Viscosimetro Ofite
Viscosimetro Ofite
Viscosimetro Ofite
Instruction Manual
Updated 3/15/2011
Ver. 1.7
OFI Testing Equipment, Inc.
11302 Steeplecrest Dr. Houston, Texas 77065 U.S.A.
Tele: 832.320.7300 Fax: 713.880.9886 www.ofite.com
Copyright OFITE 2011
Table of
Contents
Introduction ......................................................................................2
Description .......................................................................................2
Components......................................................................................3
Specifications ...................................................................................5
Setup..................................................................................................8
Calibration.........................................................................................9
Operation ........................................................................................12
Calculations ....................................................................................14
Disassembly ...................................................................................14
Maintenance....................................................................................15
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Introduction
Description
The OFITE Model 800 Viscometer determines the flow characteristics of oils
and drilling fluids in terms of shear rate and shear stress over various time
and temperature ranges at atmospheric pressure. Speeds are easily
changed with a control knob, and shear stress values are displayed on a
lighted magnified dial for ease of reading. An optional cup heater is used to
raise the temperature of the test sample.
The viscometers motor RPM is continuously monitored and automatically
adjusted by the OFITE Pulse-Power electronic speed regulator to maintain a
constant shear rate under varying input power and drilling fluid shear conditions. The eight precisely regulated test speeds (shear rates in RPM) are as
follows: 3 (Gel), 6, 30, 60, 100, 200, 300, and 600. A higher stirring speed is
also provided. Speeds may be changed with a control knob selection, without stopping the motor.
The Model 800 is suitable for both field and laboratory use and uses a motordriven electronic package to provide drilling fluid engineers with an extremely accurate and versatile tool. The Model 800 operates from a 12 Volt AC
power source, or standard rig power, either 115 or 230 Volt DC power, 50-60
Hz. The electronic regulator continuously monitors and automatically adjusts
the rotational speed to maintain a constant shear rate under varying fluid
shear conditions and input power variations that are commonly found on-site.
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Components
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Optional:
#130-10-33 Power Cord for 12-Volt Cigarette Lighter Adapter
#132-56-C Rotor, R1 Closed-Cup, 316 Stainless Steel (For completion
and fracturing fluid testing.)
#132-48
Calibration Instrument
#132-80
Calibration Fluid, Certified, 100 cP, 16 oz
#900-275 Battery Pack; 5 - 19 Volt Battery Output; Includes Case, Bag,
AC Charger, and Plug Adapters
Additional
#132-58-1
#132-58-2
#132-58-3
#132-58-4
#132-58H
#132-56H
#134-10-2
#134-10-3
#134-10-4
#134-10-5
#134-10-6
F0.2 Torsion
F0.5 Torsion
F2.0 Torsion
F3.0 Torsion
F4.0 Torsion
Spring Assembly
Spring Assembly
Spring Assembly
Spring Assembly
Spring Assembly
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Specifications
Instrument Geometry
Speed Accuracy (RPM)
Motor Speeds (RPM)
Readout
Heat Cup
Power Requirements
Weight (kg)
Dimensions (cm)
Shipping Weight (kg)
Shipping Dimensions (cm)
R1B1
1.8415
1.7245
3.8
0.117
0.9365
R1B2
1.8415
1.2276
3.8
0.6139
0.666
R1B3
1.8415
0.8622
3.8
0.9793
0.468
R1B4
1.8415
0.8622
1.9
0.9793
0.468
R1B1
R1B2
R1B3
R1B4
330
840
1680
3360
5040
6720
8400
16800
651
1657
3314
6629
9943
13257
16571
33143
1320
3359
6717
13435
20152
26870
33587
67175
2644
6730
13460
26921
40381
53841
67302
134603
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
R1B1
R1B2
R1B3
R1B4
1.7023
0.3770
0.2682
0.2682
5.11
1.13
0.80
0.80
10.21
51.07
102.14
170.23
340.46
510.69
1021.38
2.26
11.31
22.62
37.70
75.40
113.10
226.20
1.61
8.05
16.09
26.82
53.64
80.46
160.92
1.61
8.05
16.09
26.82
53.64
80.46
160.92
Viscosity Ranges<a>
(cP)
R1B1
R1B2
R1B3
R1B4
Minimum Viscosity<b>
@600 RPM
0.5<c>
4.5
12.7
25
Maximum Viscosity<d>
10,000,000 89,000,000 255,000,000 500,000,000
@0.01 RPM
<a> Computed for standard Torsion Spring (F 1.0). For other torsion springs, multiply by F factor
<b> Lower viscosities can be measured by the Model 900, however one must take into account the
effect of bearing drag, Taylor vortices, zero offset, etc. when looking at the expected accuracy of
the reading
<c> For practical purposes the minimum viscosity is limited to 0.5 cP due to Taylor Vortices
<d> Maximum viscosity is based on Maximum Shear Stress and Minimum shear rate (RPM). However,
due to practical and physical limitations, it may be difficult to take these measurements.
Viscosity Conversions
To convert from units on left side to units on top, multiply by factor @ intercept.
