Absolute Standards Inorganic 2012
Absolute Standards Inorganic 2012
ABSOLUTE STANDARDS, INC. World Class Manufacturing & Internationally Recognized Quality
As Absolute Standards enters the latter half of our second decade of service, we continue to maintain our position as the industry leader. As the largest supplier of Analytical Reference Materials (ARM) and Performance Evaluation samples, we ship our products to all fty states, several territories, and over thirty countries. Focusing on the needs of the global testing body, we strive to provide the highest quality and broadest range of analytical standards to an industry that relies on accuracy and precision. Moreover, Absolute Standards is the only company in the industry that has exceeded the international requirements of both ISO/IEC 17025 and ISO 9001:2000 for the manufacture and analytical verication of our entire product line. As an analytical standards manufacturer, we recognize our role as an important link in the analytical testing community. Your analyses require the use of accurate, traceable, and defensible reference materials. It is this requirement that drives Absolute Standards to manufacture products that lead the industry in quality and value. Our philosophy at Absolute Standards is one of compliance. High expectations backed by quality accreditations help us achieve our goals. Discover how Absolutes commitment can help satisfy your compliance needs.
ISO 9001:2000
800-368-1131 800-410-2577
...Email... [email protected]
Order on-line at www.AbsoluteStandards.com using LabCartTM Secure, Simple,Searchable, & Speedy We accept major credit cards: MasterCard / VISA / AMEX .
Orders that are placed before 5pm (EST) are shipped the same day by FedEx & UPS. Prices are F.O.B. Hamden CT. Terms are Net 30 Days. Terms and conditions of all sales contracts will be governed by the laws of The State of Connecticut. Prices are subject to change without notice. Warranty by Absolute Standards includes that our products are as described when
shipped. No warranty as to tness for any particular application is expressed or implied. Errant shipments and/or quality claims must be made within 30 days of receipt. No returns can be made without a Return Authorization Number and instructions of forwarding.
Liability by Absolute Standards is limited solely to the replacement of the product or refund
of the purchase price. These products are intended for research use only. Owing to their hazardous nature, they should be handled only by qualied, trained personnel familiar with their use.
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ISO 9001:2000
Custom Standard Quotation Request Form Fax: (800) 410-2577, Technical Service Dept, Absolute Standards, Inc. Email: [email protected] Page From: Company Contact: Company: Company Address: Telephone: Email: Product Description: Solvent/ Matrix: Volume Size: 1 x 100 mL Qty: 1 x 500 mL Qty: Other: Qty: Fax: of Date:
Account#:
Date Required: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. Comments: 4 Component
Yes
No
Concentration (ug/mL)
Absolute Standards, Inc. ISO 9001 Registered ISO 17025 Accredited P.O. Box 5585, Hamden, CT 06518 Phone (800) 368-1131
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AbsoluteGrade - Specications
Absolute Standards is the only company in the industry that has exceeded the international requirements of both ISO/IEC 17025 and ISO 9001:2000 for the manufacture and analytical verication of our entire product line. Equipped with state of the art instrumentation, our quality products are backed by the analytical power of an ICP-MS and four LCs. Included in this catalog are reference materials for calibration of the following instruments: AA, ICP, ICP-MS, IC, IE & several wet chemical methods. Method references are indicated wherever possible. In addition, the CLP section has been updated to include the latest revisions. Our capabilities are diverse and expanding. As we strive for continuous improvement, weve added the following services to better accomodate your needs: bulk sealing, on-line ordering with LabCartTM , and a fully searchable Products database available at www.AbsoluteStandards.com. We know that your requirements can be unique and varied therefore, if you would like a custom blend, please contact us with your specications. Let our experienced chemists give you a feasibility assessment of your design and work with you to enhance the stability and robustness of your custom formulation.
AbsoluteGrade - Specications
Suitable for ICP AES, DCP AES, ICP MS, High-Accuracy AA Flame or Graphite Furnace work. Manufactured using the Highest Purity starting materials available (typically 99.999%). Digestion in acid-cleaned PTFE labware to prevent possible contamination. Class A volumetric glassware used for pipetting and diluting where applicable. Signed Certicate of Analysis included with every standard. Traceable to NIST and other internationally recognized third party standards. Formulation Uncertainty provided for every analyte Density measurement allows wt/wt use. Verication of impurities in both starting materials and nal solutions. Immediate shipment from stock. Total U.S. Right To-Know, and O.S.H.A. compliance. Cost-effective packaging.
ISO 9001:2000
TABLE OF CONTENTS
TITLE PAGES
Certicate of Analysis.........................................................................................................................................7 AbsoluteGrade Specications / Certied Weight Report........................................................................... 8-9 Single Component Solutions AA/ICP Spectroscopy....................................................................................10-13 Elemental Group Kits...................................................................................................................................14-15 Matrix Modiers and Blanks (AA/ICP)............................................................................................................16 Graphite Furnace (GFAA) Standards................................................................................................................17 Contract Laboratory Program (CLP) Standards...........................................................................................18-35 ILM 05.2 ICP-AES................................................................................................................................19-22 ILM 05.2 ICP-MS..................................................................................................................................23-27 ILM 05.3 ICP-AES (Water)...................................................................................................................28-30 ILM 05.3 ICP-AES (Soil)......................................................................................................................31-32 ILM 05.3 ICP-MS (Water)....................................................................................................................33-34 ILM 06.X ICP-MS (Soil)............................................................................................................................35 TCLP Multi-Element Calibration Standards................................................................................................36-37 EPA 6010 A/B Standards.............................................................................................................................38-39 EPA 6020/ 6020A Standards.............................................................................................................................40 EPA 200.7 Standards....................................................................................................................................41-51 Calibration Standards...........................................................................................................................41 Plasma, Tuning, Lab Check Solutions.................................................................................................42 Spectral Interference............................................................................................................................43 Lab Fortifying Solution (LFS).............................................................................................................44 Spiking Standards...........................................................................................................................45-46 Drinking Water Standards....................................................................................................................47 Instrument Wavelength Standards.......................................................................................................49 Quality Control Standards...............................................................................................................50-51 EPA 200.8 Standards............................................................................................................... ....................52-56 Tuning & Internal Standards................................................................................................................52 Calibration Standards...........................................................................................................................53 Verication Standards..........................................................................................................................54 Interference / Memory Check Solutions..............................................................................................55 Multi-Element Solutions......................................................................................................................56 EPA 200.9 Standards ........................................................................................................................................57 EPA Method 1620.............................................................................................................................................58 EPA Method 1636.............................................................................................................................................59 EPA Method 1638/1640....................................................................................................................................60 EPA Method 1664.............................................................................................................................................61 Groundwater and Wastewater Standards (600/4-79-020)............................................................................62-63 Trace Metals In Fish (600/4-79-020)................................................................................................................63 Miscellaneous Mixes.........................................................................................................................................64 EPA 300.0 Standards (Anions by Ion Chromatography).............................................................................65-68 Single Components / Eluents...............................................................................................................65 Multi-Analyte Solutions.................................................................................................................66-67 Inorganic Disinfection By-Products....................................................................................................68
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TABLE OF CONTENTS
Cations ..............................................................................................................................................................69 EPA Method 314.0/ 314.1/ 332.0 (Perchlorate)................................................................................................70 EPA Method 353.2 (Nitrate & Nitrite)..............................................................................................................71 Organic Acids....................................................................................................................................................72 Miscellaneous Wet Methods........................................................................................................................72-74 Part# Index....................................................................................................................................................75-77 Custom Quotation Order Form......................................................................................................................4, 78
Certificate of Analysis
Conformance: The Certificate of Analysis and the "Certified Weight Report" fulfill the requirements in the current versions of: ISO Guides (9001, 24, 31, 34, 17025) & NIST-NVLAP Handbook 150-19. Health & Safety: See the attached MSDS & Certified Weight Report before use. Intended Use: This Analytical Reference Material (ARM) is intended primarily for use in the characterization of unknowns & the establishment of response factors by qualified personnel. Typical instrumental organic assays include: GC & LC, and inorganic assays include: ICP & AA. The product is for laboratory use only. Certified Values: In production, gravimetric/volumetric readings are certified to be within +/- 0.5% of the stated value and are valid between 18C & 30C. The measured uncertainty can be found on the Certified Weight Report. All product weighings are performed on an analytical balance that is calibrated to NIST Traceable standard weights & certified by the manufacturer. The volumetric glassware used is Class A type & conforms to ASTM E-288 unless otherwise stated. The solvents & compounds used are of the highest practical purity & typically meet or exceed ACS Reagent Grade & ACS Standards Grade specifications. Homogeneity & Stability: No heterogeneity was observed in the preparation, packaging & storage of this standard. Expiration dates can be found on the Certified Weight Report. Purity & Identity: Purity determinations are performed using at least one analytical technique. Identity assays are typically performed using two dissimilar methods.
Organic solutions & neats are typically formulated from materials whose purity & identity have been characterized by GC-MSD & LC-PDA techniques with comparison to a NIST Traceable library of mass spectra when available. Additional characterization techniques may include but are not limited to: refractive index measurements of liquids, melting point measurements of solids, & GC-FID, ECD, PID, ELCD, NPD, LC-PDA measurements for purity. Inorganic solutions & neats are typically formulated from materials whose purity & identity have been characterized by ICPMS with comparison to a NIST Standard Reference Material when available. Additional characterization techniques may include but are not limited to: titratiometry, and densitometry, AA or ICP. Final solutions are subjected to instrumental analysis to support the gravimetric values when appropriate. The data for the quality assurance testing is published with the Certified Weight Report. Typical instrumental organic assays include GC and LC. Inorganic assays include ICPMS, titratiometry, and densitometry.
