Designation: G123 00 (Reapproved 2015)

Standard Test Method for

Evaluating Stress-Corrosion Cracking of Stainless Alloys
with Different Nickel Content in Boiling Acidified Sodium
Chloride Solution1
This standard is issued under the fixed designation G123; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon () indicates an editorial change since the last revision or reapproval.

1. Scope bility of regulatory limitations prior to use. For specific hazard

1.1 This test method covers a procedure for conducting statements, see Section 8.
stress-corrosion cracking tests in an acidified boiling sodium
2. Referenced Documents
chloride solution. This test method is performed in 25 % (by
mass) sodium chloride acidified to pH 1.5 with phosphoric 2.1 ASTM Standards:2
acid. This test method is concerned primarily with the test D1193 Specification for Reagent Water
solution and glassware, although a specific style of U-bend test E8 Test Methods for Tension Testing of Metallic Materials
specimen is suggested. E691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
1.2 This test method is designed to provide better correla-
G15 Terminology Relating to Corrosion and Corrosion Test-
tion with chemical process industry experience for stainless
ing (Withdrawn 2010)3
steels than the more severe boiling magnesium chloride test of
G16 Guide for Applying Statistics to Analysis of Corrosion
Practice G36. Some stainless steels which have provided
Data
satisfactory service in many environments readily crack in
G30 Practice for Making and Using U-Bend Stress-
Practice G36, but have not cracked during interlaboratory
Corrosion Test Specimens
testing (see Section 12) using this sodium chloride test method.
G36 Practice for Evaluating Stress-Corrosion-Cracking Re-
1.3 This boiling sodium chloride test method was used in an sistance of Metals and Alloys in a Boiling Magnesium
interlaboratory test program to evaluate wrought stainless Chloride Solution
steels, including duplex (ferrite-austenite) stainless and an G49 Practice for Preparation and Use of Direct Tension
alloy with up to about 33 % nickel. It may also be employed to Stress-Corrosion Test Specimens
evaluate these types of materials in the cast or welded G107 Guide for Formats for Collection and Compilation of
conditions. Corrosion Data for Metals for Computerized Database
1.4 This test method detects major effects of composition, Input
heat treatment, microstructure, and stress on the susceptibility
of materials to chloride stress-corrosion cracking. Small dif- 3. Terminology
ferences between samples such as heat-to-heat variations of the 3.1 DefinitionsFor definitions of corrosion-related terms
same grade are not likely to be detected. used in this test method, see Terminology G15.
1.5 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information 4. Summary of Test Method
only. 4.1 A solution of 25 % sodium chloride (by mass) in reagent
1.6 This standard does not purport to address all of the water is mixed, and the pH is adjusted to 1.5 with phosphoric
safety concerns, if any, associated with its use. It is the acid. The solution is boiled and U-bends (or other stressed
responsibility of the user of this standard to establish appro- specimens) are exposed in fresh solution for successive one-
priate safety and health practices and determine the applica- week periods.

1 2
This test method is under the jurisdiction of ASTM Committee G01 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Corrosion of Metals and is the direct responsibility of Subcommittee G01.06 on contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
Environmentally Assisted Cracking. Standards volume information, refer to the standards Document Summary page on
Current edition approved Nov. 1, 2015. Published December 2015. Originally the ASTM website.
3
approved in 1994. Last previous edition approved in 2011 as G12300(2011). DOI: The last approved version of this historical standard is referenced on
10.1520/G0123-00R15. www.astm.org.

Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States

1
 G123 00 (2015)
4.2 The test may be continued for as many weeks as
necessary, but six weeks (about 1000 h) or less are expected to
be sufficient to crack susceptible materials. Longer exposures
provide greater assurance of resistance for those materials
which do not crack.
4.3 It is recommended that samples of a susceptible
material, for example, UNS S30400 or S31600 (Type 304 or
Type 316 stainless, respectively), be included as a control when
more resistant materials are evaluated.

