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Experimental Plan

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Mohamed Sayed Abdo

The document outlines an experimental procedure for hydrotreating various feedstocks over catalysts. It involves: 1) analyzing waste cooking oil (WCO), vacuum gas oil (VGO), and waste lube oil (WLO) feeds, 2) pre-treating the feeds, 3) characterizing fresh and spent catalysts, 4) preparing and configuring the catalysts in a reactor, 5) running trials with different feed compositions and conditions, and 6) analyzing products via GC, distillation, and routine tests. The goal is to hydrotreat WCO, VGO, and WLO mixtures at varying temperatures and catalysts.

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Experimental Plan

Uploaded by

Mohamed Sayed Abdo
20 views3 pages
The document outlines an experimental procedure for hydrotreating various feedstocks over catalysts. It involves: 1) analyzing waste cooking oil (WCO), vacuum gas oil (VGO), and waste lube oil (WLO) feeds, 2) pre-treating the feeds, 3) characterizing fresh and spent catalysts, 4) preparing and configuring the catalysts in a reactor, 5) running trials with different feed compositions and conditions, and 6) analyzing products via GC, distillation, and routine tests. The goal is to hydrotreat WCO, VGO, and WLO mixtures at varying temperatures and catalysts.

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HCK PHD plan

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The document outlines an experimental procedure for hydrotreating various feedstocks over catalysts. It involves: 1) analyzing waste cooking oil (WCO), vacuum gas oil (VGO), and waste lube oil (WLO) feeds, 2) pre-treating the feeds, 3) characterizing fresh and spent catalysts, 4) preparing and configuring the catalysts in a reactor, 5) running trials with different feed compositions and conditions, and 6) analyzing products via GC, distillation, and routine tests. The goal is to hydrotreat WCO, VGO, and WLO mixtures at varying temperatures and catalysts.

Copyright:

© All Rights Reserved
Download as PDF, TXT or read online from Scribd
Download as pdf or txt
20 views3 pages

Experimental Plan

Uploaded by

Mohamed Sayed Abdo
The document outlines an experimental procedure for hydrotreating various feedstocks over catalysts. It involves: 1) analyzing waste cooking oil (WCO), vacuum gas oil (VGO), and waste lube oil (WLO) feeds, 2) pre-treating the feeds, 3) characterizing fresh and spent catalysts, 4) preparing and configuring the catalysts in a reactor, 5) running trials with different feed compositions and conditions, and 6) analyzing products via GC, distillation, and routine tests. The goal is to hydrotreat WCO, VGO, and WLO mixtures at varying temperatures and catalysts.

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You are on page 1/ 3

1- Feed Analysis:

A) WCO

1) Elemental comp.

2) Species of fatty acids.

3) Density / ref. index/ P.P. / Tan / Avg. Mwt. / Flash Point / Visc. @100 F

4) ASTM Distillation.

B) VGO

1) Elemental comp.

2) ASTM Distillation.

3) Density / Sulfur content / color / carbon res. / Asph. / P.P. / Flash Point / Visc. @
100 F / Avg. Mwt. / Tan

C) WLO

1) Elemental comp.

2) ASTM Distillation.

3) Density / Sulfur content / color / carbon res. / P.P. / Flash Point / Visc. @ 100 F /
Avg. Mwt. / Tan / metal content / water content.

2- Feed Preparation:

A) WCO:

- Heating to remove water (100C)

- Use CaCl2 to remove water traces.

- Filtration.

B) VGO:

- No Preparation needed.
C) WLO:

- Heating to remove water (150C).

- Extraction of sludge with polar solvent(NMP).

- Mixing for 1 Hr.

- Settling for 24 Hr.

- Filtration.

3- Catalyst Characterization before and after runs.

4- Catalyst Preparation:
1) Calcination Up to 450 C for 3:4 Hrs.

2) Sulfiding with MSDS in the reactor.

5- Catalyst Configuration in the


reactor:

Cat. Porcelain
HCK= 70 ml + 70 ml

Cat. Porcelain
HDS= 15 ml + 15 ml

Ceramic balls = 15 ml
6- Run Conditions and order:

Between each run should be a test run.

Run Feed LHSV Feed Temp Press. H2/Oil


No. VGO WLO WCO hr-1 rate C Mpa v/v
% % %
ml/min
1 100 0 0 1.5 2.25 400 7 400
2 80 20 0 1.5 2.25 380 7 400
3 80 20 0 1.5 2.25 400 7 400
4 80 20 0 1.5 2.25 420 7 400
5 80 20 0 1.5 2.25 440 7 400
6 80 0 20 1.5 2.25 380 7 400
7 80 0 20 1.5 2.25 400 7 400
8 80 0 20 1.5 2.25 420 7 400
9 80 0 20 1.5 2.25 440 7 400
10 80 10 10 1.5 2.25 380 7 400
11 80 10 10 1.5 2.25 400 7 400
12 80 10 10 1.5 2.25 420 7 400
13 80 10 10 1.5 2.25 440 7 400
14 70 20 10 1.5 2.25 380 7 400
15 70 20 10 1.5 2.25 400 7 400
16 70 20 10 1.5 2.25 420 7 400
17 70 20 10 1.5 2.25 440 7 400
Catalyst Change 1
18 0 100 0 1.5 2.25 400 7 400
Catalyst Change 2
19 0 0 100 1.5 2.25 400 7 400

7- Product analysis:
1- GC and Distillation.

2- Distillation.

3- Routin analysis.

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