Lehman OOC4e Experiment Correlations
Lehman OOC4e Experiment Correlations
Lehman OOC4e Experiment Correlations
Introduction; Laboratory Safety; Chemistry and the Environment; Minlab: Making Useful Laboratory Items; OP-1: Cleaning and Drying Glassware; OP-4: Weighing; OP-5: Measuring Volume; OP-6: Making Transfers; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; Appendix: Writing a Laboratory Report Laboratory Safety; The Effect of pH on a Food Preservative; Identifying a Constituent of "Panacetin;" Minilab: Extraction of Iodine by Dichloromethane; OP-4: Weighing; OP-5: Measuring Volume; OP-7a: Heat Sources; OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP-18a: Liquid-Liquid Extraction; OP-19: Evaporation; OP-26: Washing and Drying Solids Separating the Components of "Panacetin;" Minilab: Purification of an Unknown Compound by Recrystallization; OP-4: Weighing; OP-7a: Heat Sources; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28a: Recrystallization from a Single Solvent; OP-33: Melting Point; Appendix: The Chemical Literature Synthesis and Spectral Analysis of Aspirin; Minilab: Developing and Testing a Hypothesis; OP-2: Using Specialized Glassware; OP-4: Weighing; OP-7a: Heat Sources; OP-7b: Smooth Boiling Devices; OP-7c: Heating Under Reflux; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Calculations of Organic Synthesis Minilab: Preparation of Acetate Esters; OP-2: Using Specialized Glassware; OP-4: Weighing; OP-7: Heating; OP-10: Mixing; OP24: Washing Liquids; OP-25: Drying Liquids; OP-30a: Distillation of Liquids; OP-37: Gas Chromatography; Appendix: Planning an Experiment Minilab: Gas Chromatographic Analysis of Commercial Xylene; OP-4: Weighing; OP-7: Heating; OP-32: Fractional Distillation; OP-37: Gas Chromatography; Appendix: Planning an Experiment Minilab: Isolation of an Expectorant from Cough Capsules; OP-4: Weighing; OP-8: Cooling; OP-9: Temperature Monitoring; OP-10: Mixing; OP-11: Addition of Reactants; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-29: Sublimation; OP-33: Melting Point; Appendix: Planning an Experiment Minilab: A Missing-Label Puzzle; OP-4: Weighing; OP-5: Measuring Volume; OP-30: Simple Distillation; OP-34: Boiling Point; OP-35: Refractive Index; Appendix: Planning an Experiment Minilab: Paper Chromatography of Dyes in Commercial Drink Mixes; OP-6: Making Transfers; OP-15: Gravity Filtration; OP18c: LiquidSolid Extraction; OP-19: Evaporation; OP-21a: LiquidSolid Column Chromatography; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-26a: Washing Solids; OP-41a: UltravioletVisible Spectra; Appendix: Planning an Experiment
Isolation and Isomerization of Lycopene from Tomato Paste. Column Chromatography, Ultraviolet Visible Spectrometry .