5. Significance and Use

5.1 This test method is designed to compare alloys and may
be used as one method of screening materials prior to service.
In general, this test method is more useful for stainless steels
than the boiling magnesium chloride test of Practice G36. The
boiling magnesium chloride test cracks materials with the
nickel levels found in relatively resistant austenitic and duplex
stainless steels, thus making comparisons and evaluations for
many service environments difficult.
5.2 This test method is intended to simulate cracking in
water, especially cooling waters that contain chloride. It is not
intended to simulate cracking that occurs at high temperatures
(greater than 200C or 390F) with chloride or hydroxide.
NOTE 1The degree of cracking resistance found in full-immersion
tests may not be indicative of that for some service conditions comprising
exposure to the water-line or in the vapor phase where chlorides may
concentrate.
5.3 Correlation with service experience should be obtained
when possible. Different chloride environments may rank
materials in a different order.
FIG. 1 Apparatus Used for Stress-Corrosion Cracking Test
5.4 In interlaboratory testing, this test method cracked
annealed UNS S30400 and S31600 but not more resistant
materials, such as annealed duplex stainless steels or higher
nickel alloys, for example, UNS N08020 (for example 20Cb-34 0.95 in.) long drip tip is used. (Modified Allihn condensers
stainless). These more resistant materials are expected to crack with no drip tip and condensers with longer drip tips may
when exposed to Practice G36 as U-bends. Materials which produce different results. These alternate Allihn condenser
withstand this sodium chloride test for a longer period than designs may be used if control samples of susceptible (for
UNS S30400 or S31600 may be candidates for more severe example, UNS S31600) and resistant (for example, UNS
service applications. N08020) materials are included in the study.)
6.1.3 Hot Plate, capable of maintaining the solution at its
5.5 The repeatability and reproducibility data from Section boiling point.
12 and Appendix X1 must be considered prior to use. Inter-
laboratory variation in results may be expected as occurs with 7. Reagents
many corrosion tests. Acceptance criteria are not part of this 7.1 Purity of ReagentsReagent grade chemicals shall be
test method and if needed are to be negotiated by the user and used in all tests. Unless otherwise indicated, it is intended that
the producer. all reagents shall conform to the specifications of the Commit-
tee on Analytical Reagents of the American Chemical Society,
6. Apparatus
where such specifications are available.5 Other grades may be
6.1 The glassware used for this test method is shown in Fig. used provided it is first ascertained that the reagent is of
1 and is as follows: sufficiently high purity to permit its use without affecting
6.1.1 Flask1000-mL Erlenmeyer flask with a 45/50 results.
ground-glass joint.
6.1.2 Condenser, a four-bulb Allihn condenser with a 45/50
ground-glass joint (water-cooled joint suggested), a water 5
Reagent Chemicals, American Chemical Society Specifications, American
jacket at least 20 cm (8 in.) long and a 1 to 2.5 cm (0.4 to Chemical Society, Washington, DC. For suggestions on the testing of reagents not
listed by the American Chemical Society, see Analar Standards for Laboratory
Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,
4
20Cb-3 is a registered trademark of Carpenter Technology Corp., Reading, PA. MD.

