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Topic 2 - Experimental techniques
2 - Experimental techniques
41. OMN/14/2"
‘An important aspect of chemistry is purity and methods of purification.
(@) Give an example of substances used in everyday life which must be pure.
(b) Alist of techniques used to separate mixtures is given below.
chromatography crystallisation diffusion _ dissolving
evaporation filtration fractional distillation —_ simple distiliation
(i) From the list, choose the most suitable technique to separate the following.
water from seawater .....
helium from @ mixture of helium and methane
ethanol from a mixture of ethanol and propanol
iron filings from a mixture of iron filings and water
a mixture of two amino acids, glycine and alanine ..
i
(li) Describe how you would obtain a pure sample of copper(II) sulfate-5-water crystals from
a mixture of copper(II) sulfate-5-water with copper(II) oxide using some of the techniques.
listed above.
4)
Total: 10]2. o/N/2012/1?
Allist of techniques used to separate mixtures is given below.
filtration
dittusion
fractional distillation
simple distillation
crystallisation
chromatography
From this list, choose the most suitable technique to separate the following mixtures,
A technique may be used once, more than once or not at all.
(a) butane from a mixture of propane and butane
(b) oxygen from liquid air
. 1
(c) water from aqueous magnesium sulfate - tt)
(d) potassium chloride from aqueous potassium chioride z exsoittl
(e) silver chloride from @ mixture of silver chloride and water ol
a)
(otal: 6]
(f)_ glucose from a mixture of glucose and maltose
3. Mig2011/1°
The following techniques are used to separate mixtures.
A simple distillation B fractional distilation C evaporation
D chromatography E filtration F diffusion
From this list, choose the most suitable technique to separate the following,
(a) methane from a mixture of the gases, methane and ethane... 1m
(b) water from aqueous magnesium sulfate = (1)
(1)
(c) glycine from a mixture of the amino acids, glycine and lysine ..
(d) iron filings from a mixture of iron filings and water ty
(e) zinc sulfate crystals from aqueous zinc sulfate 0
(f)_hexane from a mixture of the liquids, hexane and octane m4. O/N/2012/1*
Strontium chloride-6-water can be made from the insoluble compound, strontium
carbonate, by the following reactions.
SrCO{s) + 2HCI(aq) + SrCi,(aq) + CO,g) + H,0(I)
‘S1Cl, (aq) + 6HO(l) > SICI,.6H,0(s)
The following method was used to prepare the crystals.
‘Add excess strontium carbonate to hot hydrochloric acid.
Filter the resulting mixture.
Partially evaporate the filtrate and allow to cool.
Filter off the crystals of SrC1,.6H,O.
Dry the crystals between filter papers.
ahone
(i) How would you know when excess strontium carbonate had been added in step 17
ell sealord atten 4
(ii) Why is it necessary to filter the mixture in step 2?
Leta dade tetln A
(iii) In step 3, why partially evaporate the filtrate rather than evaporate to dryness?
5. O/N/20075
A list of techniques used to separate mixtures is given below.
fractional
distillation di
aon crystallization _ filtration diffusion
From the list choose the most suitable technique to separate the following.
water from aqueous copper(II) sulphate
helium from a mixture of helium and argon
copper(I) sulphate from aqueous copper(ll) sulphate
ethanol from aqueous ethanol
barium sulphate from a mixture of water and barium sulphate
(Total: 5]6. M/J/2009/1*
‘Some grass is crushed and mixed with the solvent, propanone. The colour pigments are
extracted to give a deep green solution.
{a) (i) Draw a labelled diagram to describe how you could show that there is more than
one coloured pigment in the green solution.
(3)
(ii) Given a pure sample of chlorophyll, how could you show that the green solution
from the grass contained chlorophyll?
(b) Explain the role of chlorophyll in green plants.
[Total: 8]