Storage: Sealed ampules and other containers should be stored in the dark at temperatures above the freezing point of the solution and not more than 30C. Certification by Absolute Standards, Inc. is typically valid for 5 years from the date of manufacture (Lot Number). Certified values are not applicable to opened ampules or to materials stored in re-sealable containers. See the Certified Weight Report for specific values.
Usage: Ampules & bottles should be brought to room temperature (18 to 30C) before opening. Sonication may be required for high concentration solutions. After opening, care should be exercised to avoid concentration changes owing to evaporation of the solvent or essential components. We recommend that a suitable re-sealable container be available before opening an ampule to decant the standard for short-term storage.
Legal Notice: Warranty of products are as described when shipped. No warranty as to fitness for any particular application is expressed or implied. Errant shipments and/or quality claims must be made within 10 days of receipt. Liability is limited solely to the replacement of the product or refund of purchase price. Certifying Officer: Stephen J. Arpie, M.S. Director
Absolute Standards, Inc. 44 Rossotto Drive Hamden, CT 06514 Voice: 1-203-281-2917 Fax: 1-203-281-2922 email: [email protected] www: http://www.absolutestandards.com
Document Identification: Certificate of Analysis Rev 5, Date Issued: 01/01/2006
ISO 9001:2000
AbsoluteGrade SPECIFICATIONS
Lot #
Solvent(s):
53084
L135898
Nitric Acid
Lot Number:
070102
N37G05
Hydrofluoric acid
Description:
QC Standard 1 2.0% 20.0 0.25 (mL) Formulated By: Lawrence Barry 070102 070105 100 5E-05
Balance Uncertainty Flask Uncertainty
0.025%
Reviewed By:
Expanded
Pedro L. Rentas
070102
999.88
Dilution
0.025
Initial
MSDS Information
(Solvent Safety Info. On Attached pg.)
CAS#
Uncertainty
Initial
Final
Uncertainty
Compound 1. Beryllium acetate (Be) 2. Calcium carbonate Ca) 3. Cadmium nitrate (Cd) 4. Chromium nitrate nonahydrate(Cr) 5. Cobalt nitrate (Co) 6. Copper nitrate (Cu) 7. Iron (III) Nitrate Nonahydrate 8. Lead nitrate (Pb) 9. Magnesium nitrate (Mg) 10. Manganese nitrate (Mn) 11. Ammonium molybdate (Mo) 12. Nickel nitrate (Ni) 13. Selenium oxide (Se) 14. Thallium nitrate (Tl) 15. Ammonium hexafluorotitanate (Ti) 16. Ammonium Metavanadate (V) 17. Zinc nitrate (Zn) 18. Antimony Oxide (Sb) 19. Arsenic (As)
Number
Number
Factor
Volume 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00
Pipette 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006 0.006
Conc.(ug/mL)
Conc (g/mL)
(+/-) (g/mL) 0.002334 0.002334 0.002002 0.002002 0.002002 0.002001 0.002003 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002 0.002002
LD50
57104 58120 58148 58124 57127 58129 58126 57182 58112 57125 58142 58128 58134 57181 57122 58123 58130 58151 58133
051100 012202 091400 040901 020901 062001 061002 032900 110601 060800 082901 102600 011900 120700 042400 110701 041101 071001 062000
0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100 0.0100
10000.04 10000.82 10000.19 10000.34 10000.54 10003.59 10001.80 9999.67 10000.20 10000.37 10000.17 10000.03 10001.32 10000.34 9999.90 10000.32 10000.21 10000.04 10000.48
100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0 100.0
19049-40-2 00471-34-1 10022-68-1 07789-02-8 10026-22-9 03251-23-8 07782-61-8 10099-74-8 10377-60-3 15710-66-4 13106-76-8 10377-66-9 07746-08-4 10102-45-1 16962-40-6 07803-55-6 10196-18-6 07440-36-0 07440-38-2
0.002 ug/m3 7 mg/m3 0.2 mg/m3 0.5 mg/m3 5 mg/m3 N/A 7 mg/m3 0.05 mg/m3 7 mg/m3 5 mg/m3 N/A 5 mg/m3 0.2 mg/m3 5 mg/m3 N/A 1.0 mg/m3 1 mg/m3 5.0 mg/m3 0.2 mg/m3
N/A N/A N/A orl-rat 3250mg/kg orl-rat 694 mg/kg orl-rat 940 mg/kg N/A 500 mg/kg N/A N/A orl-rat 333 mg/kg N/A N/A N/A N/A orl-rat 630 mg/kg orl-rat 1190mg/kg N/A N/A
P#53084 L#070102
Page 1 of 3
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AbsoluteGrade SPECIFICATIONS
A Certified Weight Report is generated for each lot illustrating the formulation procedure, traceability, & actual analysis.
44 Rossotto Drive Hamden, CT 06514 (800) 368-1131
AbsoluteGrade Solution
Certified Concentration (g/mL)
The certified value is the concentration calculated from gravimetric and volumetric measurements unless otherwise specified.
Traceability
NIST SRM 928 Lead Nitrate NIST Weights NIST SRM 136e Potassium Dichromate NIST SRM 999 Potassium Chloride
* * *
Cd Ca Ce Cs Cr Co Cu
* *
<0.02 <0.02
* * *
Dy Er Eu Gd Ga Ge Au
Hf Ho In Ir Fe La Pb
* *
<0.02
Li Lu Mg Mn Hg Mo Nd
<0.02 <0.02
* * *
<0.2 <0.02
Ni Nb Os Pd P Pt K
*
<0.02 <0.02 <0.02 <0.02 <0.02 <0.2
Pr Re Rh Rb Ru Sm Sc
Se Si Ag Na Sr S Ta
*
<0.02 <0.02 <0.2 <0.02 <0.02 <0.02
Tb Te Tl Th Tm Sn Ti
<0.02 <0.02
W U V Yb Y Zn Zr
<0.02 <0.02
* *
C) Physical Characterization:
1.018 Analyzed Density of Solution (g/mL): 22.6 Temperature (C): Homogeneity: No heterogeneity was observed in the preparation of this standard.
Certified by:
We use purified acids, 18 meg ohm double deionized water, calibrated Class A glassware and the highest purity raw materials available, (typically 99.999%). We meticulously clean our bottles by acid leaching and then triple rinsing with ASTM Type I water prior to use. Our standards are made gravimetrically using balances that are calibrated with weights traceable to NIST. (NIST Test #: 732/245790). We certify that all our standards are within the stated uncertainties unless otherwise stated, assuming that the bottle is kept tightly capped and stored under normal laboratory conditions.
Reference: Taylor, B.N. and Kuyatt, C.E., "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Result," NIST Technical Note 1297, U.S. government Printing Office, Washington DC, (1994).
P# 53084 L#070102, Report Page 2 of 2 Printed on 10/05/2002, 11:26AM
ISO 9001:2000
Matrix
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Bi(NO3)3/HNO3 H3BO3/H20 Cd(NO3)2/HNO3 CaCO3/HNO3 C(Citric Acid)/HNO3 Ce(NO3)3/HNO3 CsNO3/HNO3 Cr(NO3)3/HNO3 (NH4)2Cr2O7/H2O Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Dy2O3/HNO3 Er2O3/HNO3 Eu2O3/HNO3 Gd2O3/HNO3 Ga2O3/HNO3 (NH4)2GeF6/tr, HF NH4AuCl4/HCl Hf2O3/HCl Ho3O3/HNO3 In2O3/HNO3 IrCl3/HCl Fe(NO3)3/HNO3 (NH4)Fe2+(SO4)2/H2SO4 [Fe2+]+[Fe3+]/H2SO4 LaCl/HNO3 Pb(NO3)2/HNO3 LiNO3/HNO3 Li6+NO3/HNO3 Lu2O3/HNO3 Mg(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 MeHgCl/HNO3 Hg(NO3)2+MeHgCl/HNO3
Part#
57013 57051 57033 57056 57004 57083 57005 57048 57020 57006 57058 57055 57024 54161 57027 57029 57066 57068 57063 57064 57031 57032 57079 57072 57067 57049 57077 57026 54141 54140 57057 57082 57003 59021 57071 57012 57025 57080 54170 54004
$/100mL
30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 75 30 75 30 30 30 75 30 30 30 30 30 30 200 30 30 30 30 30 30
Part#
58013 58051 58033 58056 58004 58083 58005 58048 58020 58006 58058 58055 58024 54172 58027 58029 58066 58068 58063 58064 58031 58032 58079 58072 58067 58049 58077 58026 54174 54173 58057 58082 58003 59097 58071 58012 58025 58080 54171 54168
$/500mL
70 70 70 70 70 70 70 70 70 70 70 70 70 50 70 70 75 75 75 75 150 70 150 75 75 70 150 70 50 50 70 70 70 1000 75 70 70 70 50 50
10
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Matrix