2
 G123 00 (2015)
7.2 Purity of WaterSolutions shall be made with water of maximum applied tensile load experienced during fabrication.
purity conforming to at least Type IV reagent water as specified The same method must be used to fabricate all the U-bends in
in Specification D1193 (except that for this method limits for a given study.
chlorides and sodium may be ignored). 9.5.2 The bolt, nut, and flat washer must be made of a
material resistant to general corrosion, pitting, and stress
7.3 Sodium Chloride (NaCl)A solution of 25 % NaCl (by
corrosion cracking in the environment. UNS N10276 (Alloy
mass) acidified to pH 1.5 with phosphoric acid (H3PO4) is
C-276) is recommended because some other materials (for
used. The solution may be prepared by adding 750 g H2O
example, titanium or UNS N06600 [Alloy 600]) may be
(750 mL) to 250 g NaCl, and adjusting to pH 1.5 with H3PO4.
attacked resulting in an increase in solution pH.
Varying quantities of solution may be prepared and larger
9.5.3 The metallic fastener must be electrically isolated
amounts may be stored indefinitely in appropriate glassware.
from the specimen by a rigid shoulder washer (that is, zirconia
The pH must be determined prior to each use.
or another material that will not be compressed during the test).
9.5.4 The extended end of the bolt may require cutting to fit
8. Hazards
into the test vessel.
8.1 Normal precautions for handling boiling liquid should
be observed. 10. Procedure
8.2 All heating or boiling of the NaCl solution should be 10.1 Stress the specimens, examine at 20, and replace any
done in an area where personnel are not likely to accidentally specimens with cracks or other defects.
bump the flask. A hooded area is preferred. NOTE 2The direction and intensity of the incident light may affect
crack detection during the 20 examination.
8.3 Minimum personal protective equipment for handling
boiling sodium chloride should include safety glasses or 10.2 Degrease in a halogen-free solvent or laboratory
goggles, face shield, laboratory coat, and rubber gloves. detergent, rinse as necessary, and dry. It is best practice to
(WarningU-bends (and other highly stressed test speci- stress the specimens immediately before the beginning of the
mens) may be susceptible to high rates of crack propagation test. Any storage of the specimens should be in a clean
and a specimen containing more than one crack may splinter enclosure. A desiccant such as silica gel may be used. The
into two or more pieces. This may also occur due to a cracked specific level of relative humidity is not important for the
restraining bolt. Due to the highly stressed condition in a alloys of interest.
U-bend specimen, these pieces may leave the specimen at high 10.3 Place duplicate specimens in each 1000-mL Erlen-
velocity and can be dangerous.) meyer flask. Duplicate flasks (four specimens) are necessary to
evaluate a given sample of the specific material, material
9. Test Specimens condition, etc. (The specimens may be placed in the flasks after
the solution has been added, if convenient.)
9.1 U-bends are preferred but other stress corrosion crack-
ing specimens may be used with this test solution. The 10.4 The specimens in each flask must be kept separate and
specimen style chosen should provide sufficient stress to crack completely submerged. Tight crevices between the stressed
less resistant materials (for example, UNS S30400 or S31600) (bend) area and any means of specimen support should be
in 1000 h or less). (See Annex A1.) Regardless of the specimen avoided. The stressed area should be free from direct contact
style, it is recommended that UNS S30400 or UNS S31600, or with heated surfaces. Specimens may be supported on glass
both, be included as controls. rods or tubes or by glass fixtures.
9.2 The test specimen must be thick enough so that the 10.5 Drop boiling chips6 into the flasks.
applied stress does not cause mechanical rupture of less 10.6 Add 600 mL of 25 % NaCl solution, pH 1.5, to each
resistant materials if the cross section is reduced by pitting or flask. When each flask contains two U-bends as described in
general corrosion. Annex A1, the solution volume to sample surface area ratio is
5:1 mL/cm2 (33 mL/in.2).
9.3 The size of alternate specimens (other than those in
Annex A1) must allow a solution volume to specimen surface 10.7 Place the flasks on a hot plate and insert the condenser.
area ratio of at least 5:1 mL/cm2 (33 mL/in.2). Begin recording the test duration when the solution begins
boiling. The boiling point during interlaboratory testing was
9.4 A minimum of four replicates (two per flask) is required 106 to 110C (223 to 230F).
because of the variability typical in stress-corrosion testing.
10.8 After one week remove the flask from the hot plate,
9.5 Methods of fabricating U-bend specimens are provided determine the final pH of the solution at room temperature, and
in Annex A1. These procedures are based on Practice G30, but discard the remaining solution. A final pH over about 2.5
in addition provide a specimen that fits through a 45/50
ground-glass joint. Assurance that the legs are stressed suffi-
ciently by the bolt is also provided. 6
The sole source of supply of amphoteric alundum granules known to the
committee at this time is Hengar Co., Philadelphia, PA. If you are aware of
9.5.1 Other methods of producing U-bends described in
alternative suppliers, please provide this information to ASTM International
Practice G30 may be used; however, during exposure the Headquarters. Your comments will receive careful consideration at a meeting of the
U-bends must be (1) in the plastic range and (2) stressed to the responsible technical committee,1 which you may attend.

