Astm D 2583 - 95
Astm D 2583 - 95
Astm D 2583 - 95
1. Scope
1.1 This test method covers the determination of indentation
hardness of both reinforced and nonreinforced rigid plastics
using a Barcol Impressor, Model No. 934-1 and Model No.
935.
1.2 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
only.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 618 Practice for Conditioning Plastics and Electrical
Insulating Materials for Testing2
D 883 Terminology Relating to Plastics2
D 4000 Classification System for Specifying Plastic Materials3
D 4805 Terminology of Plastics Standards3
E 691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method4
3. Terminology
3.1 DefinitionsFor definitions of technical terms pertaining to plastics used in this test method, see Terminology D 883
or Terminology D 4805.
7. Test Specimens
7.1 The testing area shall be smooth and free from mechanical damage.
7.2 DimensionsTest specimens shall be at least 1.5 mm
(116 in.) thick and large enough to ensure a minimum distance
of 3 mm (18 in.) in any direction from the indentor point to the
edge of the specimen.
This test method is under the jurisdiction of ASTM Committee D-20 on Plastics
and is the direct responsibility of Subcommittee D20.10 on Mechanical Properties.
Current edition approved Oct. 10, 1995. Published December 1995. Originally
published as D 2583 67. Last previous edition D 2583 93.
2
Annual Book of ASTM Standards, Vol 08.01.
3
Annual Book of ASTM Standards, Vol 08.03.
4
Annual Book of ASTM Standards, Vol 14.02.
D 2583
TABLE 1 Recommended Sample Sizes to Equalize the Variance
of the Average for Model No. 934-1
Homogeneous Material
Hardness
M-934
Scale
Reading
Variance
Coefficient of
Variation, %
Variance
of
Average
Minimum
Number of
Readings
20
30
40
50
60
70
80
2.47
2.20
1.93
1.66
1.39
1.12
0.85
2.6
1.7
1.3
1.1
0.9
0.8
0.7
0.27
0.28
0.27
0.28
0.28
0.28
0.28
9
8
7
6
5
4
3
0.77
0.78
0.75
0.78
0.75
29
22
16
10
5
10. Conditioning
10.1 ConditioningCondition the test specimens at 23 6
2C (73.4 6 3.6F) and 50 6 5 % relative humidity for not less
than 40 h prior to test in accordance with Procedure A of
Practice D 618, for those tests where conditioning is required.
In cases of disagreement, the tolerances shall be 61C
(61.8F) and 62 % relative humidity.
10.2 Test ConditionsConduct tests in the standard laboratory atmosphere of 23 6 2C (73.4 6 3.6F) and 50 6 5 %
relative humidity, unless otherwise specified in the test methods or in this test method. In cases of disagreement, the
tolerances shall be 61C (61.8F) and 62 % relative humidity.
Nonhomogeneous Material
(Reinforced Plastics)
30
40
50
60
70
22.4
17.2
12.0
7.8
3.6
2.9
2.2
1.7
1.5
1.2
11. Procedure
11.1 Observing the precautions of Section 8, make measurements on the specimens to be tested (Note 4). Impressions
should not be made within 3 mm (18 in.) of the edge of the
specimen or of other impressions.
NOTE 4Curved surfaces may be more difficult to support. When the
load is applied, bending and spring action in the specimen should be
avoided.
8.2 Set the point sleeve on the surface to be tested. Set the
legs on the same surface or on solid material of the same
thickness, so that the indentor is perpendicular to the surface
being tested. Grasp the instrument firmly between the legs and
point sleeve. Apply quickly, by hand, uniformly increasing
force on the case until the dial indication reaches a maximum
(Note 3). Take care to avoid sliding or scraping while the
indentor is in contact with the surface being tested.
NOTE 2It is recommended that measurements be made with Model
934-1 when values above 90 are obtained with Model 935 and that
measurements be made with Model 935 when values less than 20 are
obtained with Model No. 934-1. Values below 10 using Model 935 are
inexact and should not be reported.
NOTE 3Drift in readings from the maximum may occur in some
materials. This can be nonlinear with time.
13. Report
13.1 Report the following information:
13.1.1 Identification of material tested,
13.1.2 Conditioning of specimen,
13.1.3 Model number of impressor,
13.1.4 Number of readings taken,
13.1.5 Average of hardness values rounded to the nearest
whole scale reading, and
9. Calibration
9.1 With the plunger upper guide backed out until it just
engages the spring, place the impressor on a glass surface and
press down until the point is forced all the way back into the
lower plunger guide. The indicator should now read 100. If it
does not, loosen the lock-nut and turn the lower plunger guide
2
D 2583
SAN
BMC
SAN reinforced with 20 % glass
Polyester Mat Laminate (thermoset)
SMC (sheet molding compound)
No. of Determinations
using Model No. 934-1
8
22
22
16
16
15. Keywords
15.1 Barcol Hardness Impressor; Models 934-1 and 935;
hardness; indentation hardness; rigid plastics
NOTE 6Caution: The following explanations of Ir and IR (14.314.3.3) are only intended to present a meaningful way of considering the
approximate precision of this test method. The data in Table 2 should not
be rigorously applied to acceptance or rejection of material, as those data
are specific to the round robin and may not be representative of other lots,
materials, or laboratories. Users of this test method should apply the
principles outlined in Practice E 691 to generate data specific to their
laboratory and materials, or between specific laboratories. The principles
of 14.3-14.3.3 would then be valid for such data.
Average
SrA
SRB
IrC
IRD
35
39
44
55
61
1.04
0.95
1.11
1.45
1.14
2.93
3.75
2.25
1.93
2.15
3
3
3
4
3
8
11
6
5
6
5
Supporting data are available from ASTM Headquarters. Request RR: D201087.
D 2583
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