Documents - MX API RP 42 Espanol

20-mL Retort Kit
165-80: 20-mL Retort Kit with Thermostat (115V)

165-80-1: 20-mL Retort Kit with Thermostat (230V)
165-80-2: 20-mLRetort Kit with Electronic Temperature Controller (115V)
165-80-3: 20-mL Retort Kit with Electronic Temperature Controller (230V)
Instruction Manual
Updated 12/29/2014
Ver. 2.13
OFI Testing Equipment, Inc.

11302 Steeplecrest Dr. Houston, Texas 77065 U.S.A.
Tele: 832.320.7300 Fax: 713.880.9886 www.ofite.com

Copyright OFITE 2014
Table of Intro..................................................................................................2
Specifications..................................................................................2
Contents Equipment........................................................................................2
Components....................................................................................3
Safety................................................................................................5
Quick Start.......................................................................................6
Operation.........................................................................................7
Temperature Controller................................................................. 11
Calculations...................................................................................12
Maintenance...................................................................................14
Appendix........................................................................................15
Density-Temperature Chart........................................................15
Warranty and Return Policy.........................................................16
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com 1
Intro The retort provides a means for separating and measuring the volumes of
water, oil, and solids contained in a sample of drilling fluid. A known vol-
ume of sample is heated to vaporize the liquid components which are then
condensed and collected in a graduated receiver tube. Liquid volumes are
determined from reading the oil and water phases on the graduated cylinder.
The total volume of solids, both suspended and dissolved, is obtained by
noting the difference of the total sample volume versus the final liquid volume
collected. Calculations are necessary to determine the volume of suspended
solids since any dissolved solids will be retained in the retort. Relative vol-
umes of low-gravity solids and weight materials may also be calculated.
Specifications Size: 8.25" 7" 12.5" (31 18 32 cm)

Weight: 18 lb 6 Oz. (8.3 kg)
Maximum Temperature: 1000F (537C)
Temperature Control: Standard - Electronic Fixed Temperature Control
Cell Capacity: 20 mL
Heating Capacity: 500 Watts
Power Requirement: 115 Volt at 3 Amp or 230 Volt at 1.5 Amp 50/60 Hz
Equipment Sample Cup: 20 mL capacity
Condenser: Cools the water and oil vapors below their vaporization tempera-
ture prior to leaving the condenser chamber. 464 grams.
Heating Element: Raises the temperature of the sample above its vaporiza-
tion point within API Specifications, without causing the solids to boil over.
350 watts.
Thermostat: Limits the temperature of the retort to 930 70F.
Liquid Receiver: Graduated cylinder or tube, transparent and inert to oil,

water, or salt solutions and temperatures of up to 90F (32C).
Fine Steel Wool: No. 000 Steel Wool.
Do not use liquid steel wool or coated steel wool substitutes.
Grease: Never-Seez. Used for a thread seal and lubricant at high temperatures.
T-handle Drill: Used for cleaning the retort chamber and condenser passage.
Pipe Cleaner: Used for cleaning the retort chamber and condenser passage.
Spatula: Shaped to fit the inside dimensions of the sample cup.
Components Included:
#131-15 Graduated Cylinder, 20 mL
#152-37 AC Power Cord (115 Volt)
#152-38 AC Power Cord (230 Volt)
#153-03 Graduate Brush, " 8"
#165-06 Receiver Tube, 20 mL
#165-14-13 T-handle Drill
#165-41 Corkscrew
#165-42 Steel Wool; Grade 000. Extra Fine; Package of 4 Pads
#165-43 Pipe Cleaner
#165-44-1 High-Temperature Thread Lubricant; 4-oz. Tube
#165-46 Clip for Condenser
#165-82-1 Condenser, 20 mL, with Ultra-Torr Fitting
#165-83 Retort Chamber, 20 mL
#165-88 Spatula
#280-00 Wetting Agent; 1 oz.
Replacement Parts:
#122-074-1 Fuse, 5 Amp, 5 mm 20 mm (115 Volt)
#122-073-1 Fuse, 3 Amp, 5 mm 20 mm (230 Volt)
#165-15-4 O-ring for Ultra-Torr Fitting
#165-84 Insulator Block, Top
#165-85 Insulator Block, Bottom
#165-86 Insulator Block, Cover
#165-00-10 Thermocouple, Type J
#165-14-005 Insulation Material
#165-35-1 Heating Element (115 Volt)
#165-36-1 Heating Element (230 Volt)
#165-45 Neon Lamp, Red
#165-81 Retort Adapter
For Retorts without Electronic Temperature Control (#165-80, #165-80-1):