3
 G123 00 (2015)
suggests that general corrosion or pitting of the specimen or 12. Precision and Bias7
fastening device has occurred. A pH at this level is expected to
12.1 PrecisionVariability occurred in both repeatability
reduce the test severity and may delay or preclude failures of
UNS S31600. More rapid cracking of UNS S31600 appears and reproducibility for time-to-fail data developed using UNS
likely with a final pH of about 2 or less. S30400 and S31600 in an interlaboratory test program (Ap-
pendix X1). Such variability is typical in time-to-fail data for
10.9 Rinse and dry the specimens. Examine the bend area, stress-corrosion cracking tests, and is expected to preclude
legs, and area adjacent to the crevice (at the fastener) at 20 for detection of small differences between samples.
cracking. See Note 3. Record location of cracks. Additional
12.1.1 Histograms of the time-to-crack for UNS S30400
exposures or metallographic evaluation may be used to deter-
and S31600 tested in accordance with this test method appear
mine if questionable indications are, in fact, stress-corrosion
cracks. in Appendix X1 along with data from each laboratory. The
time-to-crack values in Appendix X1 are not necessarily the
NOTE 3Any cracking at the fastener is very likely due to residual maximum or minimum values which could be obtained in other
stresses and more aggressive solution which may be formed in crevices. If
crevices are expected in service (due to design of service equipment or
testing.
deposits), a U-bend specimen employing a crevice on the bend may be 12.1.2 Every specimen of UNS S30400 and S31600 cracked
evaluated. within the 1000-h interlaboratory test duration while no crack-
10.10 Periodic removal of the specimens from the solution ing occurred for more resistant materials, UNS S32550 (Fer-
may be necessary during the first week to determine the time ralium8 Alloy 225) and N08020.
when cracks first appear. Removal of the specimens is expected 12.1.3 It has been observed in stress-corrosion tests of
to disturb local corrosion cells and may influence test results. various metal-alloy systems that the precision is best for tests
All specimens in a given test program should have the same of specimens that have either a very low probability of
removal/examination schedule. When the time-to-crack is stress-corrosion cracking (few, if any, failures in the prescribed
recorded, the test duration at the previous examination (no test duration) or a high probability (short failure times). The
cracks) should also be noted. precision is least for groups of test specimens with an inter-
10.11 Expose for additional one-week periods as necessary. mediate probability. This was observed in the interlaboratory
Fresh solution must be used for each exposure and the initial test program. There were no failures of the more resistant
and final pH (at room temperature) must be recorded weekly. materials (UNS S32550 and UNS N08020), generally rapid
See 10.8 regarding the effect of the final pH. failure of the least resistant material (UNS S30400, see Fig.
10.12 After the final 20 examination (following the last X1.3), and greater variation in failure times for the material
test period) remove the fastener and examine the crevice areas expected to have intermediate resistance (UNS S31600, see
at 20 for cracking. Fig. X1.4).
10.13 A final examination for cracks may be performed by 12.1.4 Reproducibility between laboratories frequently var-
additionally bending the specimens until the ends of the legs ied more widely than repeatability within each laboratory.
touch. This may expose tight cracks which were not previously Although this variation is substantial, it is within what may be
detected. The additional bending may not be appropriate for expected for a stress-corrosion cracking test. The effects of
materials which are susceptible to hydrogen embrittlement in interlaboratory variation must be considered if data from
this environment. Do not re-expose specimens after this multiple laboratories are used.
additional bending. 12.1.5 Analysis of the interlaboratory test data using a log
10.14 Ruptured specimens should also be examined for normal distribution appears in Appendix X1.
evidence of mechanical failure resulting from the action of 12.2 BiasThe procedure in this test method for measuring
applied stress on specimens whose cross sections have been time-to-cracking of specimens in acidified sodium chloride
reduced by general or pitting corrosion, or both. Such failures solution has no bias because the time-to-cracking is defined
usually show evidence of ductility. Repeat tests with thicker only in terms of this test method, and there is no absolute
specimens should be made in case of doubt. standard for reference. Time-to-cracking is a function of
11. Report specimen type as well as stress and material composition.
11.1 Report the type of specimen used, method of specimen 13. Keywords
fabrication, times to cracking (including maximum time with-
out cracks), location of cracks, final pH of each exposure, and 13.1 boiling acidified sodium chloride (NaCl); glassware;
details regarding the Allihn condenser drip tip. Note whether or histograms; stress corrosion cracking; U-bend specimens; UNS
not metallographic techniques or additional bending of the N08020
specimen (see 10.13) were employed. Electronic data exchange
can be facilitated by using the fields suggested in Appendix X2
(excerpted from Guide G107). 7
Supporting data (including UNS S30400, S31600, S32550, and N08020) have
been filed at ASTM International Headquarters and may be obtained by requesting
11.2 Data for resistant materials shall be accompanied by Research Report RR:G01-1013.
data for at least four susceptible control specimens; for 8
Ferralium is a registered trademark of Langley Alloys, Ltd. of Slough, United
example, UNS S30400 or UNS S31600. Kingdom.

