en

Polarimeters P8000 Series

PS8000 Series
P8000-PT Series
P3000 Series
P1000-LED
Polarimeter Accessories
innovation since 1796

www.kruess.com
 What is polarimetry?

If we regard light as an electromagnetic wave Optically active are chiral substances whose molecules
propagating through space, it is possible to illustrate the can take up different spatial arrangements that can not
phenomenon of polarized light. be aligned with by a rotation. Hence, this is a form of
The oscillation and the direction of propagation of the configuration isomerism. The different molecules of the
wave define a very specific plane. If you would look substance are called enantiomers.
towards the beam you would see this wave as a line
which is inclined at a certain angle in space. The following two enantiomers of lactic acid are an
Regular light includes waves that are inclined in any example of such a molecule:
direction of the space while polarized light is inclined
only at a defined angle.
This polarization can only be achieved by a very close
meshed grating a polarization filter. This one filters O OH O OH
out all waves from the regular light that do not have C C
the same inclination as the filters grating. Is the light
now directed to a second grating which is exactly 90 to HO C H H C OH
the first grating, no light will fall on the detector or the
human eye located behind it. If you place an optically H C H H C H
active substance between the two filters, light will again H H
pass through the second filter.
Optically active substances change the inclination of the S- (+) lactic acid R- (-) lactic acid
lightwave. Depending on the design of the device, the
second filter is rotated (manually or automatically) until
no light will fall on the detector. This technical setup
explains the terms optical rotation, rotation angle as The chiral center of the lactic acid is the middle carbon
well as the terms clockwise and anticlockwise. atom. Since the two enantiomers have different rotation
The two later terms describe the behavior of the wave angles, the polarimetry will provide information about the
mentioned above during the passage through an molecular structure.
optically active substance. Depending on the molecular In addition to the properties of the substance, the
structure of the substance, the direction of the inclination following factors also have an influence on the strength
of the wave is towards the right or towards the left. of the optical activity: the temperature, the wavelength
In order to be able to measure this change, the second of the light, the concentration of the substance and
filter has to be rotated anticlockwise or clockwise. possibly also the solvent.
Typical substances are sugar, lactic acid, tartaric acid but The following applies as well: The longer the path of the
also many other biologically active substances. light through an optically active substance, the larger the
angle of rotation.

auxiliary prism telescope

polarizer analyzer
light source sample

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 A.KRSS Optronic Polarimeters

P8000 Series Automatic Polarimeters 5

PS8000 Series Automatic Sugar Polarimeters 8

P8000-PT Series Automatic Polarimeters

with Peltier temperature control 9

P3000 Series Automatic Polarimeters 10

P1000-LED Manual Lab Polarimeter 11

Polarimeter accessories 12

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 P8000 Series | Automatic Polarimeters

The digital polarimeters of the P8000 series feature an

innovative measuring principle to measure optically
active liquids.
This patented development reduces the measuring time
to one second irrespective of the rotation angle of the
sample, which, compared to conventional polari-
meters, saves a lot of time.
All adjustments on the device are made via an
easy to use touchscreen.
In addition, an easy to understand help display
can be called up at any time.
With only very little effort, the user can carry out
a simple menu-driven calibration using test quartz.
The T-models of the P8000 series are equipped with
thermostat interfaces and the delivery includes an
external PT31 thermostat. This allows the connection of
temperature-controlled gauge heads to achieve high-
precision measuring results.
The devices are intended for use in FDA regulated
sectors due to their GLP compliance, integrated user
management and full network support, for simple
connection to the laboratory environment and an LIMS.
21 CFR Part 11 software is also available for the device.
All internal data (measurement values, parameters and
methods) are organised in an SQL database.
This can be accessed externally using SQL queries Range of applications
through a fixed interface (e.g. LIMS).
A self-explanatory touch screen with clear menu naviga- Pharmaceutical industry
tion and data output and USB/RS-232 interfaces fulfil all
Monitoring chemical processes
demands.
Purity control and determination of
concentrations
Examination of substances listed in the
German Pharmacopoeia

Chemical industry
Purity control and determination of
The features at a glance concentrations
Analysis of optically active components
Automatic, digital polarimeter with a high (qualitative and quantitative)
accuracy and resolution
Determination of changes in the configuration
Reliable, robust and easy to operate
Monitoring chemical processes
Reduces the measuring time to 1 second
irrespective of the angle of the sample
Sugar industry
Menu-driven touchscreen operation
Quality control of original and end product
Sample parameters can be customized
Determination of fructose and glucose
Ideal for individual, continuous analyses
RS-232, USB and Ethernet interfaces for PC
and printer Food industry
Simple output of all important measuring data Determination of concentration
including date and time Purity control
Low noise level Quality control

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 Main measuring display

This is where the measurement is

carried out and the results as well
as the important parameters are
displayed.