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected Then you May Want to Consider
Minilab: Gas Chromatographic Analysis of an Essential Oil from Orange Peel; OP-4: Weighing; OP-18: Extraction; OP-19: Evaporation; OP-20: Steam Distillation; OP-25: Drying Liquids; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Minilab: Identification of an Unknown Felt-Tip-Pen Ink by TLC; OP-4: Weighing; OP-5: Measuring Volume; OP-16: Vacuum Filtration; OP-22: Thin-Layer Chromatography; OP-26: Washing and Drying Solids; OP-28b: Recrystallization from Mixed Solvents; OP-33: Melting Point; OP-40a: 1H NMR Spectrometry; Appendix: Planning an Experiment Minilab: Optical Rotation of Turpentine; OP-4: Weighing; OP-10: Mixing; OP-31: Vacuum Distillation; OP-34: Boiling Point; OP-36: Optical Rotation; Appendix: Planning an Experiment Minilab: The Structures of Organic Molecules; OP-39: Infrared Spectrometry Minilab: Who Else Has My Compound?; Qualitative Organic Analysis; OP-5: Measuring Volume; OP-30: Simple Distillation; OP-34: Boiling Point; OP-39: Infrared Spectrometry Minilab: Identification of an Unknown Felt-Tip-Pen Ink by TLC; OP-6: Making Transfers; OP-22: Thin-Layer Chromatography OP-10: Mixing; OP-16: Vacuum Filtration; OP-18: Extraction; OP19: Evaporation; OP-25: Drying Liquids; OP-26: Washing and Drying Solids; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Minilab: Isomers and Molecular Structure; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-33: Melting Point OP-7: Heating; OP-10: Mixing; OP-18: Extraction; OP-19: Evaporation; OP-25: Drying Liquids; OP-34: Boiling Point; OP35: Refractive Index; OP-36: Optical Rotation; OP-37: Gas Chromatography; OP-39: Infrared Spectrometry Minilab: Reactivities of Alkyl Halides in Nucleophilic Substitution Reactions; Minilab: An S N1 Reaction of Bromotriphenylmethane; OP-5: Measuring Volume; OP-7: Heating; OP-10: Mixing Minilab: An S N1 Reaction of Bromotriphenylmethane; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-33: Melting Point; OP-38: High-Performance Liquid Chromatography; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Minilab: Preparation and Properties of a Gaseous Alkene; OP10: Mixing; OP-17: Centrifugation; OP-24: Washing Liquids; OP25: Drying Liquids; OP-30: Simple Distillation; OP-37: Gas Chromatography; Appendix: Planning an Experiment Minilab: Addition of Iodine to -Pinene; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-11: Addition of Reactants; OP-14: Trapping Gases; OP-18: Extraction; OP-18b: Salting Out; OP-19: Evaporation; OP-25: Drying Liquids; OP-30: Simple Distillation; OP:34: Boiling Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Minilab: Unsaturation in Commercial Products; OP-10: Mixing; OP-11: Addition of Reactants; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Planning an Experiment
Isolation and Identification of the Major Constituent of Clove Oil. Steam Distillation, Infrared Spectrometry .
Identification of Unknown Ketones. Thin-Layer Chromatography, NMR Spectrometry . The Optical Activity of -Pinene: A Chemical Mystery. Vacuum Distillation, Optical Rotation . Investigation of a Chemical Bond by Infrared Spectrometry
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected Then you May Want to Consider
Minilab: The Nylon Rope Trick; OP-6: Making Transfers; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Infrared Spectrometry; Appendix: Planning an Experiment
Minilab: An S N1 Reaction of Bromotriphenylmethane; Minilab: Free-Radical Stability; OP-7: Heating; OP-10: Mixing; OP-11: Addition of Reactants; OP-14: Trapping Gases; OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP-19: Evaporation; OP-26: Washing and Drying Solids; OP-27: Cleaning and Drying Gases; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Preparation of Bromotriphenylmethane and the Trityl Free Radical Planning an Experiment Minilab: The Nylon Rope Trick; OP-7: Heating; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; Chain-Growth Polymerization of Styrene and Methyl Methacrylate