
Common Fields and Buttons 3 - 2 Files
Complete, file status 3 - 7 default locations 3 - 7
Components description 3 - 7
handling J - 1 extensions defined 3 - 7
instrument 1 - 5 status 3 - 7
Computer, connect to analyzer J - 8 FoamPyc Option 1 - 3
Configuration options 1 - 8
Contact Us ii
Control chart, report 7 - 6
G
Gas
D depleted cylinder 12 - 11
guidelines for connecting 12 - 9
Data replace a gas cylinder 12 - 10
review 2 - 11 replacement cylinder 12 - 12
view results 2 - 13 Gas connection J - 6
Data Entry, Keypad 2 - 1 Gas Requirements J - 2
Density and Volume Table Glove Box 1 - 8
report options 8 - 1 Graph
Density vs Cycle Number features and shortcuts 7 - 13
report options 8 - 2 generate overlays 7 - 18
Density vs Time grid lines 7 - 17
report options 8 - 3 Report Example 7 - 24
Diagnostics, using Software 9 - 1 zoom feature 7 - 17
Display 2 - 1
Dust filter, clean 12 - 7
H
E Handling System Components J - 1
Hardware Installation 11 - 1
Equilibration
Report Example 7 - 26

Index - 2
134-42800-01 (Rev A) — Jan 2016
Index
I N
Inserts No Analysis, file status 3 - 7
10, 3.5, and 35 cm3 D - 4
Operating Parameters D - 6
Install O
software J - 19
software upgrade J - 24 Option presentation 3 - 5
Installation instructions J - 1 Options Report
Instrument components 1 - 5 report options 8 - 5
Instrument log, show 3 - 9 Overlays
generate 7 - 18
multiple graph 7 - 18
K multiple sample 7 - 19
Keyboard, connect J - 5
Keypad
about 2 - 2 P
calibrate using 10 - 12
Parameter files
about 5 - 1
L analysis 2 - 7
analysis conditions 5 - 2
Leaks directory 5 - 1
check for 12 - 5 FoamPyc application 5 - 4
check using software 12 - 5 Parts and Accessories 13 - 1
check using the keypad 12 - 5 Power Analyzer On and Off 1 - 9
List files 3 - 12 Power failure, recover from 12 - 14
Pressure and Volume Table
M Pressure calibration, reset 10 - 5
Print files 2 - 13, 3 - 12
Maintenance Pycnometer
guidelines for connecting gases 12 - 9 clean 12 - 8
replace gas cylinder 12 - 10 configure, with Keypad J - 9
Manual mode 2 - 6 High Pressure Core 1 - 7
Manual, about this iii Large Volume Core 1 - 7
Material parameters 4 - 5 reset 12 - 15
Menu structure 3 - 1 setup J - 2
Modules, connect 11 - 1 Pycnometer Configuration Diagrams J - 2
Multigas Option 1 - 8, C - 1
MultiVolume Inserts 1 - 7, D - 1
Q
QuickStart Analysis 6 - 7

Index - 3
134-42800-01 (Rev A) — Jan 2016
Index
R S
Regression Report 7 - 3 Sample
Regulator Pressure 12 - 13 Load 6 - 1
Report examples 7 - 21 Prepare 6 - 1
Combined Report 7 - 21 Sample cups, properties 4 - 4
Graph 7 - 24 Sample Defaults 3 - 9
Overlay 7 - 25 Sample file
Sample Log 7 - 27 create 4 - 1
Summary 7 - 22 defined 4 - 1
Tabular 7 - 23 open 3 - 14
Report header shortcuts 7 - 10 Sample log
Report Options 5 - 5 report 8 - 6
Density and Volume Table 8 - 1 Report Example 7 - 27
Density vs Cycle Number 8 - 2 Sample overlays 7 - 19
Density vs Time 8 - 3 Sample Volume Equation Derivation F - 1
Equilibration Report 8 - 4 Schematic
Options Report 8 - 5 instrument 3 - 10
Pressure and Volume Table 8 - 5 shortcuts 3 - 11
Sample Log Report 8 - 6 Selected Reports 8 - 1
Summary Report 8 - 6 Sequence Analysis 6 - 8
Total Pore Volume vs Temp. 8 - 8 shortcuts
Volume vs Cycle 8 - 8 application 3 - 8
Reports report header 7 - 10
about 7 - 1 schematic 3 - 11
axis cross-hair 7 - 16 Show instrument log 3 - 9
calibration 10 - 1 Show instrument schematic 3 - 10
Combined Report 8 - 1 Software
Control Chart 7 - 6 about 3 - 1
features and shortcuts 7 - 9 installation J - 19
graphs 7 - 13 reinstall or modify J - 23
reports 7 - 9 uninstall 3 - 15, J - 25
tabular report 7 - 12 SPC report 7 - 2
generate graph overlays 7 - 18 calculations A - 9
generate sample overlays 7 - 19 Specific Gravity A - 10
graph grid lines 7 - 17 Specifications 1 - 11
open and close 7 - 1 Status
Regression 7 - 3 analyzer 3 - 9, 3 - 11
SPC report options 7 - 2 Summary
start 7 - 1 Report Example 7 - 22
Tabular 8 - 7 Summary Report 8 - 6
toolbar 7 - 11
zoom feature 7 - 17
Review, data 2 - 11
RS-232 Pin Assignment E - 1
Run Precision A - 8

Index - 4
134-42800-01 (Rev A) — Jan 2016
Index
T Z
Tabular reports 8 - 7 Zero Cell Volume, calibrate 10 - 3
features and shortcuts 7 - 12 Zero Pressure, calibrate 10 - 4
TEC Module 1 - 2, G - 1
Asphalt Density Measurement G - 4
operate G - 2
set temperature G - 1, J - 5
Temperature Controlled Module 1 - 9, H - 1
Add an Analysis Module H - 2
hardware setup J - 5
Temperature offset, calibrate 10 - 2
Toolbar, Report 7 - 11
Total Pore Volume A - 10
vs Temperature
Total Solids Concentration A - 11
Trademarks 2
Transmit 2 - 7
Transmitted Data, data units I - 1
Troubleshooting and maintenance 12 - 1
U
Unit selections J - 23
V
Volume Offset A - 4
Volume Scale A - 4
calibrate 10 - 6
Volume vs Cycle
Volume, calibrate 10 - 13
W
Warranty i
Web Browser, Review Data with 2 - 11

Index - 5
134-42800-01 (Rev A) — Jan 2016

AccuPyc II Series Operator Manual

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ACCUPYC® II SERIES

GAS DISPLACEMENT PYCNOMETER

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