#130-79-53-0990 Thermostat (115 Volt)
#130-79-54-0990 Thermostat (230 Volt)
For Retorts with Electronic Temperature Control (#165-80-2, #165-80-3):

#165-80-4 Electronic Temperature Controller
Optional:
#165-80-SP Spare Parts Kit; 115V Retort Kit
Part Number Description Quantity
#122-074-1 Fuse, 5 Amp, 5 mm 20 mm 5
#131-15 Graduated Cylinder; 20 mL 1
#153-03 Brush, Graduate, " " 1
#153-07 Brush, 20 mL Receiver Tube 1
#165-06 Receiver Tube, 20-mL, 0-100%, with Certificate 2
#165-15-2 Ultra Torr Fitting 1
#165-15-4 O-ring for Ultra Torr Fitting 8
#165-41 Corkscrew 1
#165-42 Steel Wool; Grade 000. Fine; Package of 4 Pads 20
#165-43 Pipe Cleaner 6
#165-44-1 High-Temperature Thread Lubricant; 4-oz. Tube 1
#165-83-1 Lid, for 20 mL Sample Cup 1
#165-88 Spatula, for 20 mL Retort 1
#280-00 Wetting Agent 1
#165-80-1-SP Spare Parts Kit; 230V Retorts

Part Number Description Quantity
#122-073-1 Fuse, 3 Amp, 5 mm 20 mm 5
#131-15 Graduated Cylinder; 20 mL 1
#153-03 Brush, Graduate, " " 1
#153-07 Brush, 20 mL Receiver Tube 1
#165-06 Receiver Tube, 20-mL, 0-100%, with Certificate 2
#165-15-2 Ultra Torr Fitting 1
#165-15-4 O-ring for Ultra Torr Fitting 8
#165-41 Corkscrew 1
#165-42 Steel Wool; Grade 000. Fine; Package of 4 Pads 20
#165-43 Pipe Cleaner 6
#165-44-1 High-Temperature Thread Lubricant; 4-oz. Tube 1
#165-83-1 Lid, for 20 mL Sample Cup 1
#165-88 Spatula, for 20 mL Retort 1
#280-00 Wetting Agent 1
Spare parts listings are intended to be used as a guide only as individual us-
age will vary. Running a retort test twice a day will require more parts than
running a test once a week.
Safety The following guidelines should be followed to ensure safe operation of
retorts.
It is imperative that the laboratory technician be thoroughly familiar

with the proper operation and potential hazards of operating a retort.
Improper or negligent operation can result in severe burns and other
injuries.
1. The retort case will get very hot during the test and can cause severe
burns.
2. The retort chamber and tube will get very hot and can cause severe
burns.
3. Clean and dry the retort chamber and condenser, especially the inside of
the mud sample cup, lid, and the condenser passage (spout). Clean the
sample cup threads with a wire brush. The spatula, corkscrew tip, or a
knife may be used to dislodge solids inside the sample cup.
Make sure the spout and the hole in the lid of the mud sample cham-
ber are absolutely free of obstructions.
4. The assembly should be cooled to below 100F (37.8C).
5. Visually inspect the threads on the retort for any sign of damage before
use.
6. Change out the steel wool after every test to prevent solids from building
up.
7. Retorts used offshore should be changed out every 6 months for exami-
nation and cleaning.
8. Make sure the electrical source is fused and grounded. Ensure the power
cord is in good condition and the connector has a proper ground connec-
tion.
9. Pipe cleaners should be used to scrape out any residue out of the spout
leading to the condenser. An optional T-handle drill (#165-14-13) may be
used to scrape any carbon deposits that may build up inside the tube. If
the retort is used daily, the T-handle drill should be used at least once a
week.
10. The 10 mL and 20 mL Retorts are not recommended for testing cuttings.
For cuttings analysis use the 50 mL Retort.
Quick Start 1. Connect the retort to an electrical outlet and let it start heating up.
2. Pour the test sample through a Marsh Funnel screen to remove large
particles.
3. Mix the sample thoroughly, ending up with a slow speed for 2 - 3 minutes
to remove any trapped air.
4. Record the sample temperature and ensure it is within 10 degrees of the