Reading [, Z, g/ml],
optical rotation,
concentration
Tube temperature
Sample number
Tube length
Wavelength
Thermostat temperature
Status information

Parameter selection

This menu is used to adjust the

measuring parameters.

Sample designation
Comment
Tube length
Wavelength
Measuring unit [, Z, g/ml]
Specific rotation

Help monitor

The symbols used in the main

measuring display are explained on
the help monitor.

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 P8000 P8000-T P8100 P8100-T

Measuring method Optical rotation, Optical rotation, Optical rotation, Optical rotation,
int. sugar scale, int. sugar scale, int. sugar scale, int. sugar scale,
concentration, concentration, concentration, concentration,
spec. rotation, spec. rotation, spec. rotation, spec. rotation,
user-defined user-defined user-defined user-defined
Measuring range 90 90 90 90
259 Z 259 Z 259 Z 259 Z
0...99.9 g/ml 0...99.9 g/ml 0...99.9 g/ml 0...99.9 g/ml
Measuring units Angle [, Z], Angle [, Z], Angle [, Z], Angle [, Z],
conc. [g/100 ml], conc. [g/100 ml], conc. [g/100 ml], conc. [g/100 ml],
user defined user defined user defined user defined
Resolution 0.001 0.001 0.001 0.001
0.01 Z 0.01 Z 0.01 Z 0.01 Z
0.1 g/ml 0.1 g/ml 0.1 g/ml 0.1 g/ml
Accuracy 0.003 0.003 0.002 0.002
0.01 Z 0.01 Z 0.01 Z 0.01 Z
0.5 g/100ml 0.5 g/100ml 0.5 g/100ml 0.5 g/100ml
Reproducibility 0.002 0.002 0.002 0.002
Measuring time 90 1s 1s 1s 1s
Light source 1 LED with filter 589 nm 1 LED with filter 589 nm 1 LED with filter 589 nm 1 LED with filter 589 nm
Wavelength 589 nm 589 nm 589 nm 589 nm
others optional others optional others optional others optional
Wavelength selection One fixed wavelength One fixed wavelength One fixed wavelength One fixed wavelength
Connection for Special tube with Special tube with Special tube with Special tube with
temperature sensor temperature sensor temperature sensor temperature sensor temperature sensor
PT100 required PT100 required PT100 required PT100 required
Temperature measurement 0...99.9 C 0...99.9 C 0...99.9 C 0...99.9 C
Temperature resolution 0.1 C 0.1 C 0.1 C 0.1 C
Temperature accuracy 0.2 C 0.2 C 0.2 C 0.2 C
Temperature Tube Tube Tube Tube
reading point
Thermostat Peltier thermostat Peltier thermostat
with water with water
Range of 15...40.0 C 15...40.0 C
temperature control
Accuracy of 0.2 C 0.2 C
temperature control
Max. length of tube 220 mm 220 mm 220 mm 220 mm
Sensitivity min 0.1 % (OD3) min 0.1 % (OD3) min 0.1 % (OD3) min 0.1 % (OD3)
Calibration Automatic Automatic Automatic Automatic
(menu-driven) (menu-driven) (menu-driven) (menu-driven)
Display LCD 5.7 LCD 5.7 LCD 5.7 LCD 5.7
320x240 pixel 320x240 pixel 320x240 pixel 320x240 pixel
color display color display color display color display
Operation Touchscreen Touchscreen Touchscreen Touchscreen
Measured data storage 999 measurements 999 measurements 999 measurements 999 measurements
Interfaces RS-232 RS-232 RS-232 RS-232
USB USB USB USB
Ethernet Ethernet Ethernet Ethernet
Operating voltage 100 V...250 V~ 100 V...250 V~ 100 V...250 V~ 100 V...250 V~
50/60 Hz 50/60 Hz 50/60 Hz 50/60 Hz

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 PS8000 Series | Automatic Sugar Polarimeters

The PS8000 is a precise and fast polarimeter

especially designed for the application in the
sugar industry. The operation and the
measuring functions are same as those for
the P8000. The measuring values are
displayed in the international sugar scale.
The rotation angle is shown as additional
information. The display of the international
sugar scale is possible for different initial
weights: except for the standard unit of 26 g,
initial weights of 13 g and 6.5 g can also be
selected.