(NH4)MoO4/H2O Nd2O3/HNO3 Ni(NO3)2/HNO3 (NH4)NbF6/tr.HF Pd/HNO3 (NH4)H2PO4/HNO3 [Pt(NH3)4](NO3)2/HCL KNO3/HNO3 Pr6O11/HNO3 Re/HNO3 RhCl3/HCl RbNO3/HNO3 RuCl3/HNO3 Sm2O3/HNO3 Sc(NO3)3/HNO3 SeO2/HNO3 SiO2/NaOH (NH4)2SiF6/HNO3 AgNO3/HNO3 NaNO3/HNO3 Sr(NO3)2/HNO3 (NH4)2SO4/H2O NH4TaF6/tr.HF TeO2/HCl Tb4O7/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 Tm2O3/HNO3 (NH4)SnF6/HNO3/HCL (NH4)2TiF6/HNO3/tr.HF (NH4)2WO4/H2O U3O8/HNO3 NH4VO3/HNO3 Yb2O3/HNO3 Y2O3/HNO3 Zn(NO3)2/HNO3 ZrO2/HNO3
Part#
57042 57060 57028 57041 57046 57015 57078 57019 57059 57075 57045 57037 57044 57062 57021 57034 54159 57014 57047 57011 57038 57016 57073 57052 57065 57081 57090 57069 57050 57022 57074 57092 57023 57070 57039 57030 57040
$/100mL
30 30 30 30 125 30 75 30 30 125 100 30 75 30 75 30 30 30 30 30 30 30 30 50 30 30 30 30 30 30 30 30 30 30 30 30 30
Part#
58042 58060 58028 58041 58046 58015 58078 58019 58059 58075 58045 58037 58044 58062 58021 58034 54169 58014 58047 58011 58038 58016 58073 58073 58065 58081 58090 58069 58050 58022 58074 58092 58023 58070 58039 58030 58040
$/500mL
70 75 70 70 200 70 150 70 75 150 400 75 150 75 150 70 75 70 70 70 70 70 75 150 75 70 70 75 70 70 70 70 70 75 70 70 70
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or Call our Technical Department
11
ISO 9001:2000
Matrix
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Bi(NO3)3/HNO3 H3BO3/H20 Cd(NO3)2/HNO3 CaCO3/HNO3 C(Citric Acid)/HNO3 Ce(NO3)3/HNO3 CsNO3/HNO3 Cr(NO3)3/HNO3 (NH4)2Cr2O7/H2O Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Dy2O3/HNO3 Er2O3/HNO3 Eu2O3/HNO3 Gd2O3/HNO3 Ga2O3/HNO3 (NH4)2GeF6/tr, HF NH4AuCl4/HCl Hf2O3/HCl Ho3O3/HNO3 In2O3/HNO3 IrCl3/HCl Fe(NO3)3/HNO3 (NH4)Fe2+(SO4)2/H2SO4 [Fe2+]+[Fe3+]/H2SO4 LaCl/HNO3 Pb(NO3)2/HNO3 LiNO3/HNO3 Li6+NO3/HNO3 Lu2O3/HNO3 Mg(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 MeHgCl/HNO3 Hg(NO3)2+MeHgCl/HNO3
Part#
57113 57151 57133 57156 57104 57183 57105 57148 57120 57106 NA NA 57124 54175 57127 57129 NA NA NA NA NA NA 57179 NA NA NA NA 57126 NA NA NA 57182 57103 NA NA 57112 57125 57180 NA 54178
$/100mL
85 85 85 85 85 85 85 85 85 85 NA NA 85 85 85 85 NA NA NA NA NA NA 300 NA NA NA NA 85 NA NA NA 85 85 NA NA 85 85 85 NA 100
Part#
58113 58151 58133 58156 58104 58183 58105 58148 58120 58106 NA NA 58124 54176 58127 58129 NA NA NA NA NA NA 58179 NA NA NA NA 58126 NA NA NA 58182 58103 NA NA 58112 58125 58180 NA NA
$/500mL
160 160 160 160 160 160 160 160 160 160 NA NA 160 160 160 160 NA NA NA NA NA NA 600 NA NA NA NA 160 NA NA NA 160 160 NA NA 160 160 160 NA NA
12
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Matrix
(NH4)MoO4/H2O Nd2O3/HNO3 Ni(NO3)2/HNO3 (NH4)NbF6/tr.HF Pd/HNO3 (NH4)H2PO4/HNO3 [Pt(NH3)4](NO3)2/HCL KNO3/HNO3 Pr6O11/HNO3 Re/HNO3 RhCl3/HCl RbNO3/HNO3 RuCl3/HNO3 Sm2O3/HNO3 Sc(NO3)3/HNO3 SeO2/HNO3 SiO2/NaOH (NH4)2SiF6/HNO3 AgNO3/HNO3 NaNO3/HNO3 Sr(NO3)2/HNO3 (NH4)2SO4/H2O NH4TaF6/tr.HF TeO2/HCl Tb4O7/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 Tm2O3/HNO3 (NH4)SnF6/HNO3/HCL (NH4)2TiF6/HNO3/tr.HF (NH4)2WO4/H2O U3O8/HNO3 NH4VO3/HNO3 Yb2O3/HNO3 Y2O3/HNO3 Zn(NO3)2/HNO3 ZrO2/HNO3
Part#
57142 NA 57128 NA 57146 57115 57178 57119 NA NA NA NA NA NA NA 57134 NA 57114 57147 57111 57138 57116 NA NA NA 57181 NA NA 57150 57122 57174 NA 57123 NA 57139 57130 57140
$/100mL
85 NA 85 NA 500 85 300 85 NA NA NA NA NA NA NA 85 NA 85 85 85 85 85 NA NA NA 85 NA NA 85 85 85 NA 85 NA 85 85 85
Part#
58142 NA 58128 NA 58146 58115 58178 58119 NA NA NA NA NA NA NA 58134 NA 58114 58147 58111 58138 58116 NA NA NA 58181 NA NA 58150 58122 58174 NA 58123 NA 58139 58130 58140
$/500mL
160 NA 160 NA 900 160 600 160 NA NA NA NA NA NA NA 160 NA 160 160 160 160 160 NA NA NA 160 NA NA 160 160 160 NA 160 NA 160 160 160
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or Call our Technical Department
13
ISO 9001:2000
KITS
Part # 52253
$80/ 5 x 100 mL
Part # 52255
$80/ 5 x 100 mL
Part # 52256
$150/ 9 x 100 mL
Part # 52254
$240/ 14 x 100 mL
14
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KITS
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Ba(NO3)2/HNO3 Be4O(C2H3O2)6/HNO3 Cd(NO3)2/HNO3 Cr(NO3)3/HNO3 Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Pb(NO3)2/HNO3 Mn(NO3)2/HNO3 Hg(NO3)2/HNO3 (NH4)MoO4/H2O Ni(NO3)2/HNO3 SeO2/HNO3 AgNO3/HNO3 TlNO3/HNO3 Th(NO3)4/HNO3 U3O8/HNO3 NH4VO3/HNO3 Zn(NO3)2/HNO3
Part # 52251
$380/ 21 x 100 mL
Part # 52250
$600/ 32 x 100 mL
ISO 9001:2000
Blank solutions are prepared with High-Purity Acids and ASTM Type I Water. Blanks can be used to dilute your multi-element standards to run directly to establish your baseline. An Aqua Regia Blank can be prepared by mixing one part Nitric Acid Blank with three parts HCl Acid Blank. ASTM Type I H2O Part # 52000 Part # 53000 $25/ 100mL $40/ 500mL
Water Blank
Matrix Modiers suppress background interferences and help enhance sensitivity by changing the behavior of the element or the matrix in solution with respect to temperature. These modiers help prevent the loss of certain elements during pyrolysis by converting the target to a less volatile form. This allows a more optimum graphite furnace program to be utilized.
$250/100mL $450/500mL
$500/100mL $900/500mL
$125/100mL $200/500mL
$250/100mL $350/500mL
$250/100mL $350/500mL
$350/100mL $500/500mL
$250/100mL $350/500mL
$250/100mL $350/500mL
$250/100mL $350/500mL
16
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GFAA STANDARDS
GRAPHITE FURNACE AA CALIBRATION AND SPIKING GFAA Calibration GFAA Initial Calibration
Verication (2nd Source) 6 Components Matrix 5% HNO3 Element Conc.(ug/mL) Sb 50 As 25 Cd 5 Pb 25 Se 50 Tl 25
$85/100 mL $190/500 mL
$85/100 mL $190/500 mL
$85/100 mL $190/500 mL
$30/100 mL $60/500 mL
17
ISO 9001:2000
CLP
The following section illustrates the solutions appropriate for the inorganic analyitcal methods dervied from the USEPA Contract Laboratory Program. These methods are specifc for ICP-AES and ICP-MS technologies and are suitable for the detection of metals in various matrices. These methods are designed to not only isolate, but to both qualitatively and quantitatively detect specic target metals in water and soil/sediment. ACRONYM Cal CCV DESCRIPTION Calibration Standards Continuing Calibration Verication: To ensure calibration accuracy during each analysis, run a CCV standard for every wavelength/ mass used for each analyte. Contract Required Quantation Limit Standard prepared at the CRQL level Initial and Continuing Calibration Blank Interference Check Sample: To verify inter-element and background correction factors, the Contractor shall analyze and report the results for the ICS, for all elements on the Target Analyte List (TAL), and for all interferents (target and non-target), at the beginning and end of each analysis run, but not before the ICV. In addition, the Contractor shall analyze and report the results for the ICS at a frequency of not less than once per 20 analytical samples per analysis run. Initial Calibration/Verication: Immediately after each of system has been calibrated, the accuracy of the initial calibration shall be veried and documented for every analyte by the analysis of the ICV solution(s) at each wavelength/ mass used.
