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EX 6 Quality Control

This document contains data from experiments measuring absorbance of iron (Fe3+) solutions at different concentrations over five days. Absorbance increased linearly with concentration. Quality control samples, including internal and external controls, were also tested each day. Results for the internal control clustered around the expected value. While most results for the external control matched the true value, one was an outlier.

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Isuru Jayalath
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34 views6 pages

EX 6 Quality Control

This document contains data from experiments measuring absorbance of iron (Fe3+) solutions at different concentrations over five days. Absorbance increased linearly with concentration. Quality control samples, including internal and external controls, were also tested each day. Results for the internal control clustered around the expected value. While most results for the external control matched the true value, one was an outlier.

Uploaded by

Isuru Jayalath
Copyright
© Attribution Non-Commercial (BY-NC)
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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Concentration of

standard Fe3+ solution /


mol L-1
0.00000
0.00005
0.00010
0.00015
0.00020
0.00025

Absorbance at 480
nm
0.00
0.09
0.17
0.26
0.34
0.42

The graph of Absorbance at 480 nm Vs. Concentration of standard Fe 3+


solution / mol L-1 Day 2
0.45

0.40

X1unit=0.00005 mol L-1


Y1unit=0.05

0.35

Absorbance at 480 nm

0.30

y = 1698.2x
R = 0.9994

0.25

0.20

0.15

0.10

0.05

0.00
0.00000

0.00005

0.00010

Concentration of standard

0.00015

Fe3+

solution / mol

0.00020

L-1

0.00025

Concentration of standard
Fe3+ solution / mol L-1 Absorbance at 480 nm
0.00
0.00000
0.03
0.00005
0.13
0.00010
0.19
0.00015
0.31
0.00020
0.37
0.00025

The graph of Absorbance at 480 nm Vs. Concentration of standard


Fe3+ solution / mol L-1 Day 3
0.40

0.35

y = 1436.4x
R = 0.9708

X1unit=0.00005 mol L-1


Y1unit=0.05

Absorbance at 480 nm

0.30

0.25

0.20

0.15

0.10

0.05

0.00
0.00000

0.00005

0.00010

Concentration of standard

0.00015

Fe3+

solution / mol

0.00020

L-1

0.00025

Concentration of standard
Fe3+ solution / mol L-1 Absorbance at 480 nm
0.00
0.00000
0.10
0.00005
0.20
0.00010
0.30
0.00015
0.35
0.00020
0.49
0.00025

The graph of Absorbance at 480 nm Vs. Concentration of standard Fe 3+


solution / mol L-1 Day 4
0.50

0.45

y = 1909.1x
R = 0.9907

X1unit=0.00005 mol L-1


Y1unit=0.05

0.40

Absorbance at 480 nm

0.35

0.30

0.25

0.20

0.15

0.10

0.05

0.00
0.00000

0.00005

0.00010

Concentration of standard

0.00015

Fe3+

solution / mol

0.00020

L-1

0.00025

Concentration of standard
Fe3+ solution / mol L-1 Absorbance at 480 nm
0.00
0.00000
0.09
0.00005
0.16
0.00010
0.24
0.00015
0.34
0.00020
0.51
0.00025

The graph of Absorbance at 480 nm Vs. Concentration of standard Fe 3+


solution / mol L-1 Day 5
0.60

0.50

X1unit=0.00005 mol L-1


Y1unit=0.05
y = 1832.7x
R = 0.9693

Absorbance at 480 nm

0.40

0.30

0.20

0.10

0.00
0.00000

0.00005

0.00010

Concentration of standard

0.00015

Fe3+

solution / mol

0.00020

L-1

0.00025

Concentration of internal
QC / mol L-1 X10-3
2.42
1.70
1.53
1.68
1.75

Day
1
2
3
4
5

Levy-jening's plot of internal QC sample


2.90

Y1unit=0.49(SD)
X1unit=1 day

Concentration of Internal QC / mol L-1 X10-3

2.41

1.92

1.43

0.94
0

Days

True value for external


QC /mol L-1 X10-3

Result value for external


QC / mol L-1 X10-3

0.00
1.75
3.95
2.15
1.25
4.20

0.00
1.88
3.89
2.09
1.47
2.95

Line of identity plot for external QC


4.50

X1unit=0.50 mol L-1


Y1unit=0.50 mol L-1
4.00

Result value for external QC / mol L-1 X10-3

3.50

3.00

R = 0.9046
2.50

2.00

1.50

1.00

0.50

0.00
0.00

0.50

1.00

1.50

2.00

2.50

True value for external QC /mol

3.00

L-1

X10-3

3.50

4.00

4.50

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