Technical data | PS8000 and PS8000-T

PS8000 PS8000-T PS8000 PS8000-T

Measuring method International International Temperature reading Tube Tube

sugar scale sugar scale point
Measuring range 250 Z 250 Z Thermostat Peltier Thermostat
Measuring units Angle (Z) Angle (Z) with water

Resolution 0.01 Z 0.01 Z Range of temperature 15...40.0 C

control
Accuracy 0.01 Z 0.01 Z
Accuracy of 0.2 C
Reproducibility 0.02 Z 0.02 Z
temperature control
Measuring time 90 1s 1s
Max. length of tube 220 mm 220 mm
Light source 1 LED with filter 1 LED with filter
Sensitivity min 0.1 % (OD3) min 0.1 % (OD3)
Wavelength 589 nm 589 nm
(others optional) (others optional)
Calibration Automatic Automatic
(menu-driven) (menu-driven)
Wavelength selection One fixed One fixed Display LCD 5.7 LCD 5.7
wavelength wavelength 320x240 Pixel 320x240 Pixel
color display color display
Connection for Special tube Special tube
temperature sensor with temperature with temperature Operation Touchscreen Touchscreen
sensor PT100 sensor PT100
requires requires Measured data storage 999 999
measurements measurements
Temperature 0...99.9 C 0...99.9 C
Interfaces RS-232 RS-232
measurement USB USB
Ethernet Ethernet
Temperature resolution 0.1 C 0.1 C
Operating voltage 100...250 V 100...250 V
Temperature accuracy 0.2 C 0.2 C 50/60 Hz 50/60 Hz

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P8000-PT Series | Autom. Polarimeter with Peltier Temperature control

Based on the reliable P8000 series, A. Krss

Optronic has developed a polarimeter with
electronic temperature control.
This makes it possible to omit the water bath
thermostat that is otherwise required for per-
forming precise measurements.
The advantages are obvious:
There is no thermostat to be readjusted and
maintained. The set-point temperature is
entered directly on the touch-screen of the
polarimeter and the device can automatically
detect whether the tube has been connected.
Of course, it is possible to use standard tubes
without temperature control if the accuracy
of a temperature-controlled sample is not
required.
In case the sample has been warmed up
before, the time to bring it up to the right tem-
perature can be considerably reduced thus uti-
lizing the short measuring time of the P8000-
Serie approx. one second . The P8000 series
is the fastest polarimeter in the world!

Sensitivity min 0.1 % (OD3)

P8000-PT
Calibration Automatic (menu-driven)
Measuring method Optical rotation, Display LCD 5.7 320x240 Pixel,
int. sugar scale, color display
concentration,
spec. rotation, Operation Touchscreen
user defined Measured data storage 999 measurements
Measuring range 90 Interfaces RS-232
259 Z USB
0...99.9 g/ml Ethernet
Measuring units Angle [, Z] Operating voltage 100 V...250 V~, 50/60 Hz
conc. [g/100ml]
user defined
Resolution 0.001
0.01 Z Peltier Temperature Special tube PRM-100-PT
0.1 g/ml control necessary
Accuracy 0.003
Temperature 0...99.9 C
0.01 Z
0.5 g/100ml
measurement
Temperature resolution 0.1 C
Reproducibility 0.002
Temperature accuracy 0.2 C
Measuring time 90 1s
Temperature reading Tube
Light source 1 LED with filter 589 nm
point
Wavelength 589 nm
Range of temperature 15...40.0 C
others optional
control
Wavelength selection one fixed wavelength
Accuracy of 0.2 C
Max. length of tube 220 mm temperature control

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 P3000 Series | Automatic Polarimeters

The P3000 is a very easy to operate

polarimeter for the fully automatic
measurement of the optical rotation.
The measurement value is automatically
shown directly after the sample has been
inserted and output in angular degrees.
The delivery of the polarimeter includes
accessories and PC software for the operation
and storage.

Range of applications Technical data

Pharmaceutical industry
P3001RS P3002RS
Monitoring chemical processes
Purity control and determination of Measuring range 45 45
concentrations Resolution 0.005 0.001
Examination of substances listed in the
Accuracy <0.01 <0.004
German Pharmacopoeia
Measurement duration 1/ s 1/ s
Minimum light transfer
Chemical industry 10 % 1%
of sample
Purity control and determination of Light source Sodium lamp (589 nm)
concentrations
230 or 110 V, AC,
Analysis of optically active components Power supply 50/60 Hz, 100 W
(qualitative and quantitative)
Determination of changes in the configuration
Monitoring chemical processes

Sugar industry
Quality control of original and end product
Determination of fructose and glucose

Food industry Scope of delivery

Determination of concentration
Polarimeter tubes 100 and 200 mm
Purity control
Spare sodium lamp 589 nm
Quality control
Small glass cover plates for polarimeter tubes

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 P1000-LED | Manual Lab Polarimeter

The P1000-LED polarimeter is a simple and

robust device for basic applications in the lab
and for training. It operates according to the
half-shade principle and the reading takes place
via an eye-piece and two noniuses.
The P1000-LED features a high-quality metal
stand and a sample chamber for tubes of up to
220 mm length.
It is equipped with a swivel-mounted cover,
polarizer and analyzer and the delivery includes
accessories.