ICV
18
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ILM 05.2
CLP
ILM 05.2 INSTRUMENT CALIBRATION STANDARDS FOR INDUCTIVELY COUPLED PLASMA - ATOMIC EMISSION SPECTROSCOPY (ICP-AES)
Calibration Std. I
Calibration Std. II
$65/100 mL $130/500 mL
$65/100 mL $130/500 mL
Calibration Std. IV
6 Components 100 ug/mL in 5% HNO3 Al Ca Cr K Na Ni
$40/100 mL $80/500 mL
$65/100 mL $130/500 mL
Calibration Std. V
$65/100 mL $130/500 mL
19
ISO 9001:2000
METHOD
ILM 05.2
CLP
ILM 05.2 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES ICP-AES Initial Verication Std. 1
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ba 100 Be 40 Cd 50 Co 100 Cu 100 Fe 100 Pb 100 Mn 100 Ni 100 Ag 20 Tl 100 Zn 100
$95/100 mL $190/500 mL
$95/100 mL $190/500 mL
Element Ca Mg K Na Al Ba Fe Co V Ni Cu
Conc.(ug/mL) 2500 2500 2500 2500 200 200 100 50 50 40 25 Part # 52154 Part # 53154
Conc.(ug/mL) 20 15 10 10 10 10 10 10 10 10 60
20
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ILM 05.2
CLP
15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 120 As 120 Be 10 Cd 10 Cr 20 Co 100 Cu 50 Pb 120 Mn 30 Ni 80 Se 120 Ag 20 Tl 120 V 100 Zn 40
CRI Mix 1
$125/100 mL $250/500 mL
CRI Mix 2
$125/100 mL $250/500 mL
21
ISO 9001:2000
METHOD
ILM 05.2
CLP
Interferents A
$95/100 mL $190/500 mL
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 100 Ba 50 Be 50 Cd 100 Co 50 Cr 50 Cu 50 Mn 50 Ni 100 Pb 100 V 50 Zn 100
Interferents B
$95/100 mL $190/500 mL
18 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 50 As 200 Ba 200 Be 5 Cd 5 Cr 20 Co 50 Cu 25 Fe 100 Pb 50 Mn 50 Ni 50 Se 200 Ag 5 Tl 200 V 50 Zn 50
$280/100 mL $560/500 mL
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 400 Ba 400 Be 10 Cd 10 Cr 40 Co 100 Cu 50 Pb 100 Mn 100 Ni 100 Se 400 Ag 10 Tl 400 V 100 Zn 100
$160/100 mL $320/500 mL
22
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ILM 05.2
CLP
ILM 05.2 CALIBRATION, TUNING, & INTERNAL STANDARDS FOR INDUCTIVELY COUPLED PLASMA - MASS SPECTROSCOPY (ICP-MS)
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) Be 100 Mg 100 Co 100 In 100 Pb 100
Tuning Standard
$45/100 mL $90/500 mL
Element Al Sb As Ba Be Bi Cd Cr Co Cu In
23 Components Matrix 5% HNO3. Conc.(ug/mL) Element 100 Pb 100 Mg 100 Mn 100 Ni 100 Sc 100 Se 100 Ag 100 Tb 100 Tl 100 V 100 Y Zn Part # 52155 Part # 53155 $95/100 mL $190/500 mL
Conc.(ug/mL) 100 100 100 100 100 100 100 100 100 100 100 100
Element Bismuth Indium Holmium Lithium Lutetium Rhodium Scandium Terbium Yttrium Bi In Ho Li Lu Rh Sc Tb Y
Matrix Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 LiNO3/HNO3 Lu2O3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3
Conc. (ug/mL) 1000 1000 1000 1000 1000 1000 1000 1000 1000
INTERNAL STANDARDS
Part# 57083 57049 57067 57003 57071 57045 57021 57065 57039
$/100mL 25 25 25 25 30 125 75 25 25
Part# 58083 58049 58067 58003 58071 58045 58021 58065 58039
23
ISO 9001:2000
METHOD
ILM 05.2
CLP
ILM 05.2 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-MS ICP-MS ICV Standard ICP-MS CCV Standard
$95/100 mL $190/500 mL
$95/100 mL $190/500 mL
250
m/z- >
1000
10
20
30
40
50
60
70
80
90
1 00
500
m/z- >
2.0 E4
11 0
120
13 0
140
150
160
170
180
190
2 00
1.0 E4
m/z- >
21 0
220
23 0
240
250
260
24
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ILM 05.2
CLP
ILM 05.2 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & INTERFERENTS SOLUTIONS FOR ICP-MS ICP-MS - CRI Standard
23 Components Matrix 5% HNO3. Element Al Sb As Ba Be Bi Cd Cr Co Cu In Conc.(ug/mL) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Part # 52159 Part # 53159 Element Pb Mg Mn Ni Sc Se Ag Tb Tl V Y Zn $95/100 mL $190/500 mL Conc.(ug/mL) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1
ICP-MS / Interferents B
20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 20 Ba 20 Bi 20 Cd 20 Cr 20 Co 20 Cu 20 In 20 Pb 20 Mn 20 Ni 20 Sc 20 Se 20 Ag 20 Tb 20 Tl 20 V 20 Y 20 Zn 20
ICP-MS / Interferents A
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Ca 100 Fe 100 Mg 100 K 100 Na 100 P 100 SO4 100 C 200 Cl 1000 Mo 2 Ti 2
$95/100 mL $190/500 mL
$110/100 mL $220/500 mL
25
ISO 9001:2000
METHOD
ILM 05.2
CLP
$110/100 mL $220/500 mL
Place your order 24 hours a day, 7 days a week using LabCartTM, Absolutes on-line ordering system. Go to www.AbsoluteStandards.com & Click on On-Line Ordering for speedy, simple, and secure purchasing!
26
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ILM 05.2
CLP
Conc. (ug/mL)
10 20 100 200 1000 10000 100 1000 100 1000 10000
Part#
57880 52009 57280 57380 57080 57180 54006 54170 54005 54004 54178
$/100mL
25 25 25 25 25 75 25 25 25 25 100
Part#
58880 53009 58280 58380 58080 58180 NA 54171 NA 54168 NA
$/500mL
50 50 50 50 65 150 NA 50 NA 50 NA
Conc. (ug/mL)
1000 1000 1000
Part#
59017 54150 54165
$/100mL
25 25 25
Part#
54012 NA NA
$/500mL
90 NA NA
Simple Cyanide is formulated with Potassium Cyanide (KCN), no distillation is required. Total Cyanide is formulated with Potassium Ferricyanide (III), distillation is required before analysis can be performed. Free & Complexed Cyanide is formulated with both materials.
27
ISO 9001:2000
METHOD
ILM 05.3
CLP
ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX
ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES/ WATER MATRIX
22 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 60 As 10 Ba 200 Be 5 Cd 5 Ca 5000 Cr 10 Co 50 Cu 25 Fe 100 Pb 10 Mg 5000 Mn 15 Ni 40 K 5000 Se 35 Ag 10 Na 5000 Tl 25 V 50 Zn 60 Part # 52163 Part # 53163
20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Sb 30 As 5 Ba 100 Ca 2500 Cr 5 Co 25 Cu 12.5 Fe 50 Pb 5 Mn 7.5 Mg 2500 Ni 20 K 2500 Se 17.5 Ag 5 Na 2500 Tl 12.5 V 25 Zn 30 Part # 52164 Part # 53164 $150/100 mL $300/500 mL
$150/100 mL $300/500 mL
28
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ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX
ILM 05.3
CLP
ILM 05.3 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & SPIKE SOLUTIONS FOR ICP-AES/ WATER MATRIX ICP-AES CRI Mix Water Matrix ICP-AES Spike Sample Water Matrix
18 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 10 As 4 Ba 200 Be 5 Cd 5 Cr 20 Co 50 Cu 25 Fe 100 Pb 2 Mn 50 Ni 50 Se 5 Ag 5 Tl 5 V 50 Zn 50
$125/100 mL $250/500 mL
$125/100 mL $250/500 mL
10
m/z- >
20
10
20
30
40
50
60
70
80
90
100
10
m/z- >
500
110
120
130
140
150
160
170
180
190
200
250
m/z- >
210
220
230
240
250
260
29
ISO 9001:2000
METHOD
ILM 05.3
CLP
ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX
ILM 05.3 INTERFERENTS SOLUTION FOR ICP-AES/ WATER MATRIX ICP-AES Interferents A Water Matrix ICP-AES Interferents B Water Matrix
$95/100 mL $190/500 mL
Combine Interferents Mix A & B for ICSAB. Dilute Interferants A Mix into Interferants B Mix in a 1:10 ratio.
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 200 As 100 Ba 500 Be 500 Cd 1000 Co 500 Cr 500 Cu 500 Mn 500 Ni 1000 Pb 50 Sb 600 Se 50 Tl 100 V 500 Zn 1000 Part # 52167 Part # 53167 $125/100 mL $250/500 mL
Mg
Al
Ca
Fe
1.0E4
m/z->
2.0E5
10
20
30
40
50
60
70
80
90
100
1.0E5
m/z->
2.0E7
110
120
130
140
150
160
170
180
190
200
1.0E7
m/z->
210
220
230
240
250
260
30
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ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX
ILM 05.3
CLP
ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTINUING CALIBRATION VERIFICATION (CCV) SOLUTIONS FOR ICP-AES/ SOIL MATRIX ICP-AES ICV Water/Soil Matrix ICP-AES CCV Water/Soil Matrix
22 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Sb 60 As 10 Ba 200 Be 5 Cd 5 Ca 5000 Cr 10 Co 50 Cu 25 Fe 100 Pb 10 Mg 5000 Mn 15 Ni 40 K 5000 Se 35 Ag 10 Na 5000 Tl 25 V 50 Zn 60 Part # 52163 Part # 53163 $150/100 mL $300/500 mL
20 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Sb 30 As 5 Ba 100 Ca 2500 Cr 5 Co 25 Cu 12.5 Fe 50 Pb 5 Mn 7.5 Mg 2500 Ni 20 K 2500 Se 17.5 Ag 5 Na 2500 Tl 12.5 V 25 Zn 30 Part # 52164 Part # 53164 $150/100 mL $300/500 mL
31
ISO 9001:2000
METHOD
ILM 05.3
CLP
ICP-AES SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX
ILM 05.3 CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS) & SPIKE SOLUTIONS FOR ICP-AES/ SOIL MATRIX ICP-AES CRI Soil Matrix ICP-AES Spike Soil Matrix
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 600 As 100 Ba 500 Be 50 Cd 50 See page 30 Cr 100 for Co 500 Cu 250 Interferents Mixes. Pb 100 Mn 150 Ni 400 Se 350 Ag 100 Tl 250 V 500 Zn 600 $125/100 mL $250/500 mL
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 200 As 80 Ba 4000 Be 100 Cd 100 Cr 400 Co 1000 Cu 500 Pb 40 Mn 1000 Ni 1000 Se 100 Ag 100 Tl 100 V 1000 Zn 1000
$125/100 mL $250/500 mL
5000
m/z->
10
20
30
40
50
60
70
80
90
100
2000
1000
m/z->
110
120
130
140
150
160
170
180
190
200
5.0E5
2.5E5
m/z->
210
220
230
240
250
260
32
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ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX
ILM 05.3
CLP
ILM 05.3 INITIAL CALIBRATION VERIFICATION (ICV) SOLUTIONS & CONTRACT REQUIRED QUANTITATION LIMITS (CRQLS/CRI) SOLUTIONS FOR ICP-MS/ WATER MATRIX ICP-MS ICV Water Matrix ICP-MS / CRQL CHECK STANDARD-CRI Water Matrix
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 10 Ba 100 Be 10 Cd 10 Cr 20 Co 10 Cu 20 Pb 10 Mn 10 Ni 10 Se 50 Ag 10 Tl 10 V 10 Zn 20
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 20 As 10 Ba 100 Be 10 Cd 10 Cr 20 Co 10 Cu 20 Pb 10 Mn 10 Ni 10 Se 50 Ag 10 Tl 10 V 10 Zn 20 Part # 52170 Part # 53170 $125/100 mL $250/500 mL
$125/100 mL $250/500 mL
The CRI and ICV mixes are identical in element and concentration, but are prepared from separate source raw materials as specied by the method.
