04 Milling
04 Milling
04 Milling
VADE-MECUM
4. MILLING
Rev. 2002
SECTION 4 MILLING
Table of Contents
1.
2.
Separator............................................................................................ 4.12
2.1 Circulating Load......................................................................... 4.12
2.2 Tromp Curve.............................................................................. 4.12
2.3 Indicators for Cement Milling and Typical Values ....................... 4.14
2.4 Sturtevant/O'Sepa (Bath #B mill) ................................................ 4.15
2.5 Recommended Steps for Sizing a HES ........................................ 4.16
3.
4.
5.
Index - i
Rev. 2002
SECTION 4 MILLING
1. Mill
1.1 Ball Mill General
a) Mill design
General L/D ratio
Raw mills: 1.5 < L/D < 3.2
Finish / cement mills: 2.8 < L/D < 3.2
Length of first Compartments relative to total mill length
Raw mills: First compartment length equals 35 45% of total mill effective length.
Cement mill: First compartment length equals 30 35% of total mill effective length.
When L/D>1.5, classifying liners might be used.
The lower the L/D, the higher the circulating load needs to be (see below).
b) Percent loading of mill
2
r 2 r sin (h r )
% volume load = 360
r 2
where:
- r is the radius
- h is the free height
hr
- = arccos
r
- in degrees = 3.14
0.9
h/d
0.8
0.7
0.6
0.5 0
10
20
30
40
50%
% volume load
Rules of thumb
% vol. Load = 111.87 123.98 (h/d), 25 50%: error max 0.6%.
It is estimated that material increases the actual ball filling ratio by about 2%.
Another method (quick but not as accurate) consists in counting the number of visible shell liner plates (n) and
to divide by the total number of shell liner plates per circumference (N): Angle = n x 360 / N.
Values of angle h/d ratio in relation to the ball load (% filling degree)
Ball load (%)
20
21
22
23
24
25
26
27
28
29
30
h/d
.7459
.737
.7281
.7193
.7106
.702
.6926
.685
.6765
.6682
.6598
n/N
.667
.653
.639
.625
.611
.601
h/d
.6516
.6434
.6352
.627
.6189
.6109
.6028
.5948
.5868
.5789
.5709
.563
n/N
.590
.580
.569
.558
.549
.539
4.1
Rev. 2002
SECTION 4 MILLING
C
m
P
000000000000000000000000000000000000000000000000000000000000000000000000
r
60 2 g
4 2 r
C = m 2 r =
G 2 r
g
where:
- G = Weight of grinding ball in kg
- = angular velocity of mill tube (rad/sec)
- D = inside mill diameter (m)
- n = rev per minute
- C = centrifugal power kg
- D1 = inside mill diameter (ft)
P = G * sin
(P is the resulting force of gravity)
To maintain the ball in this position on the mill wall, it is
necessary that C P.
76.6
42.3
(=
), with D in meters ( D1 in feet)
D1
D
% Critical speed:
Practically, mill speed between 68and 80% of critical speed.
% critical speed is the mill actual speed in RPM divided by nc.
Example:
3.98 meter mill with rotational speed of 15.6 rpm then nc = 21.2, % critical speed = 73.6 %.
d) Retention Time
Rules of thumb:
Retention time:
Fluoresceine test:
2g/t of mill production. Prepare the fluoresceine with 800-ml alcohol and impregnate 2 kg of mill feed
material (in a plastic bag).
Put the material at mill inlet, start the time and sample every 30 s during 30 min. (others use salt).
e) Mill Throughput
Using elevator power and after calibrating we have:
A=
where:
A
kW
kW0
H
-
=
=
=
=
=
4.2
Rev. 2002
SECTION 4 MILLING
Rules of thumb
Recommended 1.5 m/s above the ball charge:
inside the trunnion: 22-25 m/s.
partitions: 8-14 m/s (<20 m/s).
hood: <5 m/s to prevent dust from being sucked up (dust pick-up is proportional to speed^2).
dropout box: <2 m/s.
0.3-0.5 Nm3/kg ck
0.6-0.8 Nm3/kg raw mix
Wet bulb temperature should be 30oC below the dry bulb temperature.
g) Optimum filling ratio:
U= (volume of powder in the mill)/ (volume of voids in the charge): between 60% and 110%, optimum around
90%.
In practical terms, material level should equal ball level.
Bond Formula
d KMAX
where:
- d KMAX is the biggest ball diameter (mm)
- d 20 is the sieve dimension () with 20% retained
Quick evaluation
For clinker:
B = 24 d 80
(Other formula exist that result in value differences
of 5%)
B = ball dimension (mm)
d 80 is the sieve with 80% passing
-
d
Wi
= 20.17 20 .3
K . Du
100
10
.1
10
100
Rowland Formula
. Wi
d 80
.
