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1 Methodology/Procedure 2 Process Flow Diagram (PFD) 3 Workbook 4 Theory

This document contains information about a laboratory experiment on separating a mixture of ammonia and water vapors. The process involves feeding the vapor mixture into a condenser, then expanding it through a valve before separating it into a vapor stream and a liquid stream in a flash vessel. Key details provided include the process flow diagram, stream table calculations, and questions about determining stream properties like temperature and composition.

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61 views6 pages

1 Methodology/Procedure 2 Process Flow Diagram (PFD) 3 Workbook 4 Theory

This document contains information about a laboratory experiment on separating a mixture of ammonia and water vapors. The process involves feeding the vapor mixture into a condenser, then expanding it through a valve before separating it into a vapor stream and a liquid stream in a flash vessel. Key details provided include the process flow diagram, stream table calculations, and questions about determining stream properties like temperature and composition.

Uploaded by

apekmh92
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© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
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UNIVERSITI TEKNOLOGI MARA FAKULTI KEJURUTERAAN KIMIA PROCESS ENGINEERING LABORATORY III (CPE612)

NAME STUDENT NO. GROUP EXPERIMENT DATE PERFORMED SEMESTER PROGRAMME / CODE SUBMIT TO

:MUHAMMAD AFIQ BIN MOHD HAFEEZ :2011814658 : 5B :SEPARATION OF AMMONIA AND WATER :15/11/2013 :5 : EH221 : LAB 1(EN AMMAR MOHD AKHIR)

No. 1 2 3 4

Title Methodology/Procedure Process Flow Diagram (PFD) Workbook Theory TOTAL MARKS

Allocated Marks (%)

Marks

50

Remarks:

Checked by:

Rechecked by:

------------------------------(FAUZIAH MARPANI) Date:

----------------------------------( ) Date:

THEORY Process given A mixture of ammonia and water in the vapour phase is fed at 143.6 ,saturated at 1724 kpa

and containing 80 wt% ammonia is passed through a condenser at a flow rate of 10000 lbmol/hr. heat is removes at the rate of 5.8x Btu/hr(make an assumption for the pressure).

Its effluent is expended with an outlet pressure of the valve is 1034 kpa and fed into a flash vessel. Flash vessel temperature is 40.63 . Hint: 1. Use SRK Equation of state fluid package. 2. Mainly water at liquid stream of separator. In this separation process, each of the equipment has their own purposes and definitions. The equipment that involves are cooler, valve and separator.

Firstly, feed consist of ammonia and water in vapor phase is cooled in the condenser. Condenser is a device that condenses a substance from its gaseous state into liquid and thus reducing temperature. The other function of the condenser is to record and determine the amount of energy to cool down the stream.

Valve is used in this process as the pressure regulator or pressure controller. In this process the valve is used to lower the pressure of the stream.

Flash vessel is the main equipment for this process. This equipment works as a separator of vapor-liquid mixture and used to separate the mixture of ammonia and water.

All calculations are done using Aspen V7.2 based on SRK Equation of state fluid.

PROCEDURES 1.New blank icon is selected to start a new case. Ammonia and water is added as the component in the Component List View. 2. The process flow diagram is form consist of cooler, valve, and separator. 3. SRK Equation of State is selected in the specification tab under Method. 4.. Information that needed to be inserted in the process such as feed flow rate, pressure for certain equipments; mole fraction and duty of the equipment were entered in the equipment as in the question that is provided. 5.Stream table is generated by clicking stream tab under the result summary.

PROCESS FLOW DIAGRAM

VAPOR

CO OLER FEED C- OU T

VALVE SEP- IN

SEPARATO

LIQ UID

PICTURE 1: PFD OF SEPARATION OF AMMONIA AND WATER

Picture 1 show the process of Separation of Ammonia and Water. The feed consist of Ammonia and water which is in vapor phase. The feed is then fed into a cooler to reduce the temperature of the feed. The stream(c-out) is then go into the valve to be expended and fed into a flash vessel.

WORKBOOK Table 1: Steam table of this process

Hea t and Material Ba la nce Table Strea m ID From To Phase Substream : MIXED Mole Flow AMMON-01 WATER Total Flow Total Flow Total Flow Temperature Pressure Vapor Frac Liquid Frac Solid Fra c Enthalpy Enthalpy Enthalpy Entropy Entropy Density Density Ave rage MW Liq Vol 60F cuft/hr Btu/lbm ol Btu/lb MMBtu/hr Btu/lbm ol-R Btu/lb-R lbmol/cuft lb/cuft lbmol/hr lb/hr cuft/hr F psia lbmol/hr 8000.000 2000.000 10000.00 1.72275E+5 8.38465E+7 321.8063 1.000000 1.000000 0.0 0.0 -34417.76 -1997.838 -344.1776 -11.38564 -.6608989 1.19266E-4 2.05465E-3 17.22750 7441.576 8000.000 2000.000 10000.00 1.72275E+5 3.02573E+5 290.4800 250.0451 1.000000 0.0 0.0 -34997.76 -2031.505 -349.9776 -22.99964 -1.335053 .0330498 .5693669 17.22750 7441.576 239.2447 1951.907 2191.152 39238.63 696.8466 105.1340 149.9690 0.0 1.000000 0.0 -1.1291E+5 -6305.015 -247.4001 -38.01753 -2.122964 3.144382 56.30884 17.90776 769.6126 8000.000 2000.000 10000.00 1.72275E+5 8.38465E+7 321.8063 1.000000 1.000000 0.0 0.0 -34417.76 -1997.838 -344.1776 -11.38564 -.6608989 1.19266E-4 2.05465E-3 17.22750 7441.576 7760.755 48.09281 7808.848 1.33036E+5 2.92078E+5 105.1340 149.9690 1.000000 0.0 0.0 -20257.96 -1189.083 -158.1913 -27.94625 -1.640363 .0267355 .4554833 17.03662 6671.963 C-OUT COOLER VALVE VAPOR COOLER VAPOR LIQUID FEED LIQUID SEPARATO SEP-IN VALVE SEPARATO VAPOR VAPOR VAPOR SEPARATO

CALCULATION

V=7808.808 lbmol/hr N3 =7760.715 lbmol.hr 2 =48.09267 lbmol/hr

F=10000lbmol/hr

N3 =0.8wt% 2 O=0.2wt%

L=2191.192 lbmol/hr N3 =239.2845 lbmol/hr 2 =1951.907 lbmol/hr

Components

Mole fraction of vapour stream

Mole fraction of liquid stream

Ammonia Water

QUESTIONS

1) What is the temperature of the outlet stream of the condenser? 198.0636

2) What are the mole fractions for ammonia and water in the vapour and liquid outlet of the separator?

Vapour outlet: Ammonia: 0.9938 Water: 0.0062

Liquid outlet: Ammonia: 0.1092 Water: 0.8908 3) Determine the mass flow rate (lb/hr) for each outlet stream of the separator.

Vapour outlet: 1.33036x

lb/hr

Liquid outlet: 39239.31 lb/hr

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