4
 G123 00 (2015)

ANNEX

(Mandatory Information)

A1. SUGGESTED TEST SPECIMEN

A1.1 Using the procedure described in this test method, the

U-bend specimen described in A1.2 has produced cracking of
UNS S30400 and S31600 in less than 1000 h, without cracking
more resistant duplex stainless and higher nickel (for example,
about 33 %) materials.
A1.2 Suggested specimen dimensions appear in Fig. A1.1.
The specimen differs slightly from those suggested in Practice
G30 to allow the completed U-bend to pass through a 45/50
ground-glass joint while being large enough to accommodate
ceramic insulators of sufficient size to resist cracking during
use.
A1.3 If surface finish is not the subject of the evaluation,
prepare the specimens to produce a 120-grit finish or its
equivalent with machining techniques.
A1.4 Bend the specimens around a 9.5 mm (0.375-in.)
diameter mandrel using an adjustable die similar to that in Fig.
A1.2 as follows. (This figure is the same as Fig. 4a in Practice
G30.)
A1.4.1 Mark the centerline on the specimen to aid aligning.
A1.4.2 Set the gap in the die at the mandrel diameter plus
two times the specimen thickness. NOTE 1Mandrel has 9.5 mm (0.375-in.) diameter. Dimension Z is
A1.4.3 First, depress the mandrel (hydraulic) until the apex mandrel diameter plus two times the specimen thickness.
of the U-bend is approximately level with the bottom of the FIG. A1.2 Suggested Stressing Fixture
(fastener inserted while specimen in die)
die. Continue stressing until the legs of the U-bend are nearly
parallel. Final stressing is preferably done with the fastener.
The specimen may be stressed in the die or it may be removed
and restressed outside the die. Partial stressing in the die
followed by final stressing outside the die may be optimum.
A1.4.4 Insert the stressing fastener. Use ceramic insulators
(zirconia or other non-compressible, corrosion resistant, non-
conductive material). Flat washers should be used between the
ceramic insulator and fastener to extend the life of the
insulator. The bolt, nut, and flat washer must resist corrosion in
the NaCl environment. UNS N10276 is recommended for all
three items.
A1.4.5 Stress the U-bend so that the legs are parallel, that is,
L, mm (in) M, mm (in) W, mm (in) T, mm (in) D, mm (in)
101.6 (4) 82.6 (314) 19.0 (34 ) ; 3.2 (; 18) 9.5 (38 )
the U-bend is more severely bent than it was due to the die
pressure. The inside dimension between the legs will be about
FIG. A1.1 Suggested U-Bend Specimen Dimensions 11.4 mm (about 0.450 in.).

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 G123 00 (2015)
APPENDIXES

(Nonmandatory Information)

X1. SUMMARY OF INTERLABORATORY TEST DATA ANALYSIS

X1.1 Test Method

X1.1.1 Testing in accordance with this test method was
performed by seven laboratories and included UNS S30400,
S31600, S32550, and N08020. Each laboratory exposed a
series of duplicate flasks, each containing two U-bends of each
grade. UNS N10276 fasteners were used by most laboratories
and the solution was replaced weekly. Examinations were
scheduled after 6 h, daily for one week, and weekly for six
weeks. Concerns of Practice E691 and Guide G16 were
considered as possible and appropriate.
X1.1.2 The pH was recorded before and after each expo-
sure. The initial pH was specified as 1.5. The change in pH
during all the one-week periods for all laboratories ranged
NOTE 1Four replicates tested per laboratory. Examinations scheduled
from +0.6 to +2.8 for UNS S30400 and 0.1 to +2.72 for UNS after 6 h, daily for one week, and weekly for six weeks.
S31600. Only one of the laboratories experienced a pH FIG. X1.2 Time-To-Crack for UNS S31600 U-Bends in pH 1.5 NaCl
increase greater than 0.55 for UNS S31600 and this increase Test
may have been related to attack of the fasteners.