OP-30: Simple Distillation; OP-39: Infrared Spectrometry OP-16: Vacuum Filtration; OP-32: Fractional Distillation; OP-34: Synthesis of Ethanol by Fermentation Boiling Point; Appendix: Planning an Experiment Minilab: Identification of an Unknown Arene by NMR Spectrometry; OP-7: Heating; OP-10: Mixing; OP-14: Trapping Gases; OP-20: Steam Distillation; OP-24: Washing Liquids; OP25: Drying Liquids; OP-30: Simple Distillation; OP-34: Boiling Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Reaction of Butanols with Hydrobromic Acid Minilab: Oxidation of Alcohols by Potassium Permanganate; Appendix: Planning an Experiment Borohydride Reduction of Vanillin to Vanillyl Alcohol Minilab: Preparation of a Fluorescent Dye; OP-7: Heating; OP10: Mixing; OP-11: Addition of Reactants; OP-12a: Using Drying Tubes; OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP19: Evaporation; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Synthesis of Triphenylmethanol and the Trityl Carbocation Minilab: Photoreduction of Benzophenone; Qualitative Organic Analysis; OP-10: Mixing; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-30: Simple Distillation; OP-34: Boiling Point; OP-39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Minilab: Diels-Alder Reaction of Maleic Anhydride and Furan; OP7: Heating; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-37: Gas Chromatography; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Minilab: Identification of an Unknown Arene by NMR Spectrometry; Minilab: Interpretation of a Mass Spectrum; OP39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; OP-41: UltravioletVisible Spectrometry Minilab: Interpretation of a Mass Spectrum; OP-7: Heating; OP10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Minilab: Free-Radical Stability; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Planning an Experiment Minilab: Nitration of Naphthalene; OP-18: Extraction; OP-19: Evaporation; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-37: Gas Chromatography; Appendix: Planning an Experiment
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected Then you May Want to Consider
Minilab: Preparation of Carbocations by the Friedel-Crafts Reaction; OP-7: Heating; OP-10: Mixing; OP-11: Addition of Reactants; OP-12: Excluding Water from Reaction Mixtures; OP14: Trapping Gases; OP-16: Vacuum Filtration; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-26: Washing and Drying Solids; OP-30: Simple Distillation; OP-33: Melting Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Isolation and Identification of the Major Constituent of Clove Oil; Steam Distillation and Infrared Spectrometry; Minilab: Air Oxidation of Fluorene to 9-Fluorenone; OP-7: Heating; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Minilab: Oxidation of Alcohols by Potassium Permanganate; Minilab: Identification of an Unknown Arene by NMR Spectrometry; Qualitative Organic Analysis; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-30: Simple Distillation; OP-33: Melting Point; OP-34: Boiling Point; OP-39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Properties of Organic Compounds OP-10: Mixing; OP-11: Addition of Reactants; OP-18: Extraction; OP-19: Evaporation; OP-25: Drying Liquids; OP-30: Simple Distillation; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Isomers and Isomerization Reactions; Qualitative Organic Analysis; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-18: Extraction; OP-19: Evaporation; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Minilab: A Nucleophilic Addition-Elimination Reaction of Benzil; OP-7: Heating; OP-10: Mixing; OP-16: Vacuum Filtration; OP-18: Extraction; OP-19: Evaporation; OP-25: Drying Liquids; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Planning an Experiment
