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Report of BET

The document details the results of an analysis of a carbon sample using a NOVA instrument. It includes raw data from the isotherm as well as calculated values from the multi-point BET analysis, determining the sample's surface area to be 7.590 m2/g.

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0% found this document useful (0 votes)
246 views3 pages

Report of BET

The document details the results of an analysis of a carbon sample using a NOVA instrument. It includes raw data from the isotherm as well as calculated values from the multi-point BET analysis, determining the sample's surface area to be 7.590 m2/g.

Uploaded by

cruise3020
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Quantachrome NovaWin - Data Acquisition and Reduction

for NOVA instruments


1994-2010, Quantachrome Instruments
version 11.0
Analysis
Operator:nova
Date:2016/07/26
Sample ID: Carbon
Filename:
Sample Desc:
Carbon active (kimia)
Comment:
Sample weight: 0.0541 g
Sample Volume:
Outgas Time:
3.0 hrs
OutgasTemp:
Analysis gas:
Nitrogen
Bath Temp:
Press. Tolerance: 0.100/0.100 (ads/des)
Equil time:
Analysis Time: 32.4 min
End of run:
Cell ID:
99

Report
Operator:nova
Date:8/9/2016
C:\QCdata\Physisorb\ 20160727_1 _diewa ayu.qps
0.1026 cc
200.0 C
77.3 K
60/60 sec (ads/des)
2016/07/26 11:03:15

Equil timeout:
Instrument:
F/W version:

240/240 sec (ads/des)


Nova Station A
0.00

Isotherm * Linear
Ads

Des

2.93
2.80

2.40

Volume @ STP (cc/g)

2.00

1.60

1.20

0.80

0.40

0.00
0.00

0.04

0.08

0.12

0.16

0.20

0.24

0.28

0.32

Relative Pressure, P/Po

Quantachrome NovaWin - Data Acquisition and Reduction for NOVA instruments 1994-2010, Quantachrome Instruments version 11.0

Report id:{244698913:20160809 134249329} Page 1 of 3

Quantachrome NovaWin - Data Acquisition and Reduction


for NOVA instruments
1994-2010, Quantachrome Instruments
version 11.0
Analysis
Operator:nova
Sample ID: Carbon

Date:2016/07/26
Filename:

Report
Operator:nova
Date:8/9/2016
C:\QCdata\Physisorb\ 20160727_1 _diewa ayu.qps

Multi-Point BET Plot


A

BF

125.0000
120.0000

1 / [ W((Po/P) - 1) ]

80.0000

40.0000

0.0000
0.000e+00

4.000e-02

8.000e-02

1.200e-01

1.600e-01

2.000e-01

Relative Pressure, P/Po

Quantachrome NovaWin - Data Acquisition and Reduction for NOVA instruments 1994-2010, Quantachrome Instruments version 11.0

Report id:{244698913:20160809 134249329} Page 2 of 3

Quantachrome NovaWin - Data Acquisition and Reduction


for NOVA instruments
1994-2010, Quantachrome Instruments
version 11.0
Analysis
Operator:nova
Sample ID: Carbon

Report
Operator:nova
Date:8/9/2016
C:\QCdata\Physisorb\ 20160727_1 _diewa ayu.qps

Date:2016/07/26
Filename:

Isotherm
Relative
Pressure

Volume @ STP

Relative
Pressure

Volume @ STP

[cc/g]
5.08630e-02
7.90620e-02
1.06544e-01
1.30120e-01

Relative
Pressure

Volume @ STP

[cc/g]

0.9769
1.2272
1.3583
1.4823

1.55491e-01
1.81746e-01
2.06825e-01
2.30940e-01

[cc/g]

1.6092
1.7366
1.8823
2.0551

2.57277e-01
2.80089e-01
3.05940e-01

2.2662
2.4573
2.6581

Multi-Point BET
Relative
Pressure
[P/Po]
5.08630e-02
7.90620e-02
1.06544e-01
1.30120e-01

Volume @ STP

1 / [ W((Po/P) - 1) ]

[cc/g]
0.9769
1.2272
1.3583
1.4823

Relative
Pressure
[P/Po]

4.3891e+01
5.5972e+01
7.0245e+01
8.0740e+01

Volume @ STP

1.55491e-01
1.81746e-01
2.06825e-01

1 / [ W((Po/P) - 1) ]

[cc/g]
1.6092
1.7366
1.8823

9.1549e+01
1.0233e+02
1.1084e+02

MBET summary
Slope =
Intercept =
Correlation coefficient, r =
C constant=

436.229
2.262e+01
0.998493
20.288

Surface Area =

7.590 m/g

Quantachrome NovaWin - Data Acquisition and Reduction for NOVA instruments 1994-2010, Quantachrome Instruments version 11.0

Report id:{244698913:20160809 134249329} Page 3 of 3

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