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Absolute Standards Inorganic 2012

Absolute STANDARDS is the largest supplier of Analytical Reference Materials (ARM)(r) and Performance Evaluation samples. We strive to provide the highest quality and broadest range of analytical standards.

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0% found this document useful (0 votes)
269 views80 pages

Absolute Standards Inorganic 2012

Absolute STANDARDS is the largest supplier of Analytical Reference Materials (ARM)(r) and Performance Evaluation samples. We strive to provide the highest quality and broadest range of analytical standards.

Uploaded by

AriCalidad
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 80

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

ABSOLUTE STANDARDS, INC. World Class Manufacturing & Internationally Recognized Quality
As Absolute Standards enters the latter half of our second decade of service, we continue to maintain our position as the industry leader. As the largest supplier of Analytical Reference Materials (ARM) and Performance Evaluation samples, we ship our products to all fty states, several territories, and over thirty countries. Focusing on the needs of the global testing body, we strive to provide the highest quality and broadest range of analytical standards to an industry that relies on accuracy and precision. Moreover, Absolute Standards is the only company in the industry that has exceeded the international requirements of both ISO/IEC 17025 and ISO 9001:2000 for the manufacture and analytical verication of our entire product line. As an analytical standards manufacturer, we recognize our role as an important link in the analytical testing community. Your analyses require the use of accurate, traceable, and defensible reference materials. It is this requirement that drives Absolute Standards to manufacture products that lead the industry in quality and value. Our philosophy at Absolute Standards is one of compliance. High expectations backed by quality accreditations help us achieve our goals. Discover how Absolutes commitment can help satisfy your compliance needs.

Stephen J. Arpie, M.S. Technical Director

John P. Criscio, President/CEO

Call Toll-Free 800-368-1131

ISO 9001:2000

Single Component Solutions: Pages 10-13

ORDERING & TECHNICAL INFORMATION


To Place an Order... please have the following information available: 1. Account # 2. Purchase Order #/ Credit Card # 3. Part # and Quantity We are available for orders & technical service from 9am-6pm (EST) by Phone, and 24 hrs. a day by Fax, Mail, & Internet. ...Phone... ...Fax...

800-368-1131 800-410-2577

...Mail... Absolute Standards, Inc. P.O. Box 5585 Hamden, CT 06518

...Email... [email protected]

Order on-line at www.AbsoluteStandards.com using LabCartTM Secure, Simple,Searchable, & Speedy We accept major credit cards: MasterCard / VISA / AMEX .

Orders that are placed before 5pm (EST) are shipped the same day by FedEx & UPS. Prices are F.O.B. Hamden CT. Terms are Net 30 Days. Terms and conditions of all sales contracts will be governed by the laws of The State of Connecticut. Prices are subject to change without notice. Warranty by Absolute Standards includes that our products are as described when

shipped. No warranty as to tness for any particular application is expressed or implied. Errant shipments and/or quality claims must be made within 30 days of receipt. No returns can be made without a Return Authorization Number and instructions of forwarding.

Liability by Absolute Standards is limited solely to the replacement of the product or refund
of the purchase price. These products are intended for research use only. Owing to their hazardous nature, they should be handled only by qualied, trained personnel familiar with their use.

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

CERTIFICATES & ACCREDITATIONS


Please visit our website at www.AbsoluteStandards.com to download current copies of our ISO 9001, ISO 17025 and A2LA certicates.

Call Toll-Free 800-368-1131

ISO 9001:2000

Custom Standard Quotation Request Form Fax: (800) 410-2577, Technical Service Dept, Absolute Standards, Inc. Email: [email protected] Page From: Company Contact: Company: Company Address: Telephone: Email: Product Description: Solvent/ Matrix: Volume Size: 1 x 100 mL Qty: 1 x 500 mL Qty: Other: Qty: Fax: of Date:

Single Component Solutions: Pages 10-13 Absolute Standards, Inc.

Account#:

Date Required: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. Comments: 4 Component

Analysis requested? (additonal charge) CAS# (optional)

Yes

No

Concentration (ug/mL)

Absolute Standards, Inc. ISO 9001 Registered ISO 17025 Accredited P.O. Box 5585, Hamden, CT 06518 Phone (800) 368-1131

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

AbsoluteGrade - Specications
Absolute Standards is the only company in the industry that has exceeded the international requirements of both ISO/IEC 17025 and ISO 9001:2000 for the manufacture and analytical verication of our entire product line. Equipped with state of the art instrumentation, our quality products are backed by the analytical power of an ICP-MS and four LCs. Included in this catalog are reference materials for calibration of the following instruments: AA, ICP, ICP-MS, IC, IE & several wet chemical methods. Method references are indicated wherever possible. In addition, the CLP section has been updated to include the latest revisions. Our capabilities are diverse and expanding. As we strive for continuous improvement, weve added the following services to better accomodate your needs: bulk sealing, on-line ordering with LabCartTM , and a fully searchable Products database available at www.AbsoluteStandards.com. We know that your requirements can be unique and varied therefore, if you would like a custom blend, please contact us with your specications. Let our experienced chemists give you a feasibility assessment of your design and work with you to enhance the stability and robustness of your custom formulation.

AbsoluteGrade - Specications
Suitable for ICP AES, DCP AES, ICP MS, High-Accuracy AA Flame or Graphite Furnace work. Manufactured using the Highest Purity starting materials available (typically 99.999%). Digestion in acid-cleaned PTFE labware to prevent possible contamination. Class A volumetric glassware used for pipetting and diluting where applicable. Signed Certicate of Analysis included with every standard. Traceable to NIST and other internationally recognized third party standards. Formulation Uncertainty provided for every analyte Density measurement allows wt/wt use. Verication of impurities in both starting materials and nal solutions. Immediate shipment from stock. Total U.S. Right To-Know, and O.S.H.A. compliance. Cost-effective packaging.

Call Toll-Free 800-368-1131

ISO 9001:2000

Single Component Solutions: Pages 10-13

TABLE OF CONTENTS
TITLE PAGES
Certicate of Analysis.........................................................................................................................................7 AbsoluteGrade Specications / Certied Weight Report........................................................................... 8-9 Single Component Solutions AA/ICP Spectroscopy....................................................................................10-13 Elemental Group Kits...................................................................................................................................14-15 Matrix Modiers and Blanks (AA/ICP)............................................................................................................16 Graphite Furnace (GFAA) Standards................................................................................................................17 Contract Laboratory Program (CLP) Standards...........................................................................................18-35 ILM 05.2 ICP-AES................................................................................................................................19-22 ILM 05.2 ICP-MS..................................................................................................................................23-27 ILM 05.3 ICP-AES (Water)...................................................................................................................28-30 ILM 05.3 ICP-AES (Soil)......................................................................................................................31-32 ILM 05.3 ICP-MS (Water)....................................................................................................................33-34 ILM 06.X ICP-MS (Soil)............................................................................................................................35 TCLP Multi-Element Calibration Standards................................................................................................36-37 EPA 6010 A/B Standards.............................................................................................................................38-39 EPA 6020/ 6020A Standards.............................................................................................................................40 EPA 200.7 Standards....................................................................................................................................41-51 Calibration Standards...........................................................................................................................41 Plasma, Tuning, Lab Check Solutions.................................................................................................42 Spectral Interference............................................................................................................................43 Lab Fortifying Solution (LFS).............................................................................................................44 Spiking Standards...........................................................................................................................45-46 Drinking Water Standards....................................................................................................................47 Instrument Wavelength Standards.......................................................................................................49 Quality Control Standards...............................................................................................................50-51 EPA 200.8 Standards............................................................................................................... ....................52-56 Tuning & Internal Standards................................................................................................................52 Calibration Standards...........................................................................................................................53 Verication Standards..........................................................................................................................54 Interference / Memory Check Solutions..............................................................................................55 Multi-Element Solutions......................................................................................................................56 EPA 200.9 Standards ........................................................................................................................................57 EPA Method 1620.............................................................................................................................................58 EPA Method 1636.............................................................................................................................................59 EPA Method 1638/1640....................................................................................................................................60 EPA Method 1664.............................................................................................................................................61 Groundwater and Wastewater Standards (600/4-79-020)............................................................................62-63 Trace Metals In Fish (600/4-79-020)................................................................................................................63 Miscellaneous Mixes.........................................................................................................................................64 EPA 300.0 Standards (Anions by Ion Chromatography).............................................................................65-68 Single Components / Eluents...............................................................................................................65 Multi-Analyte Solutions.................................................................................................................66-67 Inorganic Disinfection By-Products....................................................................................................68

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

TABLE OF CONTENTS

Cations ..............................................................................................................................................................69 EPA Method 314.0/ 314.1/ 332.0 (Perchlorate)................................................................................................70 EPA Method 353.2 (Nitrate & Nitrite)..............................................................................................................71 Organic Acids....................................................................................................................................................72 Miscellaneous Wet Methods........................................................................................................................72-74 Part# Index....................................................................................................................................................75-77 Custom Quotation Order Form......................................................................................................................4, 78

ABSOLUTE STANDARDS, INC.


ISO 9001 DLS ANSI-RAB ACCREDITED

Certificate of Analysis

Conformance: The Certificate of Analysis and the "Certified Weight Report" fulfill the requirements in the current versions of: ISO Guides (9001, 24, 31, 34, 17025) & NIST-NVLAP Handbook 150-19. Health & Safety: See the attached MSDS & Certified Weight Report before use. Intended Use: This Analytical Reference Material (ARM) is intended primarily for use in the characterization of unknowns & the establishment of response factors by qualified personnel. Typical instrumental organic assays include: GC & LC, and inorganic assays include: ICP & AA. The product is for laboratory use only. Certified Values: In production, gravimetric/volumetric readings are certified to be within +/- 0.5% of the stated value and are valid between 18C & 30C. The measured uncertainty can be found on the Certified Weight Report. All product weighings are performed on an analytical balance that is calibrated to NIST Traceable standard weights & certified by the manufacturer. The volumetric glassware used is Class A type & conforms to ASTM E-288 unless otherwise stated. The solvents & compounds used are of the highest practical purity & typically meet or exceed ACS Reagent Grade & ACS Standards Grade specifications. Homogeneity & Stability: No heterogeneity was observed in the preparation, packaging & storage of this standard. Expiration dates can be found on the Certified Weight Report. Purity & Identity: Purity determinations are performed using at least one analytical technique. Identity assays are typically performed using two dissimilar methods.

Organic solutions & neats are typically formulated from materials whose purity & identity have been characterized by GC-MSD & LC-PDA techniques with comparison to a NIST Traceable library of mass spectra when available. Additional characterization techniques may include but are not limited to: refractive index measurements of liquids, melting point measurements of solids, & GC-FID, ECD, PID, ELCD, NPD, LC-PDA measurements for purity. Inorganic solutions & neats are typically formulated from materials whose purity & identity have been characterized by ICPMS with comparison to a NIST Standard Reference Material when available. Additional characterization techniques may include but are not limited to: titratiometry, and densitometry, AA or ICP. Final solutions are subjected to instrumental analysis to support the gravimetric values when appropriate. The data for the quality assurance testing is published with the Certified Weight Report. Typical instrumental organic assays include GC and LC. Inorganic assays include ICPMS, titratiometry, and densitometry.

Storage: Sealed ampules and other containers should be stored in the dark at temperatures above the freezing point of the solution and not more than 30C. Certification by Absolute Standards, Inc. is typically valid for 5 years from the date of manufacture (Lot Number). Certified values are not applicable to opened ampules or to materials stored in re-sealable containers. See the Certified Weight Report for specific values.

Usage: Ampules & bottles should be brought to room temperature (18 to 30C) before opening. Sonication may be required for high concentration solutions. After opening, care should be exercised to avoid concentration changes owing to evaporation of the solvent or essential components. We recommend that a suitable re-sealable container be available before opening an ampule to decant the standard for short-term storage.

Legal Notice: Warranty of products are as described when shipped. No warranty as to fitness for any particular application is expressed or implied. Errant shipments and/or quality claims must be made within 10 days of receipt. Liability is limited solely to the replacement of the product or refund of purchase price. Certifying Officer: Stephen J. Arpie, M.S. Director

Absolute Standards, Inc. 44 Rossotto Drive Hamden, CT 06514 Voice: 1-203-281-2917 Fax: 1-203-281-2922 email: [email protected] www: http://www.absolutestandards.com
Document Identification: Certificate of Analysis Rev 5, Date Issued: 01/01/2006

Call Toll-Free 800-368-1131

ISO 9001:2000

Single Component Solutions: Pages 10-13

CERTIFIED WEIGHT REPORT

AbsoluteGrade SPECIFICATIONS

All of our standards are accompanied by a Certied Weight Report.


ABSOLUTE STANDARDS,INC 44 ROSSOTTO DRIVE HAMDEN, CT 06514 (800)-368-1131
ISO 9001 Quality System registered DLS ANSI/RAB Accredited

CERTIFIED WEIGHT REPORT: Part Number:

Lot #

Solvent(s):

53084

L135898

Nitric Acid

Lot Number:

070102

N37G05

Hydrofluoric acid

Description:

QC Standard 1 2.0% 20.0 0.25 (mL) Formulated By: Lawrence Barry 070102 070105 100 5E-05
Balance Uncertainty Flask Uncertainty

Expiration Date: Nominal Concentration (g/mL):

0.025%

Reviewed By:
Expanded

Pedro L. Rentas

070102

Weight(s) shown below were combined and diluted to :


Part Lot

999.88
Dilution

0.025
Initial

MSDS Information
(Solvent Safety Info. On Attached pg.)
CAS#

Uncertainty

Initial

Final

Uncertainty

Compound 1. Beryllium acetate (Be) 2. Calcium carbonate Ca) 3. Cadmium nitrate (Cd) 4. Chromium nitrate nonahydrate(Cr) 5. Cobalt nitrate (Co) 6. Copper nitrate (Cu) 7. Iron (III) Nitrate Nonahydrate 8. Lead nitrate (Pb) 9. Magnesium nitrate (Mg) 10. Manganese nitrate (Mn) 11. Ammonium molybdate (Mo) 12. Nickel nitrate (Ni) 13. Selenium oxide (Se) 14. Thallium nitrate (Tl) 15. Ammonium hexafluorotitanate (Ti) 16. Ammonium Metavanadate (V) 17. Zinc nitrate (Zn) 18. Antimony Oxide (Sb) 19. Arsenic (As)

Number

Number

Factor

Volume 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00

Pipette 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006

Conc.(ug/mL)

Conc (g/mL)

(+/-) (g/mL) 0.002334 0.002334 0.002002 0.002002 0.002002 0.002001 0.002003 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002

E OSHA PEL (TWA)

LD50

57104 58120 58148 58124 57127 58129 58126 57182 58112 57125 58142 58128 58134 57181 57122 58123 58130 58151 58133

051100 012202 091400 040901 020901 062001 061002 032900 110601 060800 082901 102600 011900 120700 042400 110701 041101 071001 062000

0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100

10000.04 10000.82 10000.19 10000.34 10000.54 10003.59 10001.80 9999.67 10000.20 10000.37 10000.17 10000.03 10001.32 10000.34 9999.90 10000.32 10000.21 10000.04 10000.48

100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0

19049-40-2 00471-34-1 10022-68-1 07789-02-8 10026-22-9 03251-23-8 07782-61-8 10099-74-8 10377-60-3 15710-66-4 13106-76-8 10377-66-9 07746-08-4 10102-45-1 16962-40-6 07803-55-6 10196-18-6 07440-36-0 07440-38-2

0.002 ug/m3 7 mg/m3 0.2 mg/m3 0.5 mg/m3 5 mg/m3 N/A 7 mg/m3 0.05 mg/m3 7 mg/m3 5 mg/m3 N/A 5 mg/m3 0.2 mg/m3 5 mg/m3 N/A 1.0 mg/m3 1 mg/m3 5.0 mg/m3 0.2 mg/m3

N/A N/A N/A orl-rat 3250mg/kg orl-rat 694 mg/kg orl-rat 940 mg/kg N/A 500 mg/kg N/A N/A orl-rat 333 mg/kg N/A N/A N/A N/A orl-rat 630 mg/kg orl-rat 1190mg/kg N/A N/A

P#53084 L#070102

Page 1 of 3

Printed on 8/13/02, 9:48 AM

ASSAYED ON AN HP 4500 ICP MS

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

AbsoluteGrade SPECIFICATIONS

CERTIFIED WEIGHT REPORT

A Certified Weight Report is generated for each lot illustrating the formulation procedure, traceability, & actual analysis.
44 Rossotto Drive Hamden, CT 06514 (800) 368-1131

Absolute Standards, Inc.

