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1) The document reports the results of chemical analysis of samples of RBD palm olein, crude palm oil, and RBD palm kernel oil. 2) Tests performed included measurement of free fatty acid content, moisture and impurities, iodine value, color, slip melting point, cloud point, DOBI, fatty acid composition, and saponification value. 3) Key results included a free fatty acid content of 0.109% for RBD palm olein, 4.27% for crude palm oil, and 0.056% for RBD palm kernel oil.

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34 views8 pages

Form Xcheck

1) The document reports the results of chemical analysis of samples of RBD palm olein, crude palm oil, and RBD palm kernel oil. 2) Tests performed included measurement of free fatty acid content, moisture and impurities, iodine value, color, slip melting point, cloud point, DOBI, fatty acid composition, and saponification value. 3) Key results included a free fatty acid content of 0.109% for RBD palm olein, 4.27% for crude palm oil, and 0.056% for RBD palm kernel oil.

Uploaded by

azlinkadir
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Participant Code No: PT008 Date Received : 8/June/2011

Name (Chemist): Pun Ai Ping Date of Analysis :


11/June/2011
Sample Name: 1) RBD Palm Olein 2) Crude Palm Oil &
3) RBD Palm Kernel Oil

ANALYSIS RESULTS

A) FREE FATTY ACID


Method : A0CS Ca 5a-40
1) RBD Palm Olein
Number of test 1st 2nd
Weight of sample (g) W 17.74 19.61
Concentration of alkali N 0.0522 0.0522
Volume of alkali for test V 1.44 1.61
sample (ml)
Acid Value: 25.6 x N x V 0.108 0.110
W
Mean Free Fatty Acid 0.109

2) Crude Palm Oil


Number of test 1st 2nd
Weight of sample (g) W 4.61 4.84
Concentration of alkali N 0.1023 0.1023
Volume of alkali for test V 7.5 7.9
sample (ml)
Acid Value: 25.6 x N x V 4.26 4.27
W
Mean Free Fatty Acid 4.27

3) RBD Palm Kernel Oil


Number of test 1st 2nd
Weight of sample (g) W 17.27 18.44
Concentration of alkali N 0.0522 0.0522
Volume of alkali for test V 0.92 0.99
sample (ml)
Acid Value: 20.0 x N x V
0.056 0.056
W
Mean Free Fatty Acid 0.056

Comment: ____________________________________________________

Participant Code No: PT 008 Date Received : 8/June/2011


Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Olein 2) Crude Palm Oil &
3) RBD Palm Kernel Oil

ANALYSIS RESULTS
B) MOISTURE & IMPURITIES
Method : AOCS Ca 2c-25

1) RBD Palm Olein


Number of test 1st 2nd
Weight of sample (g) W 5.43 5.26
Moisture, % 0.04 0.04
Mean Moisture, % 0.04

2) Crude Palm Oil


Number of test 1st 2nd
Weight of sample (g) W 5.56 5.19
Moisture, % 0.15 0.14
Mean Moisture, % 0.15

3) RBD Palm Kernel Oil


Number of test 1st 2nd
Weight of sample (g) W 5.27 5.11
Moisture, % 0.04 0.03
Mean Moisture, % 0.04

Comment: ____________________________________________________

Participant Code No: PT008 Date Received : 8/June/2011


Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Olein
2) RBD Palm Kernel Oil

ANALYSIS RESULTS

C) IODINE VALUE
Method : AOCS Cd 1b-87(97)
1) RBD Palm Olein
Number of test 1st 2nd
Weight of sample (g) W 0.3187 0.3221
Volume of Wijs (ml) 20 20
Strength of Na2S2O3 (ml) N 0.1035 0.1035
Vol. of Na2S2O3 (ml) for blank V1 37.1 37.1
Vol. of Na2S2O3 (ml) for sample V2 23.1 22.95
Iodine Value: 12.69 x N x (V2 V1) 57.70 57.70
W
Mean Iodine Value 57.70

1) RBD Palm Kernel Oil


Number of test 1st 2nd
Weight of sample (g) W 1.1463 1.1712
Volume of Wijs (ml) 20 20
Strength of Na2S2O3 (ml) N 0.1035 0.1035
Vol. of Na2S2O3 (ml) for blank V1 37.1 37.1
Vol. of Na2S2O3 (ml) for sample V2 21.8 21.45
Iodine Value: 12.69 x N x (V2 V1) 17.53 17.55
W
Mean Iodine Value 17.54
Participant Code No: PT008 Date Received : 8/June/2011
Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Olein
2) RBD Palm Kernel Oil

ANALYSIS RESULTS

D) COLOR
Method : AOCS Cc 13e-92

1) RBD Palm Olein


Number of test Red Yellow
1st 2.9 29
2nd 2.9 29
Mean Color 2.9R ; 29Y
2) RBD Palm Kernel Oil
Number of test Red Yellow
1st 0.8 8
2nd 0.8 8
Mean Color 0.8R ; 8Y

Comment: ____________________________________________________

Participant Code No: PT008 Date Received : 8/June/2011


Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Olein

ANALYSIS RESULTS

E) SLIP MELTING POINT (oC)


Method : AOCS Cc 3-25

1) RBD Palm Olein


Number of test 1st 2nd
Slip Melting Point(oC) 21.2 21.4
Mean 21.3

Comment: ____________________________________________________
ANALYSIS RESULTS

F) CLOUD POINT (oC)


Method : AOCS Cc 6-25

1) RBD Palm Olein (Set water bath at 5 oC)


Number of test 1st 2nd
Cloud Point (oC) 7.1 7.3
Mean 7.2

Comment: IWAKI ; 100ml beaker


Please mention type of beaker/ bottle used.

Participant Code No: PT008 Date Received : 8/June/2011


Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) Crude Palm Oil

ANALYSIS RESULTS

G) DOBI
Method : PORIM

1) Crude Palm Oil

Number of test 1st 2nd


Abs (nm) 446 269 446 269
DOBI 0.793 0.301 0.801 0.306
Mean DOBI 2.63 2.62

Comment: ____________________________________________________
Participant Code No: Date Received :8/June/2011
Name (Chemist): Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Kernel Oil

ANALYSIS RESULTS

H) FAC
Method : AOCS Ce 1f-96

Number of test 1st 2nd Mean


C6:0 0.18 - 0.18
C8:0 2.90 - 2.90
C10:0 3.09 - 3.09
C12:0 46.89 - 46.89
C14:0 16.49 - 16.49
C16:0 8.75 - 8.75
C16:1 - - -
C18:0 2.42 - 2.42
C18:1 16.43 - 16.43
C18:2 2.74 - 2.74
C18:3 - - -
C20:0 0.13 - 0.13
Others (please specify)
Comment: ____________________________________________________

Participant Code No: PT008 Date Received : 8/June/2011


Name (Chemist): Pun Ai Ping Date of Analysis : 11/June/2011
Sample Name: 1) RBD Palm Kernel Oil

ANALYSIS RESULTS

I) SAPONIFICATION VALUE
Method : PORIM P3.1

Number of test 1st 2nd


Weight of sample (g) W 2.0915 2.1469
Concentration of Acid, HCl N 0.4929 0.4929
Volume of Acid, HCl for blank B 101.5 101.5
Volume of Acid for test T 83.10 82.65
sample (ml)
SV: (B-T) x N x 56.1 243.27 242.78
W
Mean Saponification Value 243.03

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