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13C NMR Student Product W11

This document is a 1H NMR spectrum showing the product of a Diels-Alder reaction between anthracene and maleic anhydride. The spectrum shows multiple peaks between 120-140 ppm indicating the presence of aromatic protons and a peak at 170 ppm characteristic of a carbonyl group, confirming the [2+4] cycloaddition product was formed.

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0% found this document useful (0 votes)
111 views2 pages

13C NMR Student Product W11

This document is a 1H NMR spectrum showing the product of a Diels-Alder reaction between anthracene and maleic anhydride. The spectrum shows multiple peaks between 120-140 ppm indicating the presence of aromatic protons and a peak at 170 ppm characteristic of a carbonyl group, confirming the [2+4] cycloaddition product was formed.

Uploaded by

ahmad.a.touseef
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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Expt7 - Diels-Alder (anthracene + maleic anhydride) CHEM 2120 W11

48.22
1 3 C N M R s tu d e n t p ro d u c t W 1 1

45.65
1.0

127.98
0.9

0.8

127.38
0.7

124.64
Normalized Intensity

0.6

0.5

76.94
77.58
77.26
138.32

0.4

0.3
140.86
170.69

0.2

0.1

180 160 140 120 100 80 60 40 20


1.0 1 3 C N M R s t u d e n t p r o d u c t W 1 1
Chemical Shift (ppm)
127.98

0.9

0.8
127.38

0.7
124.64
Normalized Intensity

0.6
125.43

0.5
138.32

0.4

0.3
140.86

0.2

0.1

142 140 138 136 134 132 130 128 126 124 122 120
Chemical Shift (ppm)

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