Evaluation of Shampoos

Evaluation of shampoos comprises the quality control tests
including visual assessment and physiochemical controls

such as pH, density and viscosity. Sodium lauryl sulfate
based detergents are the most common but the
concentration will vary considerably from brand to brand
and even within a manufacturer's product range. Cheap
shampoos may contain a high detergent concentration
while expensive shampoos may contain very little of a
cheap detergent1.
Shampoos for oily hair can have exactly the same
detergent at the same concentration as shampoos for dry
hair. The difference is more likely to be a reduced amount
of oil or conditioning agent in the shampoo for oily hair or
the difference may even just be the packaging.
1. Physical appearance/visual inspection: The

formulations prepared were evaluated in terms of their
clarity, foam producing ability and fluidity2
2. Determination of pH: The pH of 10% shampoo

solution in distilled water was determined at room
temperature 25C3.
3. Determine percent of solids contents: A clean dry
evaporating dish was weighed and added 4 grams of
shampoo to the evaporating dish. The dish and
shampoo was weighed. The exact weight of the
shampoo was calculated only and put the evaporating
dish with shampoo was placed on the hot plate until
the liquid portion was evaporated. The weight of the
shampoo only (solids) after drying was calculated.
4. Rheological evaluations: The viscosity of the
shampoos was determined by using Brookfield
Viscometer (Model DV-l Plus, LV, USA) set at
different spindle speeds from 0.3 to 10 rpm3. The
viscosity of the shampoos was measured by using
spindle T95. The temperature and sample containers
size was kept constants during the study.
5. Dirt dispersion: Two drops of shampoo were added
in a large test tube contain 10 ml of distilled water. 1
drop of India ink was added; the test tube was
stoppered and shakes it ten times. The amount of ink
in the foam was estimated as None, Light, Moderate,
or Heavy.
6. Cleaning action: 5 grams of wool yarn were placed
in grease, after that it was placed in 200 ml. of water
containing 1 gram of shampoo in a flask. Temperature
of water was maintained at 350C. The flask was
shaked for 4 minutes at the rate of 50 times a minute.
The solution was removed and sample was taken out,
dried and weighed. The amount of grease removed
was calculated by using the following equation:
In which, DP is the percentage of detergency power,

C is the weight of sebum in the control sample and T
is the weight of sebum in the test sample4.
7. Surface tension measurement: Measurements were
carried out with a 10% shampoo dilution in distilled
water at room temperature. Thoroughly clean the
stalagmometer using chronic acid and purified water.
Because surface tension is highly affected with grease
or other lubricants5, 6. The data calculated by
following equation given bellow:
where W1 is weight of empty beaker.
W2 is weight of beaker with distilled water.
W3 is Weight of beaker with shampoo solution.
n1 is no. of drops of distilled water.
n2 is no. of drops of shampoo solution.
R1 is surface tension of distilled water at room
temperature.
R2 is surface tension of shampoo solution.
8. Detergency ability: The Thompson method was used
to evaluate the detergency ability of the samples.
Briefly, a crumple of hair were washed with a 5%
sodium lauryl sulfate (SLS) solution, then dried and
divided into 3g weight groups. The samples were
suspended in a n-hexane solution containing 10%
artificial sebum and the mixture was shaken for 15
minutes at room temperature. Then samples were
removed, the solvent was evaporated at room
temperature and their sebum content determined. In
the next step, each sample was divided into two equal
parts, one washed with 0.1 ml of the 10% test
shampoo and the other considered as the negative
control. After drying, the resided sebum on samples
was extracted with 20 ml n-hexane and re-weighed.
Finally, the percentage of detergency power was
calculated using the following equation:
In which, DP is the percentage of detergency power,
C is the weight of sebum in the control sample and T
is the weight of sebum in the test sample3, 4.

Evaluation of Shampoos

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Evaluation of Shampoos

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Evaluation of shampoos comprises the quality control tests

including visual assessment and physiochemical controls

1. Physical appearance/visual inspection: The

2. Determination of pH: The pH of 10% shampoo

In which, DP is the percentage of detergency power,

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