X1.2 Interlaboratory Test Data Analysis Using Histo-

grams
X1.2.1 Fig. X1.1 and Fig. X1.2 present the time-to-crack
data for all U-bends of susceptible materials, UNS S30400 and
UNS S31600, respectively. The within-laboratory repeatability
was often better than the between-laboratory reproducibility.
This could occur if different operators had different ability to
detect cracks or tended to find cracks in all samples after cracks
in one sample were noticed.
X1.2.2 The nature of the data suggest that analysis by
histogram is superior to attempting to calculate mean and
standard deviation values. NOTE 1Seven laboratories, each tested four replicates. Examinations
scheduled after 6 h, daily for one week, and weekly for six weeks.
X1.2.3 Fig. X1.3 and Fig. X1.4 present histograms of the FIG. X1.3 Histogram of Time-To-Crack Data for UNS S30400
time-to-crack data for UNS S30400 and UNS S31600, respec- Stainless U-Bends in pH 1.5 NaCl Test
tively. All but one of the failures occurred in 28 days or less.
Cracks in one sample of UNS S31600 were found after 42 days
(1000 h). An increase in pH due to attack of the UNS N06600
fasteners may have delayed this cracking for at least one week.
X1.2.4 Four U-bends of UNS S32550 and N08020 were
exposed by each laboratory. These materials have demon-
strated good resistance to stress-corrosion cracking in service
and none of the U-bends cracked in the 42-day test.
X1.2.5 Analysis of the interlaboratory test data indicates
that materials which withstand this 42-day test without cracks
are more resistant to stress-corrosion cracking than UNS
S30400 and UNS S31600. This statement is based upon use of
the sampling and testing procedures employed in this inter-
laboratory test program.
X1.3 Interlaboratory Test Data Analysis Using a Log
NOTE 1Four replicates tested per laboratory. Examinations scheduled Normal Distribution
after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.1 Time-To-Crack for UNS S30400 U-Bends in pH 1.5 NaCl X1.3.1 The average time to cracking for the four replicates
Test of each grade tested at each laboratory are plotted in Fig. X1.5.

6
 G123 00 (2015)

NOTE 1Seven laboratories, each tested four replicates. Examinations

scheduled after 6 h, daily for one week, and weekly for six weeks.
FIG. X1.4 Histogram of Time-To-Crack Data for UNS S31600
Stainless U-Bends in pH 1.5 NaCl Test

The tendency to follow straight line relationships suggests FIG. X1.5 Distribution of Average Cracking Time
these data approximate a log normal distribution.
X1.3.2 The log average time to cracking is 1.0 day for UNS interval) is 0.029 to 35.6 times the average for UNS S30400
S30400 and 6.4 days for UNS S31600. The intralaboratory and 0.15 to 6.6 times this average for UNS S31600. All
variation (95 % confidence interval) is 0.685 to 1.46 times this calculations are based on the seven participating laboratories
average for UNS S30400 and 0.36 to 2.79 times the average for and the assumption that the data follow a log normal distribu-
UNS S31600. The interlaboratory variation (95 % confidence tion.

X2. STANDARD DATA ENTRY FORMAT

X2.1 Table X2.1 defines the data categories and specific X2.2 The Guide G107 Reference Number is shown in Table
data elements (fields) considered necessary for searching and X2.1. Reference numbers not pertinent for this test method
comparing data using computerized databases. Pertinent items have been omitted from the table.
from Guide G107 have been included along with additional
X2.3 Items in Table X2.1 which are not pertinent for a
items specific to evaluation of stress-corrosion cracking using
specific test series (for example, details for wrought-annealed
this test method.
specimens) may simply be omitted from the report.