33
ISO 9001:2000
METHOD
ILM 05.3
CLP
ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM WATER MATRIX
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 10.0 As 5.0 Ba 50 Be 5.0 Cd 5.0 Cr 10.0 Co 5.0 Cu 10.0 Pb 5.0 Mn 5.0 Ni 5.0 Se 25.0 Ag 5.0 Tl 5.0 V 5.0 Zn 10.0 Part # 52172 Part # 53172 $125/100 mL $250/500 mL
$125/100 mL $250/500 mL
Dilute and Combine Interferants Mix A & B for Mix ICSAB. Interferants A Mix is 10X the method specication & Interferants B Mix is 1000X.
$125/100 mL $250/500 mL
$125/100 mL $250/500 mL
34
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ICP-MS SOLUTION STANDARDS FOR THE SUPERFUND CONTRACT LABORATORY PROGRAM SOIL MATRIX
ILM 06.X
CLP
ILM 06.X has the same target analyte list as ILM 05.3, however specications for ICP-MS in soil are given.
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 50 Ba 500 Be 50 Cd 50 Cr 100 Co 50 Cu 100 Pb 50 Mn 50 Ni 50 Se 250 Ag 50 Tl 50 V 50 Zn 100 Part # 52176 Part # 53176 $125/100 mL $250/500 mL
The CRI and ICV mixes are identical in element & concentration, but are prepared from separate source raw materials as
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 50 As 25 Ba 250 Be 25 Cd 25 Cr 50 Co 25 Cu 50 Pb 25 Mn 25 Ni 25 Se 125 Ag 25 Tl 25 V 25 Zn 50 Part # 52178 Part # 53178 $125/100 mL $250/500 mL
16 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 50 Ba 500 Be 50 Cd 50 Cr 100 Co 50 Cu 100 Pb 50 Mn 50 Ni 50 Se 250 Ag 50 Tl 50 V 50 Zn 100 Part # 52177 Part # 53177 $125/100 mL $250/500 mL
35
ISO 9001:2000
TCLP (1311)
Method
7 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 25 Ba 500 Cd 5 Cr 25 Pb 25 Se 5 Ag 25 Hg* 20 *Hg is a separate solution.
(TCLP) Standard
$50/100 mL $100/500 mL
$95/100 mL $190/500 mL
$30/100 mL $50/500 mL
$65/100 mL $130/500 mL
36
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TCLP (1312)
Part#
58048 58148 58082 58182
Method
Element
Cadmium Cadmium Lead Lead Cd Cd Pb Pb
Matrix
Cd(NO3)2/HNO3 Cd(NO3)2/HNO3 Pb(NO3)2/HNO3 Pb(NO3)2/HNO3
Part#
57048 57148 57082 57182
$/500mL
65 150 65 150
37
ISO 9001:2000
REV-1,7/92 REV-2,12/96
6010A
6010B
6 Components Matrix 2% HNO3. Element Conc.(ug/mL) Be 50 Cd 150 Pb 500 Mn 100 Se 200 Zn 150
Calibration Std. 1
$80/100 mL $160/500 mL
8 Components Matrix 2% HNO3. Element Conc.(ug/mL) Al 200 Ca 1000 Cr 20 Li 100 Ni 20 K 400 Na 200 Sr 10 Part # 52046 Part # 53046
Calibration Std. 4
5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ba 100 Co 100 Cu 100 Fe 1000 V 100
Calibration Std. 2
$90/100 mL $180/500 mL
$80/100 mL $160/500 mL
Calibration Std. 5
$80/100 mL $160/500 mL
Calibration Std. 3
$60/100 mL $120/500 mL
Calibration Std. 6
$30/100 mL $60/500 mL
38
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6010A
6010B
Interference Standards are used to set or conrm that the appropriate background correction intervals have been set for sequential ICP spectrometers & that the proper inter-element correction factors are set for simultaneous ICP spectrometer systems.
Matrix 2% HNO3. tr Tartaric acid Element Conc.(ug/mL) Sb 1000 Part # 57051 $30/100 mL Part # 58051 $70/500 mL
Interference Std. 2
17 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 100 Ba 30 Be 10 Cd 30 Cr 30 Co 30 Cu 30 Pb 100 Mn 20 Hg 5 Ni 30 K 3000 Se 50 Ag 30 Tl 100 V 30 Zn 30 Part # 52039 $230/100 mL Part # 53039 $460/500 mL
Interference Std. 1
5 Components Matrix 5% HNO3 Element Conc.(ug/mL) Li 300 Mo 300 P 1000 Sr 200 Ti 1000 Part # 52050 $80/100 mL Part # 53050 $160/500 mL
Interference Std. 3
4 Components Matrix 5% HNO3 Element Conc.(ug/mL) Al 400 Ca 2000 Fe 2000 Mg 1000 Part # 52041 $50/100 mL Part # 53041 $100/500 mL
Interference Std. 4
Matrix 2% HNO3. Element Conc.(ug/mL) Na 5000 Part # 57911 $50/100 mL Part # 58911 $100/500 mL
Interference Std. 5
39
ISO 9001:2000
6020/ 6020A
Method 6020/ 6020A is applicable to the determination of metals in low concentrations (sub-ppb) in water and watse extracts using ICP-MS.
MIX A
MIX B
ICP-MS InternalStandards
Element
Bismuth Indium Holmium Lithium Rhodium Scandium Terbium Yttrium Bi In Ho Li6+ Rh Sc Tb Y
Matrix
Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 Li6+NO3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3
Part#
57083 57049 57067 59021 57045 57021 57065 57039
(ug/mL)
1000 1000 1000 1000 1000 1000 1000 1000
$/100mL
25 25 25 200 120 75 25 25
Part#
58083 58049 58067 59097 58045 58021 58065 58039
$/500mL
65 65 75 1000 400 150 75 65
40
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200.7
Rev 5.0
METHOD
EPA Method 200.7 covers the Determination of Metals and Trace Elements in Water and Wastes by ICP Atomic Emission Spectroscopy.
$75/100 mL $150/500 mL
$80/100 mL $160/500 mL
4 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ce 200 Co 200 V 200 P 1000 Part # 52337 $75/100 mL Part # 53337 $150/500 mL
6 Components Matrix 5% HNO3. Element Conc.(ug/mL) Be 100 Fe 1000 Pb 1000 Mg 1000 Ni 200 Tl 500 Part # 52057 $110/100 mL Part # 53057 $220/500 mL
41
ISO 9001:2000
Various Revisions
200.7
METHOD
The Plasma Solution is used to determine the optimum height above the load coil for viewing the plasma in EPA Method 200.7, Section 7.6.
The Tuning Solution is used to determine the optimum height above the load coil for viewing the plasma in EPA Method 200.7, Section 7.7.
Plasma Solution
$50/100 mL $100/500 mL
Tuning Solution
$40/100 mL $80/500 mL
The Laboratory Performance Check Solution Set is used to evaluate the performance of the instrument system in EPA Method 200.7, Section 7.8.
Matrix 5% HNO Dilution : 1 to 100 P#52306 LPC-1 Element Conc. (ug/mL). Ag 50 Al 200 As 200 B 200 Ba 200 Be 200 Ca 200 Cd 200 Co 200 Cr 200 P#52307 LPC-2 P#52308 LPC-3 Element Conc. Element Conc. (ug/mL). (ug/mL). Cu 200 P 1000 Fe 200 Pb 200 Hg 200 Sb 200 K 1000 Se 1000 Li 200 Si 200 Mg 200 Sn* 200 Mn 200 Sr 200 Mo 200 Tl 200 Na 200 V 200 Ni 200 Zn 200 * (supplied as a separate solution) Part # 52060 $400/100 mL Part # 53060 $800/500 mL
42
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Various Revisions
200.7
METHOD
The Spectral Interference Check Solutions consist of higher-level, concentrated, selected method analytes and are used to evaluate the laboratorys procedure for correcting known inter-element spectral interferences.
SIC 1 is used to evaluate the Mo interelement spectral correction factors on the analytes Al, Sb, Se, Sn, and V.
Matrix H2O. Dilution : 1 to 10 Element Mo Part # 57642 Part # 58642 Conc.(ug/mL) 500 $30/100 mL $60/500 mL
SIC 1
SIC 2 is used to evaluate the Co, Cr, Mn, V, Cu, inter-element spectral correction factors on the analytes Pb, Sb, Mo, As, V, and Zn.