K 100 . . 3.281 Du
B = 25.4
4.3
Rev. 2002
SECTION 4 MILLING
13.49
10.18
16.40
15.76
11.53
16.46
11.37
7.10
8.16
10.57
Bulk density
Sand
Sand
Iron
Bauxite
Brick
Gypsum
Fluid coke
Limestone (crushed)
Silica fume
Bottom Ash
Cement T I-II
T 10
T III
Clinker
Clinker
(underburnt)
Raw mix
3.09
2.68
2.58
2.93
2.68
2.65
1.63
2.23
2.69
2.67
g/l or kg/m3
1387
1679
2629
1980
1502
1677
926
1803
1024
1241
1234
1207
1054
1575
1400
lb/ft3
86.6
104.9
164.2
123.6
93.8
104.7
57.8
112.6
63.9
77.5
77.1
75.4
65.8
98.4
87.4
1041
65.0
Quick calculation:
Ball diameter (mm) =
250 P
Weight of 1 m3 of
balls (kg)
Specific surface
(m2 / mt)
250
343
488
548
729
954
1,157
2,000
3,905
4,555
5,830
7,809
9,257
15,996
20,542
22,782
31,242
50,870
4560
4590
4620
7.854
8.728
9.812
10.207
11.222
12.276
13.085
15,708
19.628
20.664
22.437
24.730
26.173
31.408
34.139
35.337
39.259
46.185
4640
4660
4708
4760
4850
4894
4948
4989
(P = weight in g)
785 2
m / mt
d
(d = diameter in mm)
4.4
Rev. 2002
Wear rates:
Ball diameter mm
100
90
80
70
60
50
40
30
25
20
17
SECTION 4 MILLING
Wear GT ball
g/h.T
Wear / Ball
g/100h
Wear diam
mm/100h
12.9
14.4
16.7
19.3
23.1
28.9
38
46.5
58.5
68.2
38.6
30.4
23.6
17.2
11.9
7.6
4.22
2.98
1.92
1.38
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
0.4
4.5
Rev. 2002
SECTION 4 MILLING
Points to audit
Shell Liner Thickness
Shell Liner Lifter Thickness
Shell Liner Remarks
Inlet Head Liner Thickness
Inlet Head Liner Remarks
Inlet Opening Remarks
Height Liner, to Balls - Average
Width Across Balls - Average
Calculated Percent Fill
b) Polysius Design
As a rule of thumb, it suits raw mills and especially monochambers very well, especially if no classifying
liners are used.
D
ln
9.6
D = 9.6 e013.x x =
0.13
where:
D = ball (cm)
x = effective mill length (m)
Process step-by-step, calculating each effective length starting from the input and with the largest ball:
1. Calculate effective lengths and the ball sizes you plan to use.
2. Double the first effective length which is both the first interval width and the first cumulative length.
3. Calculate each succeeding interval width by taking the effective length and substract the preceding
cumulative length and doubling it. Add this value to the previous cumulative length to get the new one.
4. If an interval overlaps with the partition divide the interval at the point of overlap. The excess is carried
over to the next compartment. At the end of the mill, the interval is truncated at the point of overlap.
5. Once the intervals have been adjusted for compartment lengths as described in step (4), divide the adjusted
interval by compartment length and multiply by 100. This is the percent weight for each size to be used in
the compartment.
c) Slegten Model
1
The recommended volume loading for minimum kWh/t is based on an acceptable compromise with production. For minimum kWh/t
the volume loading can be as low as 22%.
4.6
Rev. 2002
SECTION 4 MILLING
4.7
Rev. 2002
SECTION 4 MILLING
Number/ 10 t of Charge
670
1820
1820
1820
In recent years, Slegten has favored a 3-ball size distribution in first compartments over a 4- ball size as shown
in table above.
Transition Zone
This is at the beginning of the second compartment and basically its job is to clean up anything which
penetrated the partition that is oversize for the second compartment charge to fracture.
The design for this area is to use "n" balls of 50 and 40 mm.
Ball (mm)
50
40
Number/ 10 t of Charge
1820
1820
The transition zone is made of the largest ball size used in this transition zone is sometimes identical to the
smallest ball size used in the first compartment.
5/8
Polysius design
31.0%
31.2%
37.8%
2.31%
23.73%
34.05%
2.57%
37.34%
-
Slegten design
32.1%
43.1%
24.8 %
7.67%
2.94%
10.08%
48.18%
31.13%
(Some)1
Transition
zone
4.8
Rev. 2002
SECTION 4 MILLING
A limited amount of 5/8 balls should theoretically be added but the designer decided to use as the smallest ball size.