ISO 9001 Quality System Registered DLS ANSI-RAB Accredited


Part# 53084 (g/mL) 100.0 (+,- g/mL) 0.002 Lot# 070102

AbsoluteGrade Solution
Certified Concentration (g/mL)

The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise specified.

TRACEABILITY DOCUMENTATION: A) Classical Chemical Analysis: Method


EDTA Titration Gravimetric Analysis Redox Titration Volhard Titration

Traceability
NIST SRM 928 Lead Nitrate NIST Weights NIST SRM 136e Potassium Dichromate NIST SRM 999 Potassium Chloride

Concentration N/A N/A N/A N/A

B) Instrumental Analysis by Inductively Coupled Plasma Mass Spectroscopy (ICP-MS):


This analytical solution was tested against the appropriate NIST SRM's:

Trace Metals Verification b y ICP-MS (g /mL )


Al Sb As Ba Be Bi B <0.02

* * *

<0.02 <0.02 <0.02

Cd Ca Ce Cs Cr Co Cu

* *
<0.02 <0.02

* * *

Dy Er Eu Gd Ga Ge Au

<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02

Hf Ho In Ir Fe La Pb

<0.02 <0.02 <0.02 <0.02

* *

<0.02

Li Lu Mg Mn Hg Mo Nd

<0.02 <0.02

* * *

<0.2 <0.02

Ni Nb Os Pd P Pt K

*
<0.02 <0.02 <0.02 <0.02 <0.02 <0.2

Pr Re Rh Rb Ru Sm Sc

<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02

Se Si Ag Na Sr S Ta

*
<0.02 <0.02 <0.2 <0.02 <0.02 <0.02

Tb Te Tl Th Tm Sn Ti

<0.02 <0.02

<0.02 <0.02 <0.02

W U V Yb Y Zn Zr

<0.02 <0.02

* *

<0.02 <0.02 <0.02

(*) =Target Element

C) Physical Characterization:
1.018 Analyzed Density of Solution (g/mL): 22.6 Temperature (C): Homogeneity: No heterogeneity was observed in the preparation of this standard.

Certified by:

We use purified acids, 18 meg ohm double deionized water, calibrated Class A glassware and the highest purity raw materials available, (typically 99.999%). We meticulously clean our bottles by acid leaching and then triple rinsing with ASTM Type I water prior to use. Our standards are made gravimetrically using balances that are calibrated with weights traceable to NIST. (NIST Test #: 732/245790). We certify that all our standards are within the stated uncertainties unless otherwise stated, assuming that the bottle is kept tightly capped and stored under normal laboratory conditions.
Reference: Taylor, B.N. and Kuyatt, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result," NIST Technical Note 1297, U.S. government Printing Office, Washington DC, (1994).
P# 53084 L#070102, Report Page 2 of 2 Printed on 10/05/2002, 11:26AM

Call Toll-Free 800-368-1131

SINGLE COMPONENT SOLUTIONS

ISO 9001:2000

Single Component Solutions: Pages 10-13

PLASMA EMISSION SPECTROSCOPY REFERENCE STANDARDS

1,000 ug/mL Single Components for ICP/AA


Element
Aluminum Antimony Arsenic Barium Beryllium Bismuth Boron Cadmium Calcium Carbon Cerium Cesium Chromium Chromium-Cr6+ Cobalt Copper Dysprosium Erbium Europium Gadolinium Gallium Germanium Gold Hafnium Holmium Indium Iridium Iron Iron-Ferrous Iron-Total Lanthanum Lead Lithium Lithium 6+ Lutetium Magnesium Manganese Mercury Mercury-Organic Mercury-Total Al Sb As Ba Be Bi B Cd Ca C Ce Cs Cr Cr6+ Co Cu Dy Er Eu Gd Ga Ge Au Hf Ho In Ir Fe Fe2+ Fe La Pb Li Lu Mg Mn Hg Hg Hg

Matrix
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Bi(NO3)3/HNO3 H3BO3/H20 Cd(NO3)2/HNO3 CaCO3/HNO3 C(Citric Acid)/HNO3 Ce(NO3)3/HNO3 CsNO3/HNO3 Cr(NO3)3/HNO3 (NH4)2Cr2O7/H2O Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Dy2O3/HNO3 Er2O3/HNO3 Eu2O3/HNO3 Gd2O3/HNO3 Ga2O3/HNO3 (NH4)2GeF6/tr, HF NH4AuCl4/HCl Hf2O3/HCl Ho3O3/HNO3 In2O3/HNO3 IrCl3/HCl Fe(NO3)3/HNO3 (NH4)Fe2+(SO4)2/H2SO4 [Fe2+]+[Fe3+]/H2SO4 LaCl/HNO3 Pb(NO3)2/HNO3 LiNO3/HNO3 Li6+NO3/HNO3 Lu2O3/HNO3 Mg(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 MeHgCl/HNO3 Hg(NO3)2+MeHgCl/HNO3

Part#
57013 57051 57033 57056 57004 57083 57005 57048 57020 57006 57058 57055 57024 54161 57027 57029 57066 57068 57063 57064 57031 57032 57079 57072 57067 57049 57077 57026 54141 54140 57057 57082 57003 59021 57071 57012 57025 57080 54170 54004

$/100mL
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 75 30 75 30 30 30 75 30 30 30 30 30 30 200 30 30 30 30 30 30

Part#
58013 58051 58033 58056 58004 58083 58005 58048 58020 58006 58058 58055 58024 54172 58027 58029 58066 58068 58063 58064 58031 58032 58079 58072 58067 58049 58077 58026 54174 54173 58057 58082 58003 59097 58071 58012 58025 58080 54171 54168

$/500mL
70 70 70 70 70 70 70 70 70 70 70 70 70 50 70 70 75 75 75 75 150 70 150 75 75 70 150 70 50 50 70 70 70 1000 75 70 70 70 50 50

10

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

PLASMA EMISSION SPECTROSCOPY REFERENCE STANDARDS

SINGLE COMPONENT SOLUTIONS

ISO/ IEC 17025

1,000 ug/mL Single Components for ICP/AA


Element
Molybdenum Neodymium Nickel Niobium Palladium Phosphorus Platinum Potassium Praesodymium Rhenium Rhodium Rubidium Ruthenium Samarium Scandium Selenium Silica Silicon Silver Sodium Strontium Sulfur Tantalum Tellurium Terbium Thallium Thorium Thulium Tin Titanium Tungsten Uranium Vanadium Ytterbium Yttrium Zinc Zirconium Mo Nd Ni Nb Pd P Pt K Pr Re Rh Rb Ru Sm Sc Se SiO2 Si Ag Na Sr S Ta Te Tb Tl Th Tm Sn Ti W U V Yb Y Zn Zr

Matrix
(NH4)MoO4/H2O Nd2O3/HNO3 Ni(NO3)2/HNO3 (NH4)NbF6/tr.HF Pd/HNO3 (NH4)H2PO4/HNO3 [Pt(NH3)4](NO3)2/HCL KNO3/HNO3 Pr6O11/HNO3 Re/HNO3 RhCl3/HCl RbNO3/HNO3 RuCl3/HNO3 Sm2O3/HNO3 Sc(NO3)3/HNO3 SeO2/HNO3 SiO2/NaOH (NH4)2SiF6/HNO3 AgNO3/HNO3 NaNO3/HNO3 Sr(NO3)2/HNO3 (NH4)2SO4/H2O NH4TaF6/tr.HF TeO2/HCl Tb4O7/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 Tm2O3/HNO3 (NH4)SnF6/HNO3/HCL (NH4)2TiF6/HNO3/tr.HF (NH4)2WO4/H2O U3O8/HNO3 NH4VO3/HNO3 Yb2O3/HNO3 Y2O3/HNO3 Zn(NO3)2/HNO3 ZrO2/HNO3

Part#
57042 57060 57028 57041 57046 57015 57078 57019 57059 57075 57045 57037 57044 57062 57021 57034 54159 57014 57047 57011 57038 57016 57073 57052 57065 57081 57090 57069 57050 57022 57074 57092 57023 57070 57039 57030 57040

$/100mL
30 30 30 30 125 30 75 30 30 125 100 30 75 30 75 30 30 30 30 30 30 30 30 50 30 30 30 30 30 30 30 30 30 30 30 30 30

Part#
58042 58060 58028 58041 58046 58015 58078 58019 58059 58075 58045 58037 58044 58062 58021 58034 54169 58014 58047 58011 58038 58016 58073 58073 58065 58081 58090 58069 58050 58022 58074 58092 58023 58070 58039 58030 58040

$/500mL
70 75 70 70 200 70 150 70 75 150 400 75 150 75 150 70 75 70 70 70 70 70 75 150 75 70 70 75 70 70 70 70 70 75 70 70 70

For Additional Concentrations & Matrices Visit

www.AbsoluteStandards.com
or Call our Technical Department

Call Toll-Free 800-368-1131

11

SINGLE COMPONENT SOLUTIONS

ISO 9001:2000

Single Component Solutions: Pages 10-13

PLASMA EMISSION SPECTROSCOPY REFERENCE STANDARDS

10,000 ug/mL Single Components for ICP/AA


Element
Aluminum Antimony Arsenic Barium Beryllium Bismuth Boron Cadmium Calcium Carbon Cerium Cesium Chromium Chromium-Cr6+ Cobalt Copper Dysprosium Erbium Europium Gadolinium Gallium Germanium Gold Hafnium Holmium Indium Iridium Iron Iron-Ferrous Iron-Total Lanthanum Lead Lithium Lithium 6+ Lutetium Magnesium Manganese Mercury Mercury-Organic Mercury-Total Al Sb As Ba Be Bi B Cd Ca C Ce Cs Cr Cr6+ Co Cu Dy Er Eu Gd Ga Ge Au Hf Ho In Ir Fe Fe2+ Fe La Pb Li Li 6+ Lu Mg Mn Hg Hg Hg

Matrix
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Bi(NO3)3/HNO3 H3BO3/H20 Cd(NO3)2/HNO3 CaCO3/HNO3 C(Citric Acid)/HNO3 Ce(NO3)3/HNO3 CsNO3/HNO3 Cr(NO3)3/HNO3 (NH4)2Cr2O7/H2O Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Dy2O3/HNO3 Er2O3/HNO3 Eu2O3/HNO3 Gd2O3/HNO3 Ga2O3/HNO3 (NH4)2GeF6/tr, HF NH4AuCl4/HCl Hf2O3/HCl Ho3O3/HNO3 In2O3/HNO3 IrCl3/HCl Fe(NO3)3/HNO3 (NH4)Fe2+(SO4)2/H2SO4 [Fe2+]+[Fe3+]/H2SO4 LaCl/HNO3 Pb(NO3)2/HNO3 LiNO3/HNO3 Li6+NO3/HNO3 Lu2O3/HNO3 Mg(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 MeHgCl/HNO3 Hg(NO3)2+MeHgCl/HNO3

Part#
57113 57151 57133 57156 57104 57183 57105 57148 57120 57106 NA NA 57124 54175 57127 57129 NA NA NA NA NA NA 57179 NA NA NA NA 57126 NA NA NA 57182 57103 NA NA 57112 57125 57180 NA 54178

$/100mL
85 85 85 85 85 85 85 85 85 85 NA NA 85 85 85 85 NA NA NA NA NA NA 300 NA NA NA NA 85 NA NA NA 85 85 NA NA 85 85 85 NA 100

Part#
58113 58151 58133 58156 58104 58183 58105 58148 58120 58106 NA NA 58124 54176 58127 58129 NA NA NA NA NA NA 58179 NA NA NA NA 58126 NA NA NA 58182 58103 NA NA 58112 58125 58180 NA NA

$/500mL
160 160 160 160 160 160 160 160 160 160 NA NA 160 160 160 160 NA NA NA NA NA NA 600 NA NA NA NA 160 NA NA NA 160 160 NA NA 160 160 160 NA NA

12

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Single Component Solutions: Pages 10-13

PLASMA EMISSION SPECTROSCOPY REFERENCE STANDARDS

SINGLE COMPONENT SOLUTIONS

ISO/ IEC 17025

10,000 ug/mL Single Components for ICP/AA


Element
Molybdenum Neodymium Nickel Niobium Palladium Phosphorus Platinum Potassium Praesodymium Rhenium Rhodium Rubidium Ruthenium Samarium Scandium Selenium Silica Silicon Silver Sodium Strontium Sulfur Tantalum Tellurium Terbium Thallium Thorium Thulium Tin Titanium Tungsten Uranium Vanadium Ytterbium Yttrium Zinc Zirconium Mo Nd Ni Nb Pd P Pt K Pr Re Rh Rb Ru Sm Sc Se SiO2 Si Ag Na Sr S Ta Te Tb Tl Th Tm Sn Ti W U V Yb Y Zn Zr

Matrix
(NH4)MoO4/H2O Nd2O3/HNO3 Ni(NO3)2/HNO3 (NH4)NbF6/tr.HF Pd/HNO3 (NH4)H2PO4/HNO3 [Pt(NH3)4](NO3)2/HCL KNO3/HNO3 Pr6O11/HNO3 Re/HNO3 RhCl3/HCl RbNO3/HNO3 RuCl3/HNO3 Sm2O3/HNO3 Sc(NO3)3/HNO3 SeO2/HNO3 SiO2/NaOH (NH4)2SiF6/HNO3 AgNO3/HNO3 NaNO3/HNO3 Sr(NO3)2/HNO3 (NH4)2SO4/H2O NH4TaF6/tr.HF TeO2/HCl Tb4O7/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 Tm2O3/HNO3 (NH4)SnF6/HNO3/HCL (NH4)2TiF6/HNO3/tr.HF (NH4)2WO4/H2O U3O8/HNO3 NH4VO3/HNO3 Yb2O3/HNO3 Y2O3/HNO3 Zn(NO3)2/HNO3 ZrO2/HNO3

Part#
57142 NA 57128 NA 57146 57115 57178 57119 NA NA NA NA NA NA NA 57134 NA 57114 57147 57111 57138 57116 NA NA NA 57181 NA NA 57150 57122 57174 NA 57123 NA 57139 57130 57140

$/100mL
85 NA 85 NA 500 85 300 85 NA NA NA NA NA NA NA 85 NA 85 85 85 85 85 NA NA NA 85 NA NA 85 85 85 NA 85 NA 85 85 85

Part#
58142 NA 58128 NA 58146 58115 58178 58119 NA NA NA NA NA NA NA 58134 NA 58114 58147 58111 58138 58116 NA NA NA 58181 NA NA 58150 58122 58174 NA 58123 NA 58139 58130 58140

$/500mL
160 NA 160 NA 900 160 600 160 NA NA NA NA NA NA NA 160 NA 160 160 160 160 160 NA NA NA 160 NA NA 160 160 160 NA 160 NA 160 160 160

For Additional Concentrations & Matrices Visit

www.AbsoluteStandards.com
or Call our Technical Department

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13

ISO 9001:2000

Single Component Solutions: Pages 10-13

KITS

ELEMENTAL GROUP KITS

(5 x 100ml bottles @ 1000ug/mL Each)


Element Lithium Sodium Potassium Rubidium Cesium Li Na K Rb Cs Matrix LiNO3/HNO3 NaNO3/HNO3 KNO3/HNO3 RbNO3/HNO3 CsNO3/HNO3

Group I Elements Starter Kit

(5 x 100ml bottles @ 1000ug/mL Each)