5 Components Matrix 2% HNO3. Dilution : 1 to 10 Element Conc. Corresponding (ug/mL) Interference Co Cr Mn V Cu 100 200 200 200 400 Pb Sb Mo As, Be Zn $50/100 mL $100/500 mL
SIC 2
Part # 52061 Part # 53061 SIC 3 is used to evaluate the Ni, Al, Fe, inter-element spectral correction factors on the analytes Sb, Zn, As, Ag, Mn, V, Cr.
3 Components Matrix 2% HNO3. Dilution : 1 to 10 Element Conc. Corresponding (ug/mL) Interference Ni Al Fe 200 300 1500 Sb, Zn As Ag, Cr, Mn, V $40/100 mL $80/500 mL
SIC 3
43
ISO 9001:2000
Various Revisions
200.7
METHOD
P# 52303 LFS-1 Element Conc.(ug/mL) Ag Al As B Ba Be Cd Co Cr 25 250 250 250 250 50 100 100 250
P# 52305 LFS-3 Element Conc.(ug/mL) Sb Se Si Sn* Sr Tl V Zn 250 250 250 100 250 250 100 250
1.0E5
m/z->
5.0E4
10
20
30
40
50
60
70
80
90
100
2.5E4
m/z->
5000
110
120
130
140
150
160
170
180
190
200
2500
m/z->
210
220
230
240
250
260
44
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Various Revisions
200.7
METHOD
Spiking Standard 4
$80/100 mL $160/500 mL
Spiking Standard 2
4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ca 1000 Mg 2000 K 10,000 Na 3000
Spiking Standard 5
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 2000 Cd 50 Pb 500 Se 2000 Tl 2000
$90/100 mL $180/500 mL
$100/100 mL $200/500 mL
Spiking Standard 3
12 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 2000 Ba 2000 Be 50 Cr 200 Co 500 Cu 250 Fe 1000 Mn 500 Ni 500 Ag 50 V 500 Zn 500
$180/100 mL $360/500 mL
Mercury Standard
$30/100 mL $60/500 mL
45
ISO 9001:2000
Various Revisions
200.7
METHOD
Spiking Standard 1
4 Components Matrix H2O Element Conc.(ug/mL) B 400 Mo 200 Si 2000 P 400
$90/100 mL $180/500 mL
Spiking Standard 2
4 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ca 10,000 Mg 10,000 K 10,000 Na 10,000
$120/100 mL $240/500 mL
15 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 200 Ba 200 Be 100 Cr 100 Co 200 Cu 200 Fe 400 Li 200 Mn 100 Ni 200 Ag 200 Sr 400 Sn 200 V 200 Zn 200 Part # 52072 $180/100 mL Part # 53072 $360/500 mL
Spiking Standard 3
Spiking Standard 4
Matrix 2% HNO3. Element Conc.(ug/mL) Sb 200
$30/100 mL $60/500 mL
Matrix 2% HNO3. Element Conc.(ug/mL) Hg 200 Part # 57380 Part # 58380 $30/100 mL $60/500 mL
Mercury Standard
Spiking Standard 5
5 Components Matrix 5% HNO3. Element Conc.(ug/mL) As 200 Cd 100 Pb 200 Se 400 Tl 400
$100/100 mL $200/500 mL
46
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Various Revisions
200.7
METHOD
50
m /z ->
10
2 0
30
40
50
60
70
80
90
10 0
200
100
m /z ->
110
12 0
130
140
150
16 0
170
180
190
20 0
1000
500
$80/100 mL $160/500 mL
m /z ->
210
22 0
230
240
250
26 0
$65/100 mL $130/500 mL
47
ISO 9001:2000
Our quality products are inspected by analytical chemists who have experience using a wide variety of instrumentation. Absolute maintains diverse technologies to ensure your calibration standards are accurate, reliable, & traceable. We use a ICP-MS, HPLC, and many wet methods.
ICP - MS
HPLC - PDA
48
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200.7 6010
For calibration and verication of wavelength accuracy and stability in sequential and simultaneous ICP Spectrometers. Also for use in US EPA SW-846, Method 6010 section 5.6 and Method 200.7 section 7.6.1.
1.0E4
m/z->
2000
10
20
30
40
50
60
70
80
90
100
1000
m/z->
2.0E5
110
120
130
140
150
160
170
180
190
200
1.0E5
$110/100 mL $220/500 mL
m/z->
210
220
230
240
250
260
$90/100 mL $180/500 mL
Part # 59030
$75/100 mL
49
ISO 9001:2000
METHODS
200.7 6010
Quality control standards are used to check standard curves, perform inter-element correction and other spectral interference checks. Also used in US EPA Method 200.7 and 600/482-055 Technical Additions to Methods for Chemical Analysis of Water and Wastes. Available both individually and as a complete set.
19 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 100 Be 100 Ca 100 Cd 100 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Mg 100 Mn 100 Mo 100 Ni 100 Se 100 Tl 100 Ti 100 V 100 Zn 100
QC Standard 1
$175/100 mL $350/500 mL
21 Components Matrix 5% HNO3. Element Conc.(ug/mL) Sb 100 As 100 Be 100 Ca 100 Cd 100 Cr 100 Co 100 Cu 100 Fe 100 Pb 100 Li 100 Mg 100 Mn 100 Mo 100 Ni 100 Se 100 Sr 100 Tl 100 Ti 100 V 100 Zn 100
QC Standard 2
$190/100 mL $380/500 mL
1000
m/z->
2000
10
20
30
40
50
60
70
80
90
100
1000
m/z->
1.0E5
110
120
130
140
150
160
170
180
190
200
5.0E4
m/z->
210
220
230
240
250
260
50
www.AbsoluteStandards.com
200.7 6010
QC Standard 3
7 Components Matrix 5% HNO3. Element Conc.(ug/mL) Al 100 Ba 100 B 100 K 1000 Si 500 Ag 50 Na 100
QC Standard 5
$80/100 mL $160/500 mL
$170/100 mL $340/500 mL
$310/100 mL $620/500 mL
7 Components Matrix 2% HNO3. Element Conc.(ug/mL) Al 100 Ba 100 B 100 K 1000 Si 50 Ag 100 Na 100
QC Standard 4
$80/100 mL $160/500 mL
1000
m/z->
2.0E4
10
20
30
40
50
60
70
80
90
100
$310/100 mL $620/500 mL
1.0E4
m/z->
2.0E6
110
120
130
140
150
160
170
180
190
200
1.0E6
m/z->
210
220
230
240
250
260
51
ISO 9001:2000
METHOD
200.8
$50/100 mL $200/500 mL
These internal standard stock solutions are used for: addition to blanks; calibration standards; as samples for internal standardization; and for use in US EPA SW-846 Method 200.8. Dilute 10 mL to 100 mL before using.
Element
Bismuth Indium Holmium Lithium Rhodium Scandium Terbium Yttrium Bi In Ho Li6+ Rh Sc Tb Y
Matrix
Bi(NO3)3/HNO3 In2O3/HNO3 Ho3O3/HNO3 Li6+NO3/HNO3 RhCl3/HCl Sc(NO3)3/HNO3 Tb4O7/HNO3 Y2O3/HNO3
Part#
57283 57249 57067 59036 57245 57221 57265 57239
$/100mL
25 25 25 100 100 25 25 25
Part#
58283 58249 58067 59037 58245 58221 58265 58239
$/500mL
50 50 75 300 300 50 50 50
$50/100 mL $200/500 mL
52
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$65/100 mL $200/500 mL
200.8
Part # 59388
$30/100 mL
$40/100 mL $80/500 mL
$150/100 mL $300/500 mL
2.5E6
m/z->
5.0E6
10
20
30
40
50
60
70
80
90
100
2.5E6
m/z->
2.0E6
110
120
130
140
150
160
170
180
190
200
1.0E6
m/z->
210
220
230
240
250
260
53
ISO 9001:2000
METHOD
200.8
$60/100 mL $120/500 mL
$180/100 mL $380/500 mL
Includes one each of ICP-MS Verication 1 and 2. Part # 52102 Part # 52302 $220/100 mL $440/500 mL
100
m/z- >
1000
10
20
30
40
50
60
70
80
90
100
500
m/z- >
1.0E 4
110
120
130
140
150
160
170
180
190
200
5000
m/z- >
210
220
230
240
250
260
54
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200.8
14 Components Matrix in 2%-HNO3/ tr. HF Element Conc.(ug/mL) Al 1000 Mg 1000 Na 1000 C 2000 Cl 7200 S 1000 Ti 20 Sb 20 Be 20 Cr 20 Mn 20 Ni 20 V 20 Zn 20 $100/100 mL $450/500 mL
14 Components Matrix in 2%-HNO3 Element Conc.(ug/mL) Ca 1000 Fe 1000 K 1000 P 1000 Mo 20 As 20 Ba 20 Cd 20 Co 20 Cu 20 Pb 20 Se 20 Ag 20 Tl 20 Part # 52117 $100/100 mL Part # 53117 $450/500 mL
55
ISO 9001:2000
ICP-MS
Multi-Element Solution 1
29 Components Matrix 5% HNO3. Element Conc.(ug/mL) Ag 10 Al 10 As 10 Ba 10 Be 10 Bi 10 Ca 10 Cd 10 Co 10 Cr 10 Cs 10 Cu 10 Fe 10 Ga 10 In 10 K 10 Li 10 Mg 10 Mn 10 Na 10 Ni 10 Pb 10 Rb 10 Se 10 Sr 10 Tl 10 U 10 V 10 Zn 10
Multi-Element Solution 3
10 Components Matrix 10% HCL / 1% HNO3. Element Conc.(ug/mL) Au 10 Hf 10 Ir 10 Pd 10 Pt 10 Rh 10 Ru 10 Sb 10 Sn 10 Te 10
$250/100 mL $500/500 mL
$200/100 mL $400/500 mL
Multi-Element Solution 4
12 Components Matrix H2O tr. HF Element Conc.(ug/mL) B 10 Ge 10 Mo 10 Nb 10 P 10 Re 10 S 10 Si 10 Ta 10 Ti 10 W 10 Zr 10
Multi-Element Solution 5
Matrix 2% HNO3. Element Conc.(ug/mL) Hg 10
$180/100 mL $360/500 mL
$30/100 mL $60/500 mL
Includes one each of Multi-Element 1, 2, 3, 4, & 5. Part # 52137 Part # 53137 5X100 mL 5X500 mL $650 $1300
$150/100 mL $300/500 mL
56
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200.9
METHOD
Aluminum Antimony Arsenic Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Thallium Tin
Al Sb As Be Cd Cr Co Cu Fe Pb Mn Ni Se Ag Tl Sn
Al(NO3)3/HNO3 Sb2O3/HNO3 tr.Tartaric acid As2O3/HNO3 Be4O(C2H3O2)6/HNO3 Cd(NO3)2/HNO3 Cr(NO3)3/HNO3 Co(NO3)2/HNO3 Cu(NO3)2/HNO3 Fe(NO3)3/HNO3 Pb(NO3)2/HNO3 Mn(NO3)2/HNO3 Ni(NO3)2/HNO3 SeO2/HNO3 AgNO3/HNO3 TlNO3/HNO3 (NH4)SnF6/HNO3/HCl $280/ 16 x 100 mL
Part # 52252
PT Study Schedule: January 15- March 1 April 15- May 30 *July 15- August 29 (DMR-QA) October 15- November 29 Offering our complete line of water & soil PTs EVERY study!