Technical data New LED light: saves current and lasts longer
Measuring range 2 semi-circles (0-180)
Glass tubes 100 and 200 mm
Scale division 1
Reading precision 0.05 (with nonius)
Light source LED

Scope of delivery
Polarimeter tubes 100 and 200 mm

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 Polarimeter Accessories

Polarimeter tubes made of glass

Micro glass tube for small sample volumes.

No temperature control
Article No Length in mm Volume in ccm
PRG-50-M 50 0.55
PRG-100-M 100 11.00

Glass tube with bubble trap for single measurements.

No temperature control
Article No Length in mm Volume in ccm
PRG-100 100 8.00
PRG-200 200 15.00

Glass tube with funnel.

No temperature control
Article No Length in mm Volume in ccm
PRG-50-E 50 3.00
PRG-100-E 100 6.00
PRG-200-E 200 12.00

Glass tube with funnel and temperature sensor.

With temperature control
Article No Length in mm Volume in ccm
PRG-100-ETT 100 6.00
PRG-200-ETT 200 12.00

The temperature sensor is also available with acid-resistant Teflon coating!

Custom-made product: If this selection of polarimeter tubes and quartz plates does not meet your requirements, please do not
hesitate to contact us!

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Polarimeter tubes made of stainless steel

Stainless steel micro flow-through tube with hose connectors.

No temperature control
Article-No Length in mm Volume in ccm
PRM-10-SDM 10 1.50

Stainless steel polarimeter tube with funnel.

With temperature control
Article No Length in mm Volume in ccm
PRM-100-ET 100 12.00
PRM-200-ET 200 17.00

Stainless steel flow-through tube with funnel and overflow pipe.

No temperature control
Article No Length in mm Volume in ccm
PRM-100-D 100 12.00
PRM-200-D 200 17.00

Stainless steel flow-through tube with funnel and overflow pipe.

With temperature control
Article No Length in mm Volume in ccm
PRM-100-DT 100 12.00
PRM-200-DT 200 17.00

Stainless steel flow-through tube with hose connectors.

No temperature control
Article No Length in mm Volume in ccm
PRM-50-SD 50 10.00
PRM-100-SD 100 12.00
PRM-200-SD 200 17.00

Stainless steel flow-through tube with hose connectors.

With temperature control
Article No Length in mm Volume in ccm
PRM-10-SDT 100 12.00
PRM-200-SDT 200 17.00

Stainless steel flow-through tube with hose connectors and temperature sensor.
With temperature control
Article No Length in mm Volume in ccm
PRM-100-SDTT 100 12.00
PRM-200-SDTT 200 17.00

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 Quartz Control Plates

Economy quartz control plates with manufacturers certificate

PQE+17 +17 (+/- 1), +50 Z (+/- 1Z)
PQE+34 +34 (+/- 1), +99 Z (+/- 1Z)
PQE -17 -17 (+/- 1), -50 Z (+/- 1Z)
PQE -34 -34 (+/- 1), -99 Z (+/- 1Z)

Premium quartz control plates with manufacturers cartification

traceable to official PTB certificate
(individual PTB certificate available upon request)
PQP+8 +8 (+/- 1), +25 Z (+/- 1Z)
PQP+17 +17 (+/- 1), +50 Z (+/- 1Z)
PQP+26 +26 (+/- 1), +75 Z (+/- 1Z)
PQP+33 +33 (+/- 1), +95 Z (+/- 1Z)
PQP+34 +34 (+/- 1), +99 Z (+/- 1Z)
PQP-10 -10 (+/- 1), -30 Z (+/- 1Z)

CBM910 | printer 24 characters regular paper printer for digital refractometer

from the DR6000 series and the digital Abbe refractometer
AR2008 as well as for our digital polarimeters from the
P8000 series.

Sodium Lamps P1000-300

Spare sodium lamp

Glass Cover Plate P1000-150

Glass cover plate for polarimeter tube, package of 2 pieces

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PT31 | Peltier Thermostat The electronic water bath thermostat with Peltier element is a
versatile and powerful device used to control the temperature of
refractormeters, polarimeters etc.
It is extremely robust, compact and easy to operate.
Saves space in the lab due to its small size.

Specifications PT31
Resolution 0.1 C
Heating output 30 W
Cooling efficiency 15 W
Power supply 115-230 ~
Pump pressure 2000 Pa
Pump capacity 20 l/h
Temperature 8-40 C (continuously variable)
Temperature accuracy 0.2 C
Dimensions L/B/H 140 x 80 x 210 mm
Weight 1.5 kg

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 State: June 2010 | subject to technical modification without notice / errors and omissions excepted

A.KRSS Optronic GmbH

Alsterdorfer Strae 276278
22297 Hamburg | Germany
Telefon +49-(0)40-51 43 1 7- 0
Fax +49-(0)40-51 43 1 7- 60
eMail [email protected]
Web www.kruess.com