Element Beryllium Magnesium Calcium Strontium Barium Be Mg Ca Sr Ba Matrix Be4O(C2H3O2)6/HNO3 Mg(NO3)2/HNO3 CaCO3/HNO3 Sr(NO3)2/HNO3 Ba(NO3)2/HNO3

Group II Elements Starter Kit

Part # 52253

$80/ 5 x 100 mL

Part # 52255

$80/ 5 x 100 mL

(9 x 100ml bottles @ 1000ug/mL Each)


Element Titanium Vanadium Chromium Manganese Iron Cobalt Nickel Copper Zinc Ti V Cr Mn Fe Co Ni Cu Zn Matrix (NH4)2TiF6/HNO3/tr.HF NH4VO3/HNO3 Cr(NO3)3/HNO3 Mn(NO3)2/HNO3 Fe(NO3)3/HNO3 Co(NO3)2/HNO3 Ni(NO3)2/HNO3 Cu(NO3)2/HNO3 Zn(NO3)2/HNO3

Transition Metals Starter Kit

(14 x 100ml bottles @ 1000ug/mL Each) Element


Lanthanum Cerium Praesodymium Neodymium Samarium Europium Gadolinium Terbium Dysprosium Holmium Erbium Thulium Ytterbium Lutetium La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb Lu LaCl/HNO3 Ce(NO3)3/HNO3 Pr6O11/HNO3 Nd2O3/HNO3 Sm2O3/HNO3 Eu2O3/HNO3 Gd2O3/HNO3 Tb4O7/HNO3 Dy2O3/HNO3 Ho3O3/HNO3 Er2O3/HNO3 Tm2O3/HNO3 Yb2O3/HNO3 Lu2O3/HNO3

Lanthanide Metals Starter Kit


Matrix

Part # 52256

$150/ 9 x 100 mL

Part # 52254

$240/ 14 x 100 mL

14

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

METHOD SPECIFIC SINGLE ELEMENT KITS

KITS

(32 x 100ml bottles @ 1000ug/mL Each)


Element Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Cerium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Mercury Molybdenum Nickel Phosphorus Potassium Selenium Silica Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Al Sb As Ba Be B Cd Ca Ce Cr Co Cu Fe Pb Li Mg Mn Hg Mo Ni P K Se SiO2 Ag Na Sr Tl Sn Ti V Zn Matrix Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 H3BO3/H20 Cd(NO3)2/HNO3 CaCO3/HNO3 Ce(NO3)3/HNO3 Cr(NO3)3/HNO3 Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Fe(NO3)3/HNO3 Pb(NO3)2/HNO3 LiNO3/HNO3 Mg(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 (NH4)MoO4/H2O Ni(NO3)2/HNO3 (NH4)H2PO4/HNO3 KNO3/HNO3 SeO2/HNO3 SiO2/NaOH AgNO3/HNO3 NaNO3/HNO3 Sr(NO3)2/HNO3 TlNO3/HNO3 (NH4)SnF6/HNO3/HCl (NH4)2TiF6/HNO3/tr.HF NH4VO3/HNO3 Zn(NO3)2/HNO3

Method 200.7 Complete Single Element Kit

(21 x 100ml bottles @ 1000ug/mL Each) Element


Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Mercury Molybdenum Nickel Selenium Silver Thallium Thorium Uranium Vanadium Zinc Al Sb As Ba Be Cd Cr Co Cu Pb Mn Hg Mo Ni Se Ag Tl Th U V Zn

Method 200.8 Complete Single Element Kit


Matrix

Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Cd(NO3)2/HNO3 Cr(NO3)3/HNO3 Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Pb(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 (NH4)MoO4/H2O Ni(NO3)2/HNO3 SeO2/HNO3 AgNO3/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 U3O8/HNO3 NH4VO3/HNO3 Zn(NO3)2/HNO3

Part # 52251

$380/ 21 x 100 mL

Part # 52250

$600/ 32 x 100 mL

Search our complete Products Database on-line at www.AbsoluteStandards.com


Search by: Component # of Components Concentration EPA Method 15

Call Toll-Free 800-368-1131

ISO 9001:2000

Single Component Solutions: Pages 10-13

MATRIX BLANKS & MODIFIERS

CALIBRATION BLANKS AND MATRIX MODIFIERS


MATRIX BLANKS

Blank solutions are prepared with High-Purity Acids and ASTM Type I Water. Blanks can be used to dilute your multi-element standards to run directly to establish your baseline. An Aqua Regia Blank can be prepared by mixing one part Nitric Acid Blank with three parts HCl Acid Blank. ASTM Type I H2O Part # 52000 Part # 53000 $25/ 100mL $40/ 500mL

Water Blank

Nitric Acid Blank


Matrix 5% HNO3 Part # 52002 Part # 53002 $25/100mL $40/500mL

HCI Acid Blank


Matrix 5% HCl Part # 52001 Part # 53001 $25/ 100mL $40/ 500mL

Matrix Modiers suppress background interferences and help enhance sensitivity by changing the behavior of the element or the matrix in solution with respect to temperature. These modiers help prevent the loss of certain elements during pyrolysis by converting the target to a less volatile form. This allows a more optimum graphite furnace program to be utilized.

GRAPHITE FURNACE ATOMIC ABSORPTION MATRIX MODIFIERS

Palladium and Magnesium Nitrate Modier


Matrix 0.3%(3 mg/mL) Pd & 0.2%(2 mg/mL) Mg in 5% HNO3
Starting Material Pd & Mg(NO3)2

Part # 52311 Part # 53311

$250/100mL $450/500mL

Palladium Nitrate Modier


Part # 57146 Part # 58146
Matrix 1%(10 mg/mL) in 2% HNO3
Starting Material Pd

Magnesium Nitrate Modier


Part # 52004 Part # 53004
Matrix 2%(20 mg/mL) in 5% HNO3
Starting Material Mg(NO3)2

$500/100mL $900/500mL

$125/100mL $200/500mL

Nickel Nitrate Modier


Part # 52003 Part # 53003
Matrix 5%(50 mg/mL) in 5% HNO3
Starting Material Ni(NO3)2

Ammonium Nitrate Modier


Part # 52309 Part # 53309
Matrix 2%(20 mg/mL) in H2O
Starting Material NH4NO3

$250/100mL $350/500mL

$250/100mL $350/500mL

Ammonium Dihydrogen Phosphate Modier


Part # 52005 Part # 53005
Matrix 10%(100 mg/mL) in H20
Starting Material (NH4)H2PO4

Calcium Nitrate Modier


Part # 52310 Part # 53310
Matrix 2%(20 mg/mL) in 5% HNO3
Starting Material Ca(NO3)2 4H2O

$350/100mL $500/500mL

$250/100mL $350/500mL

Lanthanum Nitrate Modier


Part # 52312 Part # 53312
Matrix 5%(50 mg/mL) in 5% HNO3
Starting Material LaNO3

Lanthanum Chloride Modier


Part # 52313 Part # 53313
Matrix 5%(50 mg/mL) in 5% HCl
Starting Material LaCl3

$250/100mL $350/500mL

$250/100mL $350/500mL

16

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

GFAA CALIBRATION AND SPIKING SOLUTIONS

GFAA STANDARDS

GRAPHITE FURNACE AA CALIBRATION AND SPIKING GFAA Calibration GFAA Initial Calibration
Verication (2nd Source) 6 Components Matrix 5% HNO3 Element Conc.(ug/mL) Sb 50 As 25 Cd 5 Pb 25 Se 50 Tl 25

Part # 52314 Part # 53314

6 Components Matrix 5% HNO3 Element Conc.(ug/mL) Sb 100 As 50 Cd 10 Pb 50 Se 100 Tl 50

$85/100 mL $190/500 mL

Part # 52315 Part # 53315

$85/100 mL $190/500 mL

GFAA Spike Standard


6 Components Matrix 5% HNO3 Element Conc.(ug/mL) Sb 100 As 40 Cd 5 Pb 20 Se 10 Tl 50

Part # 52316 Part # 53316

$85/100 mL $190/500 mL

GFAA Mercury Standard


Matrix 2% HNO3 Element Conc.(ug/mL) Hg 100

Part # 57280 Part # 58280

$30/100 mL $60/500 mL

Call Toll-Free 800-368-1131

17

ISO 9001:2000

Single Component Solutions: Pages 10-13

CLP

USEPA CONTRACT LABORATORY PROGRAM STATEMENT OF WORK FOR INORGANIC ANALYSIS

The following section illustrates the solutions appropriate for the inorganic analyitcal methods dervied from the USEPA Contract Laboratory Program. These methods are specifc for ICP-AES and ICP-MS technologies and are suitable for the detection of metals in various matrices. These methods are designed to not only isolate, but to both qualitatively and quantitatively detect specic target metals in water and soil/sediment. ACRONYM Cal CCV DESCRIPTION Calibration Standards Continuing Calibration Verication: To ensure calibration accuracy during each analysis, run a CCV standard for every wavelength/ mass used for each analyte. Contract Required Quantation Limit Standard prepared at the CRQL level Initial and Continuing Calibration Blank Interference Check Sample: To verify inter-element and background correction factors, the Contractor shall analyze and report the results for the ICS, for all elements on the Target Analyte List (TAL), and for all interferents (target and non-target), at the beginning and end of each analysis run, but not before the ICV. In addition, the Contractor shall analyze and report the results for the ICS at a frequency of not less than once per 20 analytical samples per analysis run. Initial Calibration/Verication: Immediately after each of system has been calibrated, the accuracy of the initial calibration shall be veried and documented for every analyte by the analysis of the ICV solution(s) at each wavelength/ mass used.

CRQL CRI ICB/CCB ICS

ICV

18

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2

CLP

ILM 05.2 INSTRUMENT CALIBRATION STANDARDS FOR INDUCTIVELY COUPLED PLASMA - ATOMIC EMISSION SPECTROSCOPY (ICP-AES)

5 Components 100 ug/mL in 5% HNO3 Be Cd Mn Pb Zn

Calibration Std. I

5 Components 100 ug/mL in 5% HNO3 Ba Co Cu Fe V

Calibration Std. II

Part # 52149 Part # 53149

$65/100 mL $130/500 mL

Part # 52150 Part # 53150

$65/100 mL $130/500 mL

2 Components 100 ug/mL in 5% HNO3 As Se

Calibration Std. III

Calibration Std. IV
6 Components 100 ug/mL in 5% HNO3 Al Ca Cr K Na Ni

Part # 52151 Part # 53151

$40/100 mL $80/500 mL

Part # 52152 Part # 53152

$65/100 mL $130/500 mL

4 Components 100 ug/mL in 5% HNO3 Ag Mg Sb Tl

Calibration Std. V

Part # 52153 Part # 53153

$65/100 mL $130/500 mL

Call Toll-Free 800-368-1131

19

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

ILM 05.2

CLP

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES ICP-AES Initial Verication Std. 1
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ba 100 Be 40 Cd 50 Co 100 Cu 100 Fe 100 Pb 100 Mn 100 Ni 100 Ag 20 Tl 100 Zn 100

ICP-AES Initial Verication Std. 2


10 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Sb 100 As 100 Ca 1000 Cr 100 Mg 1000 K 1000 Se 100 Na 1000 V 100

Part # 52017 Part # 53017

$95/100 mL $190/500 mL

Part # 52018 Part # 53018

$95/100 mL $190/500 mL

ICP-AES Continuing Calibration Verication Standard- CCV


22 Components Matrix 5% HNO3.

Element Ca Mg K Na Al Ba Fe Co V Ni Cu

Conc.(ug/mL) 2500 2500 2500 2500 200 200 100 50 50 40 25 Part # 52154 Part # 53154

Element Zn Mn Cr Ag Be Cd Pb As Se Tl Sb $95/100 mL $190/500 mL

Conc.(ug/mL) 20 15 10 10 10 10 10 10 10 10 60

20

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2

CLP

ILM 05.2 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) FOR ICP-AES


A standard must be run at double the Contract Required Quantation Limit (CRQL) or at two times the Instrument Detection Limits (IDL), whichever is greater. This standardization must be performed at the beginning and end of each batch of samples; or at least twice in an 8 hour shift. All elements to be analyzed must be veried except Al, Ba, Ca, Fe, Mg, Na, and K. The CRI Mix 1 contains all the required elements on the Target Analyte List (TAL) in their appropriate concentration ratios. The standard should be diluted by a factor of 1000 prior to use in the two times CRI run for ICP analysis. CRI Mix 2 is designed for ICPs equipped with ultrasonic nebulizers and offers all the elements of interest at two times the CRQL level.

Part # 52022 Part # 53022

15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 120 As 120 Be 10 Cd 10 Cr 20 Co 100 Cu 50 Pb 120 Mn 30 Ni 80 Se 120 Ag 20 Tl 120 V 100 Zn 40

CRI Mix 1

$125/100 mL $250/500 mL

Part # 52023 Part # 53023

15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 120 As 20 Be 10 Cd 10 Cr 20 Co 100 Cu 50 Pb 6 Mn 30 Ni 80 Se 10 Ag 20 Tl 20 V 100 Zn 40

CRI Mix 2

$125/100 mL $250/500 mL

Call Toll-Free 800-368-1131

21

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

ILM 05.2

CLP

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2 INTERFERENCE CHECKS FOR ICP-AES


Inter-element and background correction factors must be veried at the beginning and end of each analysis run, or at least twice in an 8 hour shift. Two solutions are required for the interference check: the interferent alone (solution A1), and the combination of interferents and analytes (solution AB1). A1 is prepared by diluting Interferents A by a factor of 5. Solution AB1 is prepared by producing a combined solution of Interferents A diluted by a factor of 5 and Analytes B diluted by a factor of 100. For example, combine 20 mL of Interferents A with 1.0 mL of analytes B and dilute the mixture to 100 mL with the calibration blank.

Part # 52024 Part # 53024

4 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 2500 Ca 2500 Fe 1000 Mg 2500

Interferents A

$95/100 mL $190/500 mL

Part # 52025 Part # 53025

12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 100 Ba 50 Be 50 Cd 100 Co 50 Cr 50 Cu 50 Mn 50 Ni 100 Pb 100 V 50 Zn 100

Interferents B

$95/100 mL $190/500 mL

Part # 52028 Part # 53028

18 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 50 As 200 Ba 200 Be 5 Cd 5 Cr 20 Co 50 Cu 25 Fe 100 Pb 50 Mn 50 Ni 50 Se 200 Ag 5 Tl 200 V 50 Zn 50

Spike Sample Standard 1

ILM 05.2 SPIKE SAMPLE FOR ICP-AES


In Spike Sample Analysis, a spike containing the required elements in their respective required amounts, is added to the sample prior to addition of any reagents, digestion, distillation, etc.