sample when density was measured.
5. Use the T-handle drill to clear the spout of any obstructions.
6. Pack steel wool into the expansion chamber.
7. Slowly fill the retort mud cup to the top.
8. Place the lid on the mud cup. Some of the liquid should extrude from the
hole in the lid.
9. Wipe away any excess liquid from the cup and the threads.
10. Lubricate the mud cup threads with thread lubricant.
11. Hand tighten the mud cup onto the expansion chamber.
12. Attach the expansion chamber tube to the condenser.
13. Carefully place the retort chamber inside the heater block taking care to
not get burned.
14. Place a drop of wetting agent inside the glass receiver tube.
15. Attach the glass receiver tube to the clip on the condenser and let it hang
off the side of the table.
16. Observe the liquid exiting the condenser and continue heating for ten
minutes after the flow stops.
17. Remove the glass receiver and allow it to cool. Record the amount of
water, oil, and solids.
18. Unplug the retort.
19. Remove the retort chamber and condenser and allow them to air cool.
20. Using the corkscrew, remove the steel wool from the expansion chamber
as soon as it is cool enough to handle.
Operation 1. Collect a representative sample of drilling fluid and pour it through a
marsh funnel screen to remove any lost circulation material, large cut-
tings, or debris.
2. Mix the drilling fluid sample thoroughly to ensure it is homogeneous. En-

sure that no air is injected into the sample.
3. If the sample contains gas or air bubbles, add 2 to 3 drops of a defoaming

agent for every 300 mL of sample fluid. Stir slowly for 2 to 3 minutes to
release any entrained gasses.
Air or gas entrapment in the sample will result in erroneously high solids
content.
Do not test fluids that may contain formates. The formates will crystalize
and block the spout.
4. Record the sample temperature. It should be within 10F (5.5C) of the

temperature at which mud density was determined.
6. Pack steel wool into the expansion chamber to approximately 3/16 inches
(4.76 mm) above the threads. As determined from experience, use only
enough steel wool to prevent a boiling over of solids into the liquid receiver.
7. Using a clean syringe, fill the retort cup slowly with the non-aerated
sample in order to avoid air entrapment. Lightly tap the side of the cup
to expel any air and place the lid onto the cup. Rotate the lid to obtain a
proper fit and be sure a small excess of fluid flows out the hole in the lid.
Expansion Chamber Lid Retort Cup
8. Lubricate the threads on the sample cup with a light coat of thread lubri-
cant. This will prevent vapor loss through the threads and will also facili-
tate disassembly of the equipment at the end of the test.
9. Carefully hand tighten the retort cup onto the Expansion Chamber.
Ultra-Torr Connection
Expansion
Chamber
Retort
Cup
Condenser
10. Insert the expansion chamber arm into the Ultra-Torr connection on the
condenser. Tighten the screw cap on the Ultra-Torr Connection. Place
the chamber into the heating jacket and close the insulating lid.
Receiver Tube
11. Place a clean, dry liquid receiver under the condenser discharge tube.
The length of this receiver may require that it be angled out from the retort
or supported off the edge of the worktable. If the condenser clip is sup-
porting the receiver, be careful not to break the lip of the glass receiver on
the condenser.
12. Connect the retort to an electrical outlet to turn it on. Observe the liquid
exiting the condenser. Continue heating for ten minutes beyond the time
that no more condensate is being collected.
If whole mud boils over into the receiver tube, the test must be rerun.
Pack the retort body with a larger amount of steel wool and rerun the
test. Allow it to run a minimum of 45 minutes. The light on the front of the
retort will turn on while the heaters are engaged.
13. Remove the liquid receiver and allow it to cool. After it has cooled to am-
bient temperature, read and record the volumes (or volume percentage)
of the following:
a. total liquid volume

b. oil volume
c. water volume
A drop of Wetting Agent will improve the meniscus for easier reading.
Always read volumes from the lowest point on the meniscus curve inside
the receiver.
Meniscus
If an emulsion interface is present between the oil and water phases,