7
 G123 00 (2015)
TABLE X2.1 Standard Data Entry Format for Corrosion Database Development
Guide G107 Refer-
Field Field Name/Description Category Sets/Fields Type/UnitsA
ence Number
1 5.1.1 Individual test number to identify grouping of specimens tested alphanumeric
concurrently. See subsequent entries for test method
Type of Test
2 5.1.2.1 Standard test specification alphanumeric
3 5.1.2.2 Laboratory test L = laboratory
4 5.1.2.3 Date test started YYYYMMDD
Test Emphasis
5 5.1.3.1 Type(s) of corrosion evaluatedB stress corrosion
Chemistry of EnvironmentC
6 5.1.4.1 Generic description of environment 25 % NaCl (by mass) acidified to pH
1.5 with H3PO4
7 5.1.4.2 Component, common name sodium chloride, phosphoric acid
8 5.1.4.3 Chemical abstracts registry number NaCl-7647-14-5
H3PO4-7664-38-2
9 5.1.4.4 Concentration (liquids) g/L
10 5.1.4.6 Component form (1) solid
(2) liquid
11 5.1.4.7 Ionic species Na+, Cl, H+, PO43
Exposure Conditions
12 5.1.5.1 Exposure duration days
13 5.1.5.4 Temperature, average boiling
14 5.1.5.7 pH, min real number
15 5.1.5.8 pH, max real number
16 5.1.5.9 pH, average real number
17 5.1.5.16 Flow none
18 5.1.5.18 Sparging none-less than saturated (open to air)
19 5.1.5.20 Exposure zone continuous immersion
20 5.1.5.24 Ratio of specimen surface area to corrodent volume mm2/L, in.2/L
21 ... Allihn condenser drip tip (1) none
(2) length in mm
Material IdentificationD
22 5.1.6.1 Material class alphanumeric
23 5.1.6.2 Subdivision of class alphanumeric
24 5.1.6.3 Finer subdivision of class alphanumeric
25 5.1.6.4 Common name/trade name (include owner of trade name) alphanumeric
26 5.1.6.5 Material DesignationUNS No. alphanumeric
27 5.1.6.6 Specification/standard alphanumeric
28 5.1.6.7 Product shape (1) pipe/tube
(2) plate
(3) sheet/strip
(4) wire/rod/bar
(5) otherdescribe in 5.1.6.8
29 5.1.6.8 Description for (5) in 5.1.6.7 alphanumeric
30 5.1.6.9 Product production method (1) extrusion
(2) forging
(3) casting
(4) rolling
(5) powder compaction
(6) otherdescribe in 5.1.6.10
31 5.1.6.10 Description of (6) in 5.1.6.9 alphanumeric
32 5.1.6.11 Heat/lot identification alphanumeric
33 5.1.6.12 Heat/lot chemical analysis alphanumeric
Specimen Identification
34 5.1.7.1 Specimen thickness mm, in.
35 5.1.7.2 Specimen width/diameter mm, in.
36 5.1.7.3 Specimen length mm, in.
37 5.1.7.4 Specimen surface area mm2, in.2
38 5.1.7.5 Density kg/mm3, lb/in.3
39 5.1.7.6 Welded specimen (1) Y = yes
(2) N = no
40 5.1.7.7 Type of weld (see section 5.1.7.8 for additional detail) (1) autogenous
(2) matching filler
(3) dissimilar metal weld
41 5.1.7.8 Weld detailsE alphanumeric
42 5.1.7.9 Welds ground or machined (1) ground
(2) machined
(3) as deposited
(4) glass bead blasted
43 5.1.7.10 Thermomechanical condition (1) standard temperdescribe in
5.1.7.11
(2) annealed
(3) normalized
(4) sensitized
(5) as-cold-worked