$280/100 mL $560/500 mL

Part # 52031 Part # 53031

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 400 Ba 400 Be 10 Cd 10 Cr 40 Co 100 Cu 50 Pb 100 Mn 100 Ni 100 Se 400 Ag 10 Tl 400 V 100 Zn 100

Spike Sample Standard 3 (Soil)

$160/100 mL $320/500 mL

22

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2

CLP

ILM 05.2 CALIBRATION, TUNING, & INTERNAL STANDARDS FOR INDUCTIVELY COUPLED PLASMA - MASS SPECTROSCOPY (ICP-MS)
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) Be 100 Mg 100 Co 100 In 100 Pb 100

Tuning Standard

Part # 52156 Part # 53156

$45/100 mL $90/500 mL

Element Al Sb As Ba Be Bi Cd Cr Co Cu In

23 Components Matrix 5% HNO3. Conc.(ug/mL) Element 100 Pb 100 Mg 100 Mn 100 Ni 100 Sc 100 Se 100 Ag 100 Tb 100 Tl 100 V 100 Y Zn Part # 52155 Part # 53155 $95/100 mL $190/500 mL

ICP-MS Calibration Standard

Conc.(ug/mL) 100 100 100 100 100 100 100 100 100 100 100 100

Element Bismuth Indium Holmium Lithium Lutetium Rhodium Scandium Terbium Yttrium Bi In Ho Li Lu Rh Sc Tb Y

Matrix Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 LiNO3/HNO3 Lu2O3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3

Conc. (ug/mL) 1000 1000 1000 1000 1000 1000 1000 1000 1000

INTERNAL STANDARDS
Part# 57083 57049 57067 57003 57071 57045 57021 57065 57039

$/100mL 25 25 25 25 30 125 75 25 25

Part# 58083 58049 58067 58003 58071 58045 58021 58065 58039

$/500mL 65 65 75 65 75 400 150 75 65

Call Toll-Free 800-368-1131

23

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

ILM 05.2

CLP

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-MS ICP-MS ICV Standard ICP-MS CCV Standard

Part # 52157 Part # 53157

23 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 50 Sb 50 As 50 Ba 50 Be 50 Bi 50 Cd 50 Cr 50 Co 50 Cu 50 In 50 Pb 50 Mg 50 Mn 50 Ni 50 Sc 50 Se 50 Ag 50 Tb 50 Tl 50 V 50 Y 50 Zn 50

$95/100 mL $190/500 mL

Part # 52158 Part # 53158

23 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 10 Sb 10 As 10 Ba 10 Be 10 Bi 10 Cd 10 Cr 10 Co 10 Cu 10 In 10 Pb 10 Mg 10 Mn 10 Ni 10 Sc 10 Se 10 Ag 10 Tb 10 Tl 10 V 10 Y 10 Zn 10

$95/100 mL $190/500 mL

P#52157-ICP-MS ICV Standard analyzed on HP 4500 ICP-MS


[1] Spe ctrum No .1 500 [ 1 7.6 14 sec]:5 3157.D# [Co unt] [Linear ]

250

m/z- >
1000

10

20

30

40

50

60

70

80

90

1 00

500

m/z- >
2.0 E4

11 0

120

13 0

140

150

160

170

180

190

2 00

1.0 E4

m/z- >

21 0

220

23 0

240

250

260

24

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2

CLP

ILM 05.2 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & INTERFERENTS SOLUTIONS FOR ICP-MS ICP-MS - CRI Standard
23 Components Matrix 5% HNO3. Element Al Sb As Ba Be Bi Cd Cr Co Cu In Conc.(ug/mL) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Part # 52159 Part # 53159 Element Pb Mg Mn Ni Sc Se Ag Tb Tl V Y Zn $95/100 mL $190/500 mL Conc.(ug/mL) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1

ICP-MS / Interferents B
20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 20 Ba 20 Bi 20 Cd 20 Cr 20 Co 20 Cu 20 In 20 Pb 20 Mn 20 Ni 20 Sc 20 Se 20 Ag 20 Tb 20 Tl 20 V 20 Y 20 Zn 20

ICP-MS / Interferents A
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Ca 100 Fe 100 Mg 100 K 100 Na 100 P 100 SO4 100 C 200 Cl 1000 Mo 2 Ti 2

Part # 52160 Part # 53160

$95/100 mL $190/500 mL

Part # 52161 Part # 53161

$110/100 mL $220/500 mL

Call Toll-Free 800-368-1131

25

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

ILM 05.2

CLP

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM

ILM 05.2 SPIKE SOLUTION FOR ICP-MS


In Spike Sample Analysis, a spike containing the required elements in their respective required amounts, is added to the sample prior to addition of any reagents, digestion, distillation, etc.

ICP-MS / Spike Sample


17 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 2000 Sb 100 As 40 Ba 2000 Be 50 Cd 50 Cr 200 Co 500 Cu 250 Pb 20 Mn 500 Ni 500 Se 10 Ag 50 Tl 50 V 500 Zn 500

Part # 52162 Part # 53162

$110/100 mL $220/500 mL

Place your order 24 hours a day, 7 days a week using LabCartTM, Absolutes on-line ordering system. Go to www.AbsoluteStandards.com & Click on On-Line Ordering for speedy, simple, and secure purchasing!

26

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

USEPA CONTRACT LABORATORY PROGRAM STATEMENT OF WORK FOR INORGANIC ANALYSIS

ILM 05.2

CLP

Cold Vapor Mercury Analysis


Element
Inorganic Mercury Inorganic Mercury Inorganic Mercury Inorganic Mercury Inorganic Mercury Inorganic Mercury Organic Mercury Organic Mercury Total Mercury Total Mercury Total Mercury

Conc. (ug/mL)
10 20 100 200 1000 10000 100 1000 100 1000 10000

Part#
57880 52009 57280 57380 57080 57180 54006 54170 54005 54004 54178

$/100mL
25 25 25 25 25 75 25 25 25 25 100

Part#
58880 53009 58280 58380 58080 58180 NA 54171 NA 54168 NA

$/500mL
50 50 50 50 65 150 NA 50 NA 50 NA

Total Cyanide Analysis


Analyte
Simple Cyanide Total Cyanide Free & Complexed Cyanide

Conc. (ug/mL)
1000 1000 1000

Part#
59017 54150 54165

$/100mL
25 25 25

Part#
54012 NA NA

$/500mL
90 NA NA

Simple Cyanide is formulated with Potassium Cyanide (KCN), no distillation is required. Total Cyanide is formulated with Potassium Ferricyanide (III), distillation is required before analysis can be performed. Free & Complexed Cyanide is formulated with both materials.

Call Toll-Free 800-368-1131

27

ISO 9001:2000
METHOD

ILM 05.3

CLP

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX

Single Component Solutions: Pages 10-13

ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES/ WATER MATRIX

22 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 60 As 10 Ba 200 Be 5 Cd 5 Ca 5000 Cr 10 Co 50 Cu 25 Fe 100 Pb 10 Mg 5000 Mn 15 Ni 40 K 5000 Se 35 Ag 10 Na 5000 Tl 25 V 50 Zn 60 Part # 52163 Part # 53163

ICP-AES ICV Water/Soil Matrix

20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Sb 30 As 5 Ba 100 Ca 2500 Cr 5 Co 25 Cu 12.5 Fe 50 Pb 5 Mn 7.5 Mg 2500 Ni 20 K 2500 Se 17.5 Ag 5 Na 2500 Tl 12.5 V 25 Zn 30 Part # 52164 Part # 53164 $150/100 mL $300/500 mL

ICP-AES CCV Water/Soil Matrix

$150/100 mL $300/500 mL

28

www.AbsoluteStandards.com

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ILM 05.3

CLP

ILM 05.3 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & SPIKE SOLUTIONS FOR ICP-AES/ WATER MATRIX ICP-AES CRI Mix Water Matrix ICP-AES Spike Sample Water Matrix
18 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 10 As 4 Ba 200 Be 5 Cd 5 Cr 20 Co 50 Cu 25 Fe 100 Pb 2 Mn 50 Ni 50 Se 5 Ag 5 Tl 5 V 50 Zn 50

Part # 59370 Part # 53165

15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 60 As 10 Be 5 Cd 5 Cr 10 Co 50 Cu 25 Pb 10 Mn 15 Ni 40 Se 35 Ag 10 Tl 25 V 50 Zn 60

$125/100 mL $250/500 mL

[1] Spectrum No.1 20

[ 16.634 sec]:59370.D# [Count] [Linear]

Part # 52166 Part # 53166

$125/100 mL $250/500 mL

10

m/z- >
20

10

20

30

40

50

60

70

80

90

100

10

m/z- >
500

110

120

130

140

150

160

170

180

190

200

250

m/z- >

210

220

230

240

250

260

P#59370-ICP-AES CRI Mix analyzed on HP 4500 ICP-MS

Call Toll-Free 800-368-1131

29

ISO 9001:2000
METHOD

ILM 05.3

CLP

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX

Single Component Solutions: Pages 10-13

ILM 05.3 INTERFERENTS SOLUTION FOR ICP-AES/ WATER MATRIX ICP-AES Interferents A Water Matrix ICP-AES Interferents B Water Matrix

Part # 52024 Part # 53024

4 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 2500 Ca 2500 Fe 1000 Mg 2500

$95/100 mL $190/500 mL

Combine Interferents Mix A & B for ICSAB. Dilute Interferants A Mix into Interferants B Mix in a 1:10 ratio.

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 200 As 100 Ba 500 Be 500 Cd 1000 Co 500 Cr 500 Cu 500 Mn 500 Ni 1000 Pb 50 Sb 600 Se 50 Tl 100 V 500 Zn 1000 Part # 52167 Part # 53167 $125/100 mL $250/500 mL

P#53024 analyzed on HP 4500/ ICP-MS


[1] Spectrum No.1 2.0E4

Mg

12.614 sec]:53024.D# [Count] [Linear]

Al

Ca

Fe

1.0E4

m/z->
2.0E5

10

20

30

40

50

60

70

80

90

100

1.0E5

m/z->
2.0E7

110

120

130

140

150

160

170

180

190

200

1.0E7

m/z->

210

220

230

240

250

260

30

www.AbsoluteStandards.com

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

ILM 05.3

CLP

ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES/ SOIL MATRIX ICP-AES ICV Water/Soil Matrix ICP-AES CCV Water/Soil Matrix

22 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 60 As 10 Ba 200 Be 5 Cd 5 Ca 5000 Cr 10 Co 50 Cu 25 Fe 100 Pb 10 Mg 5000 Mn 15 Ni 40 K 5000 Se 35 Ag 10 Na 5000 Tl 25 V 50 Zn 60 Part # 52163 Part # 53163 $150/100 mL $300/500 mL

20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Sb 30 As 5 Ba 100 Ca 2500 Cr 5 Co 25 Cu 12.5 Fe 50 Pb 5 Mn 7.5 Mg 2500 Ni 20 K 2500 Se 17.5 Ag 5 Na 2500 Tl 12.5 V 25 Zn 30 Part # 52164 Part # 53164 $150/100 mL $300/500 mL

Call Toll-Free 800-368-1131

31

ISO 9001:2000
METHOD

ILM 05.3

CLP

ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX

Single Component Solutions: Pages 10-13

ILM 05.3 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & SPIKE SOLUTIONS FOR ICP-AES/ SOIL MATRIX ICP-AES CRI Soil Matrix ICP-AES Spike Soil Matrix

Part # 52168 Part # 53168

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 600 As 100 Ba 500 Be 50 Cd 50 See page 30 Cr 100 for Co 500 Cu 250 Interferents Mixes. Pb 100 Mn 150 Ni 400 Se 350 Ag 100 Tl 250 V 500 Zn 600 $125/100 mL $250/500 mL

Part # 52169 Part # 53169

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 200 As 80 Ba 4000 Be 100 Cd 100 Cr 400 Co 1000 Cu 500 Pb 40 Mn 1000 Ni 1000 Se 100 Ag 100 Tl 100 V 1000 Zn 1000

$125/100 mL $250/500 mL

P#52168 - ICP-AES CRI analyzed on HP 4500/ ICP-MS


[1] Spectrum No.1 1.0E4 [ 42.811 sec]:52168B.D# [Count] [Linear]

5000

m/z->

10

20

30

40

50

60

70

80

90

100

2000

1000

m/z->

110

120

130

140

150

160

170

180

190

200

5.0E5

2.5E5

m/z->

210

220

230

240

250

260

32

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX

ISO/ IEC 17025


METHOD

ILM 05.3

CLP

ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS/CRI) SOLUTIONS FOR ICP-MS/ WATER MATRIX ICP-MS ICV Water Matrix ICP-MS / CRQL CHECK STANDARD-CRI Water Matrix
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 10 Ba 100 Be 10 Cd 10 Cr 20 Co 10 Cu 20 Pb 10 Mn 10 Ni 10 Se 50 Ag 10 Tl 10 V 10 Zn 20

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 10 Ba 100 Be 10 Cd 10 Cr 20 Co 10 Cu 20 Pb 10 Mn 10 Ni 10 Se 50 Ag 10 Tl 10 V 10 Zn 20 Part # 52170 Part # 53170 $125/100 mL $250/500 mL

Part # 52171 Part # 53171

$125/100 mL $250/500 mL

The CRI and ICV mixes are identical in element and concentration, but are prepared from separate source raw materials as specied by the method.

Call Toll-Free 800-368-1131

33

ISO 9001:2000
METHOD

ILM 05.3

CLP

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX

Single Component Solutions: Pages 10-13

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 10.0 As 5.0 Ba 50 Be 5.0 Cd 5.0 Cr 10.0 Co 5.0 Cu 10.0 Pb 5.0 Mn 5.0 Ni 5.0 Se 25.0 Ag 5.0 Tl 5.0 V 5.0 Zn 10.0 Part # 52172 Part # 53172 $125/100 mL $250/500 mL

ICP-MS / CCV Water Matrix

ICP-MS / Spike Sample Water Matrix


16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 40 Ba 2000 Be 50 Cd 50 Cr 200 Co 500 Cu 250 Pb 20 Mn 500 Ni 500 Se 10 Ag 50 Tl 50 V 500 Zn 500

See page 27 for Mercury & Cyanide Standards

Part # 52173 Part # 53173

$125/100 mL $250/500 mL

ICP-MS / Interferents B Water Matrix ICP-MS / Interferents A Water Matrix


12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 1000 Ca 1000 Fe 1000 Mg 1000 K 1000 Na 1000 P as PO431000 S as SO421000 C 2000 Cl 10000 Mo 20 Ti 20 15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 20 Ba 20 Cd 20 Cr 20 Co 20 Cu 20 Pb 20 Mn 20 Ni 20 Se 20 Ag 20 Tl 20 V 20 Zn 20

Dilute and Combine Interferants Mix A & B for Mix ICSAB. Interferants A Mix is 10X the method specication & Interferants B Mix is 1000X.

Part # 52174 Part # 53174

$125/100 mL $250/500 mL

Part # 52175 Part # 53175

$125/100 mL $250/500 mL

34

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX

ISO/ IEC 17025


METHOD

ILM 06.X

CLP

ILM 06.X has the same target analyte list as ILM 05.3, however specications for ICP-MS in soil are given.

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 50 Ba 500 Be 50 Cd 50 Cr 100 Co 50 Cu 100 Pb 50 Mn 50 Ni 50 Se 250 Ag 50 Tl 50 V 50 Zn 100 Part # 52176 Part # 53176 $125/100 mL $250/500 mL

ICP-MS ICV Soil Matrix

The CRI and ICV mixes are identical in element & concentration, but are prepared from separate source raw materials as

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 50 As 25 Ba 250 Be 25 Cd 25 Cr 50 Co 25 Cu 50 Pb 25 Mn 25 Ni 25 Se 125 Ag 25 Tl 25 V 25 Zn 50 Part # 52178 Part # 53178 $125/100 mL $250/500 mL

ICP-MS CCV Soil Matrix

16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 50 Ba 500 Be 50 Cd 50 Cr 100 Co 50 Cu 100 Pb 50 Mn 50 Ni 50 Se 250 Ag 50 Tl 50 V 50 Zn 100 Part # 52177 Part # 53177 $125/100 mL $250/500 mL

ICP-MS CRI Soil Matrix

Call Toll-Free 800-368-1131

35

ISO 9001:2000

Single Component Solutions: Pages 10-13

TCLP (1311)

Method

TOXICITY CHARACTERISTIC LEACHATE PROCEDURE (TCLP)


For use in accordance with the Toxicity Characteristic Rule Regulatory Levels issued in the Federal Register 55, 1.1846 March 1990: Method 1311.

Part # 52006 Part # 53006

7 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 25 Ba 500 Cd 5 Cr 25 Pb 25 Se 5 Ag 25 Hg* 20 *Hg is a separate solution.