57
ISO 9001:2000
METHOD
1620
METALS BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROSCOPY & ATOMIC ABSORPTION SPECTROSCOPY
The method is a consolidation of US EPA Methods 200.7 (ICP for trace elements), 204.2 (Sb), 206.2 (As), 239.2 (Pb), 270.2 (Se), 279.2 (Tl), 245.5 (Hg), 245.1 (Hg), and 245.2(Hg). The method is used for analysis of trace elements by ICP atomic emission spectroscopy and GFAA spectroscopy, for analysis of mercury by CVAA spectroscopy,and as a semi-quantitative ICP screen for specied elements.
$60/100 mL $120/500 mL
$60/100 mL $120/500 mL
$50/100 mL $100/500 mL
$60/100 mL $120/500 mL
$60/100 mL $120/500 mL
58
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1636
This method is for the determination of dissolved hexavalent chromium (as CrO) in ambient waters at EPA water quality criteria (WQC) levels using ion chromatography (IC). This method was developed by integrating the analytical procedures in EPA Method 218.6 with the quality control (QC) and sample handling procedures necessary to avoid contamination and ensure the validity of analytical results during sampling and analysis for metals at EPA WQC levels.
59
ISO 9001:2000
METHODS
1638 1640
DETERMINATION OF TRACE ELEMENTS IN AMBIENT WATERS BYINDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY
Method 1638 & 1640 are for the determination of dissolved elements in ambient waters at EPA water quality criteria (WQC) levels using inductively coupled plasma-mass spectrometry (ICP-MS). In addition, Method 1640 employs on-line chelation preconcentration. These methods may also be used for determination of total recoverable element concentrations in these waters.
$30/100 mL $60/500 mL
$60/100 mL $120/500 mL
Internal Standard
$60/100 mL $120/500 mL
5 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ni 10 Y 10 In 10 Tb 10 Pb 10 Part # 52147 Part # 53147 $50/100 mL $100/500 mL
$50/100 mL $200/500 mL
60
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N-HEXANE EXTRACTABLE MATERIAL (HEM; OIL & GREASE) & SILICA GEL TREATED N-HEXANE EXTRACTABLE MATERIAL BY EXTRACTION & GRAVIMETRY
1664
As a party to the Montreal Protocol on Substances that Deplete the Ozone Layer and as required by law under the Clean Air Act Amendments of 1990 (CAAA), the United States is committed to controlling and eventually phasing out the use of chlorouorocarbons (CFCs). In support of these efforts, Method 1664 was developed by the United States Environmental Protection Agency Ofce of Science and Technology to replace previously used gravimetric procedures that employed Freon-113, a Class I CFC, as the extraction solvent for the determination of oil and grease and non-polar material. This method is for determination of n-hexane extractable material (HEM; oil and grease) and n-hexane extractable material that is not adsorbed by silica gel (SGT-HEM; non-polar material) in surface and saline waters and industrial and domestic aqueous wastes. Extractable materials that may be determined are relatively non-volatile hydrocarbons, vegetable oils, animal fats, waxes, soaps, greases, and related materials. The method is based on prior Environmental Protection Agency (EPA) methods for determination of oil and grease and total petroleum hydrocarbons
Oil & Grease 8000 (ug/mL) in Acetone (1) n-Hexadecane (2) Stearic acid Part # 91958 $65/100mL
Also Available Oil & Grease 1000 ug/mL in n-Propanol/Glycerol. (1) Cooking Oil (2) Parafn
Part # 54135 $25/100 mL
61
ISO 9001:2000
METHOD
600/4-79-020
Trace Metals 1
Trace Metals 2
$50/100 mL $100/500 mL
$130/100 mL $260/500 mL
6 Components Matrix 2% HNO3. Element Conc.(ug/mL) Ba 500 Ca 500 Mg 100 Mo 500 K 100 Na 500
Trace Metals 3
$75/100 mL $150/500 mL
2.5E4
m/z->
10
20
30
40
50
60
70
80
90
100
1.0E4
5000
m/z->
110
120
130
140
150
160
170
180
190
200
2000
Includes one each of Trace Metals 1, 2, and 3. Part # 52091 $240/100 mL Part # 53091 $480/500 mL
1000
m/z->
210
220
230
240
250
260
62
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600/4-79-020
$120/100 mL $240/500 mL
Alternate Metals 2
$90/100 mL $180/500 mL
$60/100 mL $120/500 mL
For use in methods for the sampling and analysis of priority pollutants in sediments and sh tissue. Refer to the US EPA Methods Manuals, 600/4-79-020 and 600/4-81-055 for the appropriate procedures. Hg
$90/100 mL $180/500 mL
63
ISO 9001:2000
MISC.
Misc. Spike Solution #1
11 Components Matrix 5% HNO3. Element Conc.(ug/mL) Co Sr Al Ba Cd Cr Cu Se V Be As 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000
Includes one each of Solution #1 & #2. Part # 52259 $400/ 2x100 mL
Part # 59045
$250/100 mL Element Fe K Ca Na Mg Ag Al As Ba Be Cd Co
24 Components Matrix 2% HNO3. Conc.(ug/mL) Element Conc.(ug/mL) 1000 1000 1000 1000 1000 10 10 10 10 10 10 10 Cr Cu Mn Mo Ni Pb Sb Se Tl V Zn Ti 10 10 10 10 10 10 10 10 10 10 10 10
Metals Mix
Part # 59046
$250/100 mL
$195/100 mL $500/500 mL
250
m/z->
2000
10
20
30
40
50
60
70
80
90
100
1000
m/z->
5.0E4
110
120
130
140
150
160
170
180
190
200
2.5E4
m/z->
210
220
230
240
250
260
64
www.AbsoluteStandards.com
300.0
Calibration Mixes
Chloride Fluoride Nitrate as N Nitrite as N Ortho-phosphate as P Sulfate Bromide Bromate Chlorite Chlorate
Part# 100 mL
54101 54102 54103 54104 54105 54106 54107 54108 54109 54110 $25 $25 $25 $25 $25 $25 $25 $25 $25 $25
Part#
54501 54502 54503 54504 54505 54506 54507 54508 54509 54510
500mL
$90 $90 $50 $50 $90 $90 $90 $90 $90 $90
Complete set of all 10 solutions Part # 54000 $150/100 mL Part # 54500 $750/500 mL
Eluent 100 x Concentrate 0.5 M in Water. Part # 54127 $65/100 mL Part # 54527 $100/500 mL
Sodium Carbonate
Sulde
Eluent 100 x Concentrate 0.5 M in Water. Part # 54128 $25/100 mL Part # 54528 $100/500 mL
Sodium Bicarbonate
Part # 54155
$25/100 mL
$25/100 mL $100/500 mL
65
ISO 9001:2000
METHOD
300.0
A small volume of sample, typically 2 to 3 mL, is introduced into an ion chromatograph. The anions of interest are separated and measured, using a system comprised of a guard column, separator column, suppressor device, and conductivity detector. The main differences between Method A and B are the separator columns, guard columns and eluents. In order to use this method for solids, an extraction procedure must be performed. Stability of the solutions must be closely monitored. Store the materials at 4C.
$50/100 mL $200/500 mL
$50/100 mL $200/500 mL
$25/100 mL $100/500 mL
Anions
Nitrate (NO3 )-as N Nitrite (NO2 )-as N Fluoride (F ) Orthophosphate (PO4 )-as P Nitrate & Nitrite as N
3-
$50/100 mL $150/500 mL
$25/100 mL $60/500 mL
66
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300.0
$50/100 mL $200/500 mL
$100/100 mL $200/500 mL
Method: E300D.M. Column: ASAHIPACK ODP50 (5m X 250 X 4.0mm). Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas. Retention Time (min) Fluoride 3.37 Chloride 4.78 Nitrite 5.65 Bromide 6.99 Nitrate 8.67 Phosphate 9.66 Sulfate 20.9
67
ISO 9001:2000
METHOD
300.0
$35/100 mL $95/500 mL
$35/100 mL $95/500 mL
$25/100 mL $100/500 mL
mAU
16
14
12
10
8
6
4
2
0
2
Method: E300B.M. Column: ASAHIPACK ODP50 (125mm X 4.0mm ID X 5.0m df). Inj. Volume= 1.0L. Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas.