A Green Synthesis of Adipic Acid; Minilab: Preparation of Aldol Condensation Products; OP-8: Cooling; OP-10: Mixing; OP-16: Vacuum Filtration; OP-18: Extraction; OP-19: Evaporation; OP24: Washing Liquids; OP-25: Drying Liquids; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-31: Vacuum Effect of Reaction Conditions on the Condensation of Furfural with Distillation; OP-33: Melting Point; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Cyclopentanone Minilab: Acid-Base Strengths of Organic Compounds; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; Appendix: Planning an Experiment Electronic Effect of a para -Iodo Substituent Identification of a Conjugated Diene from Eucalyptus Oil; Minilab: Hydrolysis Rates of Esters; OP-10: Mixing: OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-33: Melting Point; Appendix: Planning an Experiment; Appendix: Properties of Organic Compounds Synthesis and Identification of an Unknown Carboxylic Acid Minilab: Preparation of Benzamide; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-11: Addition of Reactants; OP-14: Trapping Gases; OP-18: Extraction; OP-19: Evaporation; OP-21: Column Chromatography; OP-24: Washing Liquids; OP-25: Drying Liquids; OP-37: Gas Chromatography; OP-39: Infrared Spectrometry; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Preparation of the Insect Repellent N,N -Diethyl-meta -toluamide
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected Then you May Want to Consider
Minilab: Synthesis of Dimedone Derivatives of Benzaldehyde; OP-7: Heating; OP-10: Mixing: OP-13: Excluding Air from Reaction Mixtures; OP-16: Vacuum Filtration; OP-19: Evaporation; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-40: Nuclear Magnetic Resonance Spectrometry; Appendix: Planning an Experiment Minilab: A Diazonium Salt Reaction of 2-Aminobenzoic Acid; OP8: Cooling; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; Appendix: Planning an Experiment Minilab: Beckmann Rearrangement of Benzophenone Oxime; OP-7: Heating; OP-8: Cooling; OP-9: Temperature Monitoring; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; Appendix: Planning an Experiment Minilab: Oxidation of Alcohols by Potassium Permanganate; Minilab: Identification of an Unknown Arene by NMR Spectrometry; Qualitative Organic Analysis; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-30: Simple Distillation; OP-33: Melting Point; OP-34: Boiling Point; OP-39: Infrared Spectrometry; Appendix: Properties of Organic Compounds Minilab: Dyeing with Indigo; OP-7: Heating; OP-9: Temperature Monitoring; OP-10: Mixing; OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-29: Sublimation; OP-33: Melting Point; OP42: Mass Spectrometry; Appendix: Planning an Experiment OP-5: Measuring Volume; OP-10: Mixing; OP-41b: Colorimetry Minilab: Reactions of Monosaccharides with Phenols; OP-7: Heating; OP-8: Cooling; OP-10: Mixing; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-36: Optical Rotation; Appendix: Planning an Experiment Minilab: Isolation of Trimyristin from Nutmeg; Minilab: Preparation of a Soap Using a Phase-Transfer Catalyst; OP-7: Heating; OP-18: Extraction; OP-19: Evaporation; OP-25: Drying Liquids; OP-37: Gas Chromatography; Appendix: Planning an Experiment Minilab: Isolation of a Protein from Milk; OP-3: Using Glass Rod and Tubing; OP-18: Extraction; OP-19: Evaporation; OP-22: ThinLayer Chromatography; OP-23: Paper Chromatography; OP-24: Washing Liquids; Appendix: Planning an Experiment Minilab: A Spontaneous Reaction of Benzaldehyde; OP-7: Heating; OP-10: Mixing; OP-15: Gravity Filtration; OP-16: Vacuum Filtration; OP-26: Washing and Drying Solids; OP-28: Recrystallization; OP-33: Melting Point; OP-39: Infrared Spectrometry; Appendix: Planning an Experiment Appendix: The Chemical Literature; Bibliography Introduction; Using the Chemical Literature in an Organic Synthesis; Appendix: The Chemical Literature; Bibliography
Preparation and Mass Spectrum of 2-Phenylindole Nucleophilic Strength and Reactivity in S NAr Reactions
Multistep Synthesis of Benzilic Acid from Benzaldehyde Using the Chemical Literature in an Organic Synthesis A Research Project in Organic Chemistry Minlab: Making Useful Laboratory Items Minilab: Extraction of Iodine by Dichloromethane Minilab: Purification of an Unknown Compound by Recrystallization Minilab: Developing and Testing a Hypothesis Minilab: Preparation of Acetate Esters