(TCLP) Standard

(TCLP) GFAA Standard


3 Components Matrix 2% HNO3. Element Conc.(ug/mL) As 25 Pb 25 Se 5

Part # 52008 Part # 53008

$50/100 mL $100/500 mL

$95/100 mL $190/500 mL

(TCLP) Standard for ICP


4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ba 500 Cd 5 Cr 25 Ag 25

(TCLP) Cold Vapor Standard


Matrix 2% HNO3. Element Conc.(ug/mL) Hg 20

Part # 52009 Part # 53009

$30/100 mL $50/500 mL

Part # 52007 Part # 53007

$65/100 mL $130/500 mL

Search our complete Products Database on-line at www.AbsoluteStandards.com


Search by: Component # of Components Concentration EPA Method

36

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

SYNTHETIC PRECIPITATION LEACHING PROCEDURE

TCLP (1312)
Part#
58048 58148 58082 58182

Method

Element
Cadmium Cadmium Lead Lead Cd Cd Pb Pb

Matrix
Cd(NO3)2/HNO3 Cd(NO3)2/HNO3 Pb(NO3)2/HNO3 Pb(NO3)2/HNO3

Part#
57048 57148 57082 57182

Conc. (mg/mL) $/100mL


1.0 10.0 1.0 10.0 25 75 25 75

$/500mL
65 150 65 150

Part # 52148 Part # 53148

2 Components Matrix 2% HNO3 Element Conc.(ug/mL) Cd 1000 Pb 5000 $40/100 mL $80/500 mL

TCLP 1312 METALS

Call Toll-Free 800-368-1131

37

ISO 9001:2000
REV-1,7/92 REV-2,12/96

6010A

Single Component Solutions: Pages 10-13

6010B

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

MULTI-ELEMENT CALIBRATION STANDARDS FOR 6010A & 6010B

Part # 52043 Part # 53043

6 Components Matrix 2% HNO3. Element Conc.(ug/mL) Be 50 Cd 150 Pb 500 Mn 100 Se 200 Zn 150

Calibration Std. 1

$80/100 mL $160/500 mL

8 Components Matrix 2% HNO3. Element Conc.(ug/mL) Al 200 Ca 1000 Cr 20 Li 100 Ni 20 K 400 Na 200 Sr 10 Part # 52046 Part # 53046

Calibration Std. 4

Part # 52044 Part # 53044

5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ba 100 Co 100 Cu 100 Fe 1000 V 100

Calibration Std. 2

$90/100 mL $180/500 mL

$80/100 mL $160/500 mL

Part # 52047 Part # 53047

4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Sb 200 Mg 1000 Ag 50 Tl 200

Calibration Std. 5

$80/100 mL $160/500 mL

Part # 52045 Part # 53045

2 Components Matrix 2% HNO3 Element Conc.(ug/mL) As 500 Mo 100

Calibration Std. 3

$60/100 mL $120/500 mL

Part # 57315 Part # 58315

Matrix 2% HNO3. Element Conc.(ug/mL) P 200

Calibration Std. 6

$30/100 mL $60/500 mL

Calibration Standards Set 1-6


Part # 52042 $310/100 mL Part # 53042 $620/500 mL

38

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


REV-1,7/92 REV-2,12/96

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

6010A

6010B

Interference Standards are used to set or conrm that the appropriate background correction intervals have been set for sequential ICP spectrometers & that the proper inter-element correction factors are set for simultaneous ICP spectrometer systems.

INTERFERENCE STANDARDS FOR 6010A & 6010B

Interference Standards Set


Includes one each of Interference Standards 1,2,3,4,5 Part # 52038 $320/100 mL Part # 53038 $640/ 500mL

Matrix 2% HNO3. tr Tartaric acid Element Conc.(ug/mL) Sb 1000 Part # 57051 $30/100 mL Part # 58051 $70/500 mL

Interference Std. 2

17 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 100 Ba 30 Be 10 Cd 30 Cr 30 Co 30 Cu 30 Pb 100 Mn 20 Hg 5 Ni 30 K 3000 Se 50 Ag 30 Tl 100 V 30 Zn 30 Part # 52039 $230/100 mL Part # 53039 $460/500 mL

Interference Std. 1

5 Components Matrix 5% HNO3 Element Conc.(ug/mL) Li 300 Mo 300 P 1000 Sr 200 Ti 1000 Part # 52050 $80/100 mL Part # 53050 $160/500 mL

Interference Std. 3

4 Components Matrix 5% HNO3 Element Conc.(ug/mL) Al 400 Ca 2000 Fe 2000 Mg 1000 Part # 52041 $50/100 mL Part # 53041 $100/500 mL

Interference Std. 4

Matrix 2% HNO3. Element Conc.(ug/mL) Na 5000 Part # 57911 $50/100 mL Part # 58911 $100/500 mL

Interference Std. 5

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39

ISO 9001:2000

Single Component Solutions: Pages 10-13

6020/ 6020A

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-MS


MIXED CALIBRATION STANDARDS FOR 6020 & 6020A

Method 6020/ 6020A is applicable to the determination of metals in low concentrations (sub-ppb) in water and watse extracts using ICP-MS.

EPA Method 6020/ 6020A


12 Components Matrix 5% HNO3. Element Conc.(ug/mL) C 1000 Cl 10000 Al 500 Ca 1500 Fe 1250 Mg 500 Na 1250 P 500 K 500 S 500 Mo 10 Ti 10 Part # 59219 Part # 59249 $175/100 mL $525/500 mL

MIX A

EPA Method 6020/ 6020A


11 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 1.0 Cd 1.0 Cr 2.0 Co 2.0 Cu 2.0 Mn 2.0 Ni 2.0 Se 1.0 Ag 0.5 V 2.0 Zn 1.0 Part # 52331 Part # 53331 $125/100 mL $250/500 mL

MIX B

ICP-MS InternalStandards
Element
Bismuth Indium Holmium Lithium Rhodium Scandium Terbium Yttrium Bi In Ho Li6+ Rh Sc Tb Y

Matrix
Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 Li6+NO3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3

Part#
57083 57049 57067 59021 57045 57021 57065 57039

(ug/mL)
1000 1000 1000 1000 1000 1000 1000 1000

$/100mL
25 25 25 200 120 75 25 25

Part#
58083 58049 58067 59097 58045 58021 58065 58039

$/500mL
65 65 75 1000 400 150 75 65

40

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS- ICP-AES


MIXED CALIBRATION STANDARDS FOR 200.7

200.7
Rev 5.0

METHOD

EPA Method 200.7 covers the Determination of Metals and Trace Elements in Water and Wastes by ICP Atomic Emission Spectroscopy.

Mixed Calibration Std. 1


10 Components Matrix 5% HNO3 / tr.HF. Element Conc.(ug/mL) Ag 50 As 1000 B 100 Ba 100 Ca 1000 Cd 200 Cu 200 Mn 200 Sb 500 Se 500

Mixed Calibration Std. 2


6 Components Matrix 5% HNO3. Element Conc.(ug/mL) K 2000 Li 500 Mo 1000 Na 1000 Sr 100 Ti 1000

Part # 52336 Part # 53336

$75/100 mL $150/500 mL

Part # 52335 Part # 53335

$80/100 mL $160/500 mL

Mixed Calibration Std. 4


6 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 1000 Cr 500 Hg 200 Si 1000 Sn 400 Zn 500

4 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ce 200 Co 200 V 200 P 1000 Part # 52337 $75/100 mL Part # 53337 $150/500 mL

Mixed Calibration Std. 3

Part # 52056 Part # 53056

$80/ 100 mL $160/ 500 mL

6 Components Matrix 5% HNO3. Element Conc.(ug/mL) Be 100 Fe 1000 Pb 1000 Mg 1000 Ni 200 Tl 500 Part # 52057 $110/100 mL Part # 53057 $220/500 mL

Mixed Calibration Std. 5

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41

ISO 9001:2000

Single Component Solutions: Pages 10-13

Various Revisions

200.7

METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

The Plasma Solution is used to determine the optimum height above the load coil for viewing the plasma in EPA Method 200.7, Section 7.6.

The Tuning Solution is used to determine the optimum height above the load coil for viewing the plasma in EPA Method 200.7, Section 7.7.

Part # 52058 Part # 53058

4 Components Matrix 5% HNO3 Element Conc.(ug/mL) As 100 Pb 100 Se 200 Tl 200

Plasma Solution

$50/100 mL $100/500 mL

Part # 52059 Part # 53059

2 Components Matrix 5% HNO3. Element Conc.(ug/mL) Cu 100 Pb 100

Tuning Solution

$40/100 mL $80/500 mL

The Laboratory Performance Check Solution Set is used to evaluate the performance of the instrument system in EPA Method 200.7, Section 7.8.

Matrix 5% HNO Dilution : 1 to 100 P#52306 LPC-1 Element Conc. (ug/mL). Ag 50 Al 200 As 200 B 200 Ba 200 Be 200 Ca 200 Cd 200 Co 200 Cr 200 P#52307 LPC-2 P#52308 LPC-3 Element Conc. Element Conc. (ug/mL). (ug/mL). Cu 200 P 1000 Fe 200 Pb 200 Hg 200 Sb 200 K 1000 Se 1000 Li 200 Si 200 Mg 200 Sn* 200 Mn 200 Sr 200 Mo 200 Tl 200 Na 200 V 200 Ni 200 Zn 200 * (supplied as a separate solution) Part # 52060 $400/100 mL Part # 53060 $800/500 mL

LPC Solution Set

42

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

Various Revisions

200.7

METHOD

The Spectral Interference Check Solutions consist of higher-level, concentrated, selected method analytes and are used to evaluate the laboratorys procedure for correcting known inter-element spectral interferences.
SIC 1 is used to evaluate the Mo interelement spectral correction factors on the analytes Al, Sb, Se, Sn, and V.

Matrix H2O. Dilution : 1 to 10 Element Mo Part # 57642 Part # 58642 Conc.(ug/mL) 500 $30/100 mL $60/500 mL

SIC 1

SIC 2 is used to evaluate the Co, Cr, Mn, V, Cu, inter-element spectral correction factors on the analytes Pb, Sb, Mo, As, V, and Zn.

5 Components Matrix 2% HNO3. Dilution : 1 to 10 Element Conc. Corresponding (ug/mL) Interference Co Cr Mn V Cu 100 200 200 200 400 Pb Sb Mo As, Be Zn $50/100 mL $100/500 mL

SIC 2

Part # 52061 Part # 53061 SIC 3 is used to evaluate the Ni, Al, Fe, inter-element spectral correction factors on the analytes Sb, Zn, As, Ag, Mn, V, Cr.

3 Components Matrix 2% HNO3. Dilution : 1 to 10 Element Conc. Corresponding (ug/mL) Interference Ni Al Fe 200 300 1500 Sb, Zn As Ag, Cr, Mn, V $40/100 mL $80/500 mL

SIC 3

Part # 52062 Part # 53062

Call Toll-Free 800-368-1131

43

ISO 9001:2000

Single Component Solutions: Pages 10-13

Various Revisions

200.7

METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

LABORATORY FORTIFYING SOLUTION (LFS) FOR 200.7


The Laboratory Fortifying Solution is used in the preparation of the laboratory-fortied blank and the laboratory-fortied sample matrix solutions. The Laboratory-Fortied Blank (LFB) is an aliquot of reagent grade water to which known quantities of the method analytes are added in the laboratory. The LFB is analyzed exactly like a sample to determine whether method performance is within acceptable control limits. The Laboratory-Fortied Sample Matrix (LFM) is an aliquot of an environmental sample to which known quantities of the method analytes are added in the laboratory. The LFM is analyzed exactly like a sample to determine whether the sample matrix contributes bias to the analytical result. Note: The analytes Ca, Mg, and Na are not included in the Fortifying Solution due to their widely varying concentrations in environmental samples The analytes B & Si should be disregarded if the samples are processed and diluted in borosilicate labware due to contamination from borosilicate glass. Matrix 5% HNO3. Dilution : 1 to 100 P# 52304 LFS-2 Element Conc. (ug/mL) Cu Fe Hg K Li Mn Mo Ni Pb 250 250 50 250 250 100 250 500 250

LFS Solution Set

P# 52303 LFS-1 Element Conc.(ug/mL) Ag Al As B Ba Be Cd Co Cr 25 250 250 250 250 50 100 100 250

P# 52305 LFS-3 Element Conc.(ug/mL) Sb Se Si Sn* Sr Tl V Zn 250 250 250 100 250 250 100 250

* (supplied as a separate solution) Part # 52063 $180/100 mL Part # 53063 $360/500 mL

[1] Spectrum No.1 2.0E5

16.354 sec]:53304.D# [Count] [Linear]

1.0E5

m/z->
5.0E4

10

20

30

40

50

60

70

80

90

100

2.5E4

m/z->
5000

110

120

130

140

150

160

170

180

190

200

2500

m/z->

210

220

230

240

250

260

P#52304 - LFS Solution #2 analyzed on HP 4500/ ICP-MS

44

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

Various Revisions

200.7

METHOD

SPIKING STANDARDS FOR 200.7 Spiking Standard 1


3 Components Matrix H2O Element Conc.(ug/mL) B 500 Mo 500 Si 2000 Matrix 2% HNO3. tr Tartaric Acid Element Conc.(ug/mL) Sb 500 Part # 57651 Part # 58651 $30/100 mL $60/500 mL

Spiking Standard 4

Part # 52064 Part # 53064

$80/100 mL $160/500 mL

Spiking Standard 2
4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ca 1000 Mg 2000 K 10,000 Na 3000

Spiking Standard 5
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 2000 Cd 50 Pb 500 Se 2000 Tl 2000

Part # 52065 Part # 53065

$90/100 mL $180/500 mL

Part # 52067 Part # 53067

$100/100 mL $200/500 mL

Spiking Standard 3
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 2000 Ba 2000 Be 50 Cr 200 Co 500 Cu 250 Fe 1000 Mn 500 Ni 500 Ag 50 V 500 Zn 500

Spiking Standards Set


Part # 52068 Part # 53068 Includes one each of Spiking Standards 1,2,3,4,5 $400/100 mL $800/ 500mL

Part # 52066 Part # 53066

$180/100 mL $360/500 mL

Part # 57380 Part # 58380

Matrix 2% HNO3. Element Conc.(ug/mL) Hg 200

Mercury Standard

$30/100 mL $60/500 mL

Call Toll-Free 800-368-1131

45

ISO 9001:2000

Single Component Solutions: Pages 10-13

Various Revisions

200.7

METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS - ICP-AES

Spiking Standard 1
4 Components Matrix H2O Element Conc.(ug/mL) B 400 Mo 200 Si 2000 P 400

Part # 52069 Part # 53069

$90/100 mL $180/500 mL

Spiking Standard 2
4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ca 10,000 Mg 10,000 K 10,000 Na 10,000

Part # 52070 Part # 53070

$120/100 mL $240/500 mL

15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Ba 200 Be 100 Cr 100 Co 200 Cu 200 Fe 400 Li 200 Mn 100 Ni 200 Ag 200 Sr 400 Sn 200 V 200 Zn 200 Part # 52072 $180/100 mL Part # 53072 $360/500 mL

Spiking Standard 3

Spiking Standard 4
Matrix 2% HNO3. Element Conc.(ug/mL) Sb 200

Part # 57351 Part # 58351

$30/100 mL $60/500 mL

Matrix 2% HNO3. Element Conc.(ug/mL) Hg 200 Part # 57380 Part # 58380 $30/100 mL $60/500 mL

Mercury Standard

Spiking Standard 5
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 200 Cd 100 Pb 200 Se 400 Tl 400

Spiking Standards Set


Includes one each of Spiking Standards 1,2,3,4,5 & Hg @ 200 ug/mL

Part # 52071 Part # 53071

$100/100 mL $200/500 mL

Part # 52073 Part # 53073

$400/100 mL $800/ 500mL

46

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846-200.7 & SDWA 1310, NPDWR

Various Revisions

200.7

METHOD

DRINKING WATER STANDARDS


These standards are for use in drinking water compliance monitoring and for the analysis of ground and surface water requiring determination at drinking water contaminant levels. Refer to the US EPA SW-846, Method 1310 and US National Primary Drinking Water Regulations 40 CFR Part 141. The Second Drinking Water Metals Standard includes all metals required for US Appendix 200.7 for analysis by ICP Spectroscopy.