Peak No. 1 2
3 -
Bromide (Br )
10
12
14
16
18
min
68
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Cations
4 Components in Water.
(1) (2) (3) (4) Calcium (Ca2+) Magnesium, (Mg2+) Potassium, (K+) Sodium (Na+) 1000 1000 1000 1000
Cations Mix #1
6 Components in Water.
(1) (2) (3) (4) (5) (6) Calcium (Ca2+) Magnesium, (Mg2+) Potassium, (K+) Sodium (Na+) Ammonium (NH4+) Lithium (Li+) 100 100 100 100 100 50
Cations Mix #2
Part # 59322
$50/100 mL
Part # 59203
$85/100 mL
69
ISO 9001:2000
METHOD
314332.0
Method 314.0 was developed for the determination of perchlorate in drinking water by ion chromatography coupled with suppressed conductivity detection. Method 314.1 employs the use of inline column concentration/matrix elimination ion chromatography coupled with suppressed conductivity detection for the determination of perchlorate in drinking water.
Method 332.0 was developed for the determination of low level perchlorate in drinking water by ion chromatography coupled with suppressed conductivity and electrospray ionization mass spectroscopy. To improve the accuracy and performance of this method,18-Oxygen enriched perchlorate is utilized as an internal standard.
Part # 59344
$35/100 mL
Part # 59344
$35/100 mL
1 ug/mL in Water
Part # 54022
$30/ 1 mL
Part # 54205
$50/100 mL
Part # 59206
$60/100 mL
Part # 59206
$60/100 mL
70
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353.2
This method covers the determination of nitrite singly, or nitrite and nitrate combined in drinking, ground, and surface waters, and domestic and industrial wastes. Stability of the solution must be closely monitored. Detection is by colorimetry. Typical stability is only 1 month. Store the materials at 4C.
$25/100 mL $100/500 mL
$25/100 mL $100/500 mL
Method: E300D.M. Column: ASAHIPACK ODP50 (5m X 250 X 4.0mm). Flow Rate= 1.0mL/min.. Column Temp.= 40C. Isocratic Analysis using Anion Mobile Phase. Detector: PDA (DAD1, Sig=360,20 REF=266, 10). Analyst: Pedro Rentas. 1) Nitrite 2) Nitrate
71
ISO 9001:2000
METHOD
Misc.
Part # 59294
$350/500 mL
Total Solids
Part # 54167
100 mg Neat
$25/ 100 mg
$25/ 100 mg
$25/100 mL
72
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Misc.
The following section contains several Wet Chemical Reference Materials that can be used as quality control checks or to generate calibration curves. A few popular EPA/SW-846 and Standard Methods are depicted for easy reference. Absolute Standards, Inc. has also generated a completely searchable web-based index of EPA analytes and methods. Please see our web site: www.AbsoluteStandards.com
Organic Nutrients
Total Phosphorus as P
Part # 54133 1000 ug/mL in Water $25/100 mL
Inorganic Nutrients
Calcium Hardness
Part # 54143 1000 ug/mL in 1% HCl $25/100 mL
100 ug/mL as DOC in Water 14.4 cm-1 as Absorbance at 254 nm in Water Part # 54166 $25/100 mL
Total Hardness
Alkalinity as CaCO3
Part # 54142 Part # 54242 1000 ug/mL in Water $25/100 mL $75/500 mL
$25/100 mL $90/500 mL
73
ISO 9001:2000
METHOD
Misc.
Conductance @ 25 C
Part # 54131 1000 uMHOS/cm in Water $25/100 mL
Part # 54122
Turbidity
$25/20 mL
pH of 6
Part # 54119 in Water $25/100 mL 1000 ug/mL in Water
MBAS
Part # 54160
$25/20 mL
Color
1000 ug/mL in Water / tr. NaOH Part # 54159 Part # 54169 $25/100 mL $75/500 mL
Silica (SiO2)
Part # 54255
$75/100 mL
74
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INDEX
Part# 52142 52143 52144 52145 52146 52147 52148 52149 52150 52151 52152 52153 52154 52155 52156 52157 52158 52159 52160 52161 52162 52163 52164 52166 52167 52168 52169 52170 52171 52172 52173 52174 52175 52176 52177 52178 52250 52251 52252 52253 52254 52255 52256 52302 Page# 58 58 60 60 60 60 37 19 19 19 19 19 20 23 23 24 24 24 25 25 26 28, 31 28, 31 29 30 32 32 33 33 34 34 34 34 35 35 35 15 15 57 14 14 14 14 54
Part# 52000 52001 52002 52003 52004 52005 52006 52007 52008 52009 52017 52018 52022 52023 52024 52025 52028 52031 52038 52039 52041 52042 52043 52044 52045 52046 52047 52050 52056 52057 52058 52059 52060 52061 52063 52064 52065 52066 52067 52068 52069 52070 52071 52072
Page# 16 16 16 16 16 16 36 36 36 36 20 20 21 21 22, 30 22 22 22 39 39 39 38 38 38 38 38 38 39 41 41 42 42 42 43 44 45 45 45 45 45 46 46 46 46
Part # 52073 52074 52075 52076 52079 52081 52084 52085 52086 52087 52088 52089 52090 52091 52092 52093 52094 52095 52096 52097 52098 52100 52101 52102 52105 52106 52107 52114 52115 52116 52117 52118 52119 52120 52122 52123 52133 52134 52135 52136 52137 52139 52140 52141
75
ISO 9001:2000
INDEX
Part# 52309 52310 52311 52312 52313 52314 52315 52316 52319 52320 52331 52332 52333 52334 52335 52336 52337 53000 53001 53002 53003 53004 53005 53006 53007 53008 53009 53017 53018 53022 53023 53024 53025 53028 53031 53038 53039 53041 53042 53043 53044 53045 53046 53047 Page# 16 16 16, 57 16 16 16 16 16 52 66 40 52 53 53 41 41 41 16 16 16 16 16 16 36 36 36 36 20 20 21 21 22, 30 22 22 22 39 39 39 38 38 38 38 38 38
Part # 53050 53056 53057 53058 53059 53060 53061 53063 53064 53065 53066 53067 53068 53069 53070 53071 53072 53073 53074 53075 53076 53079 53081 53084 53085 53086 53087 53088 53089 53090 53091 53092 53093 53094 53095 53096 53097 53098 53100 53101 53105 53106 53107 53114
Page# 39 41 41 42 42 42 43 44 45 45 45 45 45 46 46 46 46 46 47 47 47 49 49 50 50 51 51 51 51 51 62 62 62 62 63 63 63 63 54 54 68 68 66 55
Part# 53115 53116 53117 53118 53119 53120 53122 53123 53133 53134 53135 53136 53137 53139 53140 53141 53142 53143 53144 53145 53146 53147 53148 53149 53150 53151 53152 53153 53154 53155 53156 53157 53158 53159 53160 53161 53162 53163 53164 53165 53166 53167 53168 53169
76
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INDEX
Page# 72 73 70 69 69 69 69 69 69 69 16 58 16 38 46 45, 46 43 45 60 56 39 16 58 16 46 45, 46 43 45 60 56 39 67 67 74 49 64 64 66 67 67 64 64 66 73 Part# 59203 59206 59219 59249 59294 59322 59344 59370 59388 91958 Page# 69 70 40 40 72 69 70 29 53 61
Part# 53170 53171 53172 53173 53174 53175 53176 53177 53178 53309 53310 53311 53312 53313 53314 53315 53316 53319 53320 53331 53332 53333 53334 53335 53336 53337 54000 54001 54022 54112 54113 54116 54117 54118 54119 54122 54124 54125 54126 54127 54128 54129 54131 54132
Page# 33 33 34 34 34 34 35 35 35 16 16 16, 57 16 16 16 16 16 52 66 40 52 53 53 41 41 41 65 69 70 69 69 72 72 72 74 74 74 72 73 65 65 65 74 73
Part # 54133 54134 54135 54136 54139 54142 54143 54148 54149 54150 54152 54153 54154 54155 54156 54157 54158 54159 54160 54161 54162 54163 54164 54165 54166 54167 54169 54172 54175 54176 54194 54196 54205 54242 54243 54255 54500 54516 54517 54518 54521 54527 54528 54529
Page# 73 72 61 72 65 73 73 73 69 74 73 73 69 65 73 69 69 74 74 59 70 65 70 74 73 72 74 59 59 59 72 72 70 73 72 74 65 72 72 72 70 65 65 65
Part# 54596 54597 57001 57003 57011 57012 57019 57020 57038 57056 57146 57250 57280 57315 57351 57380 57642 57651 57847 57880 57911 58146 58250 58280 58351 58380 58642 58651 58847 58880 58911 59010 59011 59017 59030 59045 59046 59076 59095 59096 59110 59153 59176 59179
77
ISO 9001:2000
NOTES
78
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NOTES
79
ISO 9001:2000
Custom Standard Quotation Request Form Fax: (800) 410-2577, Technical Service Dept, Absolute Standards, Inc. Email: [email protected] Page From: Company Contact: Company: Company Address: Telephone: Email: Product Description: Solvent/ Matrix: Volume Size: 1 x 100 mL Qty: 1 x 500 mL Qty: Other: Qty: Fax: of Date:
Account#:
Date Required: 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. Comments: 80 Component
Yes
No
Concentration (ug/mL)
Absolute Standards, Inc. ISO 9001 Registered ISO 17025 Accredited P.O. Box 5585, Hamden, CT 06518 Phone (800) 368-1131
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