Empirical Investigations during WEDM of Ni-27Cu-3.15Al-2Fe-1.5Mn Based Superalloy for High Temperature Corrosion Resistance Applications
Abstract
:1. Introduction
2. Materials and Methods
2.1. Experimental Setup
- Wire electrical discharge machine
- Work material
- Tool
- Dielectric fluid
2.1.1. Wire Electrical Discharge Machine
2.1.2. Work Material
2.1.3. Tool
2.1.4. Dielectric
2.2. Selected Input Parameters
2.2.1. Pulse-On Time
2.2.2. Pulse-Off Time
2.2.3. Spark Gap Voltage
2.2.4. Wire Feed Rate
2.3. Experiment Plan
3. Results and Discussion
3.1. Statistical Observations for Cutting Rate (CR)
3.2. Regression Equation for CR
3.3. Interaction Influence of Process Variables on CR
3.4. Statistical Observations for Surface Roughness (SR)
3.5. Regression Equation for SR
3.6. Correlational Influence of Input Variable on SR
4. Multi-Response Optimization Using Desirability Function
5. Conclusions
- (a)
- The process parameters like Ton, Toff, SV have significant effect on for cutting-rate. The empirical relation is:CR = 11.23430 − 0.27541 × Ton + 0.070854 × Toff + 0.034292 × SV + 0.020625 × WF − 3.075× 10−3 ×Ton × Toff − 7.41667× 10−4 ×Ton × SV + 6.25000 × 10−4 × Toff × SV + 2.40938 × 10−3 × Ton2 + 1.85938× 10−3 × Toff2
- (b)
- The process parameters like Ton and SV have major effect on for SR. The empirical relation is:SR = 10.51207 − 0.15017 × Ton + 0.06061 × Toff − 0.13619 × SV + 3.15000 × 10−3 × Ton × Toff + 1.01667 × 10−3 ×Ton × SV − 4.50693 × 10−3 × Toff2 + 5.47585 × 10−4 × WF2
- (c)
- Analysis of response surfaces exhibited that Ton has influenced the cutting rate in such as a manner that during a rise in Ton, the cutting rate goes on increasing; however, it impacted surface-roughness catastrophically. Furthermore, it was noticed that the CR as well as SR both reduces as there is increment in pulse-off time.
- (d)
- Moreover, it has been found that that CR decreases with rise in SV and vice versa. On the contrary, SR increases with decline in SV and vice versa. Also, the impact of wire-feed rate on the CR and SR has been found to be negligible.
- (e)
- The optimization of a multi-response approach by giving equal priority to both the responses achieved the highest cutting rate of 2.48 mm/min, and the lowest roughness of 2.12 µm.
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
Nomenclature
Adeq. Precision | Adequate Precision |
Adj. R2 | Adjusted-R2 |
ANOVA | Analysis of Variance |
CCD | Central Composite Design |
CNC | Computer Numerical Control |
CR | Cutting Rate |
CV | Coefficient of Variation |
DOE | Design of Experiment |
Pred. R2 | Predicted R2 |
R2 | Determination Coefficient |
RSM | Response Surface Methodology |
SV | Spark Gap Voltage |
SR | Surface Roughness |
Toff | Pulse-off Time |
Ton | Pulse-on Time |
WEDM | Wire Electrical Discharge Machining |
WF | Wire-feed rate |
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Element | Ni | Cu | Fe | S | C | Mn | Si | Al | Ti |