Slegten formula
P =W*
rpm
V cr
1.27
W=
and
* K j * K Fr
* Fr 2 * L * J * d
where:
P : the motor absorbed power (kW)
J : the ratio between the apparent ball
W : the weight of the load (T)
volume and the internal volume
- rpm: is mill speed (rpm)
Fr : internal diameter (inside liners) (m)
d is the apparent density of load (t/m3)
#1 comp :
d = 4.5
#2 comp :
d = 4.65, if fine ball size distribution (say with average ball weight < 40 g)
d = 4.6, if coarser ball size distribution (average ball weight > 40 g)
Average :
d = 4.6
Vcr is the critical speed inside liners=
42.3
Fr
K Fr is the influence of the location of the center of gravity for the moving ball charge vs. the mill center
(C is a constant depending on the material and the liners).
C=
11.262 for Clinker mill closed circuit with Slegten equipment
10.7 for clinker + slag, 12.16 for raw mix, 10.1 for slurry
0.379
4.9
Rev. 2002
P = L*
rpm
Vcr
1.27
* J*K j*
SECTION 4 MILLING
* Fr2.379 * d * C
Simplified formula
P =T *
Fr
RPM 100
*Kj *
* 9.5
*
Vcr
75
1.366
dW = cx n dx
- If W = Comminution work,
particles (initial, final)
Value of n
Energy Law
Rittinger
Kick
Bond
Value of n:
2
1
1.5
x = Size of
Blaine 1
W2 = W1
Blaine 2
n = 1.4 for high efficiency separator (HES) circuit, n = 1.6 for Sturtevant separators, bearing in mind
that 16 and 18 Sturtevant separators are more efficient than the larger 20 and 22 Sturtevant.
W: communition work, W is proportional to production rates.
Rules of thumb
Raw material: 10-16 kWh/t (target fineness: passing 200m>99%, passing 100m>90%)
4.10
Rev. 2002
SECTION 4 MILLING
4.11
Rev. 2002
SECTION 4 MILLING
2. Separator
2.1 Circulating Load
a) Junction with Three Streams
A, R, F are the feed, reject and fine of the separator
A
- ai , ri , f i are the cumulated % passing at a defined sieve(i).
- da, dr, df are the % retained corresponding to the sieve interval dx.
A=
A da
With:
R+F
=
Rdr + Fdf
da = ai + 1 ai ,
b) Drawing
Plot ( f i a ) vs ( f i ri )
If the mill circuit is steady, the graph has to be a
straight line:
( f a) = + ( f r )
- should be close to 0
R
- is the most probable value of
A
R
- The circulating load is defined as:
=
F 1
R df da
=
,
A df dr
F dr da
=
A dr df
c) CL calculation
Using the least square line calculations,
with = 0
d) Quick CL calculation
With one set of results of sieving:
R f a
=
F ar
( f i ai )( f i ri )
R i =0
=
n
A
i =0
( f i ri ) 2
4.12
Rev. 2002
SECTION 4 MILLING
where:
- d25 is the size of the particle which has 25 % chance of going to rejects
- d50 is the size of the particle which has 50 % chance of going to rejects
- d75 is the size of the particle which has 75 % chance of going to rejects
I=
Imperfection
0.42
0.40
0.38
0.36
0
100
200
300
Circ. load (%)
400
c) Acuity Limit
AL is the abscissa of the intersection of the two Tromp curve lines.
Its the size at which selection is initiated
Rule of thumb
Cement mill = Acuity limit: 20-30 m, Raw mill = Acuity limit: 30-60 m
d) Bypass
Definition:
By-pass is the ordinate of the intersection of the two Tromp curve lines.
The bypass is the lowest percentage of feed that will go to the separator rejects.
60
40
20
0
50
100
150
200
250
Feedrate to Separator (t/h)
300
80
70
60
Bypass (%)
Bypass (%)
80
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
100
50
40
30
20
10
0
0000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
Sturtevant
O-Sepa
1.0
1.5
2.0
2.5
3.0
Qf/Qa (kg feed/m3 separator sweep)
3.5
4.13
Rev. 2002
SECTION 4 MILLING
Bypass (%)
20
10
Bypass = 1 + e
- f1: coefficient for the separator
2
3
Qf/Qa (kg/m3)
1.15
1.10
1.05
1.00
0 0 0 0 0
0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
0 0 0 0 0
Qf
Qa
f1
30
0 00 00
00 0000 0000
00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000
000000000000000000000000000000000000000000000000000000000000000000000000000000000000
00 0000 0000
40
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Qf/Qa (kg/m3)
Separation Performance
Rate of recuperation in the fines of particles smaller than a given dimension.