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 G123 00 (2015)
TABLE X2.1 Continued
Guide G107 Refer-
Field Field Name/Description Category Sets/Fields Type/UnitsA
ence Number
(6) as-hot-worked
(7) aged
(8) other H.T./processingdescribe in
5.1.7.11
44 5.1.7.11 Description for (1) or (7) in 5.1.7.10 alphanumeric
45 5.1.7.12 Final reduction step (1) cold-workedgive percent reduction
in 5.1.7.13
(2) hot-worked (includes extrusion and
forging)
46 5.1.7.13 Percent cold reduction %
47 5.1.7.14 Ultimate tensile strength MPa, ksi
48 5.1.7.15 Yield strength MPa, ksi
49 5.1.7.16 Percent offset for yield strength %
50 5.1.7.17 Fracture ductility (strain) %
51 5.1.7.18 Hardness real number
52 5.1.7.19 Hardness scale alphanumeric
53 5.1.7.20 Surface condition (1) as produced
(2) scaled
(3) machined/ground
(4) chemically cleaned
(5) sand/grit blasted
(6) other
54 5.1.7.21 Surface treatment (1) none
(2) nitrided
(3) carburized
(4) plated
(5) clad
(6) other
55 5.1.7.22 If (4), (5), or (6) in 5.1.6.21, plating or cladding material or other alphanumeric
surface treatment
56 5.1.7.23 Condition of edges (1) as cut
(2) as sheared
(3) ground
(4) machined
(5) otherdescribe in 5.1.7.24
57 5.1.7.24 Description of other edge condition alphanumeric
58 5.1.7.25 Sample orientation relative to working direction (1) longitudinal
(2) transverse
(3) short transverse
59 5.1.7.26 Stress-corrosion cracking (SCC) specimen type (1) double cantilever beam (DCB)
(2) wedge open loaded (WOL)see
5.1.7.27
(3) bent beam2 loaded
(4) bent beam3 loaded
(5) bent beam4 loaded
(6) standard tension specimen (Test
Methods E8)
(7) subsize tension specimen (Test
Methods E8)
(8) C ring
(9) stressed ring
(10) U-bend
(11) other
60 5.1.7.27 Material used for wedge in WOL specimen alphanumeric
61 5.1.7.28 Was stressing device insulated from specimen? alphanumeric
62 5.1.7.29 Stress-corrosion cracking specimen test area (1) smooth
(2) notched
(3) precracked
63 5.1.7.30 Direct tension stress-corrosion cracking specimen-applied (1) constant load
stress (Practice G49)
(2) slowly increasing strain rate
(3) constant deflection
64 5.1.7.31 Stress-corrosion cracking specimenstress level (absolute) MPa, ksi
65 5.1.7.32 Stress-corrosion cracking specimenstress level (percent of %
yield strength at test temperature)
66 .... If U-bend used, note stressing method (1) single stage as in Practice G30, Fig.
4a, b, or c
(2) Two stage as in Practice G30, Fig. 5
67 .... Diameter of mandrel (if used for stressing U-bend) mm
68 .... Outside of diameter of U-bend mm
Specimen Performance
69 5.1.8.6 Reduction in elongation %
70 5.1.8.7 Reduction in fracture ductility (strain) %
71 5.1.8.8 Reduction in tensile strength %

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 G123 00 (2015)
TABLE X2.1 Continued
Guide G107 Refer-
Field Field Name/Description Category Sets/Fields Type/UnitsA
ence Number
72 5.1.8.9 Reduction in yield strength %
73 5.1.8.10 Nature of corrosion products alphanumeric
74 5.1.8.11 Visible corrosion? (1) corroded
(2) no visible corrosion
75 5.1.8.17 Weld related corrosion (1) fusion line
(2) base metal
(3) weld metal
(4) heat-affected zone
76 5.1.8.18 Stress-corrosion cracking (SCC) testseverity of attack (1) no cracking
(2) microcracks
(3) total fracture (complete separation)
77 5.1.8.19 SCC cracking mode (1) transgranular
(2) intergranular
(3) mixed mode
(4) ductile
78 5.1.8.30 Time to initial crack detection hours
79 5.1.8.31 Measured crack length at time of first detection mm, in.
80 5.1.8.32 Method used to detect initial cracking alphanumeric (naked eye, 5 to 40,
metallographic section
[mag.] or additional bending)
81 5.1.8.36 Threshold stress intensity range, K MPa m , ksi in.
82 ... Maximum time without stress-corrosion cracking hours
83 ... Stress-corrosion threshold stress intensity MPa m , ksi in.
84 ... Location of cracking alphanumeric
Documentation
85 5.1.9.1 Test number alphanumeric
86 5.1.9.2 Published reference alphanumeric
87 5.1.9.3 Unpublished datalocation alphanumeric
88 5.1.9.4 Technical committee report/file alphanumeric
89 5.1.9.5 Other documentation alphanumeric
Supplementary Notes
90 5.2.0.1 Supplementary notes alphanumericA,B,C,D,E
A
Data should be reported in the units in which the original measurements were made. Subsequent conversions are at the discretion of data base developers. Units listed
are nonmandatory examples.
B
For example, general corrosion, stress corrosion, pitting, crevice corrosion, hot or cold wall effects, fretting, stray current, weld corrosion, corrosion-fatigue, galvanic
corrosion, and microbiological corrosion.
C
Many environments contain multiple components. Reference numbers 5.1.4.1 through 5.1.4.7 should be repeated for each component and no restrictions should be
placed on the number of components to be described for any given environment.
D
Reference numbers 5.1.6.1 through 5.1.6.6 are basic fields for use in material identification in database. Refer to Committee E49 guidelines for material identification
in computerized material property databases.
E
For example, preheat, welding process, number of passes, heat input, joint shape, cover gas, etc.

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