pH-Sensitive Biocompatible Nanoparticles of Paclitaxel-Conjugated Poly(styrene-co-maleic acid) for Anticancer Drug Delivery in Solid Tumors of Syngeneic Mice

ACS Appl Mater Interfaces. 2015 Dec 9;7(48):26530-48. doi: 10.1021/acsami.5b07764. Epub 2015 Nov 23.

Abstract

In the present study, we have synthesized poly(styrene-co-maleic anhydride), a biocompatible copolymer that was further conjugated with paclitaxel (PTX) via ester linkage and self-assembled to form poly(styrene-co-maleic acid)-paclitaxel (PSMAC-PTX) nanoparticles (NPs). The in vitro release of PTX from PSMAC-PTX NPs showed a higher release at lower pH than at the physiological pH of 7.4, confirming its pH-dependent release. The cell viability of PSMAC-PTX nanoparticles was evaluated using MTT assay. IC50 values of 9.05-18.43 ng/mL of PTX equivalent were observed in various cancer cell lines after 72 h of incubation. Confocal microscopy, Western blotting, and Flow cytometry results further supported that the cellular uptake and apoptosis of cancer cells with PSMAC-PTX NPs. Pharmacokinetic studies revealed that the conjugation of PTX to the PSMAC co-polymer not only increased the plasma and tumor C(max) of PTX but also prolonged its plasma half-life and retention in tumor via enhanced permeability and retention (EPR) effect. Administration of PSMAC-PTX NPs showed significant tumor growth inhibition with improved apoptosis effects in vivo on Ehrlich Ascites Tumor (EAT)-bearing BALB/c syngeneic mice in comparison with Taxol, without showing any cytotoxicity. On the basis of preliminary results, no subacute toxicity was observed in major organs, tissues and hematological system up to a dosage of 60 mg/kg body weight in mice. Therefore, PSMAC-PTX NPs may be considered as an alternative nanodrug delivery system for the delivery of PTX in solid tumors.

Keywords: BALB/c mice; EAT; paclitaxel; pharmacokinetics; poly(styrene-co-maleic acid).

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Intravenous
  • Animals
  • Antineoplastic Agents, Phytogenic / chemistry
  • Antineoplastic Agents, Phytogenic / pharmacokinetics
  • Antineoplastic Agents, Phytogenic / pharmacology
  • Antineoplastic Agents, Phytogenic / therapeutic use*
  • Area Under Curve
  • Biocompatible Materials / chemistry*
  • Blood Cell Count
  • Body Weight / drug effects
  • Carcinoma, Ehrlich Tumor / drug therapy*
  • Carcinoma, Ehrlich Tumor / pathology
  • Cell Death / drug effects
  • Cell Line, Tumor
  • Cell Proliferation / drug effects
  • Drug Delivery Systems*
  • Drug Liberation
  • Drug Stability
  • Endocytosis / drug effects
  • Erythrocyte Aggregation / drug effects
  • Hemolysis / drug effects
  • Hydrogen-Ion Concentration
  • In Situ Nick-End Labeling
  • Inhibitory Concentration 50
  • Kaplan-Meier Estimate
  • Maleates / chemistry*
  • Maximum Tolerated Dose
  • Mice, Inbred BALB C
  • Nanoparticles / chemistry*
  • Nanoparticles / ultrastructure
  • Paclitaxel / chemistry
  • Paclitaxel / pharmacokinetics
  • Paclitaxel / pharmacology
  • Paclitaxel / therapeutic use
  • Polystyrenes / chemistry*
  • Tissue Distribution / drug effects

Substances

  • Antineoplastic Agents, Phytogenic
  • Biocompatible Materials
  • Maleates
  • Polystyrenes
  • styrene-maleic acid polymer
  • maleic acid
  • Paclitaxel