Introduction
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected
Minilab: Gas Chromatographic Analysis of Commercial Xylene Minilab: Isolation of an Expectorant from Cough Capsules Minilab: A Missing-Label Puzzle Minilab: Paper Chromatography of Dyes in Commercial Drink Mixes Minilab: Gas Chromatographic Analysis of an Essential Oil from Orange Peel Minilab: Identification of an Unknown Felt-Tip Pen Ink by TLC Minilab: Optical Rotation of Turpentine Minilab: The Structures of Organic Molecules Minilab: Who Else Has My Compound? Minilab: Isomers and Molecular Structure Minilab: Reactivities of Alkyl Halides in Nucleophilic Substitution Reactions Minilab: An S N1 Reaction of Bromotriphenylmethane Minilab: Preparation and Properties of a Gaseous Alkene Minilab: Addition of Iodine to -Pinene Minilab: Unsaturation in Commercial Products Minilab: Free-Radical Stability Minilab: The Nylon Rope Trick Minilab: Nucleophilic Substitution Rates of Alcohols Minilab: Photoreduction of Benzophenone Minilab: Oxidation of Alcohols by Potassium Permanganate Minilab: Preparation of a Fluorescent Dye Minilab: DielsAlder Reaction of Maleic Anhydride and Furan
Minilab: Identification of an Unknown Arene by NMR Spectrometry Minilab: Interpretation of a Mass Spectrum Minilab: Nitration of Naphthalene Minilab: Preparation of Carbocations by the FriedelCrafts Reaction Synthesis of Triphenylmethanol and the Trityl Carbocation Minilab: Air Oxidation of Fluorene to 9-Fluorenone Minilab: A Nucleophilic AdditionElimination Reaction of Benzil Minilab: Preparation of Aldol Condensation Products Minilab: A Spontaneous Reaction of Benzaldehyde Minilab: AcidBase Strengths of Organic Compounds Minilab: Hydrolysis Rates of Esters Minilab: Preparation of Benzamide Minilab: Synthesis of Dimedone Derivatives of Benzaldehyde Minilab: A Diazonium Salt Reaction of 2-Aminobenzoic Acid Qualitative Organic Analysis Minilab: Beckmann Rearrangement of Benzophenone Oxime Minilab: Dyeing with Indigo Minilab: Reactions of Monosaccharides with Phenols Minilab: Isolation of Trimyristin from Nutmeg Minilab: Preparation of a Soap Using a Phase-Transfer Catalyst Minilab: Isolation of a Protein from Milk Identification of an Oxygen-Containing Organic Compound; Identification of an Unknown Amine; Appendix: Properties of Organic Compounds Appendix: Laboratory Equipment
Qualitative Organic Analysis OP-1: Cleaning and Drying Glassware OP-2: Using Specialized Glassware OP-3: Using Glass Rod and Tubing OP-4: Weighing OP-5: Measuring Volume OP-6: Making Transfers OP-7: Heating OP-8: Cooling OP-9: Temperature Monitoring OP-10: Mixing OP-11: Addition of Reactants OP-12: Excluding Water from Reaction Mixtures OP-13: Excluding Air from Reaction Mixtures OP-14: Trapping Gases OP-15: Gravity Filtration
Experiment Correlations for Lehman, Operational Organic Chemistry 4/e If you selected
OP-16: Vacuum Filtration OP-17: Centrifugation OP-18: Extraction OP-19: Evaporation OP-20: Steam Distillation OP-21: Column Chromatography OP-22: Thin-Layer Chromatography OP-23: Paper Chromatography OP-24: Washing Liquids OP-25: Drying Liquids OP-26: Washing and Drying Solids OP-27: Cleaning and Drying Gases OP-28: Recrystallization OP-29: Sublimation OP-30: Simple Distillation OP-31: Vacuum Distillation OP-32: Fractional Distillation OP-33: Melting Point OP-34: Boiling Point OP-35: Refractive Index OP-36: Optical Rotation OP-37: Gas Chromatography OP-38: High-Performance Liquid Chromatography OP-39: Infrared Spectrometry OP-40: Nuclear Magnetic Resonance Spectrometry OP-41: UltravioletVisible Spectrometry OP-42: Mass Spectrometry Appendix: Laboratory Equipment Appendix: Keeping a Laboratory Notebook Appendix: Writing a Laboratory Report Appendix: Calculations for Organic Synthesis Appendix: Planning an Experiment Appendix: Properties of Organic Compounds Appendix: The Chemical Literature Bibliography
Bibliography
Bibliography