Result Disc Vidraria Aula 1 Rot 1 17 09

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RESULTADOS E DISCUSSÕES – Aula 1 – Roteiro 1

Uso de Vidrarias, Micropipetas, Pesagem e Preparo de Soluções.


Objetivo:
Permitir ao aluno conhecer e manipular as principais vidrarias e equipamentos presentes na rotina de um
laboratório químico.

Dar a função para cada um dos itens abaixo:

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Funil de decantação _______________________________________________________________________
ou funil de bromo
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Estufa _________________________________________________________
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Mufla

Parte 1: Preparo de Solução Fisiológica:

a) Ajuste a balança seguindo as orientações do professor.


b) Efetue a dobradura de papel manteiga para a pesagem.
c) Pese, exatamente, 0,9 g de NaCl.
d) Transfira, quantitativamente, a massa de NaCl pesada para um béquer de 100 mL.
e) Com auxílio de uma proveta, colete 50 mL de água destilada e transfira para o béquer.
f) Com auxílio de um bastão de vidro, dissolva os cristais com água destilada.
g) Após dissolução completa, transfira o conteúdo do béquer para um balão volumétrico de 100 mL.

a) Completar o volume do balão volumétrico obedecendo a marca de aferição e evitando


cometer erro de paralaxe referente à leitura do menisco. (Obedeça às orientações do
professor)
b) Transferir o conteúdo do balão para um frasco, devidamente identificado.

h) Efetue o cálculo da concentração em g.L-1 e em título (%) para a solução recém-preparada.

Parte 2: Atividade Complementar Obrigatória


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a) No laboratório você foi apresentado a uma série de equipamentos e vidrarias. A figura abaixo mostra
algumas delas.

Apresente a nomenclatura das vidrarias:


1:__Balão Volumétrico_____
2:- _Copo de Béquer_____
3:-_Erlenmeyer____
4:-_Pipeta Volumétrica_____
b) Caso você tenha que preparar uma solução de 100 mL de glicose (MM = 180 g/mol), qual deverá ser
a massa pesada na balança para alcançar uma concentração molar de 0,2M?

Dados:

Volume da solução = 100 mL = 0,1 L

Massa molar da glicose = 180 g/mol

Concentração da Solução = 0,2 M ou 0,2 mol/L

m1 = M . MM1 . V(L)

m1 = 0,2 mol . 180 _g_ . 0,1L


L mol

m1 = 3,6 g

c) Caso você tenha que preparar uma solução de 450 mL de sulfato de sódio, qual deverá ser a massa pesada
na balança para alcançar uma concentração em título de 2,5%?
RESPOSTA:
τ % = _m1_ x 100
m

Considerar densidade da solução = 1 g/mL


massa da solução = 450g
m1 = massa do soluto
m = massa da solução
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τ % = _m1_ x 100
450

2,5 x 450 = m1 x 100

m1 x 100 = 2,5 x 450

m1 = _2,5 x 450_
100

m1 = 11,25 g Na2SO4

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