heating the interface may break the emulsion. One way to do this is
to remove the retort assembly from the heating jacket by grasping the
condenser. Carefully heat the receiver along the emulsion band by gently
touching the receiver for short intervals with the hot retort chamber. Avoid
boiling the liquid. After the emulsion interface is broken, allow the receiv-
er to cool and read the water volume at the lowest point of the meniscus.
14. Turn off the retort and allow it to cool prior to cleaning. Do not use cold
water to try to rapidly cool down the chamber.
Ultra-Torr
Connection
Temperature
Controller
Condenser
Controller Plug
The OFITE Retort will recover nearly 100% of refined oil that is being tested.
However, if the drilling fluid is made up of crude oil, calibration runs may not
be accurate, as the known percentage of crude oil in solution will need to be
predetermined. Recovery of some crude oil may be as low as 60% due to
impurities in the fluid, so crude oil is a poor indicator of the accuracy of the
instrument.
Temperature To set the temperature on the retort with the electronic temperature controller,
press the Up or Down button.
Controller By default, the temperature controller displays temperature in F. To change
the temperature units:
1. Press and hold the Up and Down buttons together until the large dis-
play reads "A1" and the small display reads "set". About 8 seconds.
2. Press the Up button twice. The large display will read 9LbL and the
small display will read set.
3. Press the green button. The large display will read either F or C
and the small display will read C_F.
4. Press the Up or Down button to change from F to C.
5. Press the button twice to return to the main display.
Increase Decrease
Temperature Temperature
Calculations The measured volumes (mL) of oil and water are converted into volume per-
cents based on the volume of whole mud in the retort cup.
100 (Oil Volume Collected, mL)

Volume Percent (%)Oil = VO =
Sample Volume, mL
100 (Water Volume Collected, mL)

Volume Percent (%)Water = VW =
Sample Volume, mL
Volume Percent (%)Solids = VS = 100 - (VO +VW)
The volume percent solids include both suspended solids (weight material,
etc.) and dissolved materials (for example salts). This volume percent will
represent total suspended solids only if the mud is an untreated, freshwater
mud.
To find the volume percent (%) of suspended solids and relate them to the
relative volumes of low-gravity solids and weighting materials, an accurate
mud weight and Chloride concentration must be known.
Chloride Concentration, mg/L

VSS = VS - VW
1,680,000 1.21 (CS)
Where:
VSS = Volume Percent (%) Suspended Solids
CS = Chloride Concentration, mg/L
Volume percent (%) Low-Gravity solids, Vlg, are calculated as follows:

1
Vlg = [100 Pf + (Pb - Pf)VSS - 12 Wm - (Pf - PO) VO ]
Pb - Plg
Where:
Vlg =
Volume percent (%) low-gravity solids.
Wm = Mud Weight, pounds per gallon
Pf = Density of filtrate, grams per cubic meter
Pb = Density of weighting material, grams per cubic meter
Plg = Density of low gravity solids, grams per cubic meter (use 2.6 if
unknown)
Po = Density of oil, grams per cubic meter (use 0.84 if unknown)
Volume percent (%) weighting material (Vb) is calculated as follows:
Vb = VSS - Vlg
Concentrations of low gravity solids, weighting material and suspended solids
may be calculated as:
Clg = 3.49 (Plg) (Vlg)

Cb = 3.49 (Pb) (Vb)
CSS = Clg + Cb
Where:
Clg = Low gravity concentration, pounds per barrel
Cb = Weighting material concentration, pounds per barrel
CSS = Suspended solids concentration, pounds per barrel
Maintenance Calibration of Retort Mud Cups:
1. Record the temperature of the retort cup and lid to the nearest 0.5C(1F).
2. Tare an electronic balance to zero and place the clean and empty retort
cup and lid on the balance. Record the weight.
3. Fill the retort cup with deionized water. Place the lid on top of the mud
cup and ensure that a small excess of liquid comes out of the hole.
4. Wipe excess liquid from the mud cup and lid. Avoid wicking out water
from the cup.
5. Place the filled retort and lid on the previously tared balance and record
the mass of water to the nearest gram.
6. Calculate the volume of the retort (Vrc) using the density of water at ambi-
ent temperature.
(See Density - Temperature Chart on page 15)
Mass of water, (g)