---|---|---|---|---|---|---|---|---|---|
Weight (%) | 65 | 27 | 2 | 0.01 | 0.25 | 1.5 | 0.5 | 2.30–3.15 | 0.35–0.85 |
S. No. | Parameters | Units | Range | Levels | ||||
---|---|---|---|---|---|---|---|---|
1 | 2 | 3 | 4 | 5 | ||||
Coded Values | −2 | −1 | 0 | 1 | 2 | |||
1. | Pulse-on Time (A) | (µs) | 108–124 | 108 | 112 | 116 | 120 | 124 |
2. | Pulse-off Time (B) | 42–58 | 42 | 46 | 50 | 54 | 58 | |
3. | Spark Gap Voltage (C) | (volts) | 24–72 | 24 | 36 | 48 | 60 | 72 |
4. | Wire Feed rate (D) | (m/min) | 4–12 | 4 | 6 | 8 | 10 | 12 |
S. No. | Fixed Parameter | Value |
---|---|---|
1 | Peak-current | 120 amperes |
2 | Peak-voltage | 110 DC (maximum) |
3 | Wire tension | 8 units |
4 | Servo feed | 2100 units |
5 | Water pressure | 15 kg/cm2 |
Std Order | Run Order | “Pulse-on Time” (µs) | “Pulse-off Time” (µs) | “Servo-Voltage” (volts) | “Wire-Feed Rate” (m/min) | “Cutting-Rate” (mm/min) | “Surface-Roughness” (µm) |
---|---|---|---|---|---|---|---|
1 | 15 | 112 | 46 | 36 | 6 | 1.22 | 2.35 |
2 | 30 | 120 | 46 | 36 | 6 | 2.06 | 2.86 |
3 | 17 | 112 | 54 | 36 | 6 | 0.59 | 2.06 |
4 | 13 | 120 | 54 | 36 | 6 | 1.43 | 2.53 |
5 | 27 | 112 | 46 | 60 | 6 | 0.64 | 1.69 |
6 | 16 | 120 | 46 | 60 | 6 | 1.55 | 2.24 |
7 | 7 | 112 | 54 | 60 | 6 | 0.31 | 1.09 |
8 | 12 | 120 | 54 | 60 | 6 | 0.8 | 2.43 |
9 | 5 | 112 | 46 | 36 | 10 | 1.26 | 2.36 |
10 | 11 | 120 | 46 | 36 | 10 | 2.48 | 2.88 |
11 | 26 | 112 | 54 | 36 | 10 | 0.7 | 2.07 |
12 | 28 | 120 | 54 | 36 | 10 | 1.44 | 2.59 |
13 | 1 | 112 | 46 | 60 | 10 | 0.71 | 1.76 |
14 | 21 | 120 | 46 | 60 | 10 | 1.58 | 2.24 |
15 | 20 | 112 | 54 | 60 | 10 | 0.35 | 1.21 |
16 | 29 | 120 | 54 | 60 | 10 | 0.87 | 2.26 |
17 | 19 | 108 | 50 | 48 | 8 | 0.38 | 1.46 |
18 | 9 | 124 | 50 | 48 | 8 | 2.28 | 2.35 |
19 | 24 | 116 | 42 | 48 | 8 | 1.84 | 1.93 |
20 | 3 | 116 | 58 | 48 | 8 | 0.62 | 1.34 |
21 | 10 | 116 | 50 | 24 | 8 | 1.71 | 2.56 |
22 | 25 | 116 | 50 | 72 | 8 | 0.41 | 1.29 |
23 | 8 | 116 | 50 | 48 | 4 | 1.01 | 2.24 |
24 | 14 | 116 | 50 | 48 | 12 | 1.11 | 2.42 |
25 | 2 | 116 | 50 | 48 | 8 | 1.04 | 2.21 |
26 | 23 | 116 | 50 | 48 | 8 | 1.01 | 2.15 |
27 | 22 | 116 | 50 | 48 | 8 | 1.13 | 2.29 |
28 | 6 | 116 | 50 | 48 | 8 | 1.15 | 2.05 |
29 | 18 | 116 | 50 | 48 | 8 | 1.08 | 2.12 |
30 | 4 | 116 | 50 | 48 | 8 | 1.17 | 2.36 |
Source | “Sum of Squares” | “Degree of Freedom” | “Mean-Square” | “F-Value” | “Prob > F” | |
---|---|---|---|---|---|---|
Model | 8.99 | 8 | 1.12 | 128.04 | <0.0001 | Significant |
A-Pulse-on Time | 4.36 | 1 | 4.36 | 496.87 | <0.0001 | |
B-Pulse-off Time | 2.31 | 1 | 2.31 | 263.52 | <0.0001 | |
C-Spark Gap Voltage | 2.02 | 1 | 2.02 | 230.65 | <0.0001 | |
D-Wire Feed Rate | 0.0408 | 1 | 0.0408 | 4.65 | 0.0427 | |
AB | 0.0977 | 1 | 0.0977 | 11.13 | 0.0031 | |
AC | 0.0452 | 1 | 0.0452 | 5.15 | 0.0340 | |
BC | 0.0315 | 1 | 0.0315 | 3.59 | 0.0720 | |
A2 | 0.0767 | 1 | 0.0767 | 8.74 | 0.0075 | |