Primary Drinking Water Metals


8 Components Matrix 2% HNO3. Element Conc.(ug/mL) As 10 Ba 100 Cd 5 Cr 10 Pb 10 Se 5 Ag 10 Hg 10

[1] Spec trum No.1 100

[ 16.644 sec ] :53075.D# [Count] [Li near]

50

m /z ->

10

2 0

30

40

50

60

70

80

90

10 0

200

100

m /z ->

110

12 0

130

140

150

16 0

170

180

190

20 0

1000

500

Part # 52075 Part # 53075

$80/100 mL $160/500 mL

m /z ->

210

22 0

230

240

250

26 0

P#53075 - Primary Drinking Water Metals veried on HP 4500 ICP-MS

Secondary Drinking Water Metals


4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Cu 100 Fe 30 Mn 5 Zn 500

Drinking Water Standards Set


Includes one each of Primary and Secondary Standards Part # 52074 Part # 53074 $140/100 mL $280/500 mL

Part # 52076 Part # 53076

$65/100 mL $130/500 mL

Call Toll-Free 800-368-1131

47

ISO 9001:2000

Single Component Solutions: Pages 10-13

Our quality products are inspected by analytical chemists who have experience using a wide variety of instrumentation. Absolute maintains diverse technologies to ensure your calibration standards are accurate, reliable, & traceable. We use a ICP-MS, HPLC, and many wet methods.

Cations Tested Here


Brian

ICP - MS

Anions Tested Here


Pedro

HPLC - PDA

48

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHODS

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS 200.7 & 6010

200.7 6010

For calibration and verication of wavelength accuracy and stability in sequential and simultaneous ICP Spectrometers. Also for use in US EPA SW-846, Method 6010 section 5.6 and Method 200.7 section 7.6.1.

INSTRUMENT WAVELENGTH STANDARDS

Instrument Wavelength Standard


Al As Cd Cr Co Cu Fe Pb 100 100 100 100 100 100 100 100 15 Components Matrix 2% HNO3. Mg Mn Ni K Na Zn Y 100 100 100 100 100 100 600

[1] Spectrum No.1 2.0E4

[ 19.054 sec]:52081.D# [Count] [Linear]

1.0E4

m/z->
2000

10

20

30

40

50

60

70

80

90

100

1000

m/z->
2.0E5

110

120

130

140

150

160

170

180

190

200

1.0E5

Part # 52081 Part # 53081

$110/100 mL $220/500 mL

m/z->

210

220

230

240

250

260

P#52081 - 200.7 Instrument Wavelength Standard analyzed on HP 4500/ ICP-MS

Wavelength Calibration Solution 3


11 Components Matrix 2% HNO3. Element Conc.(ug/mL) As 20 La 20 Li 20 Cr 20 Mn 20 Mo 20 Ni 20 P 100 K 100 Sc 20 Na 20

Wavelength Calibration Solution 3B


11Components Matrix 2% HCl. Element Conc.(ug/mL) As 20 La 20 Li 20 Mn 20 Mo 20 Ni 20 P 100 K 100 Sc 20 Na 20 S 100

Part # 52079 Part # 53079

$90/100 mL $180/500 mL

Part # 59030

$75/100 mL

Call Toll-Free 800-368-1131

49

ISO 9001:2000
METHODS

Single Component Solutions: Pages 10-13

200.7 6010

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS 200.7 & 6010


QUALITY CONTROL STANDARDS

Quality control standards are used to check standard curves, perform inter-element correction and other spectral interference checks. Also used in US EPA Method 200.7 and 600/482-055 Technical Additions to Methods for Chemical Analysis of Water and Wastes. Available both individually and as a complete set.

Part # 52084 Part # 53084

19 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 100 Be 100 Ca 100 Cd 100 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Mg 100 Mn 100 Mo 100 Ni 100 Se 100 Tl 100 Ti 100 V 100 Zn 100

QC Standard 1

$175/100 mL $350/500 mL

Part # 52085 Part # 53085

21 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 100 Be 100 Ca 100 Cd 100 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Li 100 Mg 100 Mn 100 Mo 100 Ni 100 Se 100 Sr 100 Tl 100 Ti 100 V 100 Zn 100

QC Standard 2

$190/100 mL $380/500 mL

P#52084 - 200.7 QC Standard 1 analyzed on HP 4500/ ICP-MS


[1] Spectrum No.1 2000 [ 16.094 sec]:53084.D# [Count] [Linear]

1000

m/z->
2000

10

20

30

40

50

60

70

80

90

100

1000

m/z->
1.0E5

110

120

130

140

150

160

170

180

190

200

5.0E4

m/z->

210

220

230

240

250

260

50

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHODS

MULTI-ELEMENT SOLUTION STANDARDS FOR SW-846 METHODS 200.7 & 6010


QUALITY CONTROL STANDARDS CONTD
15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Ba 100 Ca 100 Cd 100 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Mg 100 Mn 100 Ni 100 Na 100 Ti 100 Zn 100

200.7 6010

QC Standard 3

Part # 52088 Part # 53088

7 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Ba 100 B 100 K 1000 Si 500 Ag 50 Na 100

QC Standard 5

$80/100 mL $160/500 mL

Part # 52086 Part # 53086

$170/100 mL $340/500 mL

Part # 52089 Part # 53089

Includes one each of Quality Control Standard 1, 3, 5.

Calibration Standards Set

$310/100 mL $620/500 mL

Part # 52087 Part # 53087

7 Components Matrix 2% HNO3. Element Conc.(ug/mL) Al 100 Ba 100 B 100 K 1000 Si 50 Ag 100 Na 100

QC Standard 4

$80/100 mL $160/500 mL

P#52087 - 200.7 QC Standard 4 analyzed on HP 4500/ ICP-MS


[1] Spectrum No.1 2000 [ 12.865 sec]:53087.D# [Count] [Linear]

Part # 52090 Part # 53090

Includes one each of Quality Control Standard 2, 3, 4.

Calibration Standards Set

1000

m/z->
2.0E4

10

20

30

40

50

60

70

80

90

100

$310/100 mL $620/500 mL

1.0E4

m/z->
2.0E6

110

120

130

140

150

160

170

180

190

200

1.0E6

m/z->

210

220

230

240

250

260

Call Toll-Free 800-368-1131

51

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

200.8

MULTI-ELEMENT SOLUTION STANDARDS FOR METHOD 200.8

ICP-MS MULTI-ELEMENT TUNING STANDARDS REV 5.5


These multi-element standards are designed to assist the operator in calibration of the instrument or verication of the mass range.

ICP-MS Tuning Standard 1


5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Be 10 Co 10 In 10 Pb 10 Mg 10

ICP-MS Tuning Standard 2


4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Li 10 Y 10 Ce 10 Tl 10 $50/100 mL $200/500 mL

Part # 52122 Part # 53122

$50/100 mL $200/500 mL

Part # 52123 Part # 53123

These internal standard stock solutions are used for: addition to blanks; calibration standards; as samples for internal standardization; and for use in US EPA SW-846 Method 200.8. Dilute 10 mL to 100 mL before using.

ICP-MS INTERNAL STANDARDS


(ug/mL)
100 100 1000 100 100 100 100 100

Element
Bismuth Indium Holmium Lithium Rhodium Scandium Terbium Yttrium Bi In Ho Li6+ Rh Sc Tb Y

Matrix
Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 Li6+NO3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3

Part#
57283 57249 57067 59036 57245 57221 57265 57239

$/100mL
25 25 25 100 100 25 25 25

Part#
58283 58249 58067 59037 58245 58221 58265 58239

$/500mL
50 50 75 300 300 50 50 50

Method 200.8 Rev 5.5 ICP-MS Internal Standard


5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Sc 10 Y 10 In 10 Tb 10 Bi 10

Part # 52332 Part # 53332

$50/100 mL $200/500 mL

52

www.AbsoluteStandards.com

Part # 52319 Part # 53319

7 Components Matrix 2% HNO3. Element Conc.(ug/mL) Bi 10 Ho 10 In 10 Li 10 Sc 10 Tb 10 Y 10

Multi-Element Internal Standard

$65/100 mL $200/500 mL

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR METHOD 200.8

200.8

ICP-MS CALIBRATION STANDARDS REV 5.5


These multi-element standards are designed to assist the ICP-MS operator in performing concentration verication

Method 200.8 ICP-MS CalibrationStandard 1


19 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 10 Sb 10 As 10 Be 10 Cd 10 Cr 10 Co 10 Cu 10 Pb 10 Mn 10 Hg 5 Mo 10 Ni 10 Se 50 Tl 10 Th 10 U 10 V 10 Zn 10

Method 200.8 ICP-MS CalibrationStandard 3


Matrix 2% HNO3. Element Conc.(ug/mL) Hg 5

Part # 59388

$30/100 mL

Method 200.8 ICP-MS CalibrationStandard 2


2 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ba 10 Ag 10

Part # 52334 Part # 53334

$40/100 mL $80/500 mL

Part # 52333 Part # 53333

$150/100 mL $300/500 mL

P#53332 - 200.8 Internal Standard analyzed on HP 4500/ ICP-MS


[1] Spectrum No.1 5.0E6 [ 39.862 sec]:53332B.D# [Count] [Linear]

2.5E6

m/z->
5.0E6

10

20

30

40

50

60

70

80

90

100

2.5E6

m/z->
2.0E6

110

120

130

140

150

160

170

180

190

200

1.0E6

m/z->

210

220

230

240

250

260

Call Toll-Free 800-368-1131

53

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

200.8

MULTI-ELEMENT SOLUTION STANDARDS FOR METHOD 200.8

ICP-MS VERIFICATION STANDARD

ICP-MS Verication Standard 1


Element Al As Ba Be Bi Ca Cd Cr Co Cu Fe Ga Pb (ug/mL) 10 10 10 10 10 10 10 10 10 10 10 10 10 26 Components Matrix 5% HNO3. Element Li Mg Mn Hg Ni K Se Na Ag Sr Tl V Zn (ug/mL) 10 10 10 10*Separate solution 10 10 10 10 10 10 10 10 10

Part # 52101 Part # 53101

6 Components Matrix H2O Element Conc.(ug/mL) B 10 Mo 10 S 10 Si 10 Ti 10 W 10

ICP-MS Verication Standard 2

$60/100 mL $120/500 mL

*Part# 57880 is included (Hg @ 10 ug/mL)

Part # 52100 Part # 53100

$180/100 mL $380/500 mL

Includes one each of ICP-MS Verication 1 and 2. Part # 52102 Part # 52302 $220/100 mL $440/500 mL

ICP-MS Verication Set

P#52100- 200.8 Verication Standard 1 analyzed on HP 4500/ ICP-MS


[1] Spec trum No.1 200 [ 23.254 sec ]:53100.D# [Count] [Linear]

100

m/z- >
1000

10

20

30

40

50

60

70

80

90

100

500

m/z- >
1.0E 4

110

120

130

140

150

160

170

180

190

200

5000

m/z- >

210

220

230

240

250

260

54

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR METHOD 200.8


ICP-MS INTERFERENCE CHECK SOLUTIONS ICP-MS Interference Check Solution A
12 Components Matrix in 2%-HNO3/ tr. HF Element Conc.(ug/mL) Al 500 Ca 500 Fe 500 Mg 500 Na 500 P 500 K 500 S 500 C 1000 Cl 3600 Mo 10 Ti 10 $100/100 mL $450/500 mL

200.8

ICP-MS Interference Check Solution B


11 Components Matrix in 2%-HNO3/ tr. HF Element Conc.(ug/mL) As 0.100 Cd 0.050 Cr 0.100 Co 0.200 Cu 0.100 Ni 0.200 Mn 0.100 Se 0.100 Ag 0.100 V 0.200 Zn 0.100 $100/100 mL $450/500 mL

Part # 52114 Part # 53114

Part # 52115 Part # 53115

ICP-MS MEMORY CHECK SOLUTIONS


Combine mixes A and B in equal ratios. This test will determine any memory problems that will affect the quality of the data.

ICP-MS Memory Check Solution A

Part # 52116 Part # 53116

14 Components Matrix in 2%-HNO3/ tr. HF Element Conc.(ug/mL) Al 1000 Mg 1000 Na 1000 C 2000 Cl 7200 S 1000 Ti 20 Sb 20 Be 20 Cr 20 Mn 20 Ni 20 V 20 Zn 20 $100/100 mL $450/500 mL

14 Components Matrix in 2%-HNO3 Element Conc.(ug/mL) Ca 1000 Fe 1000 K 1000 P 1000 Mo 20 As 20 Ba 20 Cd 20 Co 20 Cu 20 Pb 20 Se 20 Ag 20 Tl 20 Part # 52117 $100/100 mL Part # 53117 $450/500 mL

ICP-MS Memory Check Solution B

Call Toll-Free 800-368-1131

55

ISO 9001:2000

Single Component Solutions: Pages 10-13

ICP-MS
Multi-Element Solution 1
29 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 10 Al 10 As 10 Ba 10 Be 10 Bi 10 Ca 10 Cd 10 Co 10 Cr 10 Cs 10 Cu 10 Fe 10 Ga 10 In 10 K 10 Li 10 Mg 10 Mn 10 Na 10 Ni 10 Pb 10 Rb 10 Se 10 Sr 10 Tl 10 U 10 V 10 Zn 10

MULTI-ELEMENT SOLUTION STANDARDS FOR ICP-MS


Multi-Element Solution 2
17 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ce 10 Dy 10 Er 10 Eu 10 Gd 10 Ho 10 La 10 Lu 10 Nd 10 Pr 10 Sc 10 Sm 10 Tb 10 Th 10 Tm 10 Y 10 Yb 10

Multi-Element Solution 3
10 Components Matrix 10% HCL / 1% HNO3. Element Conc.(ug/mL) Au 10 Hf 10 Ir 10 Pd 10 Pt 10 Rh 10 Ru 10 Sb 10 Sn 10 Te 10

Part # 52135 Part # 53135

$250/100 mL $500/500 mL

Part # 52134 Part # 53134

$200/100 mL $400/500 mL

Multi-Element Solution 4
12 Components Matrix H2O tr. HF Element Conc.(ug/mL) B 10 Ge 10 Mo 10 Nb 10 P 10 Re 10 S 10 Si 10 Ta 10 Ti 10 W 10 Zr 10

Multi-Element Solution 5
Matrix 2% HNO3. Element Conc.(ug/mL) Hg 10

Part # 52133 Part # 53133

$180/100 mL $360/500 mL

Part # 57880 Part # 58880

$30/100 mL $60/500 mL

Includes one each of Multi-Element 1, 2, 3, 4, & 5. Part # 52137 Part # 53137 5X100 mL 5X500 mL $650 $1300

ICP-MS Solution Kit

Part # 52136 Part # 53136

$150/100 mL $300/500 mL

56

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Single Component Solutions: Pages 10-13

DETERMINATION OF TRACE ELEMENTS BY STABILIZED TEMPERATURE GRAPHITE FURNACE AA


Method 200.9 Complete Single Elememt Kit
Matrix

ISO/ IEC 17025

200.9

METHOD

(16 x 100ml bottles @ 1000ug/mL Each)


Element

Aluminum Antimony Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Thallium Tin

Al Sb As Be Cd Cr Co Cu Fe Pb Mn Ni Se Ag Tl Sn

Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Be4O(C2H3O2)6/HNO3 Cd(NO3)2/HNO3 Cr(NO3)3/HNO3 Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Fe(NO3)3/HNO3 Pb(NO3)2/HNO3 Mn(NO3)2/HNO3 Ni(NO3)2/HNO3 SeO2/HNO3 AgNO3/HNO3 TlNO3/HNO3 (NH4)SnF6/HNO3/HCl $280/ 16 x 100 mL

Part # 52252

Palladium and Magnesium Nitrate Modier


Matrix 0.3%(3 mg/mL) Pd & 0.2%(2 mg/mL) Mg in 5% HNO3 Part # 52311 Part # 53311 $250/100mL $450/500mL
Starting Material Pd & Mg(NO3)2

PT Study Schedule: January 15- March 1 April 15- May 30 *July 15- August 29 (DMR-QA) October 15- November 29 Offering our complete line of water & soil PTs EVERY study!

