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Experiment No. 1 Solubility of Organic Compounds Objectives

1. The document describes an experiment to investigate the solubility of organic compounds in different solvents like water, sodium hydroxide, sodium bicarbonate, and hydrochloric acid. 2. The objectives are to determine solubility, demonstrate how it relates to functional groups and compound characteristics, and classify compounds based on solubility. 3. A table outlines the experimental procedure where samples will be added to solvents and observed for solubility, with results used to classify compounds into groups A through D based on general characteristics like alcohols, acids, phenols, or hydrocarbons.

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Stephen Eleserio
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61 views2 pages

Experiment No. 1 Solubility of Organic Compounds Objectives

1. The document describes an experiment to investigate the solubility of organic compounds in different solvents like water, sodium hydroxide, sodium bicarbonate, and hydrochloric acid. 2. The objectives are to determine solubility, demonstrate how it relates to functional groups and compound characteristics, and classify compounds based on solubility. 3. A table outlines the experimental procedure where samples will be added to solvents and observed for solubility, with results used to classify compounds into groups A through D based on general characteristics like alcohols, acids, phenols, or hydrocarbons.

Uploaded by

Stephen Eleserio
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
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Pre-Laboratory Report Rating

Eleserio, Stephen Y. Group No. 3


HUB21 November 25, 2010

Experiment No. 1
Solubility of Organic Compounds
Objectives:
1. To investigate and determine the solubility of organic compounds in different solvents
2. To demonstrate how the property of solubility provides a general idea of the functional group as
well as general characteristics of the sample.
3. To determine the classification of organic compounds based on solubility to selected solvents.

Reagents:
Molecu
Meltin Boilin Specifi
lar IUPAC Structur Solubilit
g g c Safety Data
Formul Name e y
Point Point Gravity
a

99.98 1000
H2O Oxidane 0 °C N/A
°C kg/m3

10 g/L (20
Sodium 1388 2.13
NaOH Na-OH 318 °C °C) in
Hydroxide °C g/cm3
water

Sodium
NaHC 851 2.173 100 g/L
hydrogen 270 ºC
O3 ºC g/cm3 (20 °C)
carbonate

–27.32 110 °C
Hydrochloric °C in in 1.18
HCL H-Cl Miscible
acid 38% 20.2% g/cm3
solution solution Table 1: Solubility
Classifications

Clas Gen. Char.


Materials and Glasswares: s.
Small test tubes Litmus Paper (red and blue)
A Maybe alcohols,
Stirring rod Spot plate ketones, amines,
Carboxylic acids w/
Schematic Diagram < 5 C atoms

B. Solubility in NaOH and NaHCO B13 Maybe carboxylic


A. Solubility in H2O (Sample 2) acids with more >
(Sample 1) 2-3 drops/ 5 mg Compound 1 (2nd 5 C atoms, Phenols
A2-3 drops/ 5 mg Compound 1 (1st Sample) w/ electron
Sample) + 3mL 5%
+ 2mL H2O withdrawing
NaOH groups.
Shake and observe Insoluble Soluble
Miscible. B2 Phenols
Chemical + 3mL 5%
Slightly Miscible Obtain new C Amines
changes NaHCO3
Sample Insoluble Soluble
are D Hydrocarbons,
+ 5mL H2O (Sample 3)(Group B2) (Group B1)
observed alkyl halides,
Dissolved Immiscibl
(Group e C. Solubility in HCl (Sample
A) 3)
Obtain 2-3 drops/ 5 mg Compound 1 (3rd
Check pH New Sample)
+ 3mL 5%
Sample HCl
(Sample 2) Miscible (Group Immiscible
C) (Group D)

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