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starting

formulation
No. 4001* Rapid Setting, Room Temperature Cure Adhesive
EPON Resin 8111/EPI-CURE Curing Agents 3270 and 3271
This silica-filled epoxy adhesive system offers the convenience of an equal volume combining ratio of resin portion to converter portion, coupled with rapid bond strength development and good adhesion to a variety of substrates. Equal volume mix ratio Rapid gel times, less than 4 minutes for 100 gram mass Rapid bond strength development Good water resistance Thixotropic paste General purpose bonding of metals, concrete, glass and many rigid plastics. Material Part A EPON Resin 8111 CAB-O-SIL M-5 Silica (Fumed amorphous silica)1 NOVACITE 1250 (Ground quartz silica)2 Pounds Gallons

Introduction

Features

Suggested Uses Formula

100.0 5.0 75.0 180.0

10.57 0.28 3.40 14.25

Part B EPI-CURE Curing Agent 3270 EPI-CURE Curing Agent 3271 CAB-O-SIL M-5 Silica (Fumed amorphous silica)1 NOVACITE 1250 (Ground quartz silica)2
1 2

Cabot Corp. Malvern Minerals Co.

80.0 5.0 5.0 77.0 167.0

9.90 0.58 0.28 3.49 14.25

*Formerly 27-103.

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EPON

EPI-CURE

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SC:2032-01 / Starting Formulation No. 4001

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Typical Handling Properties

Table 1/ Handling Properties Resin/Curing Agent Combining Ratio by weight by volume Viscosity at 25 C, cP at 1 rpm at 5 rpm at 10 rpm at 50 rpm Pounds/Gallon Part A Part B Part A and B Gel Time at 25 C 100 gram mass, seconds Bondline Thickness, minutes

Part A 8,000 6,200 5,520 5,200

100:93 1:1 Part B 179,000 73,600 52,900 38,800 12.63 11.72 12.18 225 45

Mixing Instructions

Disperse the CAB-O-SIL M-5 into a portion of the EPON Resin 8111 using a high shear dispersing technique (note that EPON Resin 8111 is shear sensitive. Excessive shear energy may cause premature gellation.). Add the remaining EPON Resin 8111 and NOVACITE 1250 to the resulting dispersion and mix, using conventional mixing equipment, until all the NOVACITE 1250 has been wetted and a uniform consistency is attained. Blend the EPI-CURE Curing Agent 3270 and EPI-CURE Curing Agent 3271 together. Disperse the CAB-O-SIL M-5 into this blend using high shear agitation. Add the NOVACITE 1250 and continue mixing using high shear agitation until all the NOVACITE 1250 has been wetted and a uniform consistency is attained. This formulation is a basic starting point and can be modified with other filler types, such as aluminum powder, talc, alumina, wollastonite, or calcium carbonate. Modification with silane coupling agents improves bonds to concrete and glass. Pigment may be incorporated into either or both portions for the purpose of color coding.

Application

Surfaces to be bonded should be clean and free of dust, dirt, grease, or other contaminants. It is also recommended to roughen bonding surfaces with abrasive media appropriate for the materials being bonded (such as medium grit emery paper, abrasive disks, grit blasting, wire brushes, etc.). Abrasion should always be followed by degreasing to remove contaminants and loose partivles. Mix the adhesive components and apply immediately by spreading a thin film over the surface to be bonded. Maintain light pressure during cure for optimum bonding.

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Typical Cured State Properties

Table 2/ Typical Adhesive Properties Substrate Aluminum Alloy 2024T3, acid etched Cure Schedule 1 hour at 25 C 2 hours at 25 C 4 hours at 25 C 24 hours at 25 C 1 day at 25 C followed by 2 hours at 100 C 7 days at 25 C followed by 7 days water soak 1 day at 25 C followed by 2 hours at 100 C Tensile Shear Strength at 25 C 100 psi 370 psi 760 psi 2800 psi 4000 psi 3300 psi 1600 psi

Cold-rolled steel, solvent-wiped

These are starting point formulations and are not proven for use in the users particular application but are simply meant to demonstrate the efficacy of the products and to assist in the development of the users own formulations. It is the users responsibility to fully test and qualify the formulation, along with the ingredients, methods, applications, or equipment identified herein (Information), by the users knowledgeable formulator or scientist, and to determine the appropriate use conditions and legal restrictions, prior to use of any Information.

Resolution Performance Products P.O. Box 4500 Houston, Texas 77210-4500 For product prices, availability, or order placement, call our toll-free customer service number at:

1.877.859.2800
For sales in North and South America outside the United States, call:

1.832.366.2365

For literature and technical assistance, visit our website at:

www.resins.com
SAFETY & HANDLING These products are capable of producing adverse health effects ranging from minor skin irritation to serious systemic effects. Exposure to these materials should be minimized and avoided, if feasible, through the observance of proper precautions, use of appropriate engineering controls and proper personal protective clothing and equipment, and adherence to proper handling procedures. None of these materials should be used, stored, or transported until the handling precautions and recommendations as stated in the Material Safety Data Sheet (MSDS) or Preliminary Safety Information Sheet (PSIS) for these and all other products being used are understood by all persons who will work with them. Questions and requests for information on Resolution Performance Products LLC (RPPLLC) products should be directed to your RPPLLC sales representative, or the nearest RPPLLC sales office. Information and MSDSs or PSISs on non-RPPLLC products should be obtained from the respective manufacturer. NOTICE Any of the formulations or the ingredients in the formulations may present an unknown health or safety hazard. These are starting point formulations and are not proven for use in a users particular application. It is the users responsibility to fully test and qualify the formulation, its ingredients, methods, applications, or equipment identified herein (Information), by the users knowledgeable formulator or scientist, and to determine the appropriate use conditions and legal restrictions, prior to use of any Information. Reference to any commercial ingredient, process, or service by trade name, trademark, or manufacturer does not constitute or imply its endorsement, recommendation or favor in the formulation or for use in the users application. ALL WARRANTIES OF ANY KIND ARE EXPRESSLY EXCLUDED AND DISCLAIMED. WITHOUT LIMITATION, NO REPRESENTATION IS MADE AND NO WARRANTY, EXPRESS OR IMPLIED, IS EXTENDED WITH RESPECT TO THE ACCURACY, REPRODUCIBILITY, COMPLETENESS, OR USEFULNESS OF THE INFORMATION TO MEET YOUR REQUIREMENTS, OR WITH RESPECT TO THE TITLE OR MERCHANTIBILITY OF THE INFORMATION PROVIDED, OR THE FITNESS OF THE INFORMATION PROVIDED FOR A PARTICULAR PURPOSE, OR THAT THE USE OF THE INFORMATION IS FREE FROM INFRINGEMENT OF ANY PATENT OR ANY OTHER INTELLECTUAL PROPERTY RIGHT, AND EACH OF THESE ARE THE SOLE AND EXCLUSIVE RESPONSIBILITY OF THE USER. Use of the Information is at your own risk. No opinion, advice or Information, whether oral or written, obtained by you in any manner from us pertaining to the Information shall create any warranty of any kind. Your reliance on the Information presented herein for use in a particular application shall indicate your consent that in no event will Resolution Performance Products LLC or any of its affiliates be responsible for any damages of any nature whatsoever resulting from the use of or reliance upon the Information.

2001 Resolution Performance Products LLC. All rights reserved. Printed in the U.S.A.

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E P I KOT E

EPON

EPI-CURE

EPI-REZ

H E LOX Y

C A R D U R A

V E O VA