Call Toll-Free 800-368-1131

57

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

1620

METALS BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROSCOPY & ATOMIC ABSORPTION SPECTROSCOPY

The method is a consolidation of US EPA Methods 200.7 (ICP for trace elements), 204.2 (Sb), 206.2 (As), 239.2 (Pb), 270.2 (Se), 279.2 (Tl), 245.5 (Hg), 245.1 (Hg), and 245.2(Hg). The method is used for analysis of trace elements by ICP atomic emission spectroscopy and GFAA spectroscopy, for analysis of mercury by CVAA spectroscopy,and as a semi-quantitative ICP screen for specied elements.

EPA 1620 Standard 1


5 Components Matrix 5% HNO3. Element Conc.(ug/mL) Mn 100 Be 100 Cd 100 Pb 100 Zn 100

EPA 1620 Standard 2


6 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ba 100 Cu 100 Fe 100 V 100 Y 100 Co 100

Part # 52139 Part # 53139

$60/100 mL $120/500 mL

Part # 52140 Part # 53140

$60/100 mL $120/500 mL

EPA 1620 Standard 3


3 Components Matrix 5% HNO3. Element Conc.(ug/mL) Mo 100 As 100 Se 100

EPA 1620 Standard 4


5 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ca 100 Na 100 Al 100 Cr 100 Ni 100

Part # 52141 Part # 53141

$50/100 mL $100/500 mL

Part # 52142 Part # 53142

$60/100 mL $120/500 mL

EPA 1620 Standard 5


6 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 B 100 Mg 100 Ag 100 Tl 100 Ti 100

EPA 1620 Standard 6 Tin


Matrix 2% HNO3./ 6% HCL Element Conc.(ug/mL) Sn 100 $30/100 mL $60/500 mL

Part # 57250 Part # 58250

Part # 52143 Part # 53143

$60/100 mL $120/500 mL

58

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

DETERMINATION OF HEXAVALENT CHROMIUM BY ION CHROMATOGRAPHY

1636

This method is for the determination of dissolved hexavalent chromium (as CrO) in ambient waters at EPA water quality criteria (WQC) levels using ion chromatography (IC). This method was developed by integrating the analytical procedures in EPA Method 218.6 with the quality control (QC) and sample handling procedures necessary to avoid contamination and ensure the validity of analytical results during sampling and analysis for metals at EPA WQC levels.

Hexavalent Chromium (Cr6+)


1000 ug/mL in Water Part # 54161 Part # 54172 $30/100 mL $50/500 mL

Hexavalent Chromium (Cr6+)


10 mg/mL in Water Part # 54175 Part # 54176 $75/100 mL $150/500 mL

Call Toll-Free 800-368-1131

59

ISO 9001:2000
METHODS

1638 1640

DETERMINATION OF TRACE ELEMENTS IN AMBIENT WATERS BYINDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY

Single Component Solutions: Pages 10-13

Method 1638 & 1640 are for the determination of dissolved elements in ambient waters at EPA water quality criteria (WQC) levels using inductively coupled plasma-mass spectrometry (ICP-MS). In addition, Method 1640 employs on-line chelation preconcentration. These methods may also be used for determination of total recoverable element concentrations in these waters.

Method 1638 Mix A

Part # 52144 Part # 53144

8 Components Matrix 2% HNO3. Element Conc.(ug/mL) Sb 10 Cd 10 Cu 10 Pb 10 Ni 10 Se 10 Tl 10 Zn 10

Method 1640 Mix A

6 Components Matrix 2% HNO3. Element Conc.(ug/mL) As 10 Cd 10 Cu 10 Pb 10 Ni 10 Zn 10 $50/100 mL $100/500 mL

Method 1638/1640 Mix B


Silver (Ag) Matrix 2% HNO3. Element Conc.(ug/mL) Ag 20

Part # 57847 Part # 58847

$30/100 mL $60/500 mL

$60/100 mL $120/500 mL

Part # 52146 Part # 53146

Part # 52145 Part # 53145

5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Sc 10 Y 10 In 10 Tb 10 Bi 10

Internal Standard

$60/100 mL $120/500 mL

Method 1638 Tuning Standard

Part # 52122 Part # 53122

5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Be 10 Co 10 In 10 Pb 10 Mg 10

5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ni 10 Y 10 In 10 Tb 10 Pb 10 Part # 52147 Part # 53147 $50/100 mL $100/500 mL

Method 1640 Tuning Standard

$50/100 mL $200/500 mL

60

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

N-HEXANE EXTRACTABLE MATERIAL (HEM; OIL & GREASE) & SILICA GEL TREATED N-HEXANE EXTRACTABLE MATERIAL BY EXTRACTION & GRAVIMETRY

1664

As a party to the Montreal Protocol on Substances that Deplete the Ozone Layer and as required by law under the Clean Air Act Amendments of 1990 (CAAA), the United States is committed to controlling and eventually phasing out the use of chlorouorocarbons (CFCs). In support of these efforts, Method 1664 was developed by the United States Environmental Protection Agency Ofce of Science and Technology to replace previously used gravimetric procedures that employed Freon-113, a Class I CFC, as the extraction solvent for the determination of oil and grease and non-polar material. This method is for determination of n-hexane extractable material (HEM; oil and grease) and n-hexane extractable material that is not adsorbed by silica gel (SGT-HEM; non-polar material) in surface and saline waters and industrial and domestic aqueous wastes. Extractable materials that may be determined are relatively non-volatile hydrocarbons, vegetable oils, animal fats, waxes, soaps, greases, and related materials. The method is based on prior Environmental Protection Agency (EPA) methods for determination of oil and grease and total petroleum hydrocarbons

Oil & Grease 8000 (ug/mL) in Acetone (1) n-Hexadecane (2) Stearic acid Part # 91958 $65/100mL

EPA Method 1664

Also Available Oil & Grease 1000 ug/mL in n-Propanol/Glycerol. (1) Cooking Oil (2) Parafn
Part # 54135 $25/100 mL

EPA Method 413

Call Toll-Free 800-368-1131

61

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

600/4-79-020

MULTI-ELEMENT SOLUTION STANDARDS FOR GROUNDWATER AND WASTEWATER

GROUNDWATER AND WASTEWATER STANDARDS


These may be used either as standards or as a means of checking an individual analysts accuracy and precision. Refer to the US EPA Methods Manual, 600/4-79-020, Methods for Chemical Analysis of Water and Wastes for the appropriate Trace Metals I, II, III procedures.
15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 500 As 100 Be 100 Cd 25 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Mn 100 Hg 5 Ni 100 Se 25 V 250 Zn 100

Trace Metals 1

Part # 52093 Part # 53093

3 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 Ag 10 Tl 20

Trace Metals 2

$50/100 mL $100/500 mL

Part # 52092 Part # 53092

$130/100 mL $260/500 mL

Part # 52094 Part # 53094


P#52092- 600/4-79-020 Trace Metals 1 analyzed on HP 4500/ ICP-MS
[1] Spectrum No.1 5.0E4 [ 25.314 s ec]:52092.D# [Count] [Linear]

6 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ba 500 Ca 500 Mg 100 Mo 500 K 100 Na 500

Trace Metals 3

$75/100 mL $150/500 mL

2.5E4

m/z->

10

20

30

40

50

60

70

80

90

100

1.0E4

5000

m/z->

110

120

130

140

150

160

170

180

190

200

2000

Includes one each of Trace Metals 1, 2, and 3. Part # 52091 $240/100 mL Part # 53091 $480/500 mL

Trace Metals Set

1000

m/z->

210

220

230

240

250

260

62

www.AbsoluteStandards.com

Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

MULTI-ELEMENT SOLUTION STANDARDS FOR TOXIC METALS IN FISH

600/4-79-020

ALTERNATE WATER & WASTEWATER STANDARDS Alternate Metals 1

Alternate Metals Set


Includes one each of Alternate Metals 1 and 2.

Part # 52095 Part # 53095

$120/100 mL $240/500 mL

Part # 52097 Part # 53097

4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ca 500 Mg 100 K 100 Na 500

Alternate Metals 2

$90/100 mL $180/500 mL

Part # 52096 Part # 53096

11 Components Matrix 2% HNO3. Element Conc.(ug/mL) Al 20 Sb 5 Be 5 Co 10 Cu 10 Fe 20 Mn 10 Ni 10 Tl 5 V 20 Zn 10

$60/100 mL $120/500 mL

For use in methods for the sampling and analysis of priority pollutants in sediments and sh tissue. Refer to the US EPA Methods Manuals, 600/4-79-020 and 600/4-81-055 for the appropriate procedures. Hg

TRACE METALS IN FISH

Trace Metals in Fish


9 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 100 Cd 5 Cr 20 Cu 50 Pb 10 Hg 100 Ni 2 Se 10 Zn 1000

Part # 52098 Part # 53098

$90/100 mL $180/500 mL

Call Toll-Free 800-368-1131

63

ISO 9001:2000

Single Component Solutions: Pages 10-13

MISC.
Misc. Spike Solution #1
11 Components Matrix 5% HNO3. Element Conc.(ug/mL) Co Sr Al Ba Cd Cr Cu Se V Be As 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000

MISCELLANEOUS METAL STANDARDS

Misc. Spike Solution #2


10 Components Matrix 5% HNO3. Element Conc.(ug/mL) B Fe Pb Mn Mo Ni Tl Zn Ag Sb 1000 1000 1000 1000 1000 1000 1000 1000 200 1000

Includes one each of Solution #1 & #2. Part # 52259 $400/ 2x100 mL

Spike Solution Set

Part # 59045

$250/100 mL Element Fe K Ca Na Mg Ag Al As Ba Be Cd Co

24 Components Matrix 2% HNO3. Conc.(ug/mL) Element Conc.(ug/mL) 1000 1000 1000 1000 1000 10 10 10 10 10 10 10 Cr Cu Mn Mo Ni Pb Sb Se Tl V Zn Ti 10 10 10 10 10 10 10 10 10 10 10 10

Metals Mix

Part # 59046

$250/100 mL

Part # 59110 Part # 59153


[1] Spectrum No.1 500 [

$195/100 mL $500/500 mL

22.413 sec]:59153.D# [Count] [Linear]

250

m/z->
2000

10

20

30

40

50

60

70

80

90

100

1000

m/z->
5.0E4

110

120

130

140

150

160

170

180

190

200

2.5E4

m/z->

210

220

230

240

250

260

P#59153 - Metals Mix analyzed on HP 4500/ ICP-MS

64

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY

300.0

EPA Method 300.0 Anions


1000 ug/mL in Water. Single Components

Calibration Mixes
Chloride Fluoride Nitrate as N Nitrite as N Ortho-phosphate as P Sulfate Bromide Bromate Chlorite Chlorate

Part# 100 mL
54101 54102 54103 54104 54105 54106 54107 54108 54109 54110 $25 $25 $25 $25 $25 $25 $25 $25 $25 $25

Part#
54501 54502 54503 54504 54505 54506 54507 54508 54509 54510

500mL
$90 $90 $50 $50 $90 $90 $90 $90 $90 $90

Complete set of all 10 solutions Part # 54000 $150/100 mL Part # 54500 $750/500 mL

Eluent 100 x Concentrate 0.5 M in Water. Part # 54127 $65/100 mL Part # 54527 $100/500 mL

Sodium Carbonate

1000 ug/mL in Water. Part # 54139 $40/100 mL

Sulde

Eluent 100 x Concentrate 0.5 M in Water. Part # 54128 $25/100 mL Part # 54528 $100/500 mL

Sodium Bicarbonate

Part # 54155

1000 ug/mL in Water.

Chloride (Cl-) From CaCl2

$25/100 mL

EPA Method 300.0 Eluent 100 x Concentrate


Varied Molarity in Water. 100 mL Part # 54129 Part # 54529
(1) (2) Sodium carbonate Sodium bicarbonate 0.18 M 0.17 M

$25/100 mL $100/500 mL

Call Toll-Free 800-368-1131

65

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

300.0

DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY

A small volume of sample, typically 2 to 3 mL, is introduced into an ion chromatograph. The anions of interest are separated and measured, using a system comprised of a guard column, separator column, suppressor device, and conductivity detector. The main differences between Method A and B are the separator columns, guard columns and eluents. In order to use this method for solids, an extraction procedure must be performed. Stability of the solutions must be closely monitored. Store the materials at 4C.

EPA Method 300.0 Anions Mix A


1000 ug/mL in Water.
(1) (2) (3) (4) (5) (6) (7) Bromide Chloride Fluoride Nitrate as N Nitrite as N Ortho-phosphate as P Sulfate

EPA Method 300.0 Anions Mix A Alternate


1000 ug/mL in Water.
(1) (2) (3) (4) (5) (6) Bromide Chloride Fluoride Nitrate as N Ortho-phosphate as P Sulfate

Part # 52118 Part # 53118

$50/100 mL $200/500 mL

Part # 52320 Part # 53320

$50/100 mL $200/500 mL

EPA Method 300.0 Anions Mix B


1000 ug/mL in Water.
(1) (2) (3) Chlorite Chlorate Bromate

Part # 52119 Part # 53119

$25/100 mL $100/500 mL

(1) (2) (3) (4) (5)

100 ug/mL in Water.


-

Anions

Nitrate (NO3 )-as N Nitrite (NO2 )-as N Fluoride (F ) Orthophosphate (PO4 )-as P Nitrate & Nitrite as N
3-

Part # 52107 Part # 53107

$50/100 mL $150/500 mL

*Ohio Monthly QC Calibration Check


Varied ug/mL in Water.
Fluoride

Part # 59076 Part # 59176

$25/100 mL $60/500 mL

*Meets the Ohio concentration requirement of 0.5 -1.5 mg/L.

66

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY

300.0

EPA Method 300.0 Anions Mix


Varied ug/mL in Water.
Bromide Chloride Fluoride Nitrate as N Nitrite as N Ortho-phosphate as P Sulfate (1) (2) (3) (4) (5) (6) (7) 20 20 10 20 20 30 30

EPA Method 300.0 Anions


Varied ug/mL in Water.
Bromide Chloride Fluoride Nitrate as N Nitrite as N Ortho-phosphate as P Sulfate (1) (2) (3) (4) (5) (6) (7) 200 200 100 200 200 300 300

Part # 59010 Part # 59095

$50/100 mL $200/500 mL

Part # 59011 Part # 59096

$100/100 mL $200/500 mL

Method: E300D.M. Column: ASAHIPACK ODP50 (5m X 250 X 4.0mm). Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas. Retention Time (min) Fluoride 3.37 Chloride 4.78 Nitrite 5.65 Bromide 6.99 Nitrate 8.67 Phosphate 9.66 Sulfate 20.9

Call Toll-Free 800-368-1131

67

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

300.0

DETERMINATION OF INORGANIC ANIONS BY ION CHROMATOGRAPHY

INORGANIC DISINFECTION BY-PRODUCTS Inorganic Chlorinated Disinfection By-Products


1000 ug/mL in Water.
(1) (2) Chlorate (ClO3 ) Chlorite (ClO2 )
-

Inorganic Brominated Disinfection By-Products


1000 ug/mL in Water.
(1) Bromate (BrO3 ) (2) Bromide (Br )
-

Part # 52105 Part # 53105

$35/100 mL $95/500 mL

Part # 52106 Part # 53106

$35/100 mL $95/500 mL

EPA Method 300.0 Anions Mix B


1000 ug/mL in Water.
(1) (2) (3) Chlorite Chlorate Bromate

Part # 52119 Part # 53119

$25/100 mL $100/500 mL

*DAD1 A, Sig=360,20 Ref=266,10 (102604\52106A1.D - 102604\BLANK3.D)

mAU

16
14
12
10
8
6
4
2
0
2

Method: E300B.M. Column: ASAHIPACK ODP50 (125mm X 4.0mm ID X 5.0m df). Inj. Volume= 1.0L. Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas.

