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Pickling Passivation Procedure by JS

This document provides work instructions for pickling and passivating stainless steel equipment. It outlines the objectives of acid cleaning and neutralizing stainless steel materials and weld joints to remove oxide films, scale, discoloration, and welding slag. The instructions specify using a K2 pickling and passivation product to treat the surface, then applying a passivation solution for 30 minutes followed by a rinse. Safety precautions are noted such as using gloves, masks, and goggles and avoiding direct skin contact with the solutions.

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Akhilesh Kumar
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3K views2 pages

Pickling Passivation Procedure by JS

This document provides work instructions for pickling and passivating stainless steel equipment. It outlines the objectives of acid cleaning and neutralizing stainless steel materials and weld joints to remove oxide films, scale, discoloration, and welding slag. The instructions specify using a K2 pickling and passivation product to treat the surface, then applying a passivation solution for 30 minutes followed by a rinse. Safety precautions are noted such as using gloves, masks, and goggles and avoiding direct skin contact with the solutions.

Uploaded by

Akhilesh Kumar
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
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AIM Engineers

TITLE : WORK INSTRUCTION FOR


PICKLING & PASSIVATION OF
STAINLESS STEEL EQUIPMENTS
Doc. No. AIM/PPS / 01
1.0 SCOPE :

PAGE NO. 1 OF 2

This work instruction defines the method of carrying out the pickling & passivation of
stainless steel equipments.
2.0 OBJECTIVE :
For acid cleaning & neutralizing SS material/weld joints meant during fabrication of
vessels. This covers the surface treatment of austenitic stainless steel. The basic purpose
of this chemical treatment is to remove films of oxide, scale, tampering colures &
remnants of welding slag which are formed during annealing of welding.
3.0 REFERENCE :
ASTM A380
4.0 WORK INSTRUCTION :
4.1 Pre-treatment : Surface should be cleaned with brushing or grinding to remove weld
spatter & smooth out scratches & should be degreased to remove oil & grease films.

4.2 PICKLING
4.2.1 K2 a pickling and passivation products (in Paste / spray / liquid form) approved
under ASTM A380 for pickling and passivation of Stainless Steels shall be used for this
purpose.
4.2.2 The surface to be pickled and passivated shall be cleaned thoroughly and made free
from grease and oils.
4.2.3 K2 pickling paste is to be applied on the weld seam and the surrounding area with a
brush. If the surface area to be cleaned is large then K2 pickling spray is to be sprayed on
the surface to be cleaned with a spray pump or a pressurized plastic spray bottle.
4.2.4 After applying K2 (paste / spray) leave it on the surface to be cleaned for approx.30
mins.
4.2.5

Wash the surface thoroughly with water.

AIM Engineers
TITLE : WORK INSTRUCTION FOR
PICKLING & PASSIVATION OF
STAINLESS STEEL EQUIPMENTS
Doc. No. AIM/PPS / 01

PAGE NO. 2 OF 2

4.2.6 As an alternative to points no. 4.2.1 to 4.2.5 above, pickling can be carried out by
swabbing for which freshly prepared solution shall be used:
Solution:
a) Nitric Acid (HNO3)
- 20 parts by volume
b) Hydro fluoric Acid (HF) 3 parts by volume
c) Water
- 77 parts by volume.
4.3 Passivation
4.1.1 Apply K2 Passivation solution on the entire area and leave it for approx. 30 mins.
4.1.2 As an alternative to points no.4.1.1, following passivation solution can use
a) Nitric Acid (HNO3)
- 20 parts by volume
b) Water
- 80 parts by volume.
4.1.3 Finally rinse the surface thoroughly with water.
5.0 SAFETY INSTRUCTIONS:
5.1 Surface treatment only to be performed by properly trained & experienced personnel
while observing the safety regulations such as usage of gloves, masks & goggles while
performing the operation.
5.2 Proper care shall be taken while handling this solution and direct contact to the skin
of the operator shall be avoided. In case if it happens, the portion of skin shall be
cleaned with sufficient quantity of cold water.
6.0 RECORDS:
6.1 Stage Inspection Report.

Prepared By :Er. Satish Jambhale

Approved By : Er. Akhilesh kumar

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