Residual | 0.1843 | 21 | 0.0088 | |||
Lack-of-fit | 0.1640 | 16 | 0.0102 | 2.52 | 0.1562 | Not-significant |
Pure error | 0.0203 | 5 | 0.0041 | |||
Cor total | 9.17 | 29 | ||||
Standard deviation | 0.0937 | R2 | 0.9799 | |||
Mean | 1.13 | Adj. R2 | 0.9723 | |||
CV% | 8.28 | Pred. R2 | 0.9503 | |||
Adeq. Precision | 41.6418 |
Source | “Sum of Squares” | “Degree of Freedom” | “Mean-Square” | “F-Value” | “Prob > F” | |
---|---|---|---|---|---|---|
Model | 5.59 | 8 | 0.6990 | 24.24 | <0.0001 | Significant |
A-Pulse-on Time | 2.17 | 1 | 2.17 | 75.33 | <0.0001 | |
B-Pulse-off Time | 0.4593 | 1 | 0.4593 | 15.93 | 0.0007 | |
C-Spark Gap- Voltage | 2.23 | 1 | 2.23 | 77.43 | <0.0001 | |
D-Wire Feed-Rate | 0.0096 | 1 | 0.0096 | 0.3329 | 0.5701 | |
AB | 0.1089 | 1 | 0.1089 | 3.78 | 0.0655 | |
AC | 0.1225 | 1 | 0.1225 | 4.25 | 0.0519 | |
B2 | 0.2618 | 1 | 0.2618 | 9.08 | 0.0066 | |
D2 | 0.1722 | 1 | 0.1722 | 5.97 | 0.0234 | |
Residual | 0.6055 | 21 | 0.0288 | |||
Lack-of-fit | 0.5404 | 16 | 0.0338 | 2.59 | 0.1487 | Not-significant |
Pure-error | 0.0651 | 5 | 0.0130 | |||
Cor-total | 6.20 | 29 | ||||
Standard-deviation | 0.1698 | R2 | 0.9023 | |||
Mean | 2.11 | Adj. R2 | 0.8651 | |||
CV% | 8.04 | Pred. R2 | 0.7897 | |||
Adeq. Precision | 16.7976 |
Constraints | To Achieve | Limit (lower) | Limit (Upper) | Important |
---|---|---|---|---|
Ton (µs) | In range | 108 | 124 | 3 |
Toff (µs) | 42 | 58 | 3 | |
SV (volts) | 24 | 72 | 3 | |
WF (m/min.) | 4 | 12 | 3 | |
CR (mm/min.) | Maximize | 0.31 | 2.48 | 3 |
SR (µm) | Minimize | 1.09 | 2.88 | 3 |
Response | Process Parameters | Predicted Response | Desirability | ||||
---|---|---|---|---|---|---|---|
Ton (µs) | Toff (µs) | SV (volts) | WF (m/min) | CR (mm/min) | SR (µm) | ||
Single response optimization to maximize CR | 121 | 45 | 25 | 6 | 2.91 | - | 1.000 |
Single response optimization to minimize SR | 114 | 57 | 68 | 8 | - | 0.88 | 1.000 |
Multi response optimization to maximize CR and minimize SR | 124 | 42 | 60 | 8 | 2.48 | 2.12 | 0.689 |
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Aggarwal, V.; Pruncu, C.I.; Singh, J.; Sharma, S.; Pimenov, D.Y. Empirical Investigations during WEDM of Ni-27Cu-3.15Al-2Fe-1.5Mn Based Superalloy for High Temperature Corrosion Resistance Applications. Materials 2020, 13, 3470. https://doi.org/10.3390/ma13163470
Aggarwal V, Pruncu CI, Singh J, Sharma S, Pimenov DY. Empirical Investigations during WEDM of Ni-27Cu-3.15Al-2Fe-1.5Mn Based Superalloy for High Temperature Corrosion Resistance Applications. Materials. 2020; 13(16):3470. https://doi.org/10.3390/ma13163470
Chicago/Turabian StyleAggarwal, Vivek, Catalin Iulian Pruncu, Jujhar Singh, Shubham Sharma, and Danil Yurievich Pimenov. 2020. "Empirical Investigations during WEDM of Ni-27Cu-3.15Al-2Fe-1.5Mn Based Superalloy for High Temperature Corrosion Resistance Applications" Materials 13, no. 16: 3470. https://doi.org/10.3390/ma13163470