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User R. Aioanei Operator MB Instrument Bruker Avance DRX 400

The document contains data from a 1H NMR spectroscopy experiment performed on a Bruker Avance DRX 400 instrument. Key details include: - The sample was DHABE2 analyzed in CDCl3 solvent - 16 scans were collected using a 5 mm QNP 1H/29Si probehead - Chemical shifts are referenced to TMS at 0 ppm - The spectrum shows resonances between 0-13 ppm

Uploaded by

Ralu Ralluca
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© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
18 views

User R. Aioanei Operator MB Instrument Bruker Avance DRX 400

The document contains data from a 1H NMR spectroscopy experiment performed on a Bruker Avance DRX 400 instrument. Key details include: - The sample was DHABE2 analyzed in CDCl3 solvent - 16 scans were collected using a 5 mm QNP 1H/29Si probehead - Chemical shifts are referenced to TMS at 0 ppm - The spectrum shows resonances between 0-13 ppm

Uploaded by

Ralu Ralluca
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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7.

519
7.465
7.450
7.446
7.437
7.420
7.261
7.227
7.203
7.084
7.064
7.046
7.039
7.028
7.023
7.017
7.009
7.005
7.000
6.997
6.563
6.540
6.534
6.510
5.299
4.899
4.881
4.863
4.845
4.322
4.023
3.872
3.834
3.709
3.696
2.615
2.597
2.578
2.338
2.171
2.134
2.122
1.864
1.845
1.809
1.791
1.772
1.753
1.734
1.560
1.503
1.484
1.465
1.447
1.295
1.279
1.257
1.011
0.993
0.975

11.391

12.353

data
USER
nmr
NAME
EXPNO
PROCNO
Date_
Time
INSTRUM
PROBHD
PULPROG
TD
SOLVENT
NS
DS
SWH
FIDRES
AQ
RG
DW
DE
TE
D1
TD0

ICONNMRLab
100927SC41DHABE2
1
1
20100927
11.27
spect
5 mm QNP 1H/29
zg30
57470
CDCl3
16
2
7183.908 Hz
0.125003 Hz
3.9999621 sec
406.4
69.600 usec
6.00 usec
299.2 K
1.00000000 sec
1

======== CHANNEL f1 ========


NUC1
1H
P1
10.63 usec
PL1
5.00 dB
SFO1
400.1328009 MHz
SI
32768
SF
400.1300171 MHz
WDW
EM
SSB
0
LB
0.30 Hz
GB
0
PC
1.00
OFFSET
15.934 ppm
PH_mod
pk

5.97
0.38
0.18
0.40
0.07
3.02
6.40
7.36
2.05
0.36
9.10
1.58

0.33
0.08
0.20
0.52
0.30

7
2.57

0.43
8.00
1.63
0.87
0.39
2.75

1.00

ppm

10

\\Bruker1New\D\UTIFChimInd\RAioanei

0.04

11.5

11
1.34

12
0.81

DU

1.342

12.0
0.805

12.5

11.391

12.353

Instrument Bruker Avance DRX 400


Operator MB
User R. Aioanei
Registry No 10381
Sample Changer No 41
Sample Name DHABE2
#H1QNP34 CDCl3 {D:\UTIFChimInd\RAioanei} ICONNMRLab 41

ppm

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