Vrc=
Water density, (g/cm3)
Calibration Check for Temperature:
1. Remove retort chamber assembly from heating chamber.
2. Obtain a thermometer capable of 1200F (516C) (#154-25) and position

the sensing probe inside the retort adapter block when the retort is turned
fully on.
3. Let temperature stabalize. The temperature should read in the range of

930F 70F (498C 21C).
Cleaning:
Clean the expansion chamber tube thoroughly with the T-handle drill (#165-14-
13) after every test. Over time the tube can completely fill with carbon deposits.
Appendix Density of Water as a Function of Temperature
Density-Temperature C F Density g/cm3
Chart 15.0 59.0 0.9991
15.5 59.9 0.9991
16.0 60.8 0.9990
16.5 61.7 0.9989
17.0 62.6 0.9988
17.5 63.5 0.9987
18.0 64.4 0.9986
18.5 65.3 0.9985
19.0 66.2 0.9984
19.5 67.1 0.9983
20.0 68.0 0.9982
20.5 68.9 0.9981
21.0 69.8 0.9980
21.5 70.7 0.9979
22.0 71.6 0.9977
22.5 72.5 0.9976
23.0 73.4 0.9975
23.5 74.3 0.9974
24.0 75.2 0.9973
24.5 76.1 0.9971
25.0 77.0 0.9970
25.5 77.9 0.9969
26.0 78.8 0.9968
26.5 79.7 0.9966
27.0 80.6 0.9965
27.5 81.5 0.9964
28.0 82.4 0.9962
28.5 83.3 0.9961
29.0 84.2 0.9959
29.5 85.1 0.9958
30.0 86.0 0.9956
30.5 86.9 0.9955
31.0 87.8 0.9953
31.5 88.7 0.9952
32.0 89.6 0.9950
32.5 90.5 0.9949
33.0 91.4 0.9947

33.5 92.3 0.9945
34.0 93.2 0.9944
34.5 94.1 0.9942
35.0 95.0 0.9940
Warranty and Warranty:
OFI Testing Equipment, Inc. (OFITE) warrants that the products shall be free from liens and defects in
Return Policy title, and shall conform in all respects to the terms of the sales order and the specifications applicable to
the products. All products shall be furnished subject to OFITEs standard manufacturing variations and
practices. Unless the warranty period is otherwise extended in writing, the following warranty shall apply:
if, at any time prior to twelve (12) months from the date of invoice, the products, or any part thereof, do not
conform to these warranties or to the specifications applicable thereto, and OFITE is so notified in writing
upon discovery, OFITE shall promptly repair or replace the defective products. Notwithstanding the fore-
going, OFITEs warranty obligations shall not extend to any use by the buyer of the products in conditions
more severe than OFITEs recommendations, nor to any defects which were visually observable by the
buyer but which are not promptly brought to OFITEs attention.
In the event that the buyer has purchased installation and commissioning services on applicable products,
the above warranty shall extend for an additional period of twelve (12) months from the date of the original
warranty expiration for such products.
In the event that OFITE is requested to provide customized research and development for the buyer,
OFITE shall use its best efforts but makes no guarantees to the buyer that any products will be provided.
OFITE makes no other warranties or guarantees to the buyer, either express or implied, and the warranties
provided in this clause shall be exclusive of any other warranties including ANY IMPLIED OR STATUTORY
WARRANTIES OF FITNESS FOR PURPOSE, MERCHANTABILITY, AND OTHER STATUTORY REM-
EDIES WHICH ARE WAIVED.
This limited warranty does not cover any losses or damages that occur as a result of:
Improper installation or maintenance of the products