Centipoise
Poise (P) g/(cm*s) (mN*s)m2 mPa*s
(cP)
Centipoise
(cP)
Poise (P)
g/(cm*s)
(mN*s)m2
mPa*s
(lb*s)
100 ft2
(lb*s)
100 ft2
0.01
0.01
0.002088
100
100
1
1
1
1
0.01
0.01
1
1
0.01
0.01
100
100
1
1
100
100
1
1
0.2088
0.2088
0.002088
0.002088
478.93
4.789
4.789
478.93
478.93
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Pa
lb/100ft2
lb/ft2
DR
Dyne/cm2
0.1
0.2084
0.002084
0.1957
Pa
10
2.084
0.02084
1.957
4.788
0.4788
0.01
0.939
lb/ft
478.8
47.88
100
93.9
DR
5.107
0.5107
1.065
0.01065
lb/100ft
2
RPM(max) * AV(max)
BOB(F)*90000
Bob (F)
R1B1
1
R1B2
8.9
R1B3
25.4
R1B4
50.7
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Setup
Note
1. Connect the instrument to a power source. This viscometer will operate equally well at 12 Volts, 115 Volts, or 230 Volts, 50 or 60 Hz.
For longer-lasting, continuous operation, it is strongly recommended that the Model 800 Viscometer only be used with the
OFITE Power Supply (#130-10-30). This particular power supply
has the filtering range to assure true frequency under varying
input power conditions.
2. With the instrument turned off, place the splash guard onto the bob
shaft with the short tube end pointed up towards the bearings. Push up.
3. Screw on the appropriate bob with the tapered end up towards the
splash guard.
4. Place the R1 rotor onto the drive rotor over the bob. The threads
assure the rotor will attach evenly and uniformly each and every time.
5. The power switch is located on the back panel. Turn the unit on.
6. Place a properly prepared sample of test fluid in a sample cup and
immerse the rotor exactly to the fill line on the rotor by raising the platform. Tighten the lock nut on the platform.
!
Important
Drive Rotor
Splash Guard
Bob
R1 Rotor
Platform
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Calibration
The Model 800 viscometer can lose calibration while in service if the bob
shaft bearings become contaminated or if the bob shaft itself is bent. If the
dial does not read zero when it should or if there is excessive dial deflection when the main shaft is turning, this may indicate that the bob shaft
bearings are sticking. If the spring appears to be non-linear, the bob shaft
may be bent. Your viscometer will require servicing if it exhibits any of
these symptoms. Periodic calibration checks are recommended to ensure
that your instrument is in proper working condition at all times.
The OFITE Calibrating Instrument (Part No. 130-45-1) and the Calibration
Check Kit (Part No. 132-49) are available to facilitate calibration. The
Calibrating Instrument uses a dead-weight method of calibrating, while the
Calibration Check Kit is fluid based. Both are provided in the Model 800
spare parts kit (Part No. 130-10-SP).
Equipment:
#130-45-1 Calibrating Instrument for 8-Speed Viscometer (Requires a
trained technician)
#132-49
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
Procedure:
1. Choose the certified calibration fluid using the temperature-viscosity
chart supplied with the calibration fluid to cover the viscosity range of
interest. Make sure the lot number on the chart matches the lot number on the fluid container. Each lot of standard fluid is individually certified. The viscosity will normally vary slightly from lot to lot.
2. Clean and dry the viscometer bob, rotor, and cup. Place the viscometer and the calibration fluid side-by-side on the counter top in a room
with a reasonably constant temperature [< 5F (< 2.7C)]. Allow the
viscometer and the fluid to stand at least two hours to equilibrate.
3. Operate the viscometer in air for two to four minutes to loosen up the
bearings and gears. Observe the rotor for excessive wobbling and
replace if necessary.
!
4. Fill the cup to the scribed line with calibration fluid and place it on the
viscometer stage. Move the stage upward until the fluid level is to the
fill line on the rotor.
Never immerse the rotor in fluids above the fill line.
Important
Fill Line
R1 Rotor
5. Place a thermometer capable of 0.2F (0.1C) into the fluid and hold
or tape it in place to prevent breakage. Operate the viscometer at a
low speed setting until the thermometer reading becomes stable to
within 0.2F (0.1C) per 30 seconds. Note and record the temperature reading.
6. Once the temperature has stabilized, operate the viscometer at 600
RPM and then at 300 RPM. Note and record the dial readings to the
nearest 0.5 dial unit.
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
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OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
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Operation
Measuring Viscosity:
1. Mix the sample on the STIR setting for 10 seconds while heating or
cooling the fluid. Monitor the temperature with a thermometer.
Continue to mix until the sample reaches the target temperature.
2. Rotate the knob to one of the speed settings. When the dial reading
stabilizes, record the reading and the temperature. Repeat this step for
any other speeds that your test requires.
Tip
Always start with the higher RPM and work your way down to the lowest RPM. For example, if you need readings at 100 RPM, 200 RPM,
and 300 RPM, record the measurement at 300 RPM first, then 200
RPM, then 100 RPM, then gel strengths (if necessary).