Peak No. 1 2

Analyte Bromate (BrO

3 -

PDA RT (min.) ) 3.79 6.03

Bromide (Br )

P#52106 - Brominated DBPs


4

10

12

14

16

18

min

68

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

DETERMINATION OF INORGANIC CATIONS BY ION CHROMATOGRAPHY

Cations

INORGANIC CATIONS ION CHROMATOGRAPHY


Single Components 1000 ug/mL - 100 mL Volume
54112 54113 57056 57020 57003 57012 57019 57011 57038 Ammonium, NH4+ Ammonium as N Barium, Ba2+ Calcium, Ca2+ Lithium, Li+ Magnesium, Mg2+ Postassium, K+ Sodium, Na+ Strontium, Sr2+ in Water. in Water. in 2% HNO3. in 2% HNO3. in 2% HNO3. in 2% HNO3. in 2% HNO3. in 2% HNO3. in 2% HNO3. $25 $25 $30 $30 $30 $30 $30 $30 $30

Complete set of all 9 solutions, use Part # 54001 $150

Additional Inorganic Cations Ion Chromatography


Single Components 1000 ug/mL - $25/ 100 mL
54154 54157 54158 54149 Calcium (Ca2+) Magnesium (Mg2+) Potassium (K+) Sodium (Na+) in Water. in Water. in Water. in Water.

4 Components in Water.
(1) (2) (3) (4) Calcium (Ca2+) Magnesium, (Mg2+) Potassium, (K+) Sodium (Na+) 1000 1000 1000 1000

Cations Mix #1

6 Components in Water.
(1) (2) (3) (4) (5) (6) Calcium (Ca2+) Magnesium, (Mg2+) Potassium, (K+) Sodium (Na+) Ammonium (NH4+) Lithium (Li+) 100 100 100 100 100 50

Cations Mix #2

Part # 59322

$50/100 mL

Part # 59203

$85/100 mL

Call Toll-Free 800-368-1131

69

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

314332.0

DETERMINATION OF PERCHLORATE BY ION CHROMATOGRAPHY

Method 314.0 was developed for the determination of perchlorate in drinking water by ion chromatography coupled with suppressed conductivity detection. Method 314.1 employs the use of inline column concentration/matrix elimination ion chromatography coupled with suppressed conductivity detection for the determination of perchlorate in drinking water.

Method 332.0 was developed for the determination of low level perchlorate in drinking water by ion chromatography coupled with suppressed conductivity and electrospray ionization mass spectroscopy. To improve the accuracy and performance of this method,18-Oxygen enriched perchlorate is utilized as an internal standard.

Method 314 Calibration


Part # 57001 $35/100 mL Part # 54164 $150/500 mL
Sodium Perchlorate (NaClO )
4

Sodium Perchlorate (NaClO4-)

1000 ug/mL in Water

Method 332.0 Calibration


Part # 57001 $35/100 mL Part # 54164 $150/500 mL
Sodium Perchlorate (NaClO4-) Sodium Perchlorate (NaClO4-)

1000 ug/mL in Water

100 ug/mL in Water

100 ug/mL in Water.

Part # 59344

$35/100 mL

Part # 59344

$35/100 mL

Laboratory Synthetic Sample Matrix Blank (pH 8.6)


1000 ug/mL in Water
(1) Bicarbonate (HCO ) (2) Chloride (Cl-) (3) Sulfate (SO42-)
3

Method 332.0 Calibration Internal Standard


Sodium Perchlorate(18O) -(NaCl 18O4-)

1 ug/mL in Water

Part # 54022

$30/ 1 mL

Part # 54205

$50/100 mL

Laboratory Synthetic Sample Matrix Blank (pH 10)


25 mg/mL in Water
(1) Carbonate (CO32-) (2) Chloride (Cl-) (3) Sulfate (SO42-)

Laboratory Synthetic Sample Matrix Blank (pH 10)


25 mg/mL in Water
(1) Carbonate (CO32-) (2) Chloride (Cl-) (3) Sulfate (SO42-)

Part # 59206

$60/100 mL

Part # 59206

$60/100 mL

70

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

DETERMINATION OF NITRATE-NITRITE NITROGEN BY AUTOMATED COLORIMETRY

353.2

This method covers the determination of nitrite singly, or nitrite and nitrate combined in drinking, ground, and surface waters, and domestic and industrial wastes. Stability of the solution must be closely monitored. Detection is by colorimetry. Typical stability is only 1 month. Store the materials at 4C.

EPA Method 353.2 Anions Mix


1000 ug/mL in Water.
(1) Nitrate as N (2) Nitrite as N

Part # 52120 Part # 53120

$25/100 mL $100/500 mL

EPA Method 353.2 Anions Mix


Varied ug/mL in Water.
(1) Nitrate as N (2) Nitrite as N 1000 500

Part # 54162 Part # 54521

$25/100 mL $100/500 mL

Method: E300D.M. Column: ASAHIPACK ODP50 (5m X 250 X 4.0mm). Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas. 1) Nitrite 2) Nitrate

Call Toll-Free 800-368-1131

71

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

Misc.

MISCELLANEOUS ORGANIC ACIDS / WET CHEMICAL CALIBRATION STANDARDS


Formic Acid (Formate)
Part # 54117 Part # 54517 1000 ug/mL in Water. $35/100 mL $150/500 mL

Acetic Acid (Acetate)


Part # 54116 Part # 54516 1000 ug/mL in Water. $35/100 mL $150/500 mL

Oxalic Acid (Oxalate)


Part # 54196 Part # 54596 1000 ug/mL in Water. $35/100 mL $150/500 mL

Organic Acids Mix


1000 ug/mL in Water.
(1) (2) (3) (4) Acetic acid Formic acid Methoxyacetic acid Oxalic acid

Part # 59294

$350/500 mL

Tetramethyl Ammonium Hydroxide


Part # 54118 Part # 54518 1000 ug/mL in Water. $35/100 mL $150/500 mL

Phenolics (Total) 4AAP


Part # 54136 1000 ug/mL in Water $30/100 mL

Total Organic Halides (TOX)


as 2,4,6-Trichlorophenol Cl @ 100 ug/mL

Part # 54194 in Water $25/ 20 mL Part # 54243 in Methanol $25/ 20 mL

Total Solids
Part # 54167
100 mg Neat

$25/ 100 mg

Non-Filterable Solids (TSS)


Part # 54134
100 mg Neat

Total Dissolved Solids (TDS)


Part # 54125
1000 ug/mL in Water.

$25/ 100 mg

$25/100 mL

72

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025


METHOD

WET CHEMICAL CALIBRATION MISCELLANEOUS EPA & STANDARD METHODS

Misc.

The following section contains several Wet Chemical Reference Materials that can be used as quality control checks or to generate calibration curves. A few popular EPA/SW-846 and Standard Methods are depicted for easy reference. Absolute Standards, Inc. has also generated a completely searchable web-based index of EPA analytes and methods. Please see our web site: www.AbsoluteStandards.com

TKN as N, Total Phosphorus as P Part # 54152 1000 ug/mL in Water $25/100 mL

Organic Nutrients

Total Organic Carbon (TOC) & Sulphate


Part # 54148 1000 ug/mL in Watzr $25/100 mL

Total Kjeldahl Nitrogen


from Glycine Part # 54132 1000 ug/mL in Water $25/100 mL

Total Organic Carbon (TOC) from KHP


Part # 59179 1000 ug/mL in Water $25/100 mL

Total Phosphorus as P
Part # 54133 1000 ug/mL in Water $25/100 mL

Total Organic Carbon (TOC) from Sucrose


1000 ug/mL in 1% HCl/Water. Part # 54126 $25/100 mL

NH4 as N, NO3 as N, PO4 as P Part # 54153 1000 ug/mL in Water $25/100 mL

Inorganic Nutrients

Calcium Hardness
Part # 54143 1000 ug/mL in 1% HCl $25/100 mL

100 ug/mL as DOC in Water 14.4 cm-1 as Absorbance at 254 nm in Water Part # 54166 $25/100 mL

UV 254 Absorbance/ Dissolved Organic Carbon (DOC) as KHP

Part # 54156 Part # 54597

1000 ug/mL in Water

Total Hardness

Alkalinity as CaCO3
Part # 54142 Part # 54242 1000 ug/mL in Water $25/100 mL $75/500 mL

$25/100 mL $90/500 mL

Call Toll-Free 800-368-1131

73

ISO 9001:2000
METHOD

Single Component Solutions: Pages 10-13

Misc.

WET CHEMICAL CALIBRATION MISCELLANEOUS EPA & STANDARD METHODS

Conductance @ 25 C
Part # 54131 1000 uMHOS/cm in Water $25/100 mL

Part # 54122

400 NTU in Water

Turbidity

$25/20 mL

pH of 6
Part # 54119 in Water $25/100 mL 1000 ug/mL in Water

MBAS

Part # 54160

$25/20 mL

Residual Free Chlorine


Part # 54124 1000 ug/mL in Water $25/100 mL
500 Color Units in 10% HCl/H2O Potassium Chloroplatinate Cobaltous Chloride hexahydrate

Color

1000 ug/mL in Water / tr. NaOH Part # 54159 Part # 54169 $25/100 mL $75/500 mL

Silica (SiO2)

Part # 54255

$75/100 mL

Simple Cyanide as Potassium Cyanide


Part # 59017 1000 ug/mL in Water/NaOH $25/100 mL

Total Cyanide as Potassium Ferricyanide


Part # 54150 1000 ug/mL in Water/NaOH $25/100 mL

Simple & Total Cyanide


Part # 54165 1000 ug/mL in Water/NaOH $25/100 mL

74

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

PRODUCT NUMBER CROSS REFERENCE INDEX

INDEX
Part# 52142 52143 52144 52145 52146 52147 52148 52149 52150 52151 52152 52153 52154 52155 52156 52157 52158 52159 52160 52161 52162 52163 52164 52166 52167 52168 52169 52170 52171 52172 52173 52174 52175 52176 52177 52178 52250 52251 52252 52253 52254 52255 52256 52302 Page# 58 58 60 60 60 60 37 19 19 19 19 19 20 23 23 24 24 24 25 25 26 28, 31 28, 31 29 30 32 32 33 33 34 34 34 34 35 35 35 15 15 57 14 14 14 14 54

Part# 52000 52001 52002 52003 52004 52005 52006 52007 52008 52009 52017 52018 52022 52023 52024 52025 52028 52031 52038 52039 52041 52042 52043 52044 52045 52046 52047 52050 52056 52057 52058 52059 52060 52061 52063 52064 52065 52066 52067 52068 52069 52070 52071 52072

Page# 16 16 16 16 16 16 36 36 36 36 20 20 21 21 22, 30 22 22 22 39 39 39 38 38 38 38 38 38 39 41 41 42 42 42 43 44 45 45 45 45 45 46 46 46 46

Part # 52073 52074 52075 52076 52079 52081 52084 52085 52086 52087 52088 52089 52090 52091 52092 52093 52094 52095 52096 52097 52098 52100 52101 52102 52105 52106 52107 52114 52115 52116 52117 52118 52119 52120 52122 52123 52133 52134 52135 52136 52137 52139 52140 52141

Page# 46 47 47 47 49 49 50 50 51 51 51 51 51 62 62 62 62 63 63 63 63 54 54 54 68 68 66 55 55 55 55 66 66, 68 70 52, 60 52 56 56 56 56 56 58 58 58

Call Toll-Free 800-368-1131

75

ISO 9001:2000

Single Component Solutions: Pages 10-13

INDEX
Part# 52309 52310 52311 52312 52313 52314 52315 52316 52319 52320 52331 52332 52333 52334 52335 52336 52337 53000 53001 53002 53003 53004 53005 53006 53007 53008 53009 53017 53018 53022 53023 53024 53025 53028 53031 53038 53039 53041 53042 53043 53044 53045 53046 53047 Page# 16 16 16, 57 16 16 16 16 16 52 66 40 52 53 53 41 41 41 16 16 16 16 16 16 36 36 36 36 20 20 21 21 22, 30 22 22 22 39 39 39 38 38 38 38 38 38

PRODUCT NUMBER CROSS REFERENCE INDEX

Part # 53050 53056 53057 53058 53059 53060 53061 53063 53064 53065 53066 53067 53068 53069 53070 53071 53072 53073 53074 53075 53076 53079 53081 53084 53085 53086 53087 53088 53089 53090 53091 53092 53093 53094 53095 53096 53097 53098 53100 53101 53105 53106 53107 53114

Page# 39 41 41 42 42 42 43 44 45 45 45 45 45 46 46 46 46 46 47 47 47 49 49 50 50 51 51 51 51 51 62 62 62 62 63 63 63 63 54 54 68 68 66 55

Part# 53115 53116 53117 53118 53119 53120 53122 53123 53133 53134 53135 53136 53137 53139 53140 53141 53142 53143 53144 53145 53146 53147 53148 53149 53150 53151 53152 53153 53154 53155 53156 53157 53158 53159 53160 53161 53162 53163 53164 53165 53166 53167 53168 53169

Page# 55 55 55 66 66, 68 70 52, 60 52 56 56 56 56 56 58 58 58 58 58 60 60 60 60 37 19 19 19 19 19 20 23 23 24 24 24 25 25 26 28, 31 28, 31 29 29 30 32 32

76

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

PRODUCT NUMBER CROSS REFERENCE INDEX

INDEX
Page# 72 73 70 69 69 69 69 69 69 69 16 58 16 38 46 45, 46 43 45 60 56 39 16 58 16 46 45, 46 43 45 60 56 39 67 67 74 49 64 64 66 67 67 64 64 66 73 Part# 59203 59206 59219 59249 59294 59322 59344 59370 59388 91958 Page# 69 70 40 40 72 69 70 29 53 61

Part# 53170 53171 53172 53173 53174 53175 53176 53177 53178 53309 53310 53311 53312 53313 53314 53315 53316 53319 53320 53331 53332 53333 53334 53335 53336 53337 54000 54001 54022 54112 54113 54116 54117 54118 54119 54122 54124 54125 54126 54127 54128 54129 54131 54132

Page# 33 33 34 34 34 34 35 35 35 16 16 16, 57 16 16 16 16 16 52 66 40 52 53 53 41 41 41 65 69 70 69 69 72 72 72 74 74 74 72 73 65 65 65 74 73

Part # 54133 54134 54135 54136 54139 54142 54143 54148 54149 54150 54152 54153 54154 54155 54156 54157 54158 54159 54160 54161 54162 54163 54164 54165 54166 54167 54169 54172 54175 54176 54194 54196 54205 54242 54243 54255 54500 54516 54517 54518 54521 54527 54528 54529

Page# 73 72 61 72 65 73 73 73 69 74 73 73 69 65 73 69 69 74 74 59 70 65 70 74 73 72 74 59 59 59 72 72 70 73 72 74 65 72 72 72 70 65 65 65

Part# 54596 54597 57001 57003 57011 57012 57019 57020 57038 57056 57146 57250 57280 57315 57351 57380 57642 57651 57847 57880 57911 58146 58250 58280 58351 58380 58642 58651 58847 58880 58911 59010 59011 59017 59030 59045 59046 59076 59095 59096 59110 59153 59176 59179

Call Toll-Free 800-368-1131

77

ISO 9001:2000

Single Component Solutions: Pages 10-13

NOTES

78

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Single Component Solutions: Pages 10-13

ISO/ IEC 17025

NOTES

Call Toll-Free 800-368-1131

79

ISO 9001:2000

Custom Standard Quotation Request Form Fax: (800) 410-2577, Technical Service Dept, Absolute Standards, Inc. Email: [email protected] Page From: Company Contact: Company: Company Address: Telephone: Email: Product Description: Solvent/ Matrix: Volume Size: 1 x 100 mL Qty: 1 x 500 mL Qty: Other: Qty: Fax: of Date:

Single Component Solutions: Pages 10-13 Absolute Standards, Inc.

Account#:

Date Required: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. Comments: 80 Component

Analysis requested? (additonal charge) CAS# (optional)

Yes

No

Concentration (ug/mL)

Absolute Standards, Inc. ISO 9001 Registered ISO 17025 Accredited P.O. Box 5585, Hamden, CT 06518 Phone (800) 368-1131

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