F f
r= *
A a
Bypass:
Circulating load:
HES Qf/Qa:
% Passing 45 m:
4.14
Rev. 2002
SECTION 4 MILLING
After
93.3
40.3
36
34.9
358
91.6
24.8
28.9
34.4
25.8
107
25
120
225
39.0
T1
Before
71
48.6
48.0
43.7
380
90
25.2
29.7
35.2
25.3
121
65
117
218
After
79.4
47.1
42.4
41.0
361
94.7
24.7
29.2
35.2
26.4
113
25
124
231
Separator
O'Sepa N-2000
Airflow design:
Pressure drop:
Rotor speed:
Feed capacity:
Power:
3.96 m
5.04 m eff
9.72 m eff
3581 kW
Lifting
Classifying
8mm-1
8mm+1
2000 m3/mi
8"
100-230 rpm
420 tph
200 HP AC var. freq
Volume load
comp
Volume load
Power kw
3"1/2
3"
2"1/2
2"1/2
2"
1"1/2
1"1/4
1"
3/4"
Before
20%
60%
20%
33%
7%
4%
8%
9%
12%
60%
34%
3100
After
20%
60%
20%
33%
3%
6%
9%
9%
22%
51%
36%
3260
Mill sweep
Separator
Primary
Aux
Secondary
Tertiary
TOTAL
Outlet fan
Temp
C
78.3
Press
"WG
-11
Flow
m3/h
34101
Flow
Nm/h
25781
15
66487
15
15
0
0
24079
13814
61
143381
63024
1301
22825
13095
100245
117156
4.15
Rev. 2002
174 RPM
79.2 t/h
78.2
62.5
= 0.656
= 191%
= 12 m
SECTION 4 MILLING
84 C
34 kW
3101 kW
Bypass
Imperfection
Rosin-Rammler(fine)
=8%
= 0.39
= 1.15
4.16
Rev. 2002
SECTION 4 MILLING
Percent H2O in
Separator Rejects
Product
Mill Discharge
Percent Recirculating Load
%
Percent Leakage Into Separator (CFM)
Maximum Separator Inlet Temperature
Ambient Temperature
F
Percent Relative Humidity
%
Plant Altitude
FT
Fuel Type
Heat
Value
Separator Rejects Temperature F
Product Temperature
F
Baghouse Cloth Area
FT2
Number of Compartments
Number of Compartments Cleaning Together
4.17
Rev. 2002
%
%
%
%
F
SECTION 4 MILLING
4. Grinding Aid
Type of Products
Surface active agents tend to saturate the free valence and inhibit the pack-set. Typical surface-active agents
are:
- ligno-sulphonates
- polyoils
- amines
- organic acids
Polar compounds (water, ammonia) are known to have some action on such bonds through their polar moment.
However, their practical use as surface agents is limited by their other impacts on the cement properties.
Other agents, particularly coal dust, have been used in the past.
Commercial products available as grinding aids are essentially (60-800 g/t ck):
- Triethanolamine
- Polypropyleneglycols and polyethylene
HEA2, DDA& and other products cause a definite reduction of pack-set but do not prevent agglomeration or
lump-formation problems that are caused by:
- Alkalis ( K 2 SO4 )
- Moisture
HEA2/rm (Grace)
0.078% weight per weight of kk
1.48$/kg
for a higher setting time (20 min)
4.18
Rev. 2002
SECTION 4 MILLING
5. Sieve
Sieve Screen
#400
#325
#270
#230
#200
#170
#140
#120
#100
#80
#70
#60
#50
#45
#40
#35
#30
#25
#20
#18
#16
Micron
37
44
53
63
74
88
105
125
149
177
210
250
297
354
420
500
595
707
1000
Iso alter
38
45
53
63
75
90
106
125
150
180
212
250
300
355
425
500
600
710
850
1000
1180
Screen
#14
#12
#10
#8
#7
#6
#5
#4
#3.5
1/4"
5/16"
3/8"
7/16"
1/2"
5/8"
3/4"
7/8"
1"
1"1/4
1"1/2
2"
Micron
2000
6350
8000
9510
11200
12700
16000
19000
22600
25400
32000
38100
50800
Iso alter
1400
1700
2000
2360
2800
3350
4000
4750
5600
6300
8000
9500
11200
12500
16000
19000
22400
25000
31500
38100
50000
4.19
Rev. 2002