Measuring Gel Strength:
1. Mix the sample on the STIR setting for 10 seconds.
2. Rotate the knob to GEL and immediately shut off the power.
3. As soon as the rotor stops rotating, wait 10 seconds and turn the power
back on while looking at the dial. Record the maximum dial deflection
before the gel breaks. This is the 10 second gel strength.
Note
When measuring gel properties, the dial does not have to return to zero
during the quiescent period. Therefore, it should not be forced back to the
zero setting if it does not freely do so. When determining the maximum
dial deflection, no allowance needs to be made if the dial did not start at
zero. Only the maximum dial deflection is of interest. Rheological properties and characteristics of the sample will determine if the dial returns to
zero during the quiescent periods of the gel measurements.
4. For the 10 minute gel strength, re-stir the fluid and wait 10 minutes
before recording the maximum dial deflection.
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
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API Testing
1. Mix the sample on the STIR setting for 10 seconds.
2. Set the speed to 600 RPM. Wait for the reading to stabilize and then
record the dial reading and temperature.
3. Set the speed to 300 RPM. Wait for the reading to stabilize and then
record the dial reading and temperature.
4. Stir the sample again for 10 seconds.
5. Set the speed to GEL and immediately shut off the power.
6. As soon as the rotor stops rotating, wait 10 seconds and turn the power
on while looking at the dial. Record the maximum dial deflection before
the gel breaks. This is the 10 second gel strength.
7. For the 10 minute gel strength, re-stir the fluid and wait 10 minutes before
recording the maximum dial deflection.
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
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Calculations
Disassembly
!
Important
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Maintenance
From time to time, the bearings will need to be changed. Complete the following to determine if it is time to perform this maintenance procedure:
1. The viscometer should have a zero dial reading when placed in an
upright position with the rotor not immersed in fluid prior to running tests.
2. With the instrument in this position, rotate the rotor at 600 RPM. The dial
reading in air should not exceed one.
3. Place water in a suitable container and immerse the rotor to the fill line.
4. Rotate the rotor at 600 RPM. The dial reading in water should be
between 1.5 and 3.0.
5. At 300 RPM, the dial reading in water should be between 0.5 and 2.0.
If the viscometer fails to pass any one of the above tests, the bearings are
bad and should be replaced by a qualified instrument technician.
OFITE, 11302 Steeplecrest Dr., Houston, TX 77065 USA / Tel: 832-320-7300 / Fax: 713-880-9886 / www.ofite.com
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!
7. Gently lift up on the torsion spring to remove it from the clamp sleeve
and dial.
Do not stretch the torsion spring.
Important
If you are replacing only the torsion spring, discard the old spring, and
skip to step 20 to complete the process.
!
8. Remove the four screws from the bridge and lay it gently to the right
side.
Do not touch the encoder that encircles the flywheel.
Important
9. Loosen the set screw (one turn counter-clockwise) on the bottom of the
dial and pull down on the bob shaft to remove them both.
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!
10. Remove the two screws on the brass bearing mount (upper bearing).
Hold the upper brass bearing mount by hand for easier access to the
retainer ring and bearing.
Be careful not to damage the pins.
Important
Set Screw
Retainer Clip
Upper Bearing
Brass Bearing Mount
Set Screw
11. The upper bearing is located inside the brass bearing mount. Use retaining ring pliers to remove the retainer ring. Push the bearing upwards to
remove the upper bearing from the brass bearing mount.
12. Use surgical gloves to insert a new upper bearing into the brass bearing
mount and replace the retainer ring with the retaining ring pliers.
!
Important
Do not touch the bearing with bare hands. Dirt, oils, and other contaminants can damage the bearing.
13. Replace the brass bearing mount back onto the two pins and tighten the
two screws.
14. Remove the Splash Guard, loosen the set screw on the lower brass bearing shield (one turn counter-clockwise), and slide the lower bearing down
the bob shaft to remove all three components.
15. Use surgical gloves to apply a new lower bearing onto the bob shaft.
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16. Install the lower brass bearing shield and tighten the set screw. Slide the
splash guard back up the bob shaft until in touches the lower brass bearing shield.
Note
Torsion Spring
Bob Shaft
Bearing Shield
Lower Bearing
Splash Guard
17. Slide the bob shaft up through the upper brass bearing mount. Turn the
bob shaft in the direction that allows the Flat located at the top of the
bob shaft to be positioned towards you.
Note
18. Align the bottom set screw on the dial with the Flat on the bob shaft and
tighten firmly. Make sure the set screws are perpendicular to the tip of
the bob shaft.
The bob shaft should rotate smoothly without any noise.
19. Replace the bridge being careful not to touch, or bend the encoder.
Tighten the four screws.
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20. Gently slide the torsion spring through the clamp sleeve and into the dial.
Make sure the bottom of the torsion spring is seated properly inside the
dial. Tighten the set screw located at the top of the dial to secure the torsion spring.
21. Replace the stop block and the two screws. Make sure that the zero dial
reading is aligned with the fill on the stop block.
22. Press down on the torsion spring until it is flush with the clamp sleeve
and tighten the set screw.
23. Replace the bob and rotor.
24. Re-attach the main housing cover and re-calibrate.
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