Misuse
Neglect
Adjustment by non-authorized sources
Improper environment
Excessive or inadequate heating or air conditioning or electrical power failures, surges, or other
irregularities
Equipment, products, or material not manufactured by OFITE
Firmware or hardware that have been modified or altered by a third party
Consumable parts (bearings, accessories, etc.)
Returns and Repairs:
Items being returned must be carefully packaged to prevent damage in shipment and insured against pos-
sible damage or loss. OFITE will not be responsible for equipment damaged due to insufficient packaging.
Any non-defective items returned to OFITE within ninety (90) days of invoice are subject to a 15% restock-
ing fee. Items returned must be received by OFITE in original condition for it to be accepted. Reagents
and special order items will not be accepted for return or refund.
OFITE employs experienced personnel to service and repair equipment manufactured by us, as well as
other companies. To help expedite the repair process, please include a repair form with all equipment
sent to OFITE for repair. Be sure to include your name, company name, phone number, email address,
detailed description of work to be done, purchase order number, and a shipping address for returning the
equipment. All repairs performed as repair as needed are subject to the ninety (90) day limited warranty.
All Certified Repairs are subject to the twelve (12) month limited warranty.
Returns and potential warranty repairs require a Return Material Authorization (RMA) number. An RMA
form is available from your sales or service representative.
Please ship all equipment (with the RMA number for returns or warranty repairs) to the following address:
OFI Testing Equipment, Inc.

Attn: Repair Department
11302 Steeplecrest Dr.
Houston, TX 77065
USA
OFITE also offers competitive service contracts for repairing and/or maintaining your lab equipment, in-
cluding equipment from other manufacturers. For more information about our technical support and repair
services, please contact [email protected].

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20-mL Retort Kit

165-80: 20-mL Retort Kit with Thermostat (115V)

OFI Testing Equipment, Inc.

Specifications Size: 8.25" 7" 12.5" (31 18 32 cm)

Equipment Sample Cup: 20 mL capacity

Thermostat: Limits the temperature of the retort to 930 70F.

Liquid Receiver: Graduated cylinder or tube, transparent and inert to oil,

Fine Steel Wool: No. 000 Steel Wool.

Do not use liquid steel wool or coated steel wool substitutes.

Spatula: Shaped to fit the inside dimensions of the sample cup.

For Retorts without Electronic Temperature Control (#165-80, #165-80-1):

For Retorts with Electronic Temperature Control (#165-80-2, #165-80-3):

#165-80-1-SP Spare Parts Kit; 230V Retorts

It is imperative that the laboratory technician be thoroughly familiar

4. The assembly should be cooled to below 100F (37.8C).

4. Record the sample temperature and ensure it is within 10 degrees of the

5. Use the T-handle drill to clear the spout of any obstructions.

6. Pack steel wool into the expansion chamber.

7. Slowly fill the retort mud cup to the top.

10. Lubricate the mud cup threads with thread lubricant.

12. Attach the expansion chamber tube to the condenser.

18. Unplug the retort.

2. Mix the drilling fluid sample thoroughly to ensure it is homogeneous. En-

3. If the sample contains gas or air bubbles, add 2 to 3 drops of a defoaming

4. Record the sample temperature. It should be within 10F (5.5C) of the

5. Use the T-handle drill to clear the spout of any obstructions.

Expansion Chamber Lid Retort Cup

a. total liquid volume

If an emulsion interface is present between the oil and water phases,

4. Press the Up or Down button to change from F to C.

5. Press the button twice to return to the main display.

100 (Oil Volume Collected, mL)

100 (Water Volume Collected, mL)

Volume Percent (%)Solids = VS = 100 - (VO +VW)

Chloride Concentration, mg/L

Volume percent (%) Low-Gravity solids, Vlg, are calculated as follows:

Volume percent (%) weighting material (Vb) is calculated as follows:

Clg = 3.49 (Plg) (Vlg)

Mass of water, (g)

Calibration Check for Temperature:

1. Remove retort chamber assembly from heating chamber.

2. Obtain a thermometer capable of 1200F (516C) (#154-25) and position

3. Let temperature stabalize. The temperature should read in the range of

25.5 77.9 0.9969

26.0 78.8 0.9968

26.5 79.7 0.9966

27.0 80.6 0.9965

27.5 81.5 0.9964

28.0 82.4 0.9962

28.5 83.3 0.9961

29.0 84.2 0.9959

29.5 85.1 0.9958

30.0 86.0 0.9956

30.5 86.9 0.9955

31.0 87.8 0.9953

31.5 88.7 0.9952

32.0 89.6 0.9950

32.5 90.5 0.9